CN108842177B - Electrochemical deposition bracket for preparing nano material - Google Patents
Electrochemical deposition bracket for preparing nano material Download PDFInfo
- Publication number
- CN108842177B CN108842177B CN201810750796.0A CN201810750796A CN108842177B CN 108842177 B CN108842177 B CN 108842177B CN 201810750796 A CN201810750796 A CN 201810750796A CN 108842177 B CN108842177 B CN 108842177B
- Authority
- CN
- China
- Prior art keywords
- substrate
- conductive
- hole
- conductive metal
- cover plate
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- 239000002086 nanomaterial Substances 0.000 title claims abstract description 34
- 238000004070 electrodeposition Methods 0.000 title claims abstract description 33
- 239000000758 substrate Substances 0.000 claims abstract description 73
- 238000007789 sealing Methods 0.000 claims abstract description 60
- 230000000149 penetrating effect Effects 0.000 claims abstract description 3
- 229910052751 metal Inorganic materials 0.000 claims description 68
- 239000002184 metal Substances 0.000 claims description 68
- 238000002360 preparation method Methods 0.000 claims description 16
- 239000003792 electrolyte Substances 0.000 abstract description 20
- 230000000694 effects Effects 0.000 abstract description 6
- 239000003292 glue Substances 0.000 abstract description 4
- 230000007774 longterm Effects 0.000 abstract description 4
- TWNQGVIAIRXVLR-UHFFFAOYSA-N oxo(oxoalumanyloxy)alumane Chemical compound O=[Al]O[Al]=O TWNQGVIAIRXVLR-UHFFFAOYSA-N 0.000 abstract description 3
- 239000002070 nanowire Substances 0.000 description 7
- 241001391944 Commicarpus scandens Species 0.000 description 4
- 239000002120 nanofilm Substances 0.000 description 4
- 238000000034 method Methods 0.000 description 3
- 239000011148 porous material Substances 0.000 description 3
- FGRBYDKOBBBPOI-UHFFFAOYSA-N 10,10-dioxo-2-[4-(N-phenylanilino)phenyl]thioxanthen-9-one Chemical compound O=C1c2ccccc2S(=O)(=O)c2ccc(cc12)-c1ccc(cc1)N(c1ccccc1)c1ccccc1 FGRBYDKOBBBPOI-UHFFFAOYSA-N 0.000 description 2
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 2
- 229910052782 aluminium Inorganic materials 0.000 description 2
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 2
- 239000011521 glass Substances 0.000 description 2
- 229910052594 sapphire Inorganic materials 0.000 description 2
- 239000010980 sapphire Substances 0.000 description 2
- 239000002253 acid Substances 0.000 description 1
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25D—PROCESSES FOR THE ELECTROLYTIC OR ELECTROPHORETIC PRODUCTION OF COATINGS; ELECTROFORMING; APPARATUS THEREFOR
- C25D11/00—Electrolytic coating by surface reaction, i.e. forming conversion layers
- C25D11/02—Anodisation
- C25D11/04—Anodisation of aluminium or alloys based thereon
- C25D11/045—Anodisation of aluminium or alloys based thereon for forming AAO templates
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25D—PROCESSES FOR THE ELECTROLYTIC OR ELECTROPHORETIC PRODUCTION OF COATINGS; ELECTROFORMING; APPARATUS THEREFOR
- C25D11/00—Electrolytic coating by surface reaction, i.e. forming conversion layers
- C25D11/005—Apparatus specially adapted for electrolytic conversion coating
Abstract
The invention relates to the technical field of anodic aluminum oxide porous films, in particular to an electrochemical deposition bracket for preparing nano materials. The novel solar cell module comprises a substrate, a front cover plate, a support base and a conductive assembly, wherein the substrate is fixed through the front cover plate and the support base, the conductive assembly is arranged on the support base, the substrate is connected with the conductive assembly, and a through hole A is formed in the front cover plate in a penetrating mode. The device has the advantages of stable structure, good fixing effect on the substrate, good sealing performance, capability of preventing the electrolyte from corroding the conductive component, assembly type structure, no glue or bonding structure, easy disassembly and assembly and replacement of parts, and contribution to long-term effective use of the device.
Description
Technical Field
The invention relates to the technical field of anodic aluminum oxide porous films, in particular to an electrochemical deposition bracket for preparing nano materials.
Background
The AAO porous nano template is one of anodic aluminum oxide templates, has the advantages of uniform pore height distribution, uniform pore diameter, controllable pore shape, large surface area and the like, and has good market application prospect. The metal nano wire with high length-diameter ratio and high density can be conveniently prepared by using the bi-pass AAO as a template through an electrochemical deposition method. It is important that the template must be effectively sealed in order to ensure that the nanowires grow only within the nanopores within the template, and only the portions that need to be reacted are exposed to the electrolyte. In addition, in order to ensure uniformity of the nanowire growth process, the influence of the structure on the liquid fluidity needs to be fully considered. In the process of preparing the AAO porous nano template, due to the fact that a proper standard fixed support bracket does not exist, a self-made mechanism of a researcher is complex and inapplicable, a substrate for preparing the AAO porous nano template is easy to break due to the fact that the thickness is thin, sealing performance is poor, acid liquor permeation of electrolyte often occurs, and a lead connected with the substrate is corroded, so that the device cannot be effectively used for a long time, and large-area industrialization application is not facilitated. It is therefore desirable to devise a new electrochemically deposited scaffold for the preparation of nanomaterials as a support for the preparation of AAO porous nanomaterials and for the preparation of other alumina templates.
Disclosure of Invention
The invention aims to provide an electrochemical deposition bracket for preparing nano materials, which has the advantages of stable structure, good fixing effect on a substrate, good sealing performance, capability of preventing electrolyte from corroding a conductive component, assembly structure without any glue or bonding structure, easy disassembly and replacement of parts and contribution to long-term effective use of the device.
In order to solve the technical problems, the invention adopts the following technical scheme:
the electrochemical deposition support for preparing the nano material comprises a substrate, a front cover plate, a support base and a conductive component, wherein the substrate is fixed through the front cover plate and the support base, the conductive component is arranged on the support base, the substrate is connected with the conductive component, and a through hole A is further formed in the front cover plate in a penetrating mode.
The electrochemical deposition support for preparing the nano material is characterized in that the support base is provided with the mounting groove, the step groove and the through hole B, the step groove is arranged on the upper portion of the mounting groove, the substrate is arranged in the mounting groove, the step groove is internally provided with the sealing ring, one surface of the sealing ring is contacted with the substrate and the bottom of the step groove, the other surface of the sealing ring is contacted with the front cover plate, the through hole B is penetratingly arranged in the mounting groove, and the substrate is connected with the conductive assembly through the through hole B.
The electrochemical deposition support for preparing the nano material is characterized in that the side face of the support base is further integrally provided with the fixing rod, the support base and the fixing rod are further provided with the conductive wire groove connected with the through hole B, the conductive wire groove is located at one side far away from the front cover plate, the conductive wire groove is arranged at the top of the fixing rod from the through hole B, and the conductive wire groove is further provided with the back sealing strip.
The electrochemical deposition bracket for preparing the nano material comprises a conductive metal block and a conductive metal strip, wherein the conductive metal block is arranged in the through hole B, one surface of the conductive metal block is in contact with the substrate, the other surface of the conductive metal block is also connected with the conductive metal strip, and the conductive metal strip is arranged in the conductive wire groove.
The electrochemical deposition bracket for preparing the nano material, the conductive assembly further comprises a conductive metal gasket, the conductive metal gasket is arranged at the bottom of the mounting groove, one surface of the conductive metal gasket is contacted with the substrate, and the other surface of the conductive metal gasket is contacted with the conductive metal block.
The electrochemical deposition bracket for preparing the nano material is characterized in that the conductive component is a wire, and the wire is connected with the substrate through the conductive wire groove and the through hole B.
In the electrochemical deposition bracket for preparing the nano material, the through hole B is formed in the center of the mounting groove.
The electrochemical deposition bracket for preparing the nano material further comprises a fixing screw, and the front cover plate is connected with the bracket base through the fixing screw.
In the electrochemical deposition bracket for preparing the nano material, one end of the through hole A, which is far away from the bracket base, is provided with a chamfer.
Compared with the prior art, the invention has the following advantages:
1) The electrochemical deposition bracket for preparing the nano material has the advantages of stable structure, good fixing effect on a substrate, good sealing performance, capability of preventing the electrolyte from corroding the conductive component, and no glue or bonding structure, is easy to disassemble and replace parts, and is beneficial to long-term effective use of the device;
2) By forming the chamfer at one end of the through hole A far away from the bracket base, one end of the through hole A far away from the bracket base forms an inclined plane, so that the inclined plane is wider, the mobility of electrolyte in the through hole A is improved, the uniformity of nanowire growth is ensured, and the effective use area of the prepared nano film is increased;
3) The mounting groove is formed in the support base, so that the substrate and the conductive metal gasket can be safely and reliably placed in the mounting groove; the sealing ring is preferably a star-shaped sealing ring, one surface of the sealing ring is contacted with the bottom of the substrate and the bottom of the stepped groove, the other surface of the sealing ring is contacted with the front cover plate, the sealing ring, the substrate and the conductive metal gasket are clamped under the action of the clamping force of the front cover plate and the bracket base, the substrate is not easy to break and damage although being clamped due to certain softness, in addition, the sealing ring, the substrate, the stepped groove and the mounting groove form a closed space, after the through hole B and the wire groove are formed, the sealing effect of the back sealing strip is matched, and the conductive assembly can be effectively contacted with the substrate without being corroded by electrolyte; the star-shaped sealing ring is used for sealing with a stepped structure, so that the sealing of one sealing ring in two directions is realized, and the complexity of parts is reduced;
4) The fixing rod is arranged on the bracket base, so that the bracket is convenient to connect with other components such as the lifting device, and the whole bracket is convenient to be manually placed into electrolyte or lifted after finishing reaction or is fixed on the lifting device;
5) The conductive assembly is arranged to be the conductive metal block and the conductive metal strip, so that the conductive assembly is more reliably connected with the substrate, and the conductive metal block and the conductive metal strip are thicker than a conventional wire, so that the contact surface between the conductive metal block and the conductive metal strip and the substrate is larger, the conductive efficiency is higher, and the reaction is facilitated; by arranging the conductive metal gasket between the conductive metal block and the substrate, the contact area between the conductive metal gasket and the substrate is larger, the conductive efficiency is higher, and the reaction is greatly promoted; particularly, when the through hole B is formed in the center of the mounting groove, the electric conduction to the substrate is uniform, and the preparation of the AAO porous nano template is facilitated;
6) The conductive component is arranged as the wire, so that the preparation of the AAO porous nano template is realized under the condition that the whole device is simpler;
7) Through using a plurality of fixing bolts to fix front shroud and support base, guaranteed the connection and the dismouting between front shroud and the support base, make the preparation of the porous nano-template of AAO more convenient.
Drawings
FIG. 1 is an exploded view of the present invention;
FIG. 2 is also an exploded view of the present invention;
fig. 3 is a half cross-sectional view of the present invention.
Meaning of reference numerals: the device comprises a 1-substrate, a 2-front cover plate, a 3-support base, a 4-conductive component, a 5-through hole A, a 6-mounting groove, a 7-stepped groove, an 8-through hole B, a 9-sealing ring, a 10-fixing rod, an 11-conductive wire groove, a 12-back sealing strip, a 13-conductive metal block, a 14-conductive metal strip, a 15-conductive metal gasket and a 16-fixing screw.
The invention is further described below with reference to the drawings and the detailed description.
Detailed Description
Example 1 of the present invention: the utility model provides an electrochemical deposition support for preparing nano material, as shown in fig. 1-3, includes base 1, front bezel 2, support base 3 and electrically conductive subassembly 4, base 1 is fixed through front bezel 2 and support base 3, electrically conductive subassembly 4 sets up on support base 3, base 1 and electrically conductive subassembly 4 are connected, still run through on the front bezel 2 and have seted up through-hole A5, the chamfer has been seted up to the one end that support base 3 was kept away from to through-hole A5, the chamfer makes the one end that support base 3 was kept away from to through-hole A5 form the inclined plane, and is more open, has improved the mobility of electrolyte in through-hole A5, has guaranteed the homogeneity that the nanowire grows, has increased the effective usable floor area of the nano film of preparing. Wherein the substrate 1 can be made of sapphire, silicon chips, glass and the like, and the substrate 1 is plated with aluminum films with different thicknesses according to the thicknesses of the prepared AAO porous nano templates.
The electrochemical deposition support for preparing nano materials, mounting groove 6, ladder groove 7 and through hole B8 have been seted up on the support base 3, through set up mounting groove 6 on support base 3 for base 1 and electrically conductive metal gasket 15 can safe and reliable place in mounting groove 6, ladder groove 7 is located mounting groove 6 upper portion, and is offered with the form of seting up the ladder hole, base 1 sets up in mounting groove 6, still be provided with sealing washer 9 in the ladder groove 7, sealing washer 9 is the star-shaped sealing washer preferably, sealing washer 9 one side and base 1, ladder groove 7 bottom contact, and the another side contacts with front shroud 2, through hole B8 runs through and sets up in mounting groove 6, base 1 is connected with electrically conductive subassembly 4 through hole B8. Under the clamping force of the front cover plate 2 and the bracket base 3, the sealing ring 9 and the substrate 1 are clamped, and the substrate 1 is not easy to break and damage although being clamped due to certain softness of the sealing ring 9.
The electrochemical deposition bracket for preparing the nano material is characterized in that a fixing rod 10 is integrally formed on the side surface of the bracket base 3, the fixing rod 10 is long, and the whole bracket can be manually placed into electrolyte or lifted after finishing reaction or is fixed on a lifting device. The support base 3 and the fixing rod 10 are further provided with a conductive wire groove 11 connected with the through hole B8, the conductive wire groove 11 is located on one side far away from the front cover plate 2, the conductive wire groove 11 is arranged at the top of the fixing rod 10 from the position of the through hole B8, and the conductive wire groove 11 is further provided with a back sealing strip 12. Because the sealing ring 9 forms a closed space with the substrate 1, the stepped groove 7 and the mounting groove 6, and the conductive wire groove 11 is provided with the back sealing strip 12, the conductive assembly 4 can be effectively contacted with the substrate 1 without being corroded by electrolyte.
The electrochemical deposition bracket for preparing the nano material is characterized in that the conductive component 4 is a wire, the wire is connected with the substrate 1 through the conductive wire groove 11 and the through hole B8, and the conductive component 4 is arranged as the wire, so that the preparation of the AAO porous nano template is realized under the condition that the whole device is simpler.
The through hole B8 is formed in the center of the mounting groove 6, so that the substrate 1 is uniform in electric conduction, and the preparation of the AAO porous nano template is facilitated.
The electrochemical deposition bracket for preparing the nano material further comprises a plurality of fixing screws 16, the front cover plate 2 and the bracket base 3 are connected through the fixing screws 16, and the fixing screws 16 ensure the connection and disassembly between the front cover plate 2 and the bracket base 3, so that the AAO porous nano template is more convenient to prepare.
Example 2: the utility model provides an electrochemical deposition support for preparing nano material, as shown in fig. 1-3, includes base 1, front bezel 2, support base 3 and electrically conductive subassembly 4, base 1 is fixed through front bezel 2 and support base 3, electrically conductive subassembly 4 sets up on support base 3, base 1 and electrically conductive subassembly 4 are connected, still run through on the front bezel 2 and have seted up through-hole A5, the chamfer has been seted up to the one end that support base 3 was kept away from to through-hole A5, the chamfer makes the one end that support base 3 was kept away from to through-hole A5 form the inclined plane, and is more open, has improved the mobility of electrolyte in through-hole A5, has guaranteed the homogeneity that the nanowire grows, has increased the effective usable floor area of the nano film of preparing. Wherein the substrate 1 can be made of sapphire, silicon chips, glass and the like, and the substrate 1 is plated with aluminum films with different thicknesses according to the thicknesses of the prepared AAO porous nano templates.
The electrochemical deposition support for preparing nano materials, mounting groove 6, ladder groove 7 and through hole B8 have been seted up on the support base 3, through set up mounting groove 6 on support base 3 for base 1 and electrically conductive metal gasket 15 can safe and reliable place in mounting groove 6, ladder groove 7 is located mounting groove 6 upper portion, and is offered with the form of seting up the ladder hole, base 1 sets up in mounting groove 6, still be provided with sealing washer 9 in the ladder groove 7, sealing washer 9 is the star-shaped sealing washer preferably, sealing washer 9 one side and base 1, ladder groove 7 bottom contact, and the another side contacts with front shroud 2, through hole B8 runs through and sets up in mounting groove 6, base 1 is connected with electrically conductive subassembly 4 through hole B8. Under the clamping force of the front cover plate 2 and the bracket base 3, the sealing ring 9 and the substrate 1 are clamped, and the substrate 1 is not easy to break and damage although being clamped due to certain softness of the sealing ring 9.
The electrochemical deposition bracket for preparing the nano material is characterized in that a fixing rod 10 is integrally formed on the side surface of the bracket base 3, the fixing rod 10 is long, and the whole bracket can be manually placed into electrolyte or lifted after finishing reaction or is fixed on a lifting device. The support base 3 and the fixing rod 10 are further provided with a conductive wire groove 11 connected with the through hole B8, the conductive wire groove 11 is located on one side far away from the front cover plate 2, the conductive wire groove 11 is arranged at the top of the fixing rod 10 from the position of the through hole B8, and the conductive wire groove 11 is further provided with a back sealing strip 12. Because the sealing ring 9 forms a closed space with the substrate 1, the stepped groove 7 and the mounting groove 6, and the conductive wire groove 11 is provided with the back sealing strip 12, the conductive assembly 4 can be effectively contacted with the substrate 1 without being corroded by electrolyte.
The electrochemical deposition support for preparing nano materials, the conductive component 4 comprises a conductive metal block 13 and a conductive metal strip 14, the conductive metal block 13 is arranged in the through hole B8, one surface of the conductive metal block 13 is in contact with the substrate 1, the other surface of the conductive metal block is also connected with the conductive metal strip 14, and the conductive metal strip 14 is arranged in the conductive wire slot 11. The conductive metal block 13 and the conductive metal strip 14 are reliably connected with the substrate 1, and the conductive metal block 13 and the conductive metal strip 14 are thicker than a conventional wire, so that the contact surface with the substrate 1 is larger, the conductive efficiency is higher, and the reaction is facilitated.
The electrochemical deposition support for preparing nano materials, the conductive assembly 4 further comprises a conductive metal gasket 15, the conductive metal gasket 15 is arranged at the bottom of the mounting groove 6, one surface of the conductive metal gasket 15 is contacted with the substrate 1, and the other surface is contacted with the conductive metal block 13. The contact area between the conductive metal pad 15 and the substrate 1 is larger, the conductivity is higher, and the reaction is greatly promoted.
The through hole B8 is formed in the center of the mounting groove 6, so that the substrate 1 is uniform in electric conduction, and the preparation of the AAO porous nano template is facilitated.
The electrochemical deposition bracket for preparing the nano material further comprises a plurality of fixing screws 16, the front cover plate 2 and the bracket base 3 are connected through the fixing screws 16, and the fixing screws 16 ensure the connection and disassembly between the front cover plate 2 and the bracket base 3, so that the AAO porous nano template is more convenient to prepare.
The working principle of the invention is as follows: the electrochemical deposition support for preparing the nano material is formed by organically assembling the components such as the substrate 1, the front cover plate 2, the support base 3 and the conductive component 4, has stable structure, good fixing effect on the substrate 1 and good sealing performance, can prevent the conductive component 4 from being corroded by electrolyte, is of an assembled structure, has no glue or bonding structure, is easy to disassemble and replace parts, and is beneficial to long-term effective use of the device. When the AAO porous nano template is prepared, the support is placed in electrolyte, the substrate 1 is fully contacted with the electrolyte, the substrate 1 is used as an anode of a power supply, at the moment, the conductive component 4 in the support is connected with the anode of the power supply, the cathode of the power supply is connected with the cathode plate, and the whole device performs electrolytic reaction. The chamfer is formed at one end of the through hole A far away from the support base, so that one end of the through hole A far away from the support base forms an inclined plane, the inclined plane is wider, the mobility of electrolyte in the through hole A is improved, the uniformity of nanowire growth is ensured, and the effective use area of the prepared nano film is increased; the mounting groove 6 is formed in the bracket base 3, so that the substrate 1 and the conductive metal gasket 15 can be safely and reliably placed in the mounting groove 6; the step groove 7 is formed in the mounting groove 6 in a form of a step hole, so that the sealing ring 9 can be placed on the step groove 7, the sealing ring 9 is preferably a star-shaped sealing ring, one surface of the sealing ring 9 is contacted with the bottom of the substrate 1 and the bottom of the step groove 7, the other surface of the sealing ring 9 is contacted with the front cover plate 2, the sealing ring 9, the substrate 1 and the conductive metal gasket 15 are clamped under the clamping force of the front cover plate 2 and the bracket base 3, the substrate 1 is not easy to crack and damage although being clamped due to certain softness of the sealing ring 9, in addition, the sealing ring 9, the substrate 1, the step groove 7 and the mounting groove 6 form a closed space, and after the through hole B8 and the wire groove are formed, the sealing effect of the back sealing strip 12 is matched, and the conductive assembly 4 can be effectively contacted with the substrate 1 without being corroded by electrolyte; the star-shaped sealing ring is used for sealing with a stepped structure, so that the sealing of one sealing ring in two directions is realized, and the complexity of parts is reduced; the fixing rod 10 is arranged on the bracket base 3, so that the bracket is convenient to connect with other components such as the lifting device, and the whole bracket is convenient to be manually placed into electrolyte or lifted after finishing reaction or fixed on the lifting device; by arranging the conductive component 4 as the conductive metal block 13 and the conductive metal strip 14, the connection between the conductive component 4 and the substrate 1 is more reliable, and the conductive metal block 13 and the conductive metal strip 14 are thicker than a conventional wire, so that the contact surface between the conductive metal block 13 and the conductive metal strip 14 and the substrate 1 is larger, the conductive efficiency is higher, and the reaction is facilitated; by arranging the conductive metal gasket 15 between the conductive metal block 13 and the substrate 1, the contact area between the conductive metal gasket 15 and the substrate 1 is larger, the conductive efficiency is higher, and the reaction is greatly promoted; particularly, when the through hole B8 is formed in the center of the mounting groove 6, the electric conduction to the substrate 1 is uniform, and the preparation of the AAO porous nano template is facilitated; the conductive component 4 is arranged as a wire, so that the preparation of the AAO porous nano template is realized under the condition that the whole device is simpler; through using a plurality of fixing bolts to fix the front cover plate 2 and the support base 3, the connection and the disassembly and assembly between the front cover plate 2 and the support base 3 are ensured, and the preparation of the AAO porous nano template is more convenient.
Claims (5)
1. The electrochemical deposition support for preparing the nano material is characterized by comprising a substrate (1), a front cover plate (2), a support base (3) and a conductive component (4), wherein the substrate (1) is fixed through the front cover plate (2) and the support base (3), the conductive component (4) is arranged on the support base (3), the substrate (1) is connected with the conductive component (4), and a through hole A (5) is formed in the front cover plate (2) in a penetrating manner; the support base (3) is provided with a mounting groove (6), a step groove (7) and a through hole B (8), the step groove (7) is positioned at the upper part of the mounting groove (6), the substrate (1) is arranged in the mounting groove (6), the step groove (7) is internally provided with a sealing ring (9), one surface of the sealing ring (9) is contacted with the substrate (1) and the bottom of the step groove (7), the other surface is contacted with the front cover plate (2), the through hole B (8) is penetrated and arranged in the mounting groove (6), and the substrate (1) is connected with the conductive component (4) through the through hole B (8); the side of the bracket base (3) is also integrally formed with a fixing rod (10), the bracket base (3) and the fixing rod (10) are also provided with a conductive wire groove (11) connected with the through hole B (8), the conductive wire groove (11) is positioned at one side far away from the front cover plate (2), the conductive wire groove (11) is arranged from the through hole B (8) to the top of the fixing rod (10), and the conductive wire groove (11) is also provided with a back sealing strip (12); the conductive assembly (4) comprises a conductive metal block (13) and a conductive metal strip (14), wherein the conductive metal block (13) is arranged in the through hole B (8), one surface of the conductive metal block (13) is in contact with the substrate (1), the other surface of the conductive metal block is also connected with the conductive metal strip (14), and the conductive metal strip (14) is arranged in the conductive wire slot (11); the conductive assembly (4) further comprises a conductive metal gasket (15), the conductive metal gasket (15) is arranged at the bottom of the mounting groove (6), one surface of the conductive metal gasket (15) is contacted with the substrate (1), and the other surface of the conductive metal gasket is contacted with the conductive metal block (13); wherein the sealing ring (9) is a star-shaped sealing ring.
2. Electrochemical deposition support for the preparation of nanomaterials according to claim 1, characterized in that the conductive component (4) is a wire, which is connected to the substrate (1) via a conductive wire slot (11) and a through hole B (8).
3. Electrochemical deposition support for the preparation of nanomaterials according to claim 1 or 2, characterized in that the through-hole B (8) is open in the centre of the mounting slot (6).
4. Electrochemical deposition support for the preparation of nanomaterials according to claim 1, characterized in that it further comprises a set screw (16), the front cover plate (2) and the support base (3) being connected via the set screw (16).
5. Electrochemical deposition support for the preparation of nanomaterials according to claim 1, characterized in that the end of the through-hole a (5) remote from the support base (3) is provided with a chamfer.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810750796.0A CN108842177B (en) | 2018-07-10 | 2018-07-10 | Electrochemical deposition bracket for preparing nano material |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810750796.0A CN108842177B (en) | 2018-07-10 | 2018-07-10 | Electrochemical deposition bracket for preparing nano material |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN108842177A CN108842177A (en) | 2018-11-20 |
| CN108842177B true CN108842177B (en) | 2023-12-26 |
Family
ID=64196611
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201810750796.0A Active CN108842177B (en) | 2018-07-10 | 2018-07-10 | Electrochemical deposition bracket for preparing nano material |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN108842177B (en) |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110042448B (en) * | 2019-04-30 | 2021-04-30 | 铜仁学院 | Preparation method of porous anodic aluminum oxide template |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104388934A (en) * | 2014-12-11 | 2015-03-04 | 重庆墨希科技有限公司 | Tooling device for transferring graphene thin films used in chemical vapor deposition method |
| CN105862112A (en) * | 2014-12-29 | 2016-08-17 | 神华集团有限责任公司 | Clamp used for electrochemical deposition, electrochemical deposition apparatus and electrochemical deposition method thereof |
| CN206736368U (en) * | 2017-05-31 | 2017-12-12 | 新疆工程学院 | A kind of new hydrogen production machine |
| CN206783798U (en) * | 2017-04-28 | 2017-12-22 | 皖西学院 | Electrochemical deposition fixture |
| CN208667876U (en) * | 2018-07-10 | 2019-03-29 | 深圳拓扑精膜科技有限公司 | A kind of electrochemical deposition bracket being used to prepare nano material |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| TWI600796B (en) * | 2014-09-05 | 2017-10-01 | 國立清華大學 | Nanoporous thin film and method for fabricating the same |
-
2018
- 2018-07-10 CN CN201810750796.0A patent/CN108842177B/en active Active
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104388934A (en) * | 2014-12-11 | 2015-03-04 | 重庆墨希科技有限公司 | Tooling device for transferring graphene thin films used in chemical vapor deposition method |
| CN105862112A (en) * | 2014-12-29 | 2016-08-17 | 神华集团有限责任公司 | Clamp used for electrochemical deposition, electrochemical deposition apparatus and electrochemical deposition method thereof |
| CN206783798U (en) * | 2017-04-28 | 2017-12-22 | 皖西学院 | Electrochemical deposition fixture |
| CN206736368U (en) * | 2017-05-31 | 2017-12-12 | 新疆工程学院 | A kind of new hydrogen production machine |
| CN208667876U (en) * | 2018-07-10 | 2019-03-29 | 深圳拓扑精膜科技有限公司 | A kind of electrochemical deposition bracket being used to prepare nano material |
Also Published As
| Publication number | Publication date |
|---|---|
| CN108842177A (en) | 2018-11-20 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN101257059B (en) | Method for electrochemical depositing solar cell metallic electrode | |
| CN103422116B (en) | A kind of porous Ni-base ru oxide is combined the preparation method of hydrogen-precipitating electrode | |
| WO2017054392A1 (en) | Electrolytic cell apparatus with separated anode and cathode chambers for electrolytic preparation of ozone water | |
| JP2016523458A (en) | Formation of metal structures in solar cells | |
| CN103515676B (en) | All-solid-state separable aluminium-air cell | |
| CN108842177B (en) | Electrochemical deposition bracket for preparing nano material | |
| CN202037984U (en) | Screen print scraper | |
| CN205529113U (en) | Clamping device is electroplated to semiconductor wafer | |
| CN216528982U (en) | Integrated end plate for proton exchange membrane galvanic pile | |
| CN208667876U (en) | A kind of electrochemical deposition bracket being used to prepare nano material | |
| US20140083843A1 (en) | Preparation apparatus for porous alumina template | |
| CN102376783B (en) | Cuprous oxide solar battery with surface self-texture structure and manufacturing method thereof | |
| CN102800763A (en) | Solar cell and method for producing grid line electrode of solar cell | |
| CN204298493U (en) | A kind of electroplating clamp of the solar battery sheet for having back of the body electric field structure | |
| CN105633202A (en) | Surface treatment method of solar cell flexible substrate | |
| CN213652680U (en) | Electrode electroplating device for crystalline silicon battery production | |
| CN210765540U (en) | Electrolytic tank convenient for replacing cathode and anode components | |
| CN211339724U (en) | Electroplating cathode hanger | |
| CN208586367U (en) | A kind of device preparing porous anodic aluminium oxide in substrate | |
| CN206352166U (en) | Conducting beam fixed seat | |
| CN2760053Y (en) | Gripping holder for anodized electrode on chip surface of semiconductor device | |
| CN215289015U (en) | High-precision single-chip surface treatment jig | |
| CN219930307U (en) | Special clamp for ceramic plate electroplating | |
| CN210506564U (en) | Novel electrode clamp for composite electroplating | |
| CN220300895U (en) | Simple device for electroplating on semiconductor substrate |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| GR01 | Patent grant | ||
| GR01 | Patent grant |