CN108789713A - A kind of Calophyllum anticorrosion treatment technology - Google Patents
A kind of Calophyllum anticorrosion treatment technology Download PDFInfo
- Publication number
- CN108789713A CN108789713A CN201810666830.6A CN201810666830A CN108789713A CN 108789713 A CN108789713 A CN 108789713A CN 201810666830 A CN201810666830 A CN 201810666830A CN 108789713 A CN108789713 A CN 108789713A
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- CN
- China
- Prior art keywords
- calophyllum
- added
- parts
- treatment technology
- anticorrosion treatment
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B27—WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
- B27K—PROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
- B27K3/00—Impregnating wood, e.g. impregnation pretreatment, for example puncturing; Wood impregnation aids not directly involved in the impregnation process
- B27K3/52—Impregnating agents containing mixtures of inorganic and organic compounds
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B27—WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
- B27K—PROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
- B27K2240/00—Purpose of the treatment
- B27K2240/20—Removing fungi, molds or insects
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- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Inorganic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Wood Science & Technology (AREA)
- Forests & Forestry (AREA)
- Chemical And Physical Treatments For Wood And The Like (AREA)
Abstract
The invention discloses a kind of Calophyllum anticorrosion treatment technologies, including following operating procedure：（1）Licorice powder, chitosan, acetic acid, lemonade are added into deionized water, stirs, calcium activated is then added thereto, is added in vacuum reaction kettle, is reacted 4 hours, is then filtered, obtain filtered fluid；（2）By step（1）Deionized water is added in filtered fluid obtained, after mixing uniformly, obtains modification liquid, immersion treatment is then carried out to Calophyllum using modification liquid under water-bath；（3）Step will be passed through（2）The Calophyllum of processing is cleaned using ethanol solution, then uses deionized water to clean again, is then dried under vacuum to constant weight, and anti-corrosion Calophyllum is made；The method of Calophyllum preservative treatment provided by the invention, it is easy to operate, it is of low cost, in processing procedure, the excellent properties of of Calophyllum itself are not interfered with, but the antiseptic property of Calophyllum can be greatly promoted, and the anti-corrosion term of validity is long, and minimum is 15 years.
Description
Technical field
The invention belongs to wicker plaiting article working process technical fields, and in particular to a kind of Calophyllum anticorrosion treatment technology.
Background technology
Calophyllum, which becomes a useful person, needs 150-200 or more, the expensive hardwood of generic name, is commonly called as the red wingceltis in Southeast Asia, and Calophyllum drying property is good
Good, not easy to crack and warpage is the sound wood for making solid wood furniture, and Calophyllum is high-end furniture woods, due to its texture
Color also referred to as small redwood close with rosewood class color and luster.Therefore the preservative treatment of Calophyllum is particularly important, and needs to prevent
Rotten agent meets permanent effective anti-corrosion effect.In the prior art, to the preservation of timber against decay, organic anti-corrosive agent is mostly used greatly, although
Permeance property in timber is excellent, but the anti-corrosion term of validity is shorter, cannot meet the long-term corrosion-resistant needs of Calophyllum.
Invention content
The purpose of the present invention is for existing problem, provide a kind of Calophyllum anticorrosion treatment technology.
The present invention is achieved by the following technical solutions：
A kind of Calophyllum anticorrosion treatment technology, including following operating procedure：
（1）By weight, 3-6 parts of licorice powders, 5-10 parts of chitosans, 3-6 parts of acetic acid, 1-3 portions of lemonades are added to 100 parts
Deionized water in, with 500r/min rotating speeds stir 2 hours, then thereto be added 5 parts of calcium activateds, be added to vacuum reaction kettle
In, it reacts 4 hours, then filters, obtain filtered fluid；
（2）By step（1）5 times of deionized waters of its quality are added in filtered fluid obtained, after mixing uniformly, obtain modification liquid, then
Immersion treatment is carried out 2 hours to Calophyllum using modification liquid under 100 DEG C of water-baths；
（3）Step will be passed through（2）The Calophyllum of processing uses mass fraction to clean 2min for 50% ethanol solution, then adopts again
2min is cleaned with deionized water, is then dried under vacuum to constant weight, anti-corrosion Calophyllum is made.
Further, step（1）Described in lemonade be to be mixed using the clear water of 6 times of lemon peel and its quality, squeeze the juice, so
After be filtered to get lemonade.
Further, step（1）Described in vacuum reaction kettle in vacuum degree be 0.056MPa.
Further, step（1）Described in vacuum reaction kettle in reaction temperature be 105 DEG C.
Further, step（2）Described in modification liquid be that Calophyllum is sunk immersion completely to Calophyllum immersion treatment.
Further, step（3）Described in vacuum drying temperature be 100 DEG C.
The present invention has the following advantages compared with prior art：
The method of Calophyllum preservative treatment provided by the invention, it is easy to operate, it is of low cost, in processing procedure, do not interfere with sea
The excellent properties of of Chinese bush cherry wood itself, but the antiseptic property of Calophyllum can be greatly promoted, and the anti-corrosion term of validity is long, is at least
15 years.Modification liquid prepared by the present invention handles Calophyllum, significant effect, and the anti-corrosion of Calophyllum can be greatly improved
Performance can be effectively promoted and change especially by the synergistic effect in licorice powder between active material and chitosan, lemonade
Property liquid in active constituent penetrate into Calophyllum interior tissue, to can not only quickly kill allergenic inside Calophyllum
Son, meanwhile, it is capable to effectively prevent extraneous fungal infection.
Specific implementation mode
Embodiment 1
A kind of Calophyllum anticorrosion treatment technology, including following operating procedure：
（1）By weight, 3 parts of licorice powders, 5 parts of chitosans, 3 parts of acetic acid, 1 portion of lemonade are added to 100 parts of deionization
In water, is stirred 2 hours with 500r/min rotating speeds, 5 parts of calcium activateds are then added thereto, are added in vacuum reaction kettle, reaction 4
Hour, it then filters, obtains filtered fluid；
（2）By step（1）5 times of deionized waters of its quality are added in filtered fluid obtained, after mixing uniformly, obtain modification liquid, then
Immersion treatment is carried out 2 hours to Calophyllum using modification liquid under 100 DEG C of water-baths；
（3）Step will be passed through（2）The Calophyllum of processing uses mass fraction to clean 2min for 50% ethanol solution, then adopts again
2min is cleaned with deionized water, is then dried under vacuum to constant weight, anti-corrosion Calophyllum is made.
Further, step（1）Described in lemonade be to be mixed using the clear water of 6 times of lemon peel and its quality, squeeze the juice, so
After be filtered to get lemonade.
Further, step（1）Described in vacuum reaction kettle in vacuum degree be 0.056MPa.
Further, step（1）Described in vacuum reaction kettle in reaction temperature be 105 DEG C.
Further, step（2）Described in modification liquid be that Calophyllum is sunk immersion completely to Calophyllum immersion treatment.
Further, step（3）Described in vacuum drying temperature be 100 DEG C.
Embodiment 2
A kind of Calophyllum anticorrosion treatment technology, including following operating procedure：
（1）By weight, 6 parts of licorice powders, 10 parts of chitosans, 6 parts of acetic acid, 3 portions of lemonades are added to 100 parts of deionization
In water, is stirred 2 hours with 500r/min rotating speeds, 5 parts of calcium activateds are then added thereto, are added in vacuum reaction kettle, reaction 4
Hour, it then filters, obtains filtered fluid；
（2）By step（1）5 times of deionized waters of its quality are added in filtered fluid obtained, after mixing uniformly, obtain modification liquid, then
Immersion treatment is carried out 2 hours to Calophyllum using modification liquid under 100 DEG C of water-baths；
（3）Step will be passed through（2）The Calophyllum of processing uses mass fraction to clean 2min for 50% ethanol solution, then adopts again
2min is cleaned with deionized water, is then dried under vacuum to constant weight, anti-corrosion Calophyllum is made.
Further, step（1）Described in lemonade be to be mixed using the clear water of 6 times of lemon peel and its quality, squeeze the juice, so
After be filtered to get lemonade.
Further, step（1）Described in vacuum reaction kettle in vacuum degree be 0.056MPa.
Further, step（1）Described in vacuum reaction kettle in reaction temperature be 105 DEG C.
Further, step（2）Described in modification liquid be that Calophyllum is sunk immersion completely to Calophyllum immersion treatment.
Further, step（3）Described in vacuum drying temperature be 100 DEG C.
Embodiment 3
A kind of Calophyllum anticorrosion treatment technology, including following operating procedure：
（1）By weight, 3-6 parts of licorice powders, 5-10 parts of chitosans, 3-6 parts of acetic acid, 1-3 portions of lemonades are added to 100 parts
Deionized water in, with 500r/min rotating speeds stir 2 hours, then thereto be added 5 parts of calcium activateds, be added to vacuum reaction kettle
In, it reacts 4 hours, then filters, obtain filtered fluid；
（2）By step（1）5 times of deionized waters of its quality are added in filtered fluid obtained, after mixing uniformly, obtain modification liquid, then
Immersion treatment is carried out 2 hours to Calophyllum using modification liquid under 100 DEG C of water-baths；
（3）Step will be passed through（2）The Calophyllum of processing uses mass fraction to clean 2min for 50% ethanol solution, then adopts again
2min is cleaned with deionized water, is then dried under vacuum to constant weight, anti-corrosion Calophyllum is made.
Further, step（1）Described in lemonade be to be mixed using the clear water of 6 times of lemon peel and its quality, squeeze the juice, so
After be filtered to get lemonade.
Further, step（1）Described in vacuum reaction kettle in vacuum degree be 0.056MPa.
Further, step（1）Described in vacuum reaction kettle in reaction temperature be 105 DEG C.
Further, step（2）Described in modification liquid be that Calophyllum is sunk immersion completely to Calophyllum immersion treatment.
Further, step（3）Described in vacuum drying temperature be 100 DEG C.
With reference to GB/T18621《Mould inhibitor prevents the test method of timber mould and Stain fungi》In method test Calophyllum
Preventing efficiency, test result is as shown in table 1：
The bacteriostasis property of 1 Calophyllum of table
| Project | Trichoderma asperellum |
| Embodiment 1 | 99 |
| Embodiment 2 | 99 |
| Embodiment 3 | 100 |
As shown in Table 1, Calophyllum produced by the present invention, to causing the fungi of Wood staining that there is extremely effective control effect.
Finally illustrate, the above examples are only used to illustrate the technical scheme of the present invention and are not limiting, although with reference to compared with
Good embodiment describes the invention in detail, it will be understood by those of ordinary skill in the art that, it can be to the skill of the present invention
Art scheme is modified or replaced equivalently, and without departing from the objective and range of technical solution of the present invention, should all be covered at this
In the right of invention.
Claims (6)
1. a kind of Calophyllum anticorrosion treatment technology, which is characterized in that including following operating procedure：
（1）By weight, 3-6 parts of licorice powders, 5-10 parts of chitosans, 3-6 parts of acetic acid, 1-3 portions of lemonades are added to 100 parts
Deionized water in, with 500r/min rotating speeds stir 2 hours, then thereto be added 5 parts of calcium activateds, be added to vacuum reaction kettle
In, it reacts 4 hours, then filters, obtain filtered fluid；
（2）By step（1）5 times of deionized waters of its quality are added in filtered fluid obtained, after mixing uniformly, obtain modification liquid, then
Immersion treatment is carried out 2 hours to Calophyllum using modification liquid under 100 DEG C of water-baths；
（3）Step will be passed through（2）The Calophyllum of processing uses mass fraction to clean 2min for 50% ethanol solution, then adopts again
2min is cleaned with deionized water, is then dried under vacuum to constant weight, anti-corrosion Calophyllum is made.
2. a kind of Calophyllum anticorrosion treatment technology according to claim 1, which is characterized in that step（1）Described in lemon
Water is to be mixed using the clear water of 6 times of lemon peel and its quality, squeezes the juice, is then filtered to get lemonade.
3. a kind of Calophyllum anticorrosion treatment technology according to claim 1, which is characterized in that step（1）Described in it is true
Vacuum degree is 0.056MPa in empty reaction kettle.
4. a kind of Calophyllum anticorrosion treatment technology according to claim 1, which is characterized in that step（1）Described in it is true
Reaction temperature is 105 DEG C in empty reaction kettle.
5. a kind of Calophyllum anticorrosion treatment technology according to claim 1, which is characterized in that step（2）Described in it is modified
Liquid is that Calophyllum is sunk immersion completely to Calophyllum immersion treatment.
6. a kind of Calophyllum anticorrosion treatment technology according to claim 1, which is characterized in that step（3）Described in vacuum
Drying temperature is 100 DEG C.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810666830.6A CN108789713A (en) | 2018-06-26 | 2018-06-26 | A kind of Calophyllum anticorrosion treatment technology |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810666830.6A CN108789713A (en) | 2018-06-26 | 2018-06-26 | A kind of Calophyllum anticorrosion treatment technology |
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| CN108789713A true CN108789713A (en) | 2018-11-13 |
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Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1459466A (en) * | 2002-05-23 | 2003-12-03 | 中国林业科学研究院木材工业研究所 | Preparation method of chitin metal salt wood preservative and its application |
| CN102275192A (en) * | 2011-08-12 | 2011-12-14 | 东北林业大学 | Wood preservative and preparation method thereof |
| CN105965636A (en) * | 2016-07-12 | 2016-09-28 | 南京林业大学 | Method for modifying wood and bamboo wood through biopolymer-chitosan |
| CN107839045A (en) * | 2017-09-22 | 2018-03-27 | 中垣林业科技（定南）有限公司 | A kind of method of modifying of eucalyptus plate |
| CN107953433A (en) * | 2017-12-21 | 2018-04-24 | 安徽明豪实木家俱有限公司 | A kind of method of Calophyllum preservative treatment |
-
2018
- 2018-06-26 CN CN201810666830.6A patent/CN108789713A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1459466A (en) * | 2002-05-23 | 2003-12-03 | 中国林业科学研究院木材工业研究所 | Preparation method of chitin metal salt wood preservative and its application |
| CN102275192A (en) * | 2011-08-12 | 2011-12-14 | 东北林业大学 | Wood preservative and preparation method thereof |
| CN105965636A (en) * | 2016-07-12 | 2016-09-28 | 南京林业大学 | Method for modifying wood and bamboo wood through biopolymer-chitosan |
| CN107839045A (en) * | 2017-09-22 | 2018-03-27 | 中垣林业科技（定南）有限公司 | A kind of method of modifying of eucalyptus plate |
| CN107953433A (en) * | 2017-12-21 | 2018-04-24 | 安徽明豪实木家俱有限公司 | A kind of method of Calophyllum preservative treatment |
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Application publication date: 20181113 |
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