CN108774331A - A kind of complex optics pre-coating film - Google Patents

A kind of complex optics pre-coating film Download PDF

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Publication number
CN108774331A
CN108774331A CN201810440223.8A CN201810440223A CN108774331A CN 108774331 A CN108774331 A CN 108774331A CN 201810440223 A CN201810440223 A CN 201810440223A CN 108774331 A CN108774331 A CN 108774331A
Authority
CN
China
Prior art keywords
parts
coating
coating film
thickener
antioxidant
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201810440223.8A
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Chinese (zh)
Inventor
周贤敏
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Chongqing New Kang Yi Xin Dahl New Material Co Ltd
Original Assignee
Chongqing New Kang Yi Xin Dahl New Material Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Chongqing New Kang Yi Xin Dahl New Material Co Ltd filed Critical Chongqing New Kang Yi Xin Dahl New Material Co Ltd
Priority to CN201810440223.8A priority Critical patent/CN108774331A/en
Publication of CN108774331A publication Critical patent/CN108774331A/en
Pending legal-status Critical Current

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Classifications

    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08JWORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J7/00Chemical treatment or coating of shaped articles made of macromolecular substances
    • C08J7/04Coating
    • C08J7/0427Coating with only one layer of a composition containing a polymer binder
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08JWORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J2367/00Characterised by the use of polyesters obtained by reactions forming a carboxylic ester link in the main chain; Derivatives of such polymers
    • C08J2367/02Polyesters derived from dicarboxylic acids and dihydroxy compounds
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08JWORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J2483/00Characterised by the use of macromolecular compounds obtained by reactions forming in the main chain of the macromolecule a linkage containing silicon with or without sulfur, nitrogen, oxygen, or carbon only; Derivatives of such polymers
    • C08J2483/04Polysiloxanes

Abstract

The present invention relates to optics technical field of membrane, and in particular to a kind of complex optics pre-coating film.Complex optics pre-coating film is made of 70-85 parts of UV resins, 1-3 parts of curing agent, 2-5 parts of thickener, 1-3 parts of antioxidant, 2-8 parts of isobutyl triethoxy silane, 2-4 parts of coalescents, 3-10 parts of dimethyl polysiloxane etc..UV resins, curing agent, thickener, antioxidant, isobutyl triethoxy silane, coalescents, dimethyl polysiloxane, magnolol and propiconazole are added into consersion unit first, temperature reaction then cools to room temperature, and stirs to get pre-coating solution;Pre-coating solution is spread evenly across on PET matrix, coating process uses dimple coating method, solidification to use heat cure mode.The present invention by rationally design optics pre-coating film component and proportioning, to make the viscous stickiness of optical film be significantly improved.Meanwhile also having many advantages, such as that manufacturing cost is relatively low, stickiness is good.

Description

A kind of complex optics pre-coating film
Technical field
The present invention relates to optics technical field of membrane, and in particular to a kind of complex optics pre-coating film.
Background technology
Optical film is made of thin layered medium, and a kind of optical medium material of light beam is propagated by interface.Optics The application of film starts from the 1930s.Modern times, optical thin film are widely used in optics and photoelectron technical field, and manufacture is each Kind optical instrument.
But to be viscous stickiness poor etc. for the major defect of existing optical film.
Invention content
In order to solve the technical problems existing in the prior art, the present invention proposes a kind of complex optics pre-coating film, right The viscous stickiness of product is preferable.
The technical scheme is that:A kind of complex optics pre-coating film, is made of the raw material of following parts by weight:
70-85 parts of UV resins, 1-3 parts of curing agent, 2-5 parts of thickener, 1-3 parts of antioxidant, isobutyl ethyl triethoxy silicane 2-3 parts of 2-8 parts of alkane, 2-4 parts of coalescents, 3-10 parts of dimethyl polysiloxane, 1-3 parts of magnolol and propiconazole.
As the preferred embodiment of the present invention, it is made of the raw material of following parts by weight:
80 parts of UV resins, 2 parts of curing agent, 4 parts of thickener, 2 parts of antioxidant, 6 parts of isobutyl triethoxy silane, film forming 2.6 parts of 3 parts of auxiliary agent, 5 parts of dimethyl polysiloxane, 2 parts of magnolol and propiconazole.
A kind of preparation method of complex optics pre-coating film, steps are as follows:
1., first by UV resins, curing agent, thickener, antioxidant, isobutyl triethoxy silane, coalescents, two Methyl polysiloxane, magnolol and propiconazole are added into consersion unit, are warming up to 160-180 DEG C and react 3-5 hours, then cold But to room temperature, control rotating speed is 900-1200rpm/min, stirs 40-60min, obtains pre-coating solution;
2., pre-coating solution is spread evenly across on PET matrix, coating process uses dimple coating method, solidification to use thermosetting Change mode.
Beneficial effects of the present invention are shown:
By rationally designing the component and proportioning of optics pre-coating film, to make the viscous stickiness of optical film be significantly improved. Meanwhile also having many advantages, such as that manufacturing cost is relatively low, stickiness is good.
Specific implementation mode
Embodiment 1
A kind of complex optics pre-coating film, is made of the raw material of following parts by weight:
70 parts of UV resins, 3 parts of curing agent, 2 parts of thickener, 3 parts of antioxidant, 2 parts of isobutyl triethoxy silane, film forming 2 parts of 4 parts of auxiliary agent, 3 parts of dimethyl polysiloxane, 3 parts of magnolol and propiconazole.
Steps are as follows for preparation method:
1., first by UV resins, curing agent, thickener, antioxidant, isobutyl triethoxy silane, coalescents, two Methyl polysiloxane, magnolol and propiconazole are added into consersion unit, are warming up to 160 DEG C and react 5 hours, are subsequently cooled to room Temperature, control rotating speed are 900rpm/min, stir 60min, obtain pre-coating solution;
2., pre-coating solution is spread evenly across on PET matrix, coating process uses dimple coating method, solidification to use thermosetting Change mode.
Embodiment 2
A kind of complex optics pre-coating film, is made of the raw material of following parts by weight:
85 parts of UV resins, 1 part of curing agent, 5 parts of thickener, 1 part of antioxidant, 8 parts of isobutyl triethoxy silane, film forming 3 parts of 2 parts of auxiliary agent, 10 parts of dimethyl polysiloxane, 1 part of magnolol and propiconazole.
Steps are as follows for preparation method:
1., first by UV resins, curing agent, thickener, antioxidant, isobutyl triethoxy silane, coalescents, two Methyl polysiloxane, magnolol and propiconazole are added into consersion unit, are warming up to 180 DEG C and react 3 hours, are subsequently cooled to room Temperature, control rotating speed are 1200rpm/min, stir 40min, obtain pre-coating solution;
2., pre-coating solution is spread evenly across on PET matrix, coating process uses dimple coating method, solidification to use thermosetting Change mode.
Embodiment 3
A kind of complex optics pre-coating film, is made of the raw material of following parts by weight:
80 parts of UV resins, 2 parts of curing agent, 4 parts of thickener, 2 parts of antioxidant, 6 parts of isobutyl triethoxy silane, film forming 2.6 parts of 3 parts of auxiliary agent, 5 parts of dimethyl polysiloxane, 2 parts of magnolol and propiconazole.
Steps are as follows for preparation method:
1., first by UV resins, curing agent, thickener, antioxidant, isobutyl triethoxy silane, coalescents, two Methyl polysiloxane, magnolol and propiconazole are added into consersion unit, are warming up to 170 DEG C and react 4 hours, are subsequently cooled to room Temperature, control rotating speed are 1100rpm/min, stir 50min, obtain pre-coating solution;
2., pre-coating solution is spread evenly across on PET matrix, coating process uses dimple coating method, solidification to use thermosetting Change mode.
The above content is just an example and description of the concept of the present invention, affiliated those skilled in the art It makes various modifications or additions to the described embodiments or substitutes by a similar method, without departing from invention Design or beyond the scope defined by this claim, be within the scope of protection of the invention.

Claims (3)

1. a kind of complex optics pre-coating film, which is characterized in that be made of the raw material of following parts by weight:
70-85 parts of UV resins, 1-3 parts of curing agent, 2-5 parts of thickener, 1-3 parts of antioxidant, isobutyl triethoxy silane 2-8 Part, 2-4 parts of coalescents, 3-10 parts of dimethyl polysiloxane, 1-3 parts of magnolol and 2-3 parts of propiconazole.
2. complex optics pre-coating film as described in claim 1, which is characterized in that be made of the raw material of following parts by weight:
80 parts of UV resins, 2 parts of curing agent, 4 parts of thickener, 2 parts of antioxidant, 6 parts of isobutyl triethoxy silane, coalescents 2.6 parts of 3 parts, 5 parts of dimethyl polysiloxane, 2 parts of magnolol and propiconazole.
3. a kind of method preparing complex optics pre-coating film as claimed in claim 1 or 2, which is characterized in that steps are as follows:
1., first by UV resins, curing agent, thickener, antioxidant, isobutyl triethoxy silane, coalescents, dimethyl Polysiloxanes, magnolol and propiconazole are added into consersion unit, are warming up to 160-180 DEG C and react 3-5 hours, are subsequently cooled to Room temperature, control rotating speed are 900-1200rpm/min, stir 40-60min, obtain pre-coating solution;
2., pre-coating solution is spread evenly across on PET matrix, coating process uses dimple coating method, solidification to use heat cure side Formula.
CN201810440223.8A 2018-05-10 2018-05-10 A kind of complex optics pre-coating film Pending CN108774331A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201810440223.8A CN108774331A (en) 2018-05-10 2018-05-10 A kind of complex optics pre-coating film

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201810440223.8A CN108774331A (en) 2018-05-10 2018-05-10 A kind of complex optics pre-coating film

Publications (1)

Publication Number Publication Date
CN108774331A true CN108774331A (en) 2018-11-09

Family

ID=64027030

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201810440223.8A Pending CN108774331A (en) 2018-05-10 2018-05-10 A kind of complex optics pre-coating film

Country Status (1)

Country Link
CN (1) CN108774331A (en)

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS5494574A (en) * 1978-01-09 1979-07-26 Toray Ind Inc Polyester film with improved surface
CN102615897A (en) * 2012-03-30 2012-08-01 富维薄膜(山东)有限公司 Polyester film in field of optical films
CN104745116A (en) * 2012-05-02 2015-07-01 藤森工业株式会社 Surface protection film and optical component attached with the film
CN105585918A (en) * 2016-02-02 2016-05-18 江苏怡丽科姆新材料股份有限公司 Preparation method of composite optical precoating film

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS5494574A (en) * 1978-01-09 1979-07-26 Toray Ind Inc Polyester film with improved surface
CN102615897A (en) * 2012-03-30 2012-08-01 富维薄膜(山东)有限公司 Polyester film in field of optical films
CN104745116A (en) * 2012-05-02 2015-07-01 藤森工业株式会社 Surface protection film and optical component attached with the film
CN105585918A (en) * 2016-02-02 2016-05-18 江苏怡丽科姆新材料股份有限公司 Preparation method of composite optical precoating film

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Address after: 801 Jiekang Road, Jieshi Town, Banan District, Chongqing

Applicant after: Chongqing China membrane composite material Co., Ltd

Address before: 401320 3, 4-2, Shek Gui Road, Jieshi Town, Banan District, Chongqing, 4-2

Applicant before: CHONGQING XINKANGYI DAHL NEW MATERIALS Co.,Ltd.

RJ01 Rejection of invention patent application after publication
RJ01 Rejection of invention patent application after publication

Application publication date: 20181109