CN108777179B - Gel ball normal temperature aging device - Google Patents

Gel ball normal temperature aging device Download PDF

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Publication number
CN108777179B
CN108777179B CN201810607173.8A CN201810607173A CN108777179B CN 108777179 B CN108777179 B CN 108777179B CN 201810607173 A CN201810607173 A CN 201810607173A CN 108777179 B CN108777179 B CN 108777179B
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self
circulation
tank body
inlet
liquid
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CN108777179A (en
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赵兴宇
马景陶
郝少昌
邓长生
刘兵
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Tsinghua University
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Tsinghua University
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    • GPHYSICS
    • G21NUCLEAR PHYSICS; NUCLEAR ENGINEERING
    • G21CNUCLEAR REACTORS
    • G21C21/00Apparatus or processes specially adapted to the manufacture of reactors or parts thereof
    • G21C21/02Manufacture of fuel elements or breeder elements contained in non-active casings
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02EREDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E30/00Energy generation of nuclear origin
    • Y02E30/30Nuclear fission reactors

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  • Engineering & Computer Science (AREA)
  • Physics & Mathematics (AREA)
  • Manufacturing & Machinery (AREA)
  • Plasma & Fusion (AREA)
  • General Engineering & Computer Science (AREA)
  • High Energy & Nuclear Physics (AREA)
  • Feeding, Discharge, Calcimining, Fusing, And Gas-Generation Devices (AREA)
  • Colloid Chemistry (AREA)

Abstract

The invention relates to the field of nuclear fuel aging equipment, and provides a gel ball normal-temperature aging device. The device comprises a feeding pipe, a self-circulation pipeline, a tank body and a filter screen arranged in the tank body; the inlet of the feed pipe extends out of the tank body, the outlet extends to the lower part of the filter screen, and a feed valve is arranged on the feed pipe; the tank body is provided with a liquid inlet, a liquid outlet, a self-circulation inlet, a constant volume overflow port and a discharge port which can be opened and closed, the discharge port is arranged at the bottom of the tank body, the liquid outlet is positioned above the filter screen, and the liquid outlet is provided with a liquid outlet pump; the constant volume overflow port, the self-circulation outlet and the self-circulation inlet are located below the filter screen, the self-circulation outlet is communicated with the self-circulation inlet through a self-circulation pipeline, and a self-circulation pump is arranged on the self-circulation pipeline. The invention not only avoids the deformation and damage of the gel balls along with the transportation of the ammonia water, but also can drive the gel balls in the tank body to circularly move through the self-circulation of the ammonia water, thereby avoiding the deformation and uneven reaction caused by standing and stacking of the gel balls during aging.

Description

Gel ball normal temperature aging device
Technical Field
The invention relates to the technical field of nuclear fuel aging equipment, in particular to a gel ball normal-temperature aging device.
Background
In China, a High Temperature Reactor-Pebbelbedbedmodules (HTR-PM for short) is generally used for preparing uranium dioxide ceramic microspheres by an external gelling process improved by a full gelling process of a 10MW High Temperature gas cooled Reactor when producing fuel.
Wherein, the small balls after the dispersion process are sequentially subjected to the processes of normal-temperature aging, heating aging, washing, drying, roasting, reducing, sintering and the like to obtain the compact uranium dioxide ceramic microspheres. At present, a dispersion process needs a special ammonia water storage tank to provide ammonia water for a dispersion column system besides the dispersion column system. And the gel balls obtained in the dispersion process and the ammonia mother liquor enter normal-temperature aging equipment for aging. Because the gel balls need to be transported between the ammonia water storage tank and the normal-temperature aging equipment, the gel balls are easy to deform and even damage.
Disclosure of Invention
The invention aims to provide a gel ball normal-temperature aging device which is simple in structure and convenient and fast to operate, so that the gel ball is prevented from being deformed and damaged along with the transportation of ammonia water.
In order to achieve the purpose, the invention provides a gel ball normal-temperature aging device which comprises a feeding pipe, a self-circulation pipeline, a tank body and a filter screen arranged in the tank body, wherein the tank body is divided into an upper cavity and a lower cavity by the filter screen, and the aperture of the filter screen is smaller than the diameter of a gel ball; the feed pipe is inserted into the tank body, an inlet of the feed pipe extends out of the tank body, an outlet of the feed pipe extends to the position below the filter screen, and a feed valve is arranged on the feed pipe; the tank body is provided with a liquid inlet, a liquid outlet, a self-circulation inlet, a constant volume overflow port and a discharge port which can be opened and closed, the liquid outlet is positioned above the filter screen, and the liquid outlet is provided with a liquid outlet pump; the constant volume overflow port, the self-circulation outlet and the self-circulation inlet are all located below the filter screen, the self-circulation outlet is communicated with the self-circulation inlet through the self-circulation pipeline, and the self-circulation pump is arranged on the self-circulation pipeline.
Wherein, the liquid inlet is positioned above the filter screen.
Wherein the self-circulation outlet is located above the self-circulation inlet.
The self-circulation outlet, the self-circulation inlet, the discharge port and/or the constant volume overflow port are/is provided with a filter screen, and the aperture of the filter screen is smaller than the diameter of the gel ball.
The bottom surface of the tank body is a conical surface, the discharge port is arranged at the center of the bottom surface of the tank body, the discharge port is provided with a ball valve, and the top surface of the ball valve is flush with the bottom surface of the tank body.
One end of the self-circulation inlet is tangent to the conical surface of the tank body, and the other end of the self-circulation inlet is connected with the self-circulation pipeline.
Wherein, still include the feed liquor pump, the feed liquor pump pass through the inlet with jar body intercommunication.
Wherein, still including inserting and establishing the shower on the jar body, the first end of shower with the export intercommunication of feed liquor pump, second end extend to the below of filter screen, be equipped with the shower nozzle on the second end of shower.
The spray pipe comprises a main pipe and a liquid distribution head, one end of the main pipe is communicated with the liquid inlet pump, the other end of the main pipe is communicated with the liquid distribution head, the liquid distribution head comprises a plurality of liquid distribution pipes, the first ends of the liquid distribution pipes are communicated with each other, the second ends of the liquid distribution pipes extend outwards respectively, and a plurality of spray heads are arranged on the liquid distribution pipes along the length direction of the liquid distribution pipes.
Wherein, still include the controller and set up be in the internal level sensor of jar, level sensor the inlet the liquid outlet from the circulation export from the circulation import constant volume overflow mouth the discharge gate from the circulating pump the feed liquor pump with go out the liquid pump all with the controller electricity is connected.
The ammonia water circulating device is simple in structure and convenient and fast to operate, when the ammonia water circulating device is used, the feeding pipe and the liquid outlet are respectively communicated with the outlet and the inlet of the dispersion column system, and an ammonia water circulating loop can be formed between the tank body and the dispersion column system, so that an ammonia water storage tank is not required to be specially arranged for the dispersion column system. And, because the export and the liquid outlet of the inlet pipe of jar body are located the upper and lower both sides of filter screen respectively, therefore aqueous ammonia when circulation between dispersion column system and the jar body, jar internal gel ball is stored all the time in jar body and can not flow into dispersion column system along with what aqueous ammonia together, and then has just avoided the gel ball to transport along with the aqueous ammonia and cause and take place to warp, damage even. In addition, the ammonia water in the tank body is driven to flow in a self-circulation mode by the self-circulation pump, so that the gel balls in the tank body can be driven to move in a circulation mode, deformation and uneven reaction caused by standing and stacking during aging of the gel balls can be avoided, the sphericity of the gel balls can be improved, cracking of the gel balls is avoided, and the yield is greatly improved.
Drawings
FIG. 1 is a schematic structural diagram of an apparatus for aging gel beads at normal temperature according to an embodiment of the present invention;
fig. 2 is a schematic structural diagram of a shower pipe in the embodiment of the present invention.
Reference numerals:
1. a tank body; 1-1, a liquid inlet; 1-2, a liquid outlet; 1-3, a self-circulation outlet;
1-4, self-circulation inlet; 1-5, constant volume overflow port; 1-6, a discharge hole; 2. a feed pipe;
3. a self-circulating pipe; 4. a filter screen; 5. a liquid outlet pump; 6. a self-circulating pump;
7. a liquid inlet pump; 8. a main pipe; 9. a spray head; 10. a liquid distribution pipe.
Detailed Description
In order to make the objects, technical solutions and advantages of the present invention clearer, the technical solutions of the present invention will be described below with reference to the accompanying drawings, and it is obvious that the described embodiments are some embodiments of the present invention, but not all embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
In the description of the present invention, unless otherwise specified, the terms "upper", "lower", and the like indicate orientations or positional relationships based on the orientations or positional relationships shown in the drawings, and are only for convenience in describing the present invention and simplifying the description, but do not indicate or imply that the system or element referred to must have a specific orientation, be constructed in a specific orientation, and be operated, and thus, should not be construed as limiting the present invention.
It is to be understood that, unless otherwise expressly stated or limited, the term "coupled" is used in a generic sense as defined herein, e.g., fixedly attached or removably attached or integrally attached; may be directly connected or indirectly connected through an intermediate. The specific meaning of the above terms in the present invention can be understood in specific cases to those skilled in the art.
As shown in figure 1, the invention provides a gel ball normal temperature aging device, which comprises a feeding pipe 2, a self-circulation pipeline 3, a tank body 1 and a filter screen 4 arranged in the tank body 1, wherein the tank body 1 is divided into an upper cavity and a lower cavity by the filter screen 4, and the aperture of the filter screen 4 is smaller than the diameter of a gel ball; the feeding pipe 2 is inserted on the tank body 1, the inlet of the feeding pipe 2 extends out of the tank body 1, the outlet extends to the lower part of the filter screen 4, and the feeding pipe 2 is provided with a feeding valve; the tank body 1 is provided with a liquid inlet 1-1, a liquid outlet 1-2, a self-circulation outlet 1-3, a self-circulation inlet 1-4, a constant volume overflow port 1-5 and a discharge port 1-6 which can be opened and closed, the discharge port 1-6 is arranged at the bottom of the tank body 1, the liquid outlet 1-2 is positioned above the filter screen 4, and the liquid outlet 1-2 is provided with a liquid outlet pump 5; the constant volume overflow ports 1-5, the self-circulation outlets 1-3 and the self-circulation inlets 1-4 are all positioned below the filter screen 4, the self-circulation outlets 1-3 are communicated with the self-circulation inlets 1-4 through self-circulation pipelines 3, and self-circulation pumps 6 are arranged on the self-circulation pipelines 3.
When in use: firstly, a feeding pipe 2 and a liquid outlet pump 5 of the device are respectively communicated with an outlet and an inlet of a dispersion column system, and meanwhile, discharge ports 1-6 are communicated with subsequent equipment; then, injecting ammonia water into the tank body 1 through the liquid inlet 1-1 until the tank body 1 is filled with the ammonia water;
then, the liquid inlet 1-1 is closed, and the feeding valve, the liquid outlet 1-2 and the liquid outlet pump 5 are opened at the same time. From this, under the suction effect of liquid pump 5, the aqueous ammonia in jar body 1 just constantly flows into dispersion column system, and meanwhile, the gel ball that dispersion column system produced also can flow into jar body 1 through inlet pipe 2 along with the aqueous ammonia in the dispersion column system together, that is to say, the gel ball that dispersion column system produced constantly gets into jar body 1 simultaneously, and the aqueous ammonia also constantly circulates between dispersion column system and jar body 1. In addition, because the outlet of the feeding pipe 2 is positioned below the filter screen 4 and the liquid outlet 1-2 is positioned above the filter screen 4, when the ammonia water circulates between the dispersion column system and the tank body 1, the gel balls in the tank body 1 are always stored in the tank body 1 and cannot flow into the dispersion column system along with the ammonia water;
next, the self-circulation outlets 1-3, the self-circulation inlets 1-4 and the self-circulation pump 6 are turned on. Because the outlet of the feeding pipe 2 is positioned below the filter screen 4, and the aperture of the filter screen 4 is smaller than the diameter of the gel ball, the gel balls output by the dispersion column system are all positioned in the lower cavity of the tank body 1, so that when the self-circulation outlet 1-3, the self-circulation inlet 1-4 and the self-circulation pump 6 are opened, namely the ammonia water in the tank body 1 starts to self-circulate, the gel balls in the tank body 1 can circularly move in the lower cavity under the driving of the ammonia water, and normal-temperature aging is started;
then, after the dispersion column system finishes the dispersion process, namely after all gel balls generated by the dispersion column system fall into the tank body 1, opening the constant volume overflow port 1-5 until the liquid level of the ammonia water in the tank body 1 is positioned below the filter screen 4;
and finally, after the normal-temperature aging process is finished, closing the self-circulation outlet 1-3, the self-circulation pump 6 and the self-circulation inlet 1-4, and opening the constant-volume overflow port 1-5 again until the liquid level of the ammonia water in the tank body 1 is positioned below the constant-volume overflow port 1-5, opening the discharge port 1-6, and enabling the gel balls in the tank body 1 to flow into subsequent equipment along with the residual ammonia water. Therefore, the constant volume overflow ports 1-5 can be used for constant volume of the ammonia water when the gel balls are discharged.
By last, this device simple structure, simple operation, during the use, through with inlet pipe 2 and liquid outlet 1-2 respectively with dispersion column system's export and import intercommunication, just can form the circulation circuit of aqueous ammonia between jar body 1 and dispersion column system to just also need not to set up the aqueous ammonia liquid storage pot for dispersion column system specially. And, because the export and the liquid outlet 1-2 of the inlet pipe 2 of jar body 1 are located the upper and lower both sides of filter screen 4 respectively, therefore aqueous ammonia when circulating between disperse column system and jar body 1, the gel ball in jar body 1 is stored all the time and is carried out the normal atmospheric temperature ageing in jar body 1 to just also avoided the gel ball to transport along with the aqueous ammonia and cause and take place to warp, damage even. In addition, the ammonia water in the tank body 1 is driven to flow in a self-circulation mode by the self-circulation pump 6, and the gel balls in the tank body 1 can be driven to move in a circulation mode, so that deformation and uneven reaction caused by standing and stacking of the gel balls during normal-temperature aging can be avoided, the sphericity of the gel balls can be improved, cracking of the gel balls is avoided, and the yield is greatly improved.
Preferably, the liquid inlet 1-1 is located above the filter screen 4 to prevent the gel beads from entering the liquid inlet 1-1.
Preferably, the self-circulation outlet 1-3 is located above the self-circulation inlet 1-4 to increase the turbulence effect caused by the flow of ammonia in the tank 1.
Preferably, a filter screen is arranged on the self-circulation outlet 1-3, the self-circulation inlet 1-4, the discharge port 1-6 and/or the constant volume overflow port 1-5, and the aperture of the filter screen is smaller than the diameter of the gel ball.
Preferably, the bottom surface of the tank body 1 is a conical surface, the discharge port 1-6 is arranged in the center of the bottom surface of the tank body 1, the discharge port 1-6 is provided with a ball valve, and the top surface of the ball valve is flush with the bottom surface of the tank body 1. Wherein the ball valve may be, but is not limited to, a roll-down ball valve. The advantages of such an arrangement are: on one hand, the gel balls can slide to the discharge port 1-6 along the conical surface of the tank body 1 under the action of self gravity; on the other hand, because the ball valve top surface is the same level with the bottom surface of jar body 1 to not only can avoid gel ball and ball valve to bump and take place to warp, but also can avoid gel ball to remain in jar body 1.
Preferably, one end of the self-circulation inlet 1-4 is tangent to the conical surface of the tank body 1, and the other end is connected with the self-circulation pipeline 3. Therefore, when the self-circulation pump 6 is started, the ammonia water pumped out from the tank body 1 by the self-circulation pump 6 can flow into the tank body 1 along the inner wall of the tank body 1 through the self-circulation inlets 1-4 and can not be directly sprayed onto the gel balls in the tank body 1, and further the gel balls are prevented from being deformed due to water flow impact.
Further, the device also comprises a liquid inlet pump 7, and the liquid inlet pump 7 is communicated with the tank body 1 through a liquid inlet 1-1.
In addition, considering that when the ammonia water is discharged, partial gel balls can still remain in the tank body 1, the device further comprises a spray pipe inserted in the tank body 1, the first end of the spray pipe is communicated with the outlet of the liquid inlet pump 7, the second end of the spray pipe extends to the lower part of the filter screen 4, and the second end of the spray pipe is provided with a spray head 9. Therefore, after the discharge port 1-6 is opened for a period of time, the liquid inlet pump 7 can be started, ammonia water is sprayed into the tank body 1 through the spray head 9, and gel balls remained at the bottom of the tank body 1 flow into the discharge port 1-6 along with the ammonia water.
As shown in fig. 2, in order to further expand the spraying range, the spraying pipe includes a main pipe 8 and a liquid distribution head, one end of the main pipe 8 is communicated with the liquid inlet pump 7, the other end is communicated with the liquid distribution head, the liquid distribution head includes a plurality of liquid distribution pipes 10, the first ends of the plurality of liquid distribution pipes 10 are all communicated with each other, the second ends of the plurality of liquid distribution pipes extend outwards respectively, and a plurality of nozzles 9 are arranged on the liquid distribution pipes 10 along the length direction of the liquid distribution pipes 10. Wherein adjacent nozzles 9 are staggered.
Preferably, the device also comprises a controller and a liquid level sensor arranged in the tank body 1, wherein the liquid level sensor, the liquid inlet 1-1, the liquid outlet 1-2, the self-circulation outlet 1-3, the self-circulation inlet 1-4, the constant volume overflow port 1-5, the discharge port 1-6, the self-circulation pump 6, the liquid inlet pump 7 and the liquid outlet pump 5 are all electrically connected with the controller. Therefore, the controller can automatically control the opening and closing of the liquid level sensor, the liquid inlet 1-1, the liquid outlet 1-2, the self-circulation outlet 1-3, the self-circulation inlet 1-4, the constant volume overflow port 1-5, the discharge port 1-6, the self-circulation pump 6, the liquid inlet pump 7 and the liquid outlet pump 5 according to the liquid level height in the tank body 1 detected by the liquid level sensor in real time.
Finally, it should be noted that: the above examples are only intended to illustrate the technical solution of the invention, but not to limit it; although the invention has been described in detail with reference to the foregoing embodiments, it will be understood by those skilled in the art that: the technical solutions described in the foregoing embodiments may still be modified, or some technical features may be equivalently replaced; and the modifications or the substitutions do not make the essence of the corresponding technical solutions depart from the spirit and scope of the technical solutions of the embodiments of the present invention.

Claims (8)

1. A gel ball normal temperature aging device is characterized by comprising a feeding pipe, a self-circulation pipeline, a liquid inlet pump, a tank body, a spray pipe inserted on the tank body and a filter screen arranged in the tank body, wherein the tank body is divided into an upper cavity and a lower cavity by the filter screen, and the aperture of the filter screen is smaller than the diameter of a gel ball; the feed pipe is inserted into the tank body, an inlet of the feed pipe extends out of the tank body, an outlet of the feed pipe extends to the position below the filter screen, and a feed valve is arranged on the feed pipe; the tank body is provided with a liquid inlet, a liquid outlet, a self-circulation inlet, a constant volume overflow port and a discharge port which can be opened and closed, the liquid outlet is positioned above the filter screen, and the liquid outlet is provided with a liquid outlet pump; the constant volume overflow port, the self-circulation outlet and the self-circulation inlet are all positioned below the filter screen, the self-circulation outlet is communicated with the self-circulation inlet through the self-circulation pipeline, and the self-circulation pump is arranged on the self-circulation pipeline; the feed pipe and the liquid outlet are respectively communicated with an outlet and an inlet of the dispersion column system so as to form an ammonia water circulation loop of the ammonia water-free liquid storage tank between the tank body and the dispersion column system; the feed liquor pump pass through the inlet with jar body intercommunication, the first end of shower with the outlet intercommunication of feed liquor pump, second end extend to the below of filter screen, be equipped with the shower nozzle on the second end of shower.
2. The gel ball normal temperature aging device according to claim 1, wherein the liquid inlet is positioned above the filter screen.
3. The gel-ball ambient aging apparatus according to claim 1, wherein the self-circulation outlet is located above the self-circulation inlet.
4. The gel ball normal temperature aging device according to claim 1, wherein a filter screen is arranged on the self-circulation outlet, the self-circulation inlet, the discharge port and/or the constant volume overflow port, and the aperture of the filter screen is smaller than the diameter of the gel ball.
5. The gel ball normal temperature aging device according to claim 1, wherein the bottom surface of the tank body is a conical surface, the discharge port is arranged at the center of the bottom surface of the tank body, a ball valve is arranged on the discharge port, and the top surface of the ball valve is flush with the bottom surface of the tank body.
6. A gel ball normal temperature aging device as claimed in claim 5, wherein one end of the self-circulation inlet is tangent to the conical surface of the tank body, and the other end is connected with the self-circulation pipeline.
7. The gel ball normal temperature aging device according to claim 1, wherein the spray pipe comprises a main pipe and a liquid distribution head, one end of the main pipe is communicated with the liquid inlet pump, the other end of the main pipe is communicated with the liquid distribution head, the liquid distribution head comprises a plurality of liquid distribution pipes, the first ends of the plurality of liquid distribution pipes are all communicated with each other, the second ends of the plurality of liquid distribution pipes extend outwards respectively, and a plurality of spray heads are arranged on the liquid distribution pipes along the length direction of the liquid distribution pipes.
8. The gel ball normal temperature aging device according to claim 1, further comprising a controller and a liquid level sensor disposed in the tank body, wherein the liquid level sensor, the liquid inlet, the liquid outlet, the self-circulation inlet, the constant volume overflow port, the discharge port, the self-circulation pump, the liquid inlet pump and the liquid outlet pump are all electrically connected with the controller.
CN201810607173.8A 2018-06-13 2018-06-13 Gel ball normal temperature aging device Active CN108777179B (en)

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Application Number Priority Date Filing Date Title
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Application Number Priority Date Filing Date Title
CN201810607173.8A CN108777179B (en) 2018-06-13 2018-06-13 Gel ball normal temperature aging device

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CN108777179B true CN108777179B (en) 2020-03-27

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Family Cites Families (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB2405496B (en) * 2003-08-27 2007-02-07 Agilent Technologies Inc A method and a system for evaluating aging of components, and computer program product therefor
CN101953404B (en) * 2010-08-31 2012-12-12 安徽农业大学 Mechanical tea making process of Liuan Guapian
CN102496395B (en) * 2011-11-23 2014-04-02 清华大学 Dispersion column system
CN103252296A (en) * 2013-05-28 2013-08-21 清华大学 Spraying nozzle and spraying device
CN103366846B (en) * 2013-07-19 2015-08-12 清华大学 Uranium dioxide core ageing tank, ageing, washing drying system and method
CN104324520B (en) * 2014-10-27 2016-01-20 辽东学院 Ultrasonic wave form selenium separator

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