CN108773886A - A kind of textile waste cleanser and preparation method thereof - Google Patents
A kind of textile waste cleanser and preparation method thereof Download PDFInfo
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- CN108773886A CN108773886A CN201810742024.2A CN201810742024A CN108773886A CN 108773886 A CN108773886 A CN 108773886A CN 201810742024 A CN201810742024 A CN 201810742024A CN 108773886 A CN108773886 A CN 108773886A
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- textile waste
- cleanser
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/52—Treatment of water, waste water, or sewage by flocculation or precipitation of suspended impurities
- C02F1/5263—Treatment of water, waste water, or sewage by flocculation or precipitation of suspended impurities using natural chemical compounds
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/52—Treatment of water, waste water, or sewage by flocculation or precipitation of suspended impurities
- C02F1/54—Treatment of water, waste water, or sewage by flocculation or precipitation of suspended impurities using organic material
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F2103/00—Nature of the water, waste water, sewage or sludge to be treated
- C02F2103/30—Nature of the water, waste water, sewage or sludge to be treated from the textile industry
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Hydrology & Water Resources (AREA)
- Engineering & Computer Science (AREA)
- Environmental & Geological Engineering (AREA)
- Water Supply & Treatment (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Treatment Of Sludge (AREA)
Abstract
The invention discloses a kind of textile waste cleansers and preparation method thereof.The textile waste cleanser includes the component of following parts by weight：12-20 parts of silkworm excrements, 10-18 parts of leek seed powder, 11-16 parts of cornu cerve degelatinatums, 8-15 parts of white birch myrons, 2-8 parts of Argirelines, 5-11 parts of Breviscapinuns.The textile waste of the present invention can effectively reduce the coloration in textile waste with cleanser, reduce BOD, COD content in textile waste, the time for apparent aggregation occur is short, and treatment effect is preferable；The textile waste of the present invention is few with cleanser raw material, preparation process is simple, and dosage is small, to equipment fanout free region, and the harm of non-secondary pollution, it is more environmentally-friendly.
Description
Technical field
The present invention relates to a kind of cleanser, specifically a kind of textile waste cleanser and preparation method thereof.
Background technology
Textile printing and dyeing industry is one of the industrial department that water consumption is big, discharge of wastewater is more.According to statistics, China's printing and dyeing enterprise
The wastewater flow rate discharged daily reaches ten thousand tons of 300-400.Suspended matter, grease, Soft flocks, surface work are typically contained in textile waste
Property agent and various dyestuffs etc..As often contained flocking, slurry in cotton spinning waste water, wool manufacturing waste water often contains grease；Dyeing waste water
In often contain slurry, dyestuff, auxiliary agent and gas chromatography etc..
Existing textile sewage inorganic agent some is using inorganic matter as chemical floc, and dosage is big, and decolorizing effect is poor,
There is stronger corrosivity to equipment；Some is using organic matter as chemical floc, and raw material is complicated, and preparation process is cumbersome, and has
There is the harm of secondary pollution, it is not environmentally friendly enough.
Invention content
The purpose of the present invention is to provide a kind of textile waste cleansers and preparation method thereof, to solve above-mentioned background skill
The problem of being proposed in art.
To achieve the above object, the present invention provides the following technical solutions：
A kind of textile waste cleanser, the textile waste cleanser include the component of following parts by weight：12-20 parts
Silkworm excrement, 10-18 parts of leek seed powder, 11-16 parts of cornu cerve degelatinatums, 8-15 parts of white birch myrons, 2-8 parts of Argirelines, 5-11 parts of lamps
Small cup florigen.
As a further solution of the present invention：The textile waste cleanser includes the component of following parts by weight：15-18
Part silkworm excrement, 12-16 parts of leek seed powder, 13-15 parts of cornu cerve degelatinatums, 11-13 parts of white birch myrons, 4-7 parts of Argirelines, 7-10 parts
Breviscapinun.
As a further solution of the present invention：The textile waste cleanser includes the component of following parts by weight：17 parts
Silkworm excrement, 15 parts of leek seed powder, 14 parts of cornu cerve degelatinatums, 12 parts of white birch myrons, 6 parts of Argirelines, 8 parts of Breviscapinuns.
A kind of preparation method of textile waste cleanser, includes the following steps：
(1) white birch myron is mixed with 25-40 parts of water, 20-30 parts of 65% ethanol solution, is placed at 65-70 DEG C
10-20min is mixed, mixed liquor a is obtained；
(2) after mixing silkworm excrement, leek seed powder and cornu cerve degelatinatum, 35-50 parts of water is added, is placed at 95-100 DEG C and boils 25-
40min；Then on being added in step gained mixed liquor a, ultrasonic mixing 2-5min is subsequently placed at 70-73 DEG C and is stirred 30-
40min obtains mixed liquor b；
(3) Argireline is mixed with Breviscapinun, is placed at 80-92 DEG C and 10-20min is mixed；Then plus
Enter in mixed liquor b obtained by upper step, ultrasonic mixing 5-10min is subsequently placed at 75-76 DEG C and is stirred 10-15min, and decompression is steamed
Evaporate recycling ethyl alcohol after, gains continue to be placed at 105-116 DEG C be stirred to react 1-2h to get.
As a further solution of the present invention：Step (1) is molten by white birch myron and 32 parts of water, 25 parts of 65% ethyl alcohol
Liquid mixes, and is placed at 68 DEG C and mixes 17min, obtains mixed liquor a.
As a further solution of the present invention：After step (2) mixes silkworm excrement, leek seed powder and cornu cerve degelatinatum, it is added 42 parts
Water, be placed at 97 DEG C and boil 32min；Then on being added in step gained mixed liquor a, ultrasonic mixing 4min is subsequently placed at 71 DEG C
It is stirred 36min, obtains mixed liquor b.
As a further solution of the present invention：Step (3) mixes Argireline with Breviscapinun, is placed at 89 DEG C
13min is mixed；Then on being added in step gained mixed liquor b, ultrasonic mixing 8min is subsequently placed at 75.5 DEG C and is stirred
11min, vacuum distillation recycling ethyl alcohol after, gains continue to be placed at 110 DEG C be stirred to react 1.6h to get.
Compared with prior art, the beneficial effects of the invention are as follows：
The textile waste of the present invention can effectively reduce the coloration in textile waste with cleanser, reduce in textile waste
BOD, COD content, the time for apparent aggregation occur is short, and treatment effect is preferable；The textile waste of present invention cleanser original
Material less, preparation process it is simple, dosage is small, more environmentally-friendly to equipment fanout free region, and the harm of non-secondary pollution.
Specific implementation mode
The technical solution of this patent is described in more detail With reference to embodiment.
Embodiment 1
A kind of textile waste cleanser, the textile waste cleanser include the component of following parts by weight：12 portions of silkworms
Sand, 10 parts of leek seed powder, 11 parts of cornu cerve degelatinatums, 8 parts of white birch myrons, 2 parts of Argirelines, 5 parts of Breviscapinuns.
A kind of preparation method of textile waste cleanser, includes the following steps：(1) by white birch myron and 25 parts of water,
20 parts of 65% ethanol solution mixing, is placed at 65 DEG C and mixes 10min, obtain mixed liquor a；(2) by silkworm excrement, leek seed powder and
After cornu cerve degelatinatum mixing, 35 parts of water is added, is placed at 95 DEG C and boils 25min；Then on being added in step gained mixed liquor a, ultrasound is mixed
2min is closed, is subsequently placed at 70 DEG C and is stirred 30min, obtain mixed liquor b；(3) Argireline and Breviscapinun are mixed
It closes, is placed at 80 DEG C and 10min is mixed；Then on being added in step gained mixed liquor b, ultrasonic mixing 5min is subsequently placed in 75
Be stirred 10min at DEG C, after vacuum distillation recycling ethyl alcohol, gains continue to be placed at 105 DEG C be stirred to react 1h to get.
Embodiment 2
A kind of textile waste cleanser, the textile waste cleanser include the component of following parts by weight：20 portions of silkworms
Sand, 18 parts of leek seed powder, 16 parts of cornu cerve degelatinatums, 15 parts of white birch myrons, 8 parts of Argirelines, 11 parts of Breviscapinuns.
A kind of preparation method of textile waste cleanser, includes the following steps：(1) by white birch myron and 40 parts of water,
30 parts of 65% ethanol solution mixing, is placed at 70 DEG C and mixes 20min, obtain mixed liquor a；(2) by silkworm excrement, leek seed powder and
After cornu cerve degelatinatum mixing, 50 parts of water is added, is placed at 100 DEG C and boils 40min；Then on being added in step gained mixed liquor a, ultrasound is mixed
5min is closed, is subsequently placed at 73 DEG C and is stirred 40min, obtain mixed liquor b；(3) Argireline and Breviscapinun are mixed
It closes, is placed at 92 DEG C and 20min is mixed；Then on being added in step gained mixed liquor b, ultrasonic mixing 10min is subsequently placed in 76
Be stirred 15min at DEG C, after vacuum distillation recycling ethyl alcohol, gains continue to be placed at 116 DEG C be stirred to react 2h to get.
Embodiment 3
A kind of textile waste cleanser, the textile waste cleanser include the component of following parts by weight：17 portions of silkworms
Sand, 15 parts of leek seed powder, 14 parts of cornu cerve degelatinatums, 12 parts of white birch myrons, 6 parts of Argirelines, 8 parts of Breviscapinuns.
A kind of preparation method of textile waste cleanser, includes the following steps：(1) by white birch myron and 32 parts of water,
25 parts of 65% ethanol solution mixing, is placed at 68 DEG C and mixes 17min, obtain mixed liquor a.(2) by silkworm excrement, leek seed powder and
After cornu cerve degelatinatum mixing, 42 parts of water is added, is placed at 97 DEG C and boils 32min；Then on being added in step gained mixed liquor a, ultrasound is mixed
4min is closed, is subsequently placed at 71 DEG C and is stirred 36min, obtain mixed liquor b.(3) Argireline and Breviscapinun are mixed
It closes, is placed at 89 DEG C and 13min is mixed；Then on being added in step gained mixed liquor b, ultrasonic mixing 8min is subsequently placed in
11min is stirred at 75.5 DEG C, after ethyl alcohol is recycled in vacuum distillation, gains, which continue to be placed at 110 DEG C, is stirred to react 1.6h, i.e.,
?.
Embodiment 4
A kind of textile waste cleanser, the textile waste cleanser include the component of following parts by weight：15 portions of silkworms
Sand, 12 parts of leek seed powder, 13 parts of cornu cerve degelatinatums, 11 parts of white birch myrons, 4 parts of Argirelines, 7 parts of Breviscapinuns.
A kind of preparation method of textile waste cleanser, includes the following steps：(1) by white birch myron and 28 parts of water,
23 parts of 65% ethanol solution mixing, is placed at 66 DEG C and mixes 12min, obtain mixed liquor a；(2) by silkworm excrement, leek seed powder and
After cornu cerve degelatinatum mixing, 38 parts of water is added, is placed at 96 DEG C and boils 26min；Then on being added in step gained mixed liquor a, ultrasound is mixed
3min is closed, is subsequently placed at 71 DEG C and is stirred 33min, obtain mixed liquor b；(3) Argireline and Breviscapinun are mixed
It closes, is placed at 83 DEG C and 12min is mixed；Then on being added in step gained mixed liquor b, ultrasonic mixing 6min is subsequently placed in
11min is stirred at 75.2 DEG C, after ethyl alcohol is recycled in vacuum distillation, gains, which continue to be placed at 108 DEG C, is stirred to react 1.3h, i.e.,
?.
Embodiment 5
A kind of textile waste cleanser, the textile waste cleanser include the component of following parts by weight：18 portions of silkworms
Sand, 16 parts of leek seed powder, 15 parts of cornu cerve degelatinatums, 13 parts of white birch myrons, 7 parts of Argirelines, 10 parts of Breviscapinuns.
A kind of preparation method of textile waste cleanser, includes the following steps：(1) by white birch myron and 36 parts of water,
28 parts of 65% ethanol solution mixing, is placed at 69 DEG C and mixes 18min, obtain mixed liquor a；(2) by silkworm excrement, leek seed powder and
After cornu cerve degelatinatum mixing, 47 parts of water is added, is placed at 98 DEG C and boils 38min；Then on being added in step gained mixed liquor a, ultrasound is mixed
4min is closed, is subsequently placed at 72 DEG C and is stirred 38min, obtain mixed liquor b；(3) Argireline and Breviscapinun are mixed
It closes, is placed at 90 DEG C and 18min is mixed；Then on being added in step gained mixed liquor b, ultrasonic mixing 8min is subsequently placed in
14min is stirred at 75.8 DEG C, after ethyl alcohol is recycled in vacuum distillation, gains, which continue to be placed at 114 DEG C, is stirred to react 1.8h, i.e.,
?.
Comparative example 1
In addition to not containing Breviscapinun in raw material, other preparation processes are consistent with embodiment 3.
Comparative example 2
In addition to not containing white birch myron in raw material, other preparation processes are consistent with embodiment 3.
Comparative example 3
In addition to not containing Breviscapinun and white birch myron in raw material, other preparation processes are consistent with embodiment 3.
Comparative example 4
Raw material is consistent with embodiment 3, unlike in preparation process：Step (2) mixes silkworm excrement, leek seed powder and cornu cerve degelatinatum
After conjunction, 47 parts of water and mixed liquor a is added, stirs evenly, obtains mixed liquor b.
Experimental example
Sewage disposal is carried out to embodiment 1-3 and comparative example 1-4 in accordance with the following methods：Textile printing and dyeing wastewater is first passed through into lattice
After grid filtering, into sedimentation basin, it will be handled in the textile printing and dyeing wastewater in flocculant input sedimentation basin, input amount 100mg/
L.Apparent aggregation is occurred as soon as when putting into 10-20 minutes, the time for apparent aggregation occur is to reach essentially identical
Time used in apparent coacervation, after processing time 1h, effect is as shown in table 1.
Table 1
The better embodiment of this patent is explained in detail above, but this patent is not limited to above-mentioned embodiment party
Formula, one skilled in the relevant art within the scope of knowledge, can also be under the premise of not departing from this patent objective
Various changes can be made.
Claims (7)
1. a kind of textile waste cleanser, which is characterized in that the textile waste cleanser includes the group of following parts by weight
Point：12-20 parts of silkworm excrements, 10-18 parts of leek seed powder, 11-16 parts of cornu cerve degelatinatums, 8-15 parts of white birch myrons, 2-8 parts of acetyl group hexapeptides-
8,5-11 parts of Breviscapinuns.
2. textile waste cleanser according to claim 1, which is characterized in that the textile waste includes with cleanser
The component of following parts by weight：15-18 parts of silkworm excrements, 12-16 parts of leek seed powder, 13-15 parts of cornu cerve degelatinatums, 11-13 parts of white birch myrons, 4-
7 parts of Argirelines, 7-10 parts of Breviscapinuns.
3. textile waste cleanser according to claim 1, which is characterized in that the textile waste includes with cleanser
The component of following parts by weight：17 parts of silkworm excrements, 15 parts of leek seed powder, 14 parts of cornu cerve degelatinatums, 12 parts of white birch myrons, 6 parts of acetyl group hexapeptides-
8,8 parts of Breviscapinuns.
4. a kind of preparation method according to any textile waste cleansers of claim 1-3, which is characterized in that including
Following steps：
(1) white birch myron is mixed with 25-40 parts of water, 20-30 parts of 65% ethanol solution, is placed at 65-70 DEG C and mixes
10-20min obtains mixed liquor a；
(2) after mixing silkworm excrement, leek seed powder and cornu cerve degelatinatum, 35-50 parts of water is added, is placed at 95-100 DEG C and boils 25-
40min；Then on being added in step gained mixed liquor a, ultrasonic mixing 2-5min is subsequently placed at 70-73 DEG C and is stirred 30-
40min obtains mixed liquor b；
(3) Argireline is mixed with Breviscapinun, is placed at 80-92 DEG C and 10-20min is mixed；Then on being added
In step gained mixed liquor b, ultrasonic mixing 5-10min is subsequently placed at 75-76 DEG C and is stirred 10-15min, is evaporated under reduced pressure back
Receive ethyl alcohol after, gains continue to be placed at 105-116 DEG C be stirred to react 1-2h to get.
5. the preparation method of textile waste cleanser according to claim 4, which is characterized in that step (1) is by white birch
Myron is mixed with 32 parts of water, 25 parts of 65% ethanol solution, is placed at 68 DEG C and is mixed 17min, obtains mixed liquor a.
6. the preparation method of textile waste cleanser according to claim 4, which is characterized in that step (2) by silkworm excrement,
After leek seed powder and cornu cerve degelatinatum mixing, 42 parts of water is added, is placed at 97 DEG C and boils 32min；Then step gained mixed liquor a on being added
In, ultrasonic mixing 4min is subsequently placed at 71 DEG C and is stirred 36min, obtains mixed liquor b.
7. the preparation method of textile waste cleanser according to claim 4, which is characterized in that step (3) is by acetyl
Base hexapeptide -8 is mixed with Breviscapinun, is placed at 89 DEG C and 13min is mixed；Then on being added in step gained mixed liquor b, ultrasound
8min is mixed, is subsequently placed at 75.5 DEG C and is stirred 11min, after vacuum distillation recycling ethyl alcohol, gains continue to be placed in 110 DEG C
Under be stirred to react 1.6h to get.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810742024.2A CN108773886A (en) | 2018-07-09 | 2018-07-09 | A kind of textile waste cleanser and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810742024.2A CN108773886A (en) | 2018-07-09 | 2018-07-09 | A kind of textile waste cleanser and preparation method thereof |
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| Publication Number | Publication Date |
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| CN108773886A true CN108773886A (en) | 2018-11-09 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201810742024.2A Pending CN108773886A (en) | 2018-07-09 | 2018-07-09 | A kind of textile waste cleanser and preparation method thereof |
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Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106629973A (en) * | 2016-12-18 | 2017-05-10 | 钦州市科学技术开发中心 | Treating agent for tannery wastewater and preparation method thereof |
| CN107758823A (en) * | 2017-11-30 | 2018-03-06 | 杨威 | A kind of domestic sewage treating compound and preparation method thereof |
| CN107902769A (en) * | 2017-11-30 | 2018-04-13 | 广西南宁途御科技有限公司 | Sewage-treating agent of Biocomposite material and preparation method thereof |
-
2018
- 2018-07-09 CN CN201810742024.2A patent/CN108773886A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106629973A (en) * | 2016-12-18 | 2017-05-10 | 钦州市科学技术开发中心 | Treating agent for tannery wastewater and preparation method thereof |
| CN107758823A (en) * | 2017-11-30 | 2018-03-06 | 杨威 | A kind of domestic sewage treating compound and preparation method thereof |
| CN107902769A (en) * | 2017-11-30 | 2018-04-13 | 广西南宁途御科技有限公司 | Sewage-treating agent of Biocomposite material and preparation method thereof |
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Application publication date: 20181109 |