CN108841348A - A kind of bolt fastening glue and preparation method thereof - Google Patents
A kind of bolt fastening glue and preparation method thereof Download PDFInfo
- Publication number
- CN108841348A CN108841348A CN201810480426.XA CN201810480426A CN108841348A CN 108841348 A CN108841348 A CN 108841348A CN 201810480426 A CN201810480426 A CN 201810480426A CN 108841348 A CN108841348 A CN 108841348A
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- China
- Prior art keywords
- parts
- calcium carbonate
- bolt fastening
- fastening glue
- micro
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J163/00—Adhesives based on epoxy resins; Adhesives based on derivatives of epoxy resins
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J11/00—Features of adhesives not provided for in group C09J9/00, e.g. additives
- C09J11/02—Non-macromolecular additives
- C09J11/04—Non-macromolecular additives inorganic
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J11/00—Features of adhesives not provided for in group C09J9/00, e.g. additives
- C09J11/02—Non-macromolecular additives
- C09J11/06—Non-macromolecular additives organic
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
- C08K3/24—Acids; Salts thereof
- C08K3/26—Carbonates; Bicarbonates
- C08K2003/265—Calcium, strontium or barium carbonate
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K2201/00—Specific properties of additives
- C08K2201/011—Nanostructured additives
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K2201/00—Specific properties of additives
- C08K2201/014—Additives containing two or more different additives of the same subgroup in C08K
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Adhesives Or Adhesive Processes (AREA)
Abstract
The invention discloses a kind of bolt fastening glue and preparation method thereof.A kind of bolt fastening glue, is made of raw material from the following weight：100 parts of bisphenol A type epoxy resin, 15-25 parts of liquid silastic, 5-8 parts of glass fibre, 5-10 parts of carbon fiber, 4-6 parts of micro-calcium carbonate, 6-8 parts of nanometer calcium carbonate, 4-6 parts of furnace black, 20-30 parts of triethylene tetramine, 2-4 parts of zinc stearate, 2-4 parts of anti-aging agent, 2-4 parts of colorant.The invention has the advantages that：At the gap of main end or linking coated in bolt, the locking glue at internal whorl is cooperated to use, and can have preferable ductile strength and wear-resisting property with the bonding of metal in close, prevent the corrosion of metal from aoxidizing, improve the service life of material.
Description
Technical field
The present invention relates to a kind of metal protection glue, specifically a kind of bolt fastening glue and preparation method thereof.
Background technique
Thread locking glue is a kind of one pack system anaerobism locking agent, it has filled up small between the connection screw thread of interface completely
Gap, and when contacting in the case where no air metal, locking agent aggregates into hard solid, to reach enhancing locking force and close
Seal the purpose of anti-corrosion.
Currently, generally lock rapidly in 10 seconds after bolt fastening glue locking glue bolt both domestic and external and internal screw thread screw,
It can not adjust, and many occasions, it after needing bolt and internal screw thread to screw, is adjusted in certain time, this requires certain after screwing
Cannot lock in time, but cannot the time it is too long.Therefore it will appear to adjust repeatedly in actual use and be not fixed with the time
Factor cause bolt install precision and quality.For this purpose, applicant proposed a kind of new technical solutions, and provide one kind
Novel bolt fastening glue, the fastening glue mainly cooperate existing internal whorl fastening glue to use, and important use is at the end of bolt
Portion and seam crossing further improve locking force, and improve the performance of anti-corrosion.
Summary of the invention
Technical problem to be solved by the invention is to provide a kind of bolt fastening glue and preparation method thereof.
In order to solve the above technical problems, technical solution of the present invention solves from the following aspect：Bisphenol A type epoxy resin is to gold
The cohesive force of category is very strong, while there is good chemical corrosion resistance, mechanical property, electrical insulating property etc., to the armour of metal
There is excellent effect；And in order to make up the toughness of bisphenol A type epoxy resin, it joined liquid silastic, liquid silastic can
Solidify at normal temperature, the two produces the effect of collaboration；Since the use environment of bolt is different, in order to further improve material
Ductile strength, joined glass fibre, carbon fiber, micro-calcium carbonate and nanometer calcium carbonate etc.；It joined others simultaneously to help
Agent, to reconcile the performance of sizing material；Applicant provides a kind of corresponding preparation method also directed to raw material of the invention.And by more
Secondary experiment adjustment, ultimately provides technical solution below：
A kind of bolt fastening glue, is made of raw material from the following weight：100 parts of bisphenol-A type epoxy resin, liquid silastic 15-
25 parts, 5-8 parts of glass fibre, 5-10 parts of carbon fiber, 4-6 parts of micro-calcium carbonate, 6-8 parts of nanometer calcium carbonate, furnace black 4-6
Part, 20-30 parts of triethylene tetramine, 2-4 parts of zinc stearate, 2-4 parts of anti-aging agent, 2-4 parts of colorant.
Further, the weight ratio of bisphenol-A type epoxy resin and liquid silastic is 5:1.
Further, the weight ratio of micro-calcium carbonate and nanometer calcium carbonate is 5:7.
Preferably, a kind of bolt fastening glue, which is characterized in that be made of raw material from the following weight：Bisphenol-A
100 parts of type epoxy resin, 20 parts of liquid silastic, 7 parts of glass fibre, 7 parts of carbon fiber, 5 parts of micro-calcium carbonate, nanometer calcium carbonate
7 parts, 5 parts of furnace black, 25 parts of triethylene tetramine, 3 parts of zinc stearate, 3 parts of anti-aging agent, 3 parts of colorant.
Further, the production method of a kind of bolt fastening glue, which is characterized in that include the following steps：By weight
Amount part weighs each raw material；Bisphenol-A type epoxy resin and liquid silastic are added in kneader and stir 20-30min, temperature is
45-55 DEG C, then sequentially add glass fibre, carbon fiber, micro-calcium carbonate, nanometer calcium carbonate, furnace black, anti-aging agent,
Toner, stirs 10-15min, and temperature is 50-60 DEG C；It is eventually adding triethylene tetramine and zinc stearate, is sufficiently stirred
It is sealed after uniformly, and use in applicator gun is added.
By adopting the above-described technical solution, a kind of bolt fastening glue, is made of following raw material：Bisphenol-A type ring
100 parts of oxygen resin, 15-25 parts of liquid silastic, 5-8 parts of glass fibre, 5-10 parts of carbon fiber, 4-6 parts of micro-calcium carbonate, nanometer
6-8 parts of calcium carbonate, 4-6 parts of furnace black, 20-30 parts of triethylene tetramine, 2-4 parts of zinc stearate, 2-4 parts of anti-aging agent, colorant
2-4 parts；The invention has the advantages that：At the gap of main end or linking coated in bolt, cooperate internal whorl
The locking glue at place uses, and can have preferable ductile strength and wear-resisting property with the bonding of metal in close, prevent metal
Corrosion oxidation, improves the service performance of material.
Specific embodiment
The present invention is described further combined with specific embodiments below.
Embodiment 1
A kind of bolt fastening glue, is made of following raw material：100 parts of bisphenol-A type epoxy resin, 15 parts of liquid silastic,
5 parts of glass fibre, 5 parts of carbon fiber, 4 parts of micro-calcium carbonate, 6 parts of nanometer calcium carbonate, 4 parts of furnace black, 20 parts of triethylene tetramine,
2 parts of zinc stearate, 2 parts of anti-aging agent, 2 parts of colorant.
A kind of production method of bolt fastening glue, includes the following steps：Each raw material is weighed by weight；By bisphenol-A type ring
Oxygen resin and liquid silastic, which are added in kneader, stirs 20-30min, and temperature is 45-55 DEG C, then sequentially adds glass fibers
Dimension, carbon fiber, micro-calcium carbonate, nanometer calcium carbonate, furnace black, anti-aging agent, colorant, stir 10-15min,
Temperature is 50-60 DEG C；It is eventually adding triethylene tetramine and zinc stearate, is sealed after stirring, and sizing is added
Use in rifle.
Embodiment 2
A kind of bolt fastening glue, is made of following raw material：100 parts of bisphenol-A type epoxy resin, 20 parts of liquid silastic,
7 parts of glass fibre, 7 parts of carbon fiber, 5 parts of micro-calcium carbonate, 7 parts of nanometer calcium carbonate, 5 parts of furnace black, 25 parts of triethylene tetramine,
3 parts of zinc stearate, 3 parts of anti-aging agent, 3 parts of colorant.
A kind of production method of bolt fastening glue, includes the following steps：Each raw material is weighed by weight；By bisphenol-A type ring
Oxygen resin and liquid silastic, which are added in kneader, stirs 20-30min, and temperature is 45-55 DEG C, then sequentially adds glass fibers
Dimension, carbon fiber, micro-calcium carbonate, nanometer calcium carbonate, furnace black, anti-aging agent, colorant, stir 10-15min,
Temperature is 50-60 DEG C；It is eventually adding triethylene tetramine and zinc stearate, is sealed after stirring, and sizing is added
Use in rifle.
Embodiment 3
A kind of bolt fastening glue, is made of following raw material：100 parts of bisphenol-A type epoxy resin, 25 parts of liquid silastic,
8 parts of glass fibre, 10 parts of carbon fiber, 6 parts of micro-calcium carbonate, 8 parts of nanometer calcium carbonate, 6 parts of furnace black, triethylene tetramine 30
Part, 4 parts of zinc stearate, 4 parts of anti-aging agent, 4 parts of colorant.
A kind of production method of bolt fastening glue, includes the following steps：Each raw material is weighed by weight；By bisphenol-A type ring
Oxygen resin and liquid silastic, which are added in kneader, stirs 20-30min, and temperature is 45-55 DEG C, then sequentially adds glass fibers
Dimension, carbon fiber, micro-calcium carbonate, nanometer calcium carbonate, furnace black, anti-aging agent, colorant, stir 10-15min,
Temperature is 50-60 DEG C；It is eventually adding triethylene tetramine and zinc stearate, is sealed after stirring, and sizing is added
Use in rifle.
The external protection for being equally applicable to other connecting components with locking glue made from embodiment 1-3 fastens, and can be used
It is fastened in the internal Protection of larger model bolt.Wherein elongation at break has good chemical corrosion resistance up to 18%.Through
Overtesting, the material can reliably be bonded with metal, expulsion rate zero, and have good toughness and intensity, be had superior
Locking, waterproof, the function of protection collision.
The equipment used in the present invention is the commonly used equipment of this field, and details are not described herein.
The foregoing is merely the schematical specific embodiment of the present invention, the range being not intended to limit the invention.It is any
Those skilled in the art, made equivalent changes and modifications under the premise of not departing from design and the principle of the present invention,
It should belong to the scope of protection of the invention.
Claims (5)
1. a kind of bolt fastening glue, which is characterized in that be made of raw material from the following weight：100 parts of bisphenol-A type epoxy resin,
15-25 parts of liquid silastic, 5-8 parts of glass fibre, 5-10 parts of carbon fiber, 4-6 parts of micro-calcium carbonate, 6-8 parts of nanometer calcium carbonate,
4-6 parts of furnace black, 20-30 parts of triethylene tetramine, 2-4 parts of zinc stearate, 2-4 parts of anti-aging agent, 2-4 parts of colorant.
2. a kind of bolt fastening glue according to claim 1, it is characterised in that：Bisphenol-A type epoxy resin and liquid silicon rubber
The weight ratio of glue is 5:1.
3. a kind of bolt fastening glue according to claim 1, it is characterised in that：The weight of micro-calcium carbonate and nanometer calcium carbonate
Amount is than being 5:7.
4. a kind of bolt fastening glue according to claim 1, which is characterized in that be made of raw material from the following weight：It is double
100 parts of phenol A type epoxy resin, 20 parts of liquid silastic, 7 parts of glass fibre, 7 parts of carbon fiber, 5 parts of micro-calcium carbonate, nano-sized carbon
7 parts of sour calcium, 5 parts of furnace black, 25 parts of triethylene tetramine, 3 parts of zinc stearate, 3 parts of anti-aging agent, 3 parts of colorant.
5. a kind of production method of bolt fastening glue according to claim 1 or 2, which is characterized in that include the following steps：
Each raw material is weighed by weight；Bisphenol-A type epoxy resin and liquid silastic are added in kneader and stir 20-30min, temperature
Degree is 45-55 DEG C, then sequentially adds glass fibre, carbon fiber, micro-calcium carbonate, nanometer calcium carbonate, furnace black, prevents always
Agent, colorant, stir 10-15min, and temperature is 50-60 DEG C；It is eventually adding triethylene tetramine and zinc stearate, is filled
Divide and be sealed after mixing evenly, and use in applicator gun is added.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810480426.XA CN108841348A (en) | 2018-05-18 | 2018-05-18 | A kind of bolt fastening glue and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810480426.XA CN108841348A (en) | 2018-05-18 | 2018-05-18 | A kind of bolt fastening glue and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN108841348A true CN108841348A (en) | 2018-11-20 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201810480426.XA Pending CN108841348A (en) | 2018-05-18 | 2018-05-18 | A kind of bolt fastening glue and preparation method thereof |
Country Status (1)
| Country | Link |
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| CN (1) | CN108841348A (en) |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103709984A (en) * | 2013-12-31 | 2014-04-09 | 中材金晶玻纤有限公司 | In-situ thread adhesive for fiber reinforced plastic pipeline |
| CN104650788A (en) * | 2015-02-04 | 2015-05-27 | 江苏大力士投资有限公司 | Caulking adhesive with favorable retractility and preparation method thereof |
-
2018
- 2018-05-18 CN CN201810480426.XA patent/CN108841348A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103709984A (en) * | 2013-12-31 | 2014-04-09 | 中材金晶玻纤有限公司 | In-situ thread adhesive for fiber reinforced plastic pipeline |
| CN104650788A (en) * | 2015-02-04 | 2015-05-27 | 江苏大力士投资有限公司 | Caulking adhesive with favorable retractility and preparation method thereof |
Non-Patent Citations (2)
| Title |
|---|
| 丁浩 主编: "《塑料工业实用手册 上册》", 31 May 1995, 化学工业出版社 * |
| 蔡永源 主编: "《实用胶粘剂技术手册》", 30 September 1990, 化学工业部科学技术情报研究所 * |
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Application publication date: 20181120 |
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