CN108815923A - The manufacturing method of air purification filter skeletal support material - Google Patents

The manufacturing method of air purification filter skeletal support material Download PDF

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Publication number
CN108815923A
CN108815923A CN201810641176.3A CN201810641176A CN108815923A CN 108815923 A CN108815923 A CN 108815923A CN 201810641176 A CN201810641176 A CN 201810641176A CN 108815923 A CN108815923 A CN 108815923A
Authority
CN
China
Prior art keywords
support material
fiber
manufacturing
skeletal support
air purification
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201810641176.3A
Other languages
Chinese (zh)
Inventor
陈建斌
赵天君
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Winbond Ancient Building New Material Co Ltd
Zhejiang Lover Health Science and Technology Development Co Ltd
Zhejiang University of Science and Technology ZUST
Original Assignee
Winbond Ancient Building New Material Co Ltd
Zhejiang Lover Health Science and Technology Development Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Winbond Ancient Building New Material Co Ltd, Zhejiang Lover Health Science and Technology Development Co Ltd filed Critical Winbond Ancient Building New Material Co Ltd
Priority to CN201810641176.3A priority Critical patent/CN108815923A/en
Publication of CN108815923A publication Critical patent/CN108815923A/en
Pending legal-status Critical Current

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Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D39/00Filtering material for liquid or gaseous fluids
    • B01D39/14Other self-supporting filtering material ; Other filtering material
    • B01D39/16Other self-supporting filtering material ; Other filtering material of organic material, e.g. synthetic fibres
    • B01D39/1607Other self-supporting filtering material ; Other filtering material of organic material, e.g. synthetic fibres the material being fibrous
    • B01D39/1623Other self-supporting filtering material ; Other filtering material of organic material, e.g. synthetic fibres the material being fibrous of synthetic origin
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D46/00Filters or filtering processes specially modified for separating dispersed particles from gases or vapours

Abstract

The invention discloses a kind of manufacturing methods of air purification filter skeletal support material, it is intended to provide that a kind of manufacturing process is simple, air permeability is high, stiffness is high, vapour lock is small, the manufacturing method of the skeleton support material of free from extraneous odour, its key points of the technical solution are that the PET fiber of several different sizes is mixed, body paper is manufactured paper with pulp into through oblique net paper machine wet process and passes through coating process, and the present invention is suitable for indoor air purification material preparation technical field.

Description

The manufacturing method of air purification filter skeletal support material
Technical field
The invention belongs to indoor air purification material preparation technical fields, refer in particular to a kind of air purification filter skeletal support material The manufacturing method of material.
Background technique
With the development of society, air pollution is increasingly severe, fog is increasingly severe in city, with people's life matter The continuous promotion of amount, is also being continuously increased the attention degree of health problem, family higher and higher to the purity requirements of air It is becoming increasingly popular with air purifier, the air filting material of selection needs superior filter efficiency.Existing high filtration effect The filtering material of rate is mainly to be compounded on skeletal support material by one layer of filter membrane with very filtration efficiency, existing bone Frame backing material usually passes through plant fiber and chemical fibre is mixed to prepare, but selects plant fiber not environmentally friendly enough;And it selects single When the chemical fibre of one specification, fiber bonding strength difference causes body paper without intensity, and application difficulties, chemical fibre dispersion is compared with wood pulp fibre Dimension difference causes formation of sheet difference quantitatively to fluctuate greatly;Furthermore also use inorfil for material, such as glass fibre, but glass fibers Tie up higher cost, cause filtering material vapour lock big there is also gas permeability is poor, very difference of hardness, fold poor in processability the problems such as.
Summary of the invention
That the object of the present invention is to provide a kind of manufacturing processes is simple, air permeability is high, stiffness is high, vapour lock is small, the bone of free from extraneous odour The manufacturing method of frame support material.
The object of the present invention is achieved like this:The manufacturing method of air purification filter skeletal support material, feature exist In:Include the following steps:
(1), the PET fiber of at least two specifications is proportionally added into stock tank and discongests mashing processing, it is fine that mixing is made Dimension, and sequentially add dispersing agent and wet strength agent is stirred, PET fiber specification requirement be rugosity between 1.5-25dtex, it is long Degree is between 12-25mm.
(2), composite fibre is manufactured paper with pulp into body paper through oblique net paper machine, body paper is batched after dry by coating fluid coating process At finished product.
The present invention is further arranged to:The coating fluid is the acrylic latex or styrene-acrylic latex of 20%-30% concentration.
The present invention is further arranged to:PET fiber body paper made from the different size accounts for air filting material skeleton branch Mass percent in timbering material is 65%-75%, and coating fluid accounts for the quality percentage in air filting material skeletal support material Than for 25%-35%.
The present invention is further arranged to:In step (1), composite fibre slurry concentration is controlled between 3-5%, and adjusts Ph value is heated to 120 DEG C and stirs 5 minutes to 9, and later plus cold water is diluted between concentration 0.5-0.7%, and be down to room temperature and Adjust PH to 6.
The present invention is further arranged to:The coating fluid is modified processing in advance, adds nanometer in coating fluid per hundred parts 1 part of copper, 2 parts of nano-calcium carbonate calcium powder, 2 parts of nano active powdered carbon and 3 parts of aqueous compound emulsifying agent.
The present invention is further arranged to:In step (2), by being sucked by vacuum dehydration before the coating of body paper caused by copying, Make moisture percentage between 50-55%.
The present invention is further arranged to:It is dry in step (2):It first passes through infrared drier and carries out pre-dried, it is dry Temperature is 200 DEG C;It is dried using air drier, drying temperature is 180 DEG C;It is finally dried by baking oven, baking oven temperature Degree is 210 DEG C.
The present invention is further arranged to:The PET fiber specification is that two kinds of 7dtex*12mm including 20-40% content are fine Tie up the fiber B of the 25dtex*25mm of A and 60-80% content.
The present invention is further arranged to:The PET fiber specification is that three kinds of 7dtex*12mm including 30-60% content are fine Tie up 1.5dtex*12mm fiber C, fiber A, the fiber B of 25dtex*25mm fiber B and the 10-20% content of A, 20-60% content Total amount with the sum of fiber C three is 100%.
It is had the following advantages that by using above-mentioned technical proposal:
1, body paper is manufactured paper with pulp by inclined wire wet process, and fiber interweaving is good, and Air permenbility is high, and vapour lock is small, and stiff degree is high;
2, with coating fluid it is compound after, filtering accuracy and Air permenbility can be increased, the whole of filtering material can be effectively reduced Body vapour lock;
It 3, can be by adjusting the ratio of different rugosity fibers, the permeability and stiffness of controlled material.
4, this material selects PET fiber, and low in cost, fold processability is good, and manufacturing process is also simple, is more suitable and pushes away Extensively.
Detailed description of the invention
Fig. 1 is the linear graph that body paper moisture percentage of the invention influences the absorbability of 25% acrylic latex.
Specific embodiment
With specific embodiment, the invention will be further described with reference to the accompanying drawing:
The manufacturing method of air purification filter skeletal support material, includes the following steps:
(1) PET fiber of at least two specifications is proportionally added into the stock tank of beater and discongest mashing processing, Composite fibre is made, composite fibre slurry concentration controls between 3-5%, and adjusts ph value to 9, and is heated to 120 DEG C of stirrings 5 Minute, later plus cold water is diluted between concentration 0.5-0.7%, and is down to room temperature and is adjusted PH to 6, and dispersing agent and wet is added Strong agent continues stirring 10 minutes, PET fiber specification requirement be rugosity between 1.5-25dtex, length is between 12-25mm;
(2), composite fibre is manufactured paper with pulp into body paper through oblique net paper machine;
(3), it is dehydrated:By body paper by vacuum suction dehydration, make moisture percentage between 50-55%;
(4), coating fluid selects the acrylic latex or styrene-acrylic latex of 20%-30% concentration, addition in coating fluid per hundred parts 1 part of Nanometer Copper, 2 parts of nano-calcium carbonate calcium powder, 2 parts of nano active powdered carbon and 3 parts of aqueous compound emulsifying agent, stir evenly mixing, into Row modification;
(5), it is glued:Coating fluid is sprayed at dewatered body paper surface;
(6), dry:It first passes through infrared drier and carries out pre-dried, drying temperature is 200 DEG C;Using hot air drying Dry machine is dried, and drying temperature is 180 DEG C;It is finally dried by baking oven, oven temperature is 210 DEG C;Using this drying side Method, reaching required standard moisture content only needed in 60-70 seconds, and rate of drying greatly improves;
(7), it is wound into finished product.
In step (1), this product selects PET fiber, and fold processability is good, low in cost, the composite fibre of different size Slurry carries out basic treatment by heating in advance and lye being added, and can improve the smoothness of fiber surface, improves soil resistance, and It enables to after causing body paper, air permeability improves;Acid solution is added later to neutralize, and makes its slant acidity, is convenient for after forming and coating Liquid can be preferably compound;Dispersing agent can be such that PET fiber is preferably dispersed in water, soluble easily in water;Wet strength agent can increase Wet strength.
In step (2), body paper is manufactured paper with pulp by inclined wire wet process, and fiber interweaving is good, and Air permenbility is high, and vapour lock is small, stiff degree It is high.
In step (3), it is dehydrated by the way of vacuum dehydration, vacuum degree control makes it in 0.12MPa-0.13MPa Moisture percentage between 50-55%, show by test of many times as shown in Figure 1, when moisture percentage be higher than 55% when, body paper absorbability Small, coating fluid is not easy to be absorbed, application difficulties;When moisture percentage is lower than 50%, when spraying, body paper absorbability increase increased Fastly, it being easy transfer accumulation after coating fluid spraying, uniformity is bad, lead to air permeability and the stiffness decline of backing material, so its Make moisture percentage between 50-55% when, Painting effect is best, and be coated with after air permeability and stiffness be preferably also.
In step (4), acrylic latex or styrene-acrylic latex can increase the intensity and stiffness of backing material, and to support The resistance performance Index Influence of material is also small, wherein select 20%-30% concentration when, effect is best, by addition Nanometer Copper and The wearability of backing material can be improved in the addition of nano-calcium carbonate calcium powder, improves material by the addition of nano active powdered carbon Antibiotic property can make Nanometer Copper, nano-calcium carbonate calcium powder and nano active powdered carbon more equal by the addition of aqueous compound emulsifying agent Even is dispersed in acrylic latex or styrene-acrylic latex, improves final using effect.
In step (6), before drying, body paper also has more water content, directlys adopt baking oven according to traditional The mode of drying, drying time is long, and moisture is not easy outlet, although final water content is extremely low, can surpass and body paper hole is caused to receive Contracting, air permeability and stiffness decline, this technology carry out pre-dried by infrared drier, and thermal break-through ability is strong, can be to material Inside carries out convection drying, and by air drier, carries out quick outlet to the steam generated after material heating, finally by Baking oven carries out freeze-day with constant temperature, short the time required to dry, can reach standard needed for moisture content, backing material will not generate change Shape, it is ensured that the requirement of air permeability and stiffness.
Wherein PET fiber body paper made from different size accounts for the mass percent in air filting material skeletal support material For 65%-75%, coating fluid accounts for the mass percent in air filting material skeletal support material for 25%-35%, in use State proportion, the spraying effect of PET fiber body paper and coating fluid is best, and backing material stiffness obtained is high, air permeability is high.
Specific embodiment 1-8 is made by above-mentioned manufacturing method according to the different ratio system of different ratio different size fiber, As shown in table 1.
Table 1:
Experimental test is carried out by backing material made from embodiment 1-8, such as the following table 2 is made:
Table 2:
In conjunction with table 1-2 it is recognized that while can be reached when using two kinds, three kinds, four kinds or the fiber with more kinds of specifications To control standard, but when using three kinds of gauge fiber proportions, attainable air permeability and stiffness are best, and embodiment 4-6 is equal For optimum embodiment, and in embodiment 4 fiber by 30%7dtex*12mmPET fiber+60%25dtex*25mmPET fiber+ When the ratio investment of 10%1.5dtex*12mmPET, effect is best.
Continue test obtain when selecting above-mentioned three kinds of specifications, with 25dtex*25mmPET fiber content by 30% to 60% is gradually increased, and stiffness and air permeability will be slow raising, but when 25dtex*25mmPET fiber content is higher than 60%, Stiffness and air permeability can accelerate to decline, therefore when PET fiber specification is three kinds of 7dtex*12mm fibers including 30-60% content A, the 1.5dtex*12mm fiber C of 25dtex*25mm fiber B and the 10-20% content of 20-60% content, and fiber A, fiber B Total amount with the sum of fiber C three is 100%, and backing material comprehensive performance obtained is best.
In addition, in embodiment 4-6, but the rugosity of fiber A can float between 6-8dtex, and the rugosity of fiber B can be with It floats between 23-25dtex, the rugosity of fiber C can float between 1.5-3dtex, and backing material obtained is comprehensive It can be closer to.
Above-described embodiment is only presently preferred embodiments of the present invention, is not limited the scope of the invention according to this, therefore:It is all according to The equivalence changes that structure of the invention, shape, principle are done, should all be covered by within protection scope of the present invention.

Claims (9)

1. the manufacturing method of air purification filter skeletal support material, it is characterised in that:Include the following steps:
(1), the PET fiber of at least two specifications is proportionally added into stock tank and discongests mashing processing, composite fibre is made, and Sequentially add dispersing agent and wet strength agent be stirred, PET fiber specification requirement be rugosity between 1.5-25dtex, length exists Between 12-25mm;
(2), composite fibre is manufactured paper with pulp into body paper through oblique net paper machine, body paper is coiled into after dry by coating fluid coating process Product.
2. the manufacturing method of air purification filter skeletal support material according to claim 1, it is characterised in that:The painting Cloth liquid is the acrylic latex or styrene-acrylic latex of 20%-30% concentration.
3. the manufacturing method of air purification filter skeletal support material according to claim 1, it is characterised in that:It is described not It is 65%-75% that PET fiber body paper made from same specification, which accounts for the mass percent in air filting material skeletal support material, is applied It is 25%-35% that cloth liquid, which accounts for the mass percent in air filting material skeletal support material,.
4. the manufacturing method of air purification filter skeletal support material according to claim 1, it is characterised in that:Step (1) in, composite fibre slurry concentration is controlled between 3-5%, and adjusts ph value to 9, and is heated to 120 DEG C and is stirred 5 minutes, Later plus cold water is diluted between concentration 0.5-0.7%, and is down to room temperature and is adjusted PH to 6.
5. the manufacturing method of air purification filter skeletal support material according to claim 1, it is characterised in that:The painting Cloth liquid is modified processing in advance, adds 1 part of Nanometer Copper, 2 parts of nano-calcium carbonate calcium powder, nano active powdered carbon in coating fluid per hundred parts 2 parts and 3 parts of aqueous compound emulsifying agent.
6. the manufacturing method of air purification filter skeletal support material according to claim 1, it is characterised in that:Step (2) in, by vacuum suction dehydration before the coating of body paper caused by copying, make moisture percentage between 50-55%.
7. the manufacturing method of air purification filter skeletal support material according to claim 1, it is characterised in that:Step (2) dry in:It first passes through infrared drier and carries out pre-dried, drying temperature is 200 DEG C;Using air drier into Row drying, drying temperature are 180 DEG C;It is finally dried by baking oven, oven temperature is 210 DEG C.
8. the manufacturing method of air purification filter skeletal support material according to claim 1, it is characterised in that:It is described PET fiber specification is the 25dtex*25mm's of two kinds of 7dtex*12mm fiber A and 60-80% contents for including 20-40% content Fiber B.
9. the manufacturing method of air purification filter skeletal support material according to claim 1, it is characterised in that:It is described PET fiber specification is that the 25dtex*25mm of three kinds of 7dtex*12mm fiber A, 20-60% contents for including 30-60% content is fine The total amount for tieing up the sum of 1.5dtex*12mm fiber C, fiber A, fiber B and fiber C three of B and 10-20% content is 100%.
CN201810641176.3A 2018-06-21 2018-06-21 The manufacturing method of air purification filter skeletal support material Pending CN108815923A (en)

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Application Number Priority Date Filing Date Title
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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110523141A (en) * 2019-07-26 2019-12-03 杭州特种纸业有限公司 A kind of air filtering material skeleton
CN115069098A (en) * 2022-08-23 2022-09-20 佛山(华南)新材料研究院 Alumina fiber filter membrane and preparation method thereof

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105934266A (en) * 2014-01-28 2016-09-07 帝人株式会社 Multilayer filtration material for filter, method for manufacturing same, and air filter
WO2017208952A1 (en) * 2016-06-01 2017-12-07 ダイニック株式会社 Air-filter medium

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105934266A (en) * 2014-01-28 2016-09-07 帝人株式会社 Multilayer filtration material for filter, method for manufacturing same, and air filter
WO2017208952A1 (en) * 2016-06-01 2017-12-07 ダイニック株式会社 Air-filter medium

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110523141A (en) * 2019-07-26 2019-12-03 杭州特种纸业有限公司 A kind of air filtering material skeleton
CN115069098A (en) * 2022-08-23 2022-09-20 佛山(华南)新材料研究院 Alumina fiber filter membrane and preparation method thereof
CN115069098B (en) * 2022-08-23 2022-11-08 佛山(华南)新材料研究院 Alumina fiber filter membrane and preparation method thereof

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Application publication date: 20181116

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