CN108821401A - A kind of sewage-treating agent and preparation method thereof for inhaling loach extract containing China - Google Patents
A kind of sewage-treating agent and preparation method thereof for inhaling loach extract containing China Download PDFInfo
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- CN108821401A CN108821401A CN201810703229.XA CN201810703229A CN108821401A CN 108821401 A CN108821401 A CN 108821401A CN 201810703229 A CN201810703229 A CN 201810703229A CN 108821401 A CN108821401 A CN 108821401A
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- china
- sewage
- loach
- treating agent
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/50—Treatment of water, waste water, or sewage by addition or application of a germicide or by oligodynamic treatment
Abstract
The invention discloses a kind of sewage-treating agents and preparation method thereof that loach extract is inhaled containing China.The sewage-treating agent includes the raw material of following parts by weight：15-20 parts of loach extract, 8-15 parts of Geniposidic acid, 4-8 parts of dust-brand reindeer moss, 5-14 parts of L-carnitine-L-tartrate, 6-12 parts of pyrrolidone sodium carboxylate are inhaled by China.COD, BOD, SS, NH in sanitary sewage can be greatly lowered in sewage-treating agent of the invention3- N and Pb content, and there is apparent fungistatic effect；Raw material of the present invention is easy to get environmental protection, and treated, and water reaches recycling standard, and treatment effect is fairly obvious, is worth of widely use.
Description
Technical field
The present invention relates to a kind of sewage-treating agent, specifically a kind of sewage-treating agent and its system that loach extract is inhaled containing China
Preparation Method.
Background technique
The sewage generated during human lives, is one of primary pollution source of water body.Mainly excrement and wash water.
Everyone sanitary sewage amount being discharged daily of city is 150-400L, and amount and living standard have substantial connection.Contain in sanitary sewage
There are large amount of organic, such as cellulose, starch, carbohydrate and fat protein；Also often contain pathogen, virus and parasitic ovum；
Chloride, sulfate, phosphate, bicarbonate and the sodium of inorganic salts, potassium, calcium, magnesium etc..Total feature be nitrogenous, sulfur-bearing and
Phosphorous height, under anaerobic bacteria effect, easily raw odorant.
The chemical agent of raw material complexity is mostly used for the processing of sanitary sewage at present, treated, and that sewage contains is biggish
Toxicity is unfavorable for the recycling of sewage.Therefore, the present invention provides a kind of sewage treatment that loach extract is inhaled containing China of environmental protection
Agent and preparation method thereof.
Summary of the invention
The purpose of the present invention is to provide a kind of sewage-treating agents and preparation method thereof that loach extract is inhaled containing China, with solution
Certainly the problems mentioned above in the background art.
To achieve the above object, the present invention provides the following technical solutions：
A kind of sewage-treating agent for inhaling loach extract containing China, the raw material including following parts by weight：Loach extract is inhaled by China
15-20 parts, 8-15 parts of Geniposidic acid, 4-8 parts of dust-brand reindeer moss, 5-14 parts of L-carnitine-L-tartrate, pyrrolidone sodium carboxylate
6-12 parts.
As a further solution of the present invention：Raw material including following parts by weight：16-18 parts of loach extract, capital are inhaled by China
Buddhist nun is thuja acid 10-13 parts flat, 5-7 parts of dust-brand reindeer moss, 8-12 parts of L-carnitine-L-tartrate, 8-10 parts of pyrrolidone sodium carboxylate.
As a further solution of the present invention：Raw material including following parts by weight：17 parts of loach extract, Geniposide are inhaled by China
12 parts of thuja acid, 6 parts of dust-brand reindeer moss, 10 parts of L-carnitine-L-tartrate, 9 parts of pyrrolidone sodium carboxylate.
As a further solution of the present invention：It is described China inhale loach extract preparation method be：Loach dissection is inhaled by China, is first put
It is placed at subzero 10 to subzero 5 DEG C and freezes 20-30h；It is then placed at 100-200 DEG C and dries 4-7h, be ground up, sieved after taking-up
200-300 mesh；Gains are added in the ethanol solution that 30-50 parts of mass fractions are 85% later, are placed at 45-60 DEG C and stir
React 3-5h, vacuum distillation recycling ethyl alcohol；Residue is placed at subzero 10 to subzero 5 DEG C and freezes 15-20h, and 65-85 is then added
It in the water of 75 DEG C of part, is placed at 85-90 DEG C and is stirred 1-2h, filter, obtain filtrate to get China and inhale loach extract.
A kind of preparation method of sewage-treating agent that inhaling loach extract containing China, includes the following steps：
(1) loach extract is inhaled by China to mix with L-carnitine-L-tartrate, is placed at 85-95 DEG C and is stirred to react 10-
20min；
(2) Geniposidic acid is mixed with 20-30 parts of water, pyrrolidone sodium carboxylate is then added, is placed at 90-100 DEG C
It is stirred to react 1-3h；
(3) dust-brand reindeer moss is pulverized and sieved into 300-400 mesh, then dust-brand reindeer moss powder is put into step (1) gains,
It is placed at 90-98 DEG C and is stirred to react 10-20min；
(4) step (2) gains are mixed with step (3) gains, are placed at 75-90 DEG C and are stirred to react 10-35min,
Then by gains it is dry to get.
As a further solution of the present invention：China is inhaled loach extract and mixed with L-carnitine-L-tartrate by step (1), is set
16min is stirred to react at 90 DEG C.
As a further solution of the present invention：Step (2) mixes Geniposidic acid with 26 parts of water, and pyrrolidines is then added
Keto carboxylic acid sodium is placed at 96 DEG C and is stirred to react 2h.
As a further solution of the present invention：Dust-brand reindeer moss is pulverized and sieved 350 mesh by step (3), then by dust-brand reindeer moss
Powder is put into step (1) gains, is placed at 95 DEG C and is stirred to react 14min.
As a further solution of the present invention：Step (4) mixes step (2) gains with step (3) gains, is placed in
22min is stirred to react at 82 DEG C, then by gains it is dry to get.
Compared with prior art, the beneficial effects of the invention are as follows：
Sewage-treating agent of the invention inhales loach extract, Geniposidic acid, dust-brand reindeer moss, L-Carnitine tartrate by China
Salt and pyrrolidone sodium carboxylate are prepared as a raw material, and COD, BOD, SS, NH in sanitary sewage can be greatly lowered3- N and Pb
Content, and there is apparent fungistatic effect；Raw material of the present invention is easy to get environmental protection, and treated, and water reaches recycling standard, processing
Effect is fairly obvious, is worth of widely use.
Specific embodiment
The technical solution of the patent is explained in further detail With reference to embodiment.
Embodiment 1
A kind of sewage-treating agent for inhaling loach extract containing China, the raw material including following parts by weight：Loach extract is inhaled by China
15 parts, 8 parts of Geniposidic acid, 4 parts of dust-brand reindeer moss, 5 parts of L-carnitine-L-tartrate, 6 parts of pyrrolidone sodium carboxylate.The China inhales
Loach is that loach inhales in the China of artificial breeding.
It is described China inhale loach extract preparation method be：Loach dissection is inhaled by China, is first placed at subzero 10 DEG C and freezes 20h；
It is then placed at 100 DEG C and dries 4h, 200 mesh are ground up, sieved after taking-up；It is 85% that 30 parts of mass fractions, which are added, in gains later
Ethanol solution in, be placed at 45 DEG C and be stirred to react 3h, vacuum distillation recycling ethyl alcohol；Residue is placed at subzero 10 DEG C and freezes
Then 15h is added in 65 parts 75 DEG C of water, is placed at 85 DEG C and is stirred 1h, filters, obtain filtrate to get China and inhale loach extraction
Object.
A kind of preparation method of sewage-treating agent that inhaling loach extract containing China, includes the following steps：
(1) loach extract is inhaled by China to mix with L-carnitine-L-tartrate, is placed at 85 DEG C and is stirred to react 10min；
(2) Geniposidic acid is mixed with 20 parts of water, pyrrolidone sodium carboxylate is then added, is placed at 90 DEG C and is stirred to react
1h；
(3) dust-brand reindeer moss is pulverized and sieved into 300 mesh, then dust-brand reindeer moss powder is put into step (1) gains, is placed in
10min is stirred to react at 90 DEG C；
(4) step (2) gains are mixed with step (3) gains, is placed at 75 DEG C and is stirred to react 10min, then will
Gains it is dry to get.
Embodiment 2
A kind of sewage-treating agent for inhaling loach extract containing China, the raw material including following parts by weight：Loach extract is inhaled by China
20 parts, 15 parts of Geniposidic acid, 8 parts of dust-brand reindeer moss, 14 parts of L-carnitine-L-tartrate, 12 parts of pyrrolidone sodium carboxylate.
It is described China inhale loach extract preparation method be：Loach dissection is inhaled by China, is first placed at subzero 5 DEG C and freezes 30h；So
After be placed at 200 DEG C and dry 7h, 300 mesh are ground up, sieved after taking-up；It is 85% that 50 parts of mass fractions, which are added, in gains later
In ethanol solution, it is placed at 60 DEG C and is stirred to react 5h, vacuum distillation recycling ethyl alcohol；Residue is placed at subzero 5 DEG C and freezes 20h,
Then it is added in 85 parts 75 DEG C of water, is placed at 90 DEG C and is stirred 2h, filter, obtain filtrate to get China and inhale loach extract.
A kind of preparation method of sewage-treating agent that inhaling loach extract containing China, includes the following steps：
(1) loach extract is inhaled by China to mix with L-carnitine-L-tartrate, is placed at 95 DEG C and is stirred to react 20min；
(2) Geniposidic acid is mixed with 30 parts of water, pyrrolidone sodium carboxylate is then added, be placed at 100 DEG C and stir instead
Answer 3h；
(3) dust-brand reindeer moss is pulverized and sieved into 400 mesh, then dust-brand reindeer moss powder is put into step (1) gains, is placed in
20min is stirred to react at 98 DEG C；
(4) step (2) gains are mixed with step (3) gains, is placed at 90 DEG C and is stirred to react 35min, then will
Gains it is dry to get.
Embodiment 3
A kind of sewage-treating agent for inhaling loach extract containing China, the raw material including following parts by weight：Loach extract is inhaled by China
17 parts, 12 parts of Geniposidic acid, 6 parts of dust-brand reindeer moss, 10 parts of L-carnitine-L-tartrate, 9 parts of pyrrolidone sodium carboxylate.
It is described China inhale loach extract preparation method be：Loach dissection is inhaled by China, is first placed at subzero 6 DEG C and freezes 25h；So
After be placed at 128 DEG C and dry 5h, 260 mesh are ground up, sieved after taking-up；It is 85% that 42 parts of mass fractions, which are added, in gains later
In ethanol solution, it is placed at 50 DEG C and is stirred to react 4h, vacuum distillation recycling ethyl alcohol；Residue is placed at subzero 7 DEG C and freezes 17h,
Then it is added in 75 parts 75 DEG C of water, is placed at 88 DEG C and is stirred 1.3h, filter, obtain filtrate to get China and inhale loach extract.
A kind of preparation method of sewage-treating agent that inhaling loach extract containing China, includes the following steps：
(1) loach extract is inhaled by China to mix with L-carnitine-L-tartrate, is placed at 90 DEG C and is stirred to react 16min.
(2) Geniposidic acid is mixed with 26 parts of water, pyrrolidone sodium carboxylate is then added, is placed at 96 DEG C and is stirred to react
2h。
(3) dust-brand reindeer moss is pulverized and sieved into 350 mesh, then dust-brand reindeer moss powder is put into step (1) gains, is placed in
14min is stirred to react at 95 DEG C.
(4) step (2) gains are mixed with step (3) gains, is placed at 82 DEG C and is stirred to react 22min, then will
Gains it is dry to get.
Embodiment 4
As different from Example 3, sewage-treating agent includes the raw material of following parts by weight：China's 16 parts of loach extract of suction,
10 parts of Geniposidic acid, 5 parts of dust-brand reindeer moss, 8 parts of L-carnitine-L-tartrate, 8 parts of pyrrolidone sodium carboxylate.
Embodiment 5
As different from Example 3, sewage-treating agent includes the raw material of following parts by weight：China's 18 parts of loach extract of suction,
13 parts of Geniposidic acid, 7 parts of dust-brand reindeer moss, 12 parts of L-carnitine-L-tartrate, 10 parts of pyrrolidone sodium carboxylate.
Comparative example 1
In addition to inhaling loach extract without containing China in raw material, other preparation processes are consistent with embodiment 3.
Comparative example 2
In addition to not containing Geniposidic acid in raw material, other preparation processes are consistent with embodiment 3.
Comparative example 3
In addition to inhaling loach extract and Geniposidic acid without containing China in raw material, other preparation processes and embodiment 3 keep one
It causes.
Comparative example 4
Raw material is consistent with embodiment 3, preparation process：By all raw materials be uniformly mixed together to get.
Experimental example
The sewage-treating agent of Application Example 1-3 and comparative example 1-4 preparation carries out sanitary sewage disposal, and treatment effect is as follows
Shown in table, (unit mg/L).
Table 1
The fungistatic effect of embodiment 3 and the sewage-treating agent of comparative example 1-4 preparation is as shown in the table.
Table 2
The preferred embodiment of the patent is described in detail above, but this patent is not limited to above-mentioned embodiment party
Formula within the knowledge of one of ordinary skill in the art can also be under the premise of not departing from this patent objective
Various changes can be made.
Claims (9)
1. a kind of sewage-treating agent for inhaling loach extract containing China, which is characterized in that the raw material including following parts by weight：China inhales
15-20 parts of loach extract, 8-15 parts of Geniposidic acid, 4-8 parts of dust-brand reindeer moss, 5-14 parts of L-carnitine-L-tartrate, pyrrolidines
6-12 parts of keto carboxylic acid sodium.
2. the sewage-treating agent method according to claim 1 for inhaling loach extract containing China, which is characterized in that including following heavy
Measure the raw material of number：16-18 parts of loach extract, 10-13 parts of Geniposidic acid, 5-7 parts of dust-brand reindeer moss, L-carnitine winestone are inhaled by China
8-12 parts of hydrochlorate, 8-10 parts of pyrrolidone sodium carboxylate.
3. the sewage-treating agent method according to claim 1 for inhaling loach extract containing China, which is characterized in that including following heavy
Measure the raw material of number：17 parts of loach extract, 12 parts of Geniposidic acid, 6 parts of dust-brand reindeer moss, L-carnitine-L-tartrate 10 are inhaled by China
Part, 9 parts of pyrrolidone sodium carboxylate.
4. the sewage-treating agent method according to claim 1 for inhaling loach extract containing China, which is characterized in that loach inhales in the China
The preparation method of extract is：Loach dissection is inhaled by China, is first placed at subzero 10 to subzero 5 DEG C and freezes 20-30h；Then it places
4-7h is dried at 100-200 DEG C, and 200-300 mesh is ground up, sieved after taking-up；It is by gains 30-50 parts of mass fractions of addition later
In 85% ethanol solution, it is placed at 45-60 DEG C and is stirred to react 3-5h, vacuum distillation recycling ethyl alcohol；Residue is placed in subzero 10
15-20h is freezed to subzero 5 DEG C, is then added in the water of 75 DEG C of 65-85 part, is placed at 85-90 DEG C and is stirred 1-2h, mistake
Filter obtains filtrate to get China and inhales loach extract.
5. a kind of preparation method of the sewage-treating agent according to claim 1 to 4 that loach extract is inhaled containing China,
It is characterized in that, includes the following steps：
(1) loach extract is inhaled by China to mix with L-carnitine-L-tartrate, is placed at 85-95 DEG C and is stirred to react 10-20min；
(2) Geniposidic acid is mixed with 20-30 parts of water, pyrrolidone sodium carboxylate is then added, is placed at 90-100 DEG C and stirs
React 1-3h；
(3) dust-brand reindeer moss is pulverized and sieved into 300-400 mesh, then dust-brand reindeer moss powder is put into step (1) gains, is placed in
10-20min is stirred to react at 90-98 DEG C；
(4) step (2) gains are mixed with step (3) gains, is placed at 75-90 DEG C and is stirred to react 10-35min, then
By gains it is dry to get.
6. the preparation method of the sewage-treating agent according to claim 5 for inhaling loach extract containing China, which is characterized in that step
Suddenly China is inhaled loach extract and mixed with L-carnitine-L-tartrate by (1), is placed at 90 DEG C and is stirred to react 16min.
7. the preparation method of the sewage-treating agent according to claim 5 for inhaling loach extract containing China, which is characterized in that step
Suddenly (2) mix Geniposidic acid with 26 parts of water, and pyrrolidone sodium carboxylate is then added, and are placed at 96 DEG C and are stirred to react 2h.
8. the preparation method of the sewage-treating agent according to claim 5 for inhaling loach extract containing China, which is characterized in that step
Suddenly dust-brand reindeer moss is pulverized and sieved 350 mesh by (3), and then dust-brand reindeer moss powder is put into step (1) gains, is placed at 95 DEG C
It is stirred to react 14min.
9. the preparation method of the sewage-treating agent according to claim 5 for inhaling loach extract containing China, which is characterized in that step
Suddenly (4) mix step (2) gains with step (3) gains, are placed at 82 DEG C and are stirred to react 22min, then by gains
It is dry to get.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810703229.XA CN108821401A (en) | 2018-06-30 | 2018-06-30 | A kind of sewage-treating agent and preparation method thereof for inhaling loach extract containing China |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810703229.XA CN108821401A (en) | 2018-06-30 | 2018-06-30 | A kind of sewage-treating agent and preparation method thereof for inhaling loach extract containing China |
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| Publication Number | Publication Date |
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| CN108821401A true CN108821401A (en) | 2018-11-16 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201810703229.XA Withdrawn CN108821401A (en) | 2018-06-30 | 2018-06-30 | A kind of sewage-treating agent and preparation method thereof for inhaling loach extract containing China |
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Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0928565A1 (en) * | 1997-12-17 | 1999-07-14 | Meta Handelsgesellschaft m.b.H. | Drinking liquid |
| CN108147478A (en) * | 2017-12-26 | 2018-06-12 | 刘春丽 | It is a kind of to be used to administer sewage-treating agent of cyanobacteria pollution and its preparation method and application |
| CN108147550A (en) * | 2017-11-30 | 2018-06-12 | 安徽宏远职业卫生技术服务有限公司 | A kind of special sewage-treating agent of trade effluent and preparation method thereof |
-
2018
- 2018-06-30 CN CN201810703229.XA patent/CN108821401A/en not_active Withdrawn
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0928565A1 (en) * | 1997-12-17 | 1999-07-14 | Meta Handelsgesellschaft m.b.H. | Drinking liquid |
| CN108147550A (en) * | 2017-11-30 | 2018-06-12 | 安徽宏远职业卫生技术服务有限公司 | A kind of special sewage-treating agent of trade effluent and preparation method thereof |
| CN108147478A (en) * | 2017-12-26 | 2018-06-12 | 刘春丽 | It is a kind of to be used to administer sewage-treating agent of cyanobacteria pollution and its preparation method and application |
Non-Patent Citations (3)
| Title |
|---|
| 丁彤等: "《中国化工产品大全 下》", 31 October 1994, 化学工业出版社 * |
| 朱亚民等: "《内蒙古植物药志 第一卷》", 31 December 2000, 内蒙古人民出版社 * |
| 顾觉奋等: "《离子交换与吸附树脂在制药工业上的应用》", 30 April 2008, 中国医药科技出版社 * |
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Application publication date: 20181116 |
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