CN108835466A - A kind of production method that jujube juice is concentrated - Google Patents

A kind of production method that jujube juice is concentrated Download PDF

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Publication number
CN108835466A
CN108835466A CN201810617297.4A CN201810617297A CN108835466A CN 108835466 A CN108835466 A CN 108835466A CN 201810617297 A CN201810617297 A CN 201810617297A CN 108835466 A CN108835466 A CN 108835466A
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jujube juice
production method
concentrated
jujube
treated
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CN201810617297.4A
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苗笑阳
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    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L2/00Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
    • A23L2/02Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation containing fruit or vegetable juices
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L2/00Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
    • A23L2/02Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation containing fruit or vegetable juices
    • A23L2/04Extraction of juices
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L2/00Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
    • A23L2/70Clarifying or fining of non-alcoholic beverages; Removing unwanted matter
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23VINDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
    • A23V2002/00Food compositions, function of food ingredients or processes for food or foodstuffs

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  • Health & Medical Sciences (AREA)
  • Nutrition Science (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Food Science & Technology (AREA)
  • Polymers & Plastics (AREA)
  • Non-Alcoholic Beverages (AREA)

Abstract

A kind of production method that jujube juice is concentrated disclosed by the invention, including sorting, cleaning, extraction, enzymatic hydrolysis, decoloration, diatomite filtering, centrifugal filtration, primary sterilization, a ultrafiltration, electrodialysis process, re-pasteurization, second ultrafiltration, vacuum concentration, sterilize three times, filling and package.The present invention uses ultrasonic-leaching, substantially reduces the process time of conventional water leaching and reduces Extracting temperature, the loss of the caramelization and thermal energy of product in process can be greatly reduced;The bitter taste of conventional water leaching is removed and removed simultaneously to the heavy metal substance in jujube present invention uses electrodialysis process, while meeting the improved demand for producing energy-efficient demand instantly and jujube juice product special flavour being concentrated.

Description

A kind of production method that jujube juice is concentrated
Technical field
The present invention relates to the production method of red date concentrated juice more particularly to a kind of meet production energy-saving demand, can improve The production method that the concentration jujube juice of jujube juice product special flavour is concentrated.
Background technique
Jujube also known as jujube are just listed in one of " five fruits " (peach, Lee, plum, apricot, jujube) since ancient times, with a long history.It is red Jujube originates in China, belongs to the fruit of Rhamnaceae plant, has more than 3,000 years cultivation histories in China.Jujube is rich in Nutritional ingredient, in addition to containing sugar, protein, organic acid, vitamin, microelement, also containing flavone compound and saponin(e etc. Medicinal ingredient, thus there is good healthy nutritive value and medical value.
Jujube deep processing at present is mainly to produce based on clarifying jujube juice and red date concentrated juice, in the processing of red date concentrated juice In the process, water leaching can be used, in conventional water leaching, process time is longer, and Extracting temperature is high, such as Publication No. " CN102907736A " discloses in the patent of invention specification of entitled " a kind of processing method of red date concentrated juice " " extraction:Smashed jujube is poured into closed jacketed pan, the softened water boiling of heat, extraction is added, coarse filtration obtains Leaching liquor " can aggravate caramelization and improve the loss of thermal energy, lead to jujube in such high temperature water leaching The natural scents of itself cannot save substantially, seriously affect product quality, and after by water leaching, jujube Often there is bitter taste in juice, this has resulted in certain mass defect.
Summary of the invention
In place of avoiding the deficiencies in the prior art, a kind of production method that jujube juice is concentrated is provided, To effectively solve the shortcomings of the prior art.
To achieve the above object, the technical scheme adopted by the invention is as follows:A kind of production method that jujube juice is concentrated, including Following steps:
(1) sorting:Jujube is chosen, pest and disease damage fruit is removed, go mouldy fruit;
(2) it cleans:Through being bubbled the soil and partial impurities on flotation washer removal raw material surface, then by spray and two Cleaning machine is thoroughly cleaned;
(3) it extracts:After cleaning up red dates, weighed addition temperature control ultrasonic extraction tank, addition is had warmed up to 70- 80 DEG C of water obtains leaching liquor after extraction;
(4) it digests:The leaching liquor that step (3) processing obtains squeeze into enzymatic vessel after cooling to 48-55 DEG C, enzyme Enzymolysis liquid is obtained after solution;
(5) it decolourizes:Active carbon powder is added into enzymolysis liquid obtained in step (4), is stood after mixing evenly;
Wherein, the mass ratio of active carbon powder and enzymolysis liquid is 1: 1000-5: 1000;
(6) diatomite filters:Step (5) treated feed liquid is subjected to diatomite filtering;
(7) centrifugal filtration:Step (6) treated feed liquid is subjected to centrifugal filtration by disk plate centrifuge;
(8) primary sterilization:Enzyme deactivation sterilization is carried out to step (7) treated feed liquid using tubulation sterilization machine;
(9) ultrafiltration:Step (8) treated jujube juice is subjected to ultra-filtration filters by ultrafiltration system;
(10) electrodialysis process:By step (9), treated that jujube juice is pumped into electrodialysis plant carries out de- suffering reason;
(11) re-pasteurization:Using tubulation sterilization machine, to step (10), treated, and feed liquid is sterilized;
(12) second ultrafiltration:Step (11) treated jujube juice is subjected to ultra-filtration filters by ultrafiltration system;
(13) it is concentrated in vacuo:By step (12), treated that jujube juice is pumped into triple effect falling film evaporator is concentrated, and obtains half Finished product jujube juice;
(14) it sterilizes three times:Semi-finished product jujube juice after concentration in step (13) is sterilized through casing sterilization machine;
(15) filling and package:Concentration jujube juice after sterilization in step (14) is carried out using aseptic filler filling.
Further, in step (3), ultrasonic power is set as 180-250W, setpoint frequency 35-45kHz is extracted 30-60min。
Further, in step (4), hydrolysis temperature is set as 48-55 DEG C, pectase additive amount is 80-150ppm, is formed sediment Powder enzyme additive amount is 20-40ppm, enzymolysis time 60-120min.
Further, in step (5), time of repose 10-20min.
Further, in step (8) and (11), control sterilization temperature is 90-92 DEG C, and outlet temperature is less than 35 DEG C.
Further, in step (9) and step (12), ultrafiltration membrane aperture is 0.45 μm.
Further, in step (10), control voltage is 180V, electric current 20mA, and discharging conductance is 1100 μ s/cm.
Further, in step (13), control thickening temperature is 70-80 DEG C, and control discharging soluble solid is 69- 71%.
Further, in step (14), control sterilization temperature is 100-105 DEG C, and time 80-100s, drop temperature is less than 60℃。
Above-mentioned technical proposal of the invention has the advantages that:
(1) present invention uses ultrasonic-leaching, substantially reduces the process time of conventional water leaching and reduces and mentions Temperature is taken, the loss of the caramelization and thermal energy of product in process can be greatly reduced;
(2) heavy metal substance in jujube is removed present invention uses electrodialysis process and removes routine simultaneously The bitter taste of water leaching, while meeting the improved need for producing energy-efficient demand instantly and jujube juice product special flavour being concentrated It asks.
Specific embodiment
Embodiments of the present invention are described in further detail below with reference to embodiment.Following embodiment is for illustrating The present invention, but cannot be used to limit the scope of the invention.
In the description of the present invention, it should be noted that unless otherwise clearly defined and limited, term " connected ", " connection " shall be understood in a broad sense, for example, it may be being fixedly connected, may be a detachable connection, or be integrally connected;It can be with It is mechanical connection, is also possible to be electrically connected;It can be directly connected, it can also be indirectly connected through an intermediary.For ability For the those of ordinary skill in domain, the concrete meaning of above-mentioned term in the present invention can be understood with concrete condition.
Embodiment 1:
1, a kind of production method that jujube juice is concentrated, includes the following steps:
(1) sorting:Jujube is chosen, pest and disease damage fruit is removed, go mouldy fruit, uses high-quality golden jujube, it is desirable that meet GB/T 5835 regulation, pesticide residue and heavy metal index correspond with the regulation of GB 2763 and GB 2762;
(2) it cleans:Through being bubbled the soil and partial impurities on flotation washer removal raw material surface, then by spray and two Cleaning machine is thoroughly cleaned;
(3) it extracts:After cleaning up red dates, weighed addition temperature control ultrasonic extraction tank, addition is had warmed up to 70 DEG C Water, set ultrasonic power as 180W, setpoint frequency 35kHz extracts 30min, leaching liquor is obtained after extraction, wherein The quality of the water of addition is 3 times of jujube quality;
(4) it digests:It is squeezed into enzymatic vessel after the leaching liquor that step (3) processing obtains is cooled down, sets hydrolysis temperature It is 48 DEG C, pectase additive amount is 100ppm, and amylase additive amount is 20ppm, enzymolysis time 60min, obtains enzyme after enzymatic hydrolysis Solve liquid;
(5) it decolourizes:Active carbon powder is added into enzymolysis liquid obtained in step (4), is stood after mixing evenly 10min, wherein the mass ratio of active carbon powder and enzymolysis liquid is 5: 1000;
(6) diatomite filters:Step (5) treated feed liquid is subjected to diatomite filtering;
(7) centrifugal filtration:Step (6) treated feed liquid is subjected to centrifugal filtration by disk plate centrifuge;
(8) primary sterilization:Enzyme deactivation sterilization, control sterilization are carried out to step (7) treated feed liquid using tubulation sterilization machine Temperature is 90 DEG C, otherwise outlet temperature needs to cool down to discharging through plate heat exchanger less than 35 DEG C;
(9) ultrafiltration:Step (8) treated jujube juice is subjected to ultra-filtration filters, ultrafiltration membrane aperture by ultrafiltration system It is 0.45 μm.
(10) electrodialysis process:By step (9), treated that jujube juice is pumped into electrodialysis plant carries out de- suffering reason, control Voltage processed is 180V, electric current 20mA, and discharging conductance is 1100 μ s/cm.
(11) re-pasteurization:Using tubulation sterilization machine, to step (10), treated, and feed liquid is sterilized, control sterilization temperature Degree is 90 DEG C, otherwise outlet temperature needs to cool down to discharging through plate heat exchanger less than 35 DEG C;
(12) second ultrafiltration:Step (11) treated jujube juice is subjected to ultra-filtration filters, ultrafiltration fenestra by ultrafiltration system Diameter is 0.45 μm;
(13) it is concentrated in vacuo:By step (12), treated that jujube juice is pumped into triple effect falling film evaporator is concentrated, and obtains half Finished product jujube juice, in step (13), control thickening temperature is 70 DEG C, and control discharging soluble solid accounting is 69-71%;
(14) it sterilizes three times:Semi-finished product jujube juice after concentration in step (13) is sterilized through casing sterilization machine, is controlled Sterilization temperature is 100 DEG C, and time 80s, drop temperature is less than 60 DEG C.
(15) filling and package:Concentration jujube juice after sterilization in step (14) is carried out using aseptic filler it is filling, it is filling Into aseptic packaging complex pocket, outer packing uses carton or opening steel drum, and storage temperature is refrigerated less than 10 DEG C, cannot be freezed.
In the present embodiment, which clarifies bright, fragrant and sweet strong, sour and sweet palatability in brown color to sepia, Without the visible exogenous impurity of twenty-twenty vision.
Using ultrasonic-leaching, substantially reduces the process time of conventional water leaching and reduce Extracting temperature, energy The loss of the caramelization and thermal energy of product in process is greatly reduced;In addition used electrodialysis process to jujube In heavy metal substance removed and remove the bitter taste of conventional water leaching simultaneously, i.e., the technique simultaneously meet instantly It produces energy-efficient demand and the improved demand of jujube juice product special flavour is concentrated.
Embodiment 2:
1, a kind of production method that jujube juice is concentrated, includes the following steps:
(1) sorting:Jujube is chosen, pest and disease damage fruit is removed, go mouldy fruit, uses high-quality golden jujube, it is desirable that meet GB/T 5835 regulation, pesticide residue and heavy metal index correspond with the regulation of GB 2763 and GB 2762;
(2) it cleans:Through being bubbled the soil and partial impurities on flotation washer removal raw material surface, then by spray and two Cleaning machine is thoroughly cleaned;
(3) it extracts:After cleaning up red dates, weighed addition temperature control ultrasonic extraction tank, addition is had warmed up to 75 DEG C Water, set ultrasonic power as 200W, setpoint frequency 40kHz extracts 40min, leaching liquor is obtained after extraction, wherein The quality of the water of addition is 4 times of jujube quality;
(4) it digests:It is squeezed into enzymatic vessel after the leaching liquor that step (3) processing obtains is cooled down, sets hydrolysis temperature It is 52 DEG C, pectase additive amount is 120ppm, and amylase additive amount is 35ppm, enzymolysis time 80min, obtains enzyme after enzymatic hydrolysis Solve liquid;
(5) it decolourizes:Active carbon powder is added into enzymolysis liquid obtained in step (4), is stood after mixing evenly 15min, wherein the mass ratio of active carbon powder and enzymolysis liquid is 3: 1000;
(6) diatomite filters:Step (5) treated feed liquid is subjected to diatomite filtering;
(7) centrifugal filtration:Step (6) treated feed liquid is subjected to centrifugal filtration by disk plate centrifuge;
(8) primary sterilization:Enzyme deactivation sterilization, control sterilization are carried out to step (7) treated feed liquid using tubulation sterilization machine Temperature is 92 DEG C, otherwise outlet temperature needs to cool down to discharging through plate heat exchanger less than 35 DEG C;
(9) ultrafiltration:Step (8) treated jujube juice is subjected to ultra-filtration filters, ultrafiltration membrane aperture by ultrafiltration system It is 0.45 μm.
(10) electrodialysis process:By step (9), treated that jujube juice is pumped into electrodialysis plant carries out de- suffering reason, control Voltage processed is 180V, electric current 20mA, and discharging conductance is 1100 μ s/cm.
(11) re-pasteurization:Using tubulation sterilization machine, to step (10), treated, and feed liquid is sterilized, control sterilization temperature Degree is 92 DEG C, otherwise outlet temperature needs to cool down to discharging through plate heat exchanger less than 35 DEG C;
(12) second ultrafiltration:Step (11) treated jujube juice is subjected to ultra-filtration filters, ultrafiltration fenestra by ultrafiltration system Diameter is 0.45 μm;
(13) it is concentrated in vacuo:By step (12), treated that jujube juice is pumped into triple effect falling film evaporator is concentrated, and obtains half Finished product jujube juice, in step (13), control thickening temperature is 80 DEG C, and control discharging soluble solid accounting is 69-71%;
(14) it sterilizes three times:Semi-finished product jujube juice after concentration in step (13) is sterilized through casing sterilization machine, is controlled Sterilization temperature is 105 DEG C, and time 100s, drop temperature is less than 60 DEG C.
(15) filling and package:Concentration jujube juice after sterilization in step (14) is carried out using aseptic filler it is filling, it is filling Into aseptic packaging complex pocket, outer packing uses carton or opening steel drum, and storage temperature is refrigerated less than 10 DEG C, cannot be freezed.
The embodiment of the present invention is given for the purpose of illustration and description, and is not that exhaustively or incite somebody to action this Invention is limited to disclosed form.Many modifications and variations are obvious for the ordinary skill in the art. Selection and description embodiment are and to make the ordinary skill of this field to more preferably illustrate the principle of the present invention and practical application Personnel it will be appreciated that the present invention to designing various embodiments suitable for specific applications with various modifications.

Claims (9)

1. a kind of production method that jujube juice is concentrated, which is characterized in that include the following steps:
(1) sorting:Jujube is chosen, pest and disease damage fruit is removed, go mouldy fruit;
(2) it cleans:Through being bubbled the soil and partial impurities on flotation washer removal raw material surface, then by spray and two cleaning machines Thoroughly cleaned;
(3) it extracts:After cleaning up red dates, weighed addition temperature control ultrasonic extraction tank, addition is had warmed up to 70-80 DEG C Water obtains leaching liquor after extraction;
(4) it digests:The leaching liquor that step (3) processing obtains is cooled down, is squeezed into enzymatic vessel after cooling to 48-55 DEG C, enzyme Enzymolysis liquid is obtained after solution;
(5) it decolourizes:Active carbon powder is added into enzymolysis liquid obtained in step (4), is stood after mixing evenly;
Wherein, the mass ratio of active carbon powder and enzymolysis liquid is 1: 1000-5: 1000;
(6) diatomite filters:Step (5) treated feed liquid is subjected to diatomite filtering;
(7) centrifugal filtration:Step (6) treated feed liquid is subjected to centrifugal filtration by disk plate centrifuge;
(8) primary sterilization:Enzyme deactivation sterilization is carried out to step (7) treated feed liquid using tubulation sterilization machine;
(9) ultrafiltration:Step (8) treated jujube juice is subjected to ultra-filtration filters by ultrafiltration system;
(10) electrodialysis process:By step (9), treated that jujube juice is pumped into electrodialysis plant carries out de- suffering reason;
(11) re-pasteurization:Using tubulation sterilization machine, to step (10), treated, and feed liquid is sterilized;
(12) second ultrafiltration:Step (11) treated jujube juice is subjected to ultra-filtration filters by ultrafiltration system;
(13) it is concentrated in vacuo:By step (12), treated that jujube juice is pumped into triple effect falling film evaporator is concentrated, and obtains semi-finished product Jujube juice;
(14) it sterilizes three times:Semi-finished product jujube juice after concentration in step (13) is sterilized through casing sterilization machine;
(15) filling and package:Concentration jujube juice after sterilization in step (14) is carried out using aseptic filler filling.
2. a kind of production method that jujube juice is concentrated according to claim 1, which is characterized in that in step (3), setting Ultrasonic power is 180-250W, setpoint frequency 35-45kHz, extracts 30-60min.
3. a kind of production method that jujube juice is concentrated according to claim 1, which is characterized in that in step (4), setting Hydrolysis temperature is 48-55 DEG C, and pectase additive amount is 80-150ppm, and amylase additive amount is 20-40ppm, and enzymolysis time is 60-120min。
4. a kind of production method that jujube juice is concentrated according to claim 1, which is characterized in that in step (5), stand Time is 10-20min.
5. a kind of production method that jujube juice is concentrated according to claim 1, which is characterized in that in step (8) and (11) In, control sterilization temperature is 90-92 DEG C, and outlet temperature is less than 35 DEG C.
6. a kind of production method that jujube juice is concentrated according to claim 1, which is characterized in that in step (9) and step (12) in, ultrafiltration membrane aperture is 0.45 μm.
7. a kind of production method that jujube juice is concentrated according to claim 1, which is characterized in that in step (10), control Voltage processed is 180V, electric current 20mA, and discharging conductance is 1100 μ s/cm.
8. a kind of production method that jujube juice is concentrated according to claim 1, which is characterized in that in step (13), control Thickening temperature processed is 70-80 DEG C, and control discharging soluble solid is 69-71%.
9. a kind of production method that jujube juice is concentrated according to claim 1, which is characterized in that in step (14), control Sterilization temperature processed is 100-105 DEG C, and time 80-100s, drop temperature is less than 60 DEG C.
CN201810617297.4A 2018-06-15 2018-06-15 A kind of production method that jujube juice is concentrated Pending CN108835466A (en)

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CN111938047A (en) * 2020-09-03 2020-11-17 河北沛然世纪生物食品有限公司 Preparation method of concentrated black date clear juice

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Publication number Priority date Publication date Assignee Title
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