CN108753450A - A kind of gleditsia sinensis knockout tower and the method for preparing cottonseed refined oil with mixed cotton seed oil using the device - Google Patents
A kind of gleditsia sinensis knockout tower and the method for preparing cottonseed refined oil with mixed cotton seed oil using the device Download PDFInfo
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- CN108753450A CN108753450A CN201810468843.2A CN201810468843A CN108753450A CN 108753450 A CN108753450 A CN 108753450A CN 201810468843 A CN201810468843 A CN 201810468843A CN 108753450 A CN108753450 A CN 108753450A
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- gleditsia sinensis
- oil
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- disk
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B3/00—Refining fats or fatty oils
- C11B3/02—Refining fats or fatty oils by chemical reaction
- C11B3/06—Refining fats or fatty oils by chemical reaction with bases
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B3/00—Refining fats or fatty oils
- C11B3/001—Refining fats or fatty oils by a combination of two or more of the means hereafter
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B3/00—Refining fats or fatty oils
- C11B3/16—Refining fats or fatty oils by mechanical means
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02W—CLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
- Y02W30/00—Technologies for solid waste management
- Y02W30/50—Reuse, recycling or recovery technologies
- Y02W30/74—Recovery of fats, fatty oils, fatty acids or other fatty substances, e.g. lanolin or waxes
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- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Microbiology (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Mechanical Engineering (AREA)
- General Chemical & Material Sciences (AREA)
- Fats And Perfumes (AREA)
Abstract
The invention discloses a kind of gleditsia sinensis knockout towers of static separation soap oil, it is characterised in that：Including tank body B, the tank body B is equipped with oil export, arrange gleditsia sinensis pipe and material inlet, the oil export is located at the top of tank body B, row's gleditsia sinensis pipe is located at the lower part of tank body B, at least one set of soap oil separator disk is equipped between oil export and row's gleditsia sinensis pipe, the soap oil separator disk includes separator disk disk body, the separator disk disk body is in umbrella, its surface is equipped with fold, that is fold A and fold B, fold A rolls over downwards, fold B rolls over upwards, fold A and fold B are arranged alternately, the axle center of the separator disk disk body is equipped with materail tube, at least one end of the materail tube is open end, open end is feed inlet, the described feed inlet is connect with material inlet, the materail tube tube surfaces are equipped with bleed opening, the bleed opening is located in the umbrella that separator disk disk body is covered.
Description
Technical field
The present invention relates to a kind of gleditsia sinensis knockout tower and the methods for preparing cottonseed refined oil with mixed cotton seed oil using the device.
Background technology
At present when cottonseed processing, obtained miscella carries out refined oil preparation, needs first to carry out twice evaporation, be added later
Lye carries out alkali refining, and alkali refining process saponification forms gleditsia sinensis, needs to detach refined oil and gleditsia sinensis later, soap stock detaches at present
Equipment is mostly self-cleaning type centrifuge, although self-cleaning type centrifuge separation soap stock is with obvious effects, the equipment investment is big, dynamic to disappear
Consumption, it is high to the competency profiling of operating personnel, it needs regular maintenance and upkeep cost is high, filled using needs in explosion-proof workshop
Nitrogen, subsidiary engine auxiliary facility are more.
Therefore, a kind of simple in structure, it is not necessarily to extra power, no security risk, gleditsia sinensis good separating effect can avoid secondary
Mixing, and the gleditsia sinensis knockout tower of the static separation soap without the leakage of inflammable and explosive solvent and oil is suggested.
Invention content
The invention discloses the devices that each step in a kind of method of refining of mixed cotton seed oil refining oil and this method uses.
The invention discloses a kind of mixed cotton seed oil refining methods, it is characterised in that：Including at least following steps：
Oily alkali mixing and alkali refining：Cottonseed mixing crude oil is mixed with lye, after mixing heating carry out alkali refining, when mixing
Using oily alkali static mixing device, alkali refining is heated later；
Gleditsia sinensis detaches：The liquid obtained after alkali refining carries out the separation of soap and oil using gleditsia sinensis separator, after collecting separation
Oil and gleditsia sinensis；
Gleditsia sinensis precipitation：The gleditsia sinensis that gleditsia sinensis separates and collects is pumped into gleditsia sinensis exsolution apparatus, carries out gleditsia sinensis carrying out precipitation treatment, recycling is molten
Agent and gleditsia sinensis.
The concrete structure of the oil alkali static mixing device is as follows：
Including tank body A (1), miscella oil inlet pipe (1-1), lye alkali inlet tube (1-6) and mixing chamber B (1-4), mixing chamber B
(1-4) is located in tank body A (1), and the surface of shell of the mixing chamber B (1-4) is equipped with mixed liquor bleeding holes (1-5), in mixing chamber
Chamber is connected to (1) inner cavities tank body A by mixed liquor bleeding holes (1-5), and the outlet end of the miscella oil inlet pipe (1-1) is placed in mixed
It closes in chamber, at least one section of lye alkali inlet tube (1-6) is placed in miscella oil inlet pipe (1-1), and lye alkali inlet tube (1-6) is placed in
The part of miscella oil inlet pipe (1-1) is equipped with lye bleeding holes (1-2).
When oily alkali mixing, miscella enters mixing chamber B (1-4) by pump, by miscella oil inlet pipe (1-1), is entering
Before mixing chamber B (1-4), it is located at lye inlet tube (1-6) in the lye bleeding holes (1-6) of miscella oil inlet pipe (1-1) section
The lye mixed once of exudation, after entering mixing chamber B (1-4), and from the mixed liquor bleeding holes (1-5) of mixing chamber B (1-4)
Exudation, when exudation, secondary mixing can be mixed more uniformly by mixing twice.
The tank body A (1) is equipped with mixed liquor liquid outlet (1-7), and miscella and lye are after mixing from the mixed liquor
Liquid outlet (1-7) is discharged, and by heating devices heat, is reacted in delay reaction unit (20) later.
External are cased with of mixing chamber B (1-4) is equipped at least one set mixing chamber A (1-3), the surface of shell of mixing chamber A (1-3)
Equipped with mixed liquor bleeding holes (1-5), one layer of mixing chamber A (1-3) is equipped with mixing chamber B (1-4) is external, can be increased primary mixed
It closes, that is, when mixed liquor is oozed out from mixing chamber A (1-3) to tank body A (1), mixed again.
The mixing chamber A (1-3) can also be equipped with it is multigroup, the group number being equipped with is more, then what is mixed is about uniform, mixing chamber B
(1-4) is located at innermost layer, and multigroup mixing chamber A (1-3) is arranged successively, the oily alkali mixing liquid being discharged from tank body A (1), it is necessary to from
After mixed liquor bleeding holes (1-5) exudation of mixing chamber A (1-3) and mixing chamber B (1-4), it could be discharged from outlet.
In actual use：Miscella inputs mixing chamber by miscella oil inlet pipe (1-1), and lye passes through lye alkali inlet tube
(1-6) enters miscella oil inlet pipe (1-1), and under miscella mobilization, lye is inhaled from the interior negative pressure of lye alkali inlet tube (1-6)
Go out, tentatively mixed, enter mixing chamber later, since mixing chamber surface is equipped with mixed liquor bleeding holes (1-5), can mix again
It closes, realizes that oily alkali is sufficiently mixed, the oily alkali being finally discharged from tank body A (1) mixed liquor liquid outlet (1-7) can reach fully mixed
It closes.
This oil alkali static mixing device is in actual use, it is only necessary to carry out liquid using miscella oil feed pump and lye pump
Conveying, without being additionally provided power, not only reduces power consumption, and avoid easy when mixing when two kinds of liquid are mixed
The volatilization for firing explosive solvent, eliminates safe hidden trouble, and improves production safety.
This oil alkali static mixing device is not only simple in structure, and mixing efficiency is high, while can also be energy saving, is not pacified
Full hidden danger is realized when oily alkali mixes and is achieved many things at one stroke.
The concrete structure of the gleditsia sinensis separator is as follows：Including tank body B (3), the tank body B (3) is equipped with oil export
(3-5), row's gleditsia sinensis pipe (3-8) and material inlet (3-3), the oil export (3-5) are located at the top of (3) tank body B, arrange gleditsia sinensis pipe
(3-8) is located at the lower part of (3) tank body B, and at least one set of soap oil separator disk is equipped between oil export (3-5) and row's gleditsia sinensis pipe (3-8)
(3-4), material inlet (3-3) are connect with gleditsia sinensis separator disk (3-4), and the liquid of tank body B (3) is entered by material inlet (3-3),
Soap oil separation can be carried out in gleditsia sinensis separator disk (3-4), oil is discharged from oil export (3-5) and collects, and soap is precipitated to row's gleditsia sinensis pipe (3-
8), gleditsia sinensis is collected later.
The soap oil separator disk (3-4), including separator disk disk body (3-45), the separator disk disk body (3-45) is in umbrella,
Its surface is equipped with fold, i.e. fold A (3-42) and fold B (3-43), fold A (3-42) roll over downwards, and fold B (3-43) is upward
Folding, fold A (3-42) and fold B (3-43) are arranged alternately, and the fold A (3-42) and fold B (3-43) are linked up disk body
The edge (3-45) constitutes undaform, and the axle center of the separator disk disk body (3-45) is equipped with materail tube (3-48), the materail tube (3-
48) at least one end is open end, and open end is feed inlet (3-41), the described feed inlet (3-41) and material inlet (3-3)
Connection, materail tube (3-48) tube surfaces are equipped with bleed opening (3-47), and the bleed opening (3-47) is located at separator disk disk body
In the umbrella that (3-45) is covered, and close to umbrella point position.
The soap oil separator disk in actual use, can unpowered separation gleditsia sinensis and oil, no security risk, energy-saving and emission-reduction.
It refer to the lower section of separator disk disk body (3-45) in the umbrella that the separator disk disk body (3-45) is covered.
In actual use：Soap oil mixed liquor enters materail tube (3-48) by material inlet (3-3), and from materail tube (3-
48) bleed opening (3-47) discharge of surface setting, in the range of being covered into disk body (3-45) lower section, the gleditsia sinensis separator disk
(3-4) can be equipped with one group, can also be equipped with group.
The disk body is center height, and disk body edge is low, and bleed opening (3-47) is positioned close to the position of umbrella point, that is, oozes out
The height of mouth is higher, and disk body edge is relatively low, the separated obtained oil and gleditsia sinensis of soap oil mixed liquor, and oil is lighter, and gleditsia sinensis is heavier, compared with
To floating, heavier gleditsia sinensis precipitates downwards light oil.
If be provided only with one group of gleditsia sinensis separator disk, the gleditsia sinensis of bleed opening (3-47) exudation precipitates directly down, and oil is necessary
Along disk body (3-45), finally from the edge disk body (3-45), disengaging could be floated upwards, due to fold A (3-42) and fold B (3-
43) it is arranged alternately, i.e. a fold A (3-42), a fold B (3-43), therefore, lighter oil can be floating to fold B (3-43)
It is dynamic, and the region that finally disengaging disk body (3-45) is covered at fold B (3-43)；
If being equipped with multigroup separator disk, the liquid of bleed opening (3-47) exudation moves downward between two separate disk, compared with
The gleditsia sinensis of weight is precipitated to upper surface fold A (3-42) of lower layer, and disk body (3-45) is finally slid out at fold A (3-42),
And precipitated to tank body B (3) lower part, and lighter oil then floats to the lower surface fold B (3-43) on upper layer, and finally from fold B
It is detached from disk body (3-45) at (3-43) and floats up, is finally discharged and collects from oil export (3-5).
Above-mentioned fold A (3-42) and fold B (3-43) are V-type or arc.
It can be very good to carry out gleditsia sinensis and oil by the fold A (3-42) and fold B (3-43) that roll over and roll over downwards upwards
It is oriented to shunting, can be achieved with detaching for the first time before being detached from disk body (3-45), never flowed with route, avoid the secondary of soap oil
Mixing, while fold A (3-42) and fold B (3-43) they are to be arranged alternately, and it is corresponding in same vertical direction, i.e., it is same vertical
All it is fold A (3-42) on straight line or is all fold B (3-43), oil floats up to is encountered when last layer disk body or oil, soap
Encountered when next layer of disk body or soap is sunk to, therefore, gleditsia sinensis sinking route and oily floating route are in different vertical lines
On, in actual use, the soap and oil detached is not in secondary mixing, and whole separation effect is good, and separation rate is higher.
And it is the unpowered type separation taken in soap oil separation process, need not only uses electric energy, save energy consumption,
And when detaching, the secondary contact of soap oil can be avoided, improves separative efficiency.
As an improvement, being equipped with baffle (3-46) at bleed opening (3-47), the liquid that bleed opening (3-47) comes out is flushed to baffle
It on (3-46), can prevent from being vortexed, the liquid that bleed opening (3-47) comes out is enable slowly to flow.
Annularly, i.e., baffle (3-46) is the ring-type being set on the outside of materail tube (3-48) to the baffle (3-46).
Gleditsia sinensis by separation is precipitated to the lower part of (3) tank body B, that is, the row's of being deposited to gleditsia sinensis pipe (3-8) is inner, row's gleditsia sinensis
It manages and is equipped with drawing liquid pump in (3-8), can will arrange the gleditsia sinensis in gleditsia sinensis pipe (3-8) and be discharged.
The junction of the tank body B (3) and row's gleditsia sinensis pipe (3-8) is tapered, i.e. the ends tank body B (3) are thicker, arranges gleditsia sinensis pipe
(3-8) is relatively thin, is connected the two by bullet, and gleditsia sinensis is precipitated in the conical region, enters row's gleditsia sinensis pipe (3-8) later.
Row's gleditsia sinensis pipe (3-8) is equipped with gleditsia sinensis accumulated amount controller, and the gleditsia sinensis accumulated amount controller includes control device
(3-6) and at least one set of light sensitive component, the light sensitive component include light-emitting device (3-1) and photosensitive device (3-7)；The drawing liquid
Motor is connected at pump；The control device (3-6) is electrically connected between the light sensitive component and the motor, i.e. control device
(3-6) constitutes control loop with the light sensitive component and the motor, and the photosensitive device (3-7) in the light sensitive component can incite somebody to action
Photoreceptor signal feeds back to control device (3-6) to control electric motor starting or stopping, and then controls drawing liquid pump and be turned on and off.
Row's gleditsia sinensis pipe (3-8) is in vertical tubulose, and the light sensitive component is arranged on the madial wall of the column structure,
And light-emitting device (3-1) in the light sensitive component and the photosensitive device (3-7) are in the same horizontal position.
The madial wall of the column structure is equipped with casing, and the top of the tube body (3-2) of the casing is transparent material or sets
There are through-hole, the light-emitting device (3-1) and/or the photosensitive device (3-7) to be fixed in the casing.
As an improvement, the gleditsia sinensis accumulated amount controller includes multigroup photosensitive element, and multigroup light sensitive component is in Vertical Square
It is mutually juxtaposed upwards, and motor is variable-frequency motor.
Photoreceptor signal can be fed back to control device (3-6) to control by the photosensitive device (3-7) in the light sensitive component
Electric motor starting or stopping, and then control drawing liquid pump and be turned on and off, specially：Light-emitting device is perceived in photosensitive device (3-7)
When the light that (3-1) is sent out, generates a trigger signal and give control device (3-6), control device (3-6) is according to the trigger signal
Start motor rotation, and then controls drawing liquid pump and open；The light that light-emitting device (3-1) is sent out is not perceived in photosensitive device (3-7)
When line, generates an interrupt signal and control device (3-6), control device (3-6) is given to stop motor according to the interrupt signal and rotate,
And then it controls drawing liquid pump and closes.
The gleditsia sinensis separator in actual use, can realize unpowered separation gleditsia sinensis and oil, only in material inlet (3-
3) and row's gleditsia sinensis pipe (3-8) is equipped with pump, you can completes whole device operation, centre separation is not necessarily to extra power completely, energy saving
While emission reduction, and without security risk, and leakage is not will produce.
The concrete structure of the gleditsia sinensis exsolution apparatus is as follows：Including tank body C (4), tank body C (4) top is equipped with solvent
Steam (vapor) outlet (4-4), bottom are equipped with gleditsia sinensis discharge pipe (4-6), and the tank body C (4) is equipped with heating and mixing device,
The heating and mixing device includes：Containing molten gleditsia sinensis inlet tube (4-2), steam inlet (4-1) and outer cover (4-3), institute
It states outer cover (4-3) and is set in the heating room (4-9) for forming strip on the outside of tank body C (4), the tank body C at heating room (4-9)
(4) surface is equipped with spray-hole (4-8), described to be connected to heating room (4-9) containing molten gleditsia sinensis inlet tube (4-2), the steam inlet
(4-1) is connected to containing molten gleditsia sinensis inlet tube (4-2), i.e., steam can be entered by steam inlet (4-1) and contain molten gleditsia sinensis inlet tube
It in (4-2), and is mixed, and is heated containing in molten gleditsia sinensis inlet tube (4-21) with containing the liquid in molten gleditsia sinensis inlet tube (4-2)
Liquid, and from spray-hole (4-8) enter tank body C (4) inner cavity.
As an improvement, the liquid outlet height of the gleditsia sinensis discharge pipe (4-6) is higher than the liquid level in tank body C (4).
In actual use：Enter tank body C by containing molten gleditsia sinensis inlet tube (4-2) by the isolated molten gleditsia sinensis that contains of gleditsia sinensis
(4), described containing steam inlet (4-1) is connected on molten gleditsia sinensis inlet tube (4-2), steam, which enters, contains molten gleditsia sinensis inlet tube (4-2)
Mixed afterwards with containing molten gleditsia sinensis, and molten gleditsia sinensis liquid will be contained and heated, at this point, the solvent contained in gleditsia sinensis can be gasified, from
When spray-hole (4-8) sprays, solvent vapo(u)r realizes that solvent is collected from solvent vapo(u)r outlet (4-4) discharge, and gleditsia sinensis or liquid
Body retains in tank body C (4) lower part, since the liquid outlet of gleditsia sinensis discharge pipe (4-6) is higher than the liquid levels in tank body C (4), only
Have when the liquid in tank body C (4) is higher than the liquid outlet of gleditsia sinensis discharge pipe (4-6), gleditsia sinensis can be just discharged, is realized unpowered molten
Agent seperator gleditsia sinensis is collected.
As an improvement, steam inlet (4-1) and containing the molten gleditsia sinensis inlet tube junction (4-2) with heat room (4-9) between
At least one set of barrier piece (4-7) is equipped in tube body containing molten gleditsia sinensis inlet tube (4-2).
In actual use：Containing barrier piece (4-7) is equipped in molten gleditsia sinensis inlet tube (4-2), can adequately make steam with
The mixing of liquid, it is more thorough to being heated containing the solvent in molten gleditsia sinensis liquid, improve the rate of recovery of solvent.
As an improvement, the corresponding outer cover (4-3) of spray-hole (4-8) is equipped with adjusting bolt (4-5), by screwing the adjusting
Bolt (4-5) can adjust the size of spray-hole (4-8), i.e. the end of adjusting bolt (4-5) is tapered, and can be fastened on injection
At hole (4-8), and spray-hole (4-8) can be blocked.
In actual use：Spray-hole (4-8) size can be adjusted, it is easy to use, it is adaptable.
Description of the drawings
Fig. 1 is refined oil process flow chart.
Fig. 2 is static mixing device structural schematic diagram.
Fig. 3 is gleditsia sinensis separator structural schematic diagram.
Fig. 4 is gleditsia sinensis separator disk main structure diagram.
Fig. 5 is gleditsia sinensis separator disk schematic cross-sectional view.
Fig. 6 is gleditsia sinensis separator disk overlooking structure diagram.
Fig. 7 is the directions Fig. 3 A-A schematic cross-sectional view.
Fig. 8 is gleditsia sinensis exsolution apparatus structural schematic diagram.
Fig. 9 is the schematic cross-sectional view of Fig. 8 gleditsia sinensis exsolution apparatus.
Figure 10 is Fig. 8 A-A direction structure schematic diagrames.
As shown in the figure：10 be static mixing device, and 1 is tank body A, and 1-1 is miscella oil inlet pipe, and 1-2 is lye bleeding holes,
1-3 is mixing chamber A, and 1-4 is mixing chamber B, and 1-5 is mixed liquor bleeding holes, and 1-6 is lye alkali inlet tube, and 1-7 is that mixed liquor goes out liquid
Mouthful, 20 be delay reaction unit, and 30 be gleditsia sinensis separator, and 3 be tank body B, and 3-1 is light-emitting device, and 3-2 is tube body, and 3-3 is object
Expect import, 3-4 is soap oil separator disk, and 3-41 is feed inlet, and 3-42 is fold A, and 3-43 is fold B, and 3-44 is connector, 3-45
It is disk body, 3-46 is baffle, and 3-47 is bleed opening, and 3-48 materail tubes, 3-5 is oil export, and 3-6 is control device, and 3-7 is photosensitive
Device, 3-8 are row's gleditsia sinensis pipes, and 40 be gleditsia sinensis exsolution apparatus, and 4 be tank body C, and 4-1 is steam inlet, and 4-2 is to contain molten gleditsia sinensis feed liquor
Pipe, 4-3 are outer covers, and 4-4 is solvent vapo(u)r outlet, and 4-5 is adjusting bolt, and 4-6 is gleditsia sinensis discharge pipe, and 4-7 is barrier piece, 4-8
It is spray-hole, 4-9 is heating room, and 50 be heating device, and 60 be solvent recovery unit.
Specific implementation mode
Embodiment 1：Present embodiment discloses a kind of mixed cotton seed oil refining methods, it is characterised in that：Including at least oily alkali
Mixing step, oily alkali mixing step are to mix cottonseed mixing crude oil with lye, after mixing heating carry out alkali refining, when mixing
Using oily alkali static mixing device, alkali refining is heated later.
The oil alkali static mixing device include tank body A (1), miscella oil inlet pipe (1-1), lye alkali inlet tube (1-6) and
Mixing chamber B (1-4), mixing chamber B (1-4) are located in tank body A (1), and the surface of shell of the mixing chamber B (1-4) is equipped with mixed liquor
Bleeding holes (1-5), mixing chamber inner cavity and (1) inner cavities tank body A are connected to by mixed liquor bleeding holes (1-5), the miscella oil inlet
The outlet end of pipe (1-1) is placed in mixing chamber intracavitary, and at least one section of lye alkali inlet tube (1-6) is placed in miscella oil inlet pipe (1-1),
And lye alkali inlet tube (1-6) is placed in the part of miscella oil inlet pipe (1-1) equipped with lye bleeding holes (1-2).
When oily alkali mixing, miscella enters mixing chamber B (1-4) by pump, by miscella oil inlet pipe (1-1), is entering
Before mixing chamber B (1-4), it is located at lye inlet tube (1-6) in the lye bleeding holes (1-6) of miscella oil inlet pipe (1-1) section
The lye mixed once of exudation, after entering mixing chamber B (1-4), and from the mixed liquor bleeding holes (1-5) of mixing chamber B (1-4)
Exudation, when exudation, secondary mixing can be mixed more uniformly by mixing twice.
The tank body A (1) is equipped with mixed liquor liquid outlet (1-7), and miscella and lye are after mixing from the mixed liquor
Liquid outlet (1-7) is discharged, and by heating devices heat, is reacted in delay reaction unit (20) later.
External are cased with of mixing chamber B (1-4) is equipped at least one set mixing chamber A (1-3), the surface of shell of mixing chamber A (1-3)
Equipped with mixed liquor bleeding holes (1-5), one layer of mixing chamber A (1-3) is equipped with mixing chamber B (1-4) is external, can be increased primary mixed
It closes, that is, when mixed liquor is oozed out from mixing chamber A (1-3) to tank body A (1), mixed again.
The mixing chamber A (1-3) can also be equipped with it is multigroup, the group number being equipped with is more, then what is mixed is about uniform, mixing chamber B
(1-4) is located at innermost layer, and multigroup mixing chamber A (1-3) is arranged successively, the oily alkali mixing liquid being discharged from tank body A (1), it is necessary to from
After mixed liquor bleeding holes (1-5) exudation of mixing chamber A (1-3) and mixing chamber B (1-4), it could be discharged from outlet.
In actual use：Miscella inputs mixing chamber by miscella oil inlet pipe (1-1), and lye passes through lye alkali inlet tube
(1-6) enters miscella oil inlet pipe (1-1), and under miscella mobilization, lye is inhaled from the interior negative pressure of lye alkali inlet tube (1-6)
Go out, tentatively mixed, enter mixing chamber later, since mixing chamber surface is equipped with mixed liquor bleeding holes (1-5), can mix again
It closes, realizes that oily alkali is sufficiently mixed, the oily alkali being finally discharged from tank body A (1) mixed liquor liquid outlet (1-7) can reach fully mixed
It closes.
This oil alkali static mixing device is in actual use, it is only necessary to carry out liquid using miscella oil feed pump and lye pump
Conveying, without being additionally provided power, not only reduces power consumption, and avoid easy when mixing when two kinds of liquid are mixed
The volatilization for firing explosive solvent, eliminates safe hidden trouble, and improves production safety.
This oil alkali static mixing device is not only simple in structure, and mixing efficiency is high, while can also be energy saving, is not pacified
Full hidden danger is realized when oily alkali mixes and is achieved many things at one stroke.
Embodiment 2：Present embodiment discloses a kind of mixed cotton seed oil refining methods, it is characterised in that：Including at least gleditsia sinensis
Separating step, gleditsia sinensis separating step are to detach the liquid obtained after mixed cotton seed oil alkali refining, and gleditsia sinensis separating step uses
Gleditsia sinensis separator carries out the separation of soap and oil, collects oil and gleditsia sinensis after separation respectively.
The gleditsia sinensis separator includes tank body B (3), and the tank body B (3) is equipped with oil export (3-5), row's gleditsia sinensis pipe
(3-8) and material inlet (3-3), the oil export (3-5) are located at the top of (3) tank body B, and row's gleditsia sinensis pipe (3-8) is located at tank body B
(3) lower part is equipped at least one set of soap oil separator disk (3-4), material inlet between oil export (3-5) and row's gleditsia sinensis pipe (3-8)
(3-3) is connect with gleditsia sinensis separator disk (3-4), and the liquid of tank body B (3) is entered by material inlet (3-3), can be detached in gleditsia sinensis
Disk (3-4) carries out soap oil separation, and oil is discharged from oil export (3-5) and collects, and soap is precipitated to row's gleditsia sinensis pipe (3-8), later to gleditsia sinensis
It is collected.
The soap oil separator disk (3-4), including separator disk disk body (3-45), the separator disk disk body (3-45) is in umbrella,
Its surface is equipped with fold, i.e. fold A (3-42) and fold B (3-43), fold A (3-42) roll over downwards, and fold B (3-43) is upward
Folding, fold A (3-42) and fold B (3-43) are arranged alternately, and the fold A (3-42) and fold B (3-43) are linked up disk body
The edge (3-45) constitutes undaform, and the axle center of the separator disk disk body (3-45) is equipped with materail tube (3-48), the materail tube (3-
48) at least one end is open end, and open end is feed inlet (3-41), the described feed inlet (3-41) and material inlet (3-3)
Connection, materail tube (3-48) tube surfaces are equipped with bleed opening (3-47), and the bleed opening (3-47) is located at separator disk disk body
In the umbrella that (3-45) is covered, and close to umbrella point position.
The soap oil separator disk in actual use, can unpowered separation gleditsia sinensis and oil, no security risk, energy-saving and emission-reduction.
It refer to the lower section of separator disk disk body (3-45) in the umbrella that the separator disk disk body (3-45) is covered.
In actual use：Soap oil mixed liquor enters materail tube (3-48) by material inlet (3-3), and from materail tube (3-
48) bleed opening (3-47) discharge of surface setting, in the range of being covered into disk body (3-45) lower section, the gleditsia sinensis separator disk
(3-4) can be equipped with one group, can also be equipped with group.
The disk body is center height, and disk body edge is low, and bleed opening (3-47) is positioned close to the position of umbrella point, that is, oozes out
The height of mouth is higher, and disk body edge is relatively low, the separated obtained oil and gleditsia sinensis of soap oil mixed liquor, and oil is lighter, and gleditsia sinensis is heavier, compared with
To floating, heavier gleditsia sinensis precipitates downwards light oil.
If be provided only with one group of gleditsia sinensis separator disk, the gleditsia sinensis of bleed opening (3-47) exudation precipitates directly down, and oil is necessary
Along disk body (3-45), finally from the edge disk body (3-45), disengaging could be floated upwards, due to fold A (3-42) and fold B (3-
43) it is arranged alternately, i.e. a fold A (3-42), a fold B (3-43), therefore, lighter oil can be floating to fold B (3-43)
It is dynamic, and the region that finally disengaging disk body (3-45) is covered at fold B (3-43)；
If being equipped with multigroup separator disk, the liquid of bleed opening (3-47) exudation moves downward between two separate disk, compared with
The gleditsia sinensis of weight is precipitated to upper surface fold A (3-42) of lower layer, and disk body (3-45) is finally slid out at fold A (3-42),
And precipitated to tank body B (3) lower part, and lighter oil then floats to the lower surface fold B (3-43) on upper layer, and finally from fold B
It is detached from disk body (3-45) at (3-43) and floats up, is finally discharged and collects from oil export (3-5).
Above-mentioned fold A (3-42) and fold B (3-43) are V-type or arc.
It can be very good to carry out gleditsia sinensis and oil by the fold A (3-42) and fold B (3-43) that roll over and roll over downwards upwards
It is oriented to shunting, can be achieved with detaching for the first time before being detached from disk body (3-45), never flowed with route, avoid the secondary of soap oil
Mixing, while fold A (3-42) and fold B (3-43) they are to be arranged alternately, and it is corresponding in same vertical direction, i.e., it is same vertical
All it is fold A (3-42) on straight line or is all fold B (3-43), oil floats up to is encountered when last layer disk body or oil, soap
Encountered when next layer of disk body or soap is sunk to, therefore, gleditsia sinensis sinking route and oily floating route are in different vertical lines
On, in actual use, the soap and oil detached is not in secondary mixing, and whole separation effect is good, and separation rate is higher.
And it is the unpowered type separation taken in soap oil separation process, need not only uses electric energy, save energy consumption,
And when detaching, the secondary contact of soap oil can be avoided, improves separative efficiency.
As an improvement, being equipped with baffle (3-46) at bleed opening (3-47), the liquid that bleed opening (3-47) comes out is flushed to baffle
It on (3-46), can prevent from being vortexed, the liquid that bleed opening (3-47) comes out is enable slowly to flow.
Annularly, i.e., baffle (3-46) is the ring-type being set on the outside of materail tube (3-48) to the baffle (3-46).
Gleditsia sinensis by separation is precipitated to the lower part of (3) tank body B, that is, the row's of being deposited to gleditsia sinensis pipe (3-8) is inner, row's gleditsia sinensis
It manages and is equipped with drawing liquid pump in (3-8), can will arrange the gleditsia sinensis in gleditsia sinensis pipe (3-8) and be discharged.
The junction of the tank body B (3) and row's gleditsia sinensis pipe (3-8) is tapered, i.e. the ends tank body B (3) are thicker, arranges gleditsia sinensis pipe
(3-8) is relatively thin, is connected the two by bullet, and gleditsia sinensis is precipitated in the conical region, enters row's gleditsia sinensis pipe (3-8) later.
Row's gleditsia sinensis pipe (3-8) is equipped with gleditsia sinensis accumulated amount controller, and the gleditsia sinensis accumulated amount controller includes control device
(3-6) and at least one set of light sensitive component, the light sensitive component include light-emitting device (3-1) and photosensitive device (3-7)；The drawing liquid
Motor is connected at pump；The control device (3-6) is electrically connected between the light sensitive component and the motor, i.e. control device
(3-6) constitutes control loop with the light sensitive component and the motor, and the photosensitive device (3-7) in the light sensitive component can incite somebody to action
Photoreceptor signal feeds back to control device (3-6) to control electric motor starting or stopping, and then controls drawing liquid pump and be turned on and off.
Row's gleditsia sinensis pipe (3-8) is in vertical tubulose, and the light sensitive component is arranged on the madial wall of the column structure,
And light-emitting device (3-1) in the light sensitive component and the photosensitive device (3-7) are in the same horizontal position.
The madial wall of the column structure is equipped with casing, and the top of the tube body (3-2) of the casing is transparent material or sets
There are through-hole, the light-emitting device (3-1) and/or the photosensitive device (3-7) to be fixed in the casing.
As an improvement, the gleditsia sinensis accumulated amount controller includes multigroup photosensitive element, and multigroup light sensitive component is in Vertical Square
It is mutually juxtaposed upwards, and motor is variable-frequency motor.
Photoreceptor signal can be fed back to control device (3-6) to control by the photosensitive device (3-7) in the light sensitive component
Electric motor starting or stopping, and then control drawing liquid pump and be turned on and off, specially：Light-emitting device is perceived in photosensitive device (3-7)
When the light that (3-1) is sent out, generates a trigger signal and give control device (3-6), control device (3-6) is according to the trigger signal
Start motor rotation, and then controls drawing liquid pump and open；The light that light-emitting device (3-1) is sent out is not perceived in photosensitive device (3-7)
When line, generates an interrupt signal and control device (3-6), control device (3-6) is given to stop motor according to the interrupt signal and rotate,
And then it controls drawing liquid pump and closes.
The gleditsia sinensis separator in actual use, can realize unpowered separation gleditsia sinensis and oil, only in material inlet (3-
3) and row's gleditsia sinensis pipe (3-8) is equipped with pump, you can completes whole device operation, centre separation is not necessarily to extra power completely, energy saving
While emission reduction, and without security risk, and leakage is not will produce.
Embodiment 3：Present embodiment discloses a kind of mixed cotton seed oil refining methods, it is characterised in that：Including at least gleditsia sinensis
Precipitation step, gleditsia sinensis precipitation step are the progress carrying out precipitation treatment of body containing soap lye for obtaining gleditsia sinensis separating step, and to precipitation step
Solvent recycled, the precipitation step carries out precipitation, and recycling design and gleditsia sinensis using gleditsia sinensis exsolution apparatus.
The gleditsia sinensis exsolution apparatus includes tank body C (4), and being equipped with solvent vapo(u)r at the top of the tank body C (4) exports (4-4), bottom
Portion is equipped with gleditsia sinensis discharge pipe (4-6), and the tank body C (4) is equipped with heating and mixing device,
The heating and mixing device includes：Containing molten gleditsia sinensis inlet tube (4-2), steam inlet (4-1) and outer cover (4-3), institute
It states outer cover (4-3) and is set in the heating room (4-9) for forming strip on the outside of tank body C (4), the tank body C at heating room (4-9)
(4) surface is equipped with spray-hole (4-8), described to be connected to heating room (4-9) containing molten gleditsia sinensis inlet tube (4-2), the steam inlet
(4-1) is connected to containing molten gleditsia sinensis inlet tube (4-2), i.e., steam can be entered by steam inlet (4-1) and contain molten gleditsia sinensis inlet tube
It in (4-2), and is mixed, and is heated containing in molten gleditsia sinensis inlet tube (4-21) with containing the liquid in molten gleditsia sinensis inlet tube (4-2)
Liquid, and from spray-hole (4-8) enter tank body C (4) inner cavity.
As an improvement, the liquid outlet height of the gleditsia sinensis discharge pipe (4-6) is higher than the liquid level in tank body C (4).
In actual use：Enter tank body C by containing molten gleditsia sinensis inlet tube (4-2) by the isolated molten gleditsia sinensis that contains of gleditsia sinensis
(4), described containing steam inlet (4-1) is connected on molten gleditsia sinensis inlet tube (4-2), steam, which enters, contains molten gleditsia sinensis inlet tube (4-2)
Mixed afterwards with containing molten gleditsia sinensis, and molten gleditsia sinensis liquid will be contained and heated, at this point, the solvent contained in gleditsia sinensis can be gasified, from
When spray-hole (4-8) sprays, solvent vapo(u)r realizes that solvent is collected from solvent vapo(u)r outlet (4-4) discharge, and gleditsia sinensis or liquid
Body retains in tank body C (4) lower part, since the liquid outlet of gleditsia sinensis discharge pipe (4-6) is higher than the liquid levels in tank body C (4), only
Have when the liquid in tank body C (4) is higher than the liquid outlet of gleditsia sinensis discharge pipe (4-6), gleditsia sinensis can be just discharged, is realized unpowered molten
Agent seperator gleditsia sinensis is collected.
As an improvement, steam inlet (4-1) and containing the molten gleditsia sinensis inlet tube junction (4-2) with heat room (4-9) between
At least one set of barrier piece (4-7) is equipped in tube body containing molten gleditsia sinensis inlet tube (4-2).
In actual use：Containing barrier piece (4-7) is equipped in molten gleditsia sinensis inlet tube (4-2), can adequately make steam with
The mixing of liquid, it is more thorough to being heated containing the solvent in molten gleditsia sinensis liquid, improve the rate of recovery of solvent.
As an improvement, the corresponding outer cover (4-3) of spray-hole (4-8) is equipped with adjusting bolt (4-5), by screwing the adjusting
Bolt (4-5) can adjust the size of spray-hole (4-8), i.e. the end of adjusting bolt (4-5) is tapered, and can be fastened on injection
At hole (4-8), and spray-hole (4-8) can be blocked.
In actual use：Spray-hole (4-8) size can be adjusted, it is easy to use, it is adaptable.
Embodiment 4：With reference to the structural schematic diagram that Fig. 2 is the embodiment of the present invention 4, present embodiment discloses a kind of oily alkali is static
Mixing arrangement, it is characterised in that：Including tank body A (1), miscella oil inlet pipe (1-1), lye alkali inlet tube (1-6) and mixing chamber B
(1-4), mixing chamber B (1-4) are located in tank body A (1), and the surface of shell of the mixing chamber B (1-4) is equipped with mixed liquor bleeding holes
(1-5), mixing chamber inner cavity and (1) inner cavities tank body A are connected to by mixed liquor bleeding holes (1-5), the miscella oil inlet pipe (1-1)
Outlet end be placed in mixing chamber intracavitary, at least one section of lye alkali inlet tube (1-6) is placed in miscella oil inlet pipe (1-1), and lye
The part that alkali inlet tube (1-6) is placed in miscella oil inlet pipe (1-1) is equipped with lye bleeding holes (1-2).
When oily alkali mixing, miscella enters mixing chamber B (1-4) by pump, by miscella oil inlet pipe (1-1), is entering
Before mixing chamber B (1-4), it is located at lye inlet tube (1-6) in the lye bleeding holes (1-6) of miscella oil inlet pipe (1-1) section
The lye mixed once of exudation, after entering mixing chamber B (1-4), and from the mixed liquor bleeding holes (1-5) of mixing chamber B (1-4)
Exudation, when exudation, secondary mixing can be mixed more uniformly by mixing twice.
The tank body A (1) is equipped with mixed liquor liquid outlet (1-7), and miscella and lye are after mixing from the mixed liquor
Liquid outlet (1-7) is discharged, and by heating devices heat, is reacted in delay reaction unit (20) later.
External are cased with of mixing chamber B (1-4) is equipped at least one set mixing chamber A (1-3), the surface of shell of mixing chamber A (1-3)
Equipped with mixed liquor bleeding holes (1-5), one layer of mixing chamber A (1-3) is equipped with mixing chamber B (1-4) is external, can be increased primary mixed
It closes, that is, when mixed liquor is oozed out from mixing chamber A (1-3) to tank body A (1), mixed again.
The mixing chamber A (1-3) can also be equipped with it is multigroup, the group number being equipped with is more, then what is mixed is about uniform, mixing chamber B
(1-4) is located at innermost layer, and multigroup mixing chamber A (1-3) is arranged successively, the oily alkali mixing liquid being discharged from tank body A (1), it is necessary to from
After mixed liquor bleeding holes (1-5) exudation of mixing chamber A (1-3) and mixing chamber B (1-4), it could be discharged from outlet.
In actual use：Miscella inputs mixing chamber by miscella oil inlet pipe (1-1), and lye passes through lye alkali inlet tube
(1-6) enters miscella oil inlet pipe (1-1), and under miscella mobilization, lye is inhaled from the interior negative pressure of lye alkali inlet tube (1-6)
Go out, tentatively mixed, enter mixing chamber later, since mixing chamber surface is equipped with mixed liquor bleeding holes (1-5), can mix again
It closes, realizes that oily alkali is sufficiently mixed, the oily alkali being finally discharged from tank body A (1) mixed liquor liquid outlet (1-7) can reach fully mixed
It closes.
This oil alkali static mixing device is in actual use, it is only necessary to carry out liquid using miscella oil feed pump and lye pump
Conveying, without being additionally provided power, not only reduces power consumption, and avoid easy when mixing when two kinds of liquid are mixed
The volatilization for firing explosive solvent, eliminates safe hidden trouble, and improves production safety.
This oil alkali static mixing device is not only simple in structure, and mixing efficiency is high, while can also be energy saving, is not pacified
Full hidden danger is realized when oily alkali mixes and is achieved many things at one stroke.
Embodiment 5：With reference to the structural schematic diagram that Fig. 3~6 are the embodiment of the present invention 5, present embodiment discloses a kind of energy is quiet
State detaches soap oil gleditsia sinensis separator, it is characterised in that：Including tank body B (3), the tank body B (3) be equipped with oil export (3-5),
Gleditsia sinensis pipe (3-8) and material inlet (3-3) are arranged, the oil export (3-5) is located at the top of (3) tank body B, row's gleditsia sinensis pipe (3-8)
It is located at the lower part of (3) tank body B, at least one set of soap oil separator disk (3-4) is equipped between oil export (3-5) and row's gleditsia sinensis pipe (3-8),
Material inlet (3-3) is connect with gleditsia sinensis separator disk (3-4), and the liquid of tank body B (3), Neng Gou are entered by material inlet (3-3)
Gleditsia sinensis separator disk (3-4) carries out soap oil separation, and oil is discharged from oil export (3-5) and collects, and soap is precipitated to row's gleditsia sinensis pipe (3-8), it
Gleditsia sinensis is collected afterwards.
The soap oil separator disk (3-4), including separator disk disk body (3-45), the separator disk disk body (3-45) is in umbrella,
Its surface is equipped with fold, i.e. fold A (3-42) and fold B (3-43), fold A (3-42) roll over downwards, and fold B (3-43) is upward
Folding, fold A (3-42) and fold B (3-43) are arranged alternately, and the fold A (3-42) and fold B (3-43) are linked up disk body
The edge (3-45) constitutes undaform, and the axle center of the separator disk disk body (3-45) is equipped with materail tube (3-48), the materail tube (3-
48) at least one end is open end, and open end is feed inlet (3-41), the described feed inlet (3-41) and material inlet (3-3)
Connection, materail tube (3-48) tube surfaces are equipped with bleed opening (3-47), and the bleed opening (3-47) is located at separator disk disk body
In the umbrella that (3-45) is covered, and close to umbrella point position.
The soap oil separator disk in actual use, can unpowered separation gleditsia sinensis and oil, no security risk, energy-saving and emission-reduction.
It refer to the lower section of separator disk disk body (3-45) in the umbrella that the separator disk disk body (3-45) is covered.
In actual use：Soap oil mixed liquor enters materail tube (3-48) by material inlet (3-3), and from materail tube (3-
48) bleed opening (3-47) discharge of surface setting, in the range of being covered into disk body (3-45) lower section, the gleditsia sinensis separator disk
(3-4) can be equipped with one group, can also be equipped with group.
The disk body is center height, and disk body edge is low, and bleed opening (3-47) is positioned close to the position of umbrella point, that is, oozes out
The height of mouth is higher, and disk body edge is relatively low, the separated obtained oil and gleditsia sinensis of soap oil mixed liquor, and oil is lighter, and gleditsia sinensis is heavier, compared with
To floating, heavier gleditsia sinensis precipitates downwards light oil.
If be provided only with one group of gleditsia sinensis separator disk, the gleditsia sinensis of bleed opening (3-47) exudation precipitates directly down, and oil is necessary
Along disk body (3-45), finally from the edge disk body (3-45), disengaging could be floated upwards, due to fold A (3-42) and fold B (3-
43) it is arranged alternately, i.e. a fold A (3-42), a fold B (3-43), therefore, lighter oil can be floating to fold B (3-43)
It is dynamic, and the region that finally disengaging disk body (3-45) is covered at fold B (3-43)；
If being equipped with multigroup separator disk, the liquid of bleed opening (3-47) exudation moves downward between two separate disk, compared with
The gleditsia sinensis of weight is precipitated to upper surface fold A (3-42) of lower layer, and disk body (3-45) is finally slid out at fold A (3-42),
And precipitated to tank body B (3) lower part, and lighter oil then floats to the lower surface fold B (3-43) on upper layer, and finally from fold B
It is detached from disk body (3-45) at (3-43) and floats up, is finally discharged and collects from oil export (3-5).
Above-mentioned fold A (3-42) and fold B (3-43) are V-type or arc.
It can be very good to carry out gleditsia sinensis and oil by the fold A (3-42) and fold B (3-43) that roll over and roll over downwards upwards
It is oriented to shunting, can be achieved with detaching for the first time before being detached from disk body (3-45), never flowed with route, avoid the secondary of soap oil
Mixing, while fold A (3-42) and fold B (3-43) they are to be arranged alternately, and it is corresponding in same vertical direction, i.e., it is same vertical
All it is fold A (3-42) on straight line or is all fold B (3-43), oil floats up to is encountered when last layer disk body or oil, soap
Encountered when next layer of disk body or soap is sunk to, therefore, gleditsia sinensis sinking route and oily floating route are in different vertical lines
On, in actual use, the soap and oil detached is not in secondary mixing, and whole separation effect is good, and separation rate is higher.
And it is the unpowered type separation taken in soap oil separation process, need not only uses electric energy, save energy consumption,
And when detaching, the secondary contact of soap oil can be avoided, improves separative efficiency.
As an improvement, being equipped with baffle (3-46) at bleed opening (3-47), the liquid that bleed opening (3-47) comes out is flushed to baffle
It on (3-46), can prevent from being vortexed, the liquid that bleed opening (3-47) comes out is enable slowly to flow.
Annularly, i.e., baffle (3-46) is the ring-type being set on the outside of materail tube (3-48) to the baffle (3-46).
Gleditsia sinensis by separation is precipitated to the lower part of (3) tank body B, that is, the row's of being deposited to gleditsia sinensis pipe (3-8) is inner, row's gleditsia sinensis
It manages and is equipped with drawing liquid pump in (3-8), can will arrange the gleditsia sinensis in gleditsia sinensis pipe (3-8) and be discharged.
The junction of the tank body B (3) and row's gleditsia sinensis pipe (3-8) is tapered, i.e. the ends tank body B (3) are thicker, arranges gleditsia sinensis pipe
(3-8) is relatively thin, is connected the two by bullet, and gleditsia sinensis is precipitated in the conical region, enters row's gleditsia sinensis pipe (3-8) later.
Embodiment 6：With reference to the structural schematic diagram that Fig. 4~6 are the embodiment of the present invention 6, described in one kind
Soap oil separator disk (3-4), including separator disk disk body (3-45), the separator disk disk body (3-45) is in umbrella, and surface is equipped with pleat
Wrinkle, i.e. fold A (3-42) and fold B (3-43), fold A (3-42) roll over downwards, and fold B (3-43) rolls over upwards, fold A (3-42)
It is arranged alternately with fold B (3-43), the fold A (3-42) and fold B (3-43) are linked up and constituted the edge disk body (3-45)
The axle center of undaform, the separator disk disk body (3-45) is equipped with materail tube (3-48), at least one end of the materail tube (3-48)
For open end, open end is feed inlet (3-41), and the described feed inlet (3-41) is connect with material inlet (3-3), the material
It manages (3-48) tube surfaces and is equipped with bleed opening (3-47), the bleed opening (3-47) is located at what separator disk disk body (3-45) was covered
In umbrella, and close to umbrella point position.
The soap oil separator disk in actual use, can unpowered separation gleditsia sinensis and oil, no security risk, energy-saving and emission-reduction.
It refer to the lower section of separator disk disk body (3-45) in the umbrella that the separator disk disk body (3-45) is covered.
In actual use：Soap oil mixed liquor enters materail tube (3-48) by material inlet (3-3), and from materail tube (3-
48) bleed opening (3-47) discharge of surface setting, in the range of being covered into disk body (3-45) lower section, the gleditsia sinensis separator disk
(3-4) can be equipped with one group, can also be equipped with group.
The disk body is center height, and disk body edge is low, and bleed opening (3-47) is positioned close to the position of umbrella point, that is, oozes out
The height of mouth is higher, and disk body edge is relatively low, the separated obtained oil and gleditsia sinensis of soap oil mixed liquor, and oil is lighter, and gleditsia sinensis is heavier, compared with
To floating, heavier gleditsia sinensis precipitates downwards light oil.
If be provided only with one group of gleditsia sinensis separator disk, the gleditsia sinensis of bleed opening (3-47) exudation precipitates directly down, and oil is necessary
Along disk body (3-45), finally from the edge disk body (3-45), disengaging could be floated upwards, due to fold A (3-42) and fold B (3-
43) it is arranged alternately, i.e. a fold A (3-42), a fold B (3-43), therefore, lighter oil can be floating to fold B (3-43)
It is dynamic, and the region that finally disengaging disk body (3-45) is covered at fold B (3-43)；
If being equipped with multigroup separator disk, the liquid of bleed opening (3-47) exudation moves downward between two separate disk, compared with
The gleditsia sinensis of weight is precipitated to upper surface fold A (3-42) of lower layer, and disk body (3-45) is finally slid out at fold A (3-42),
And precipitated to tank body B (3) lower part, and lighter oil then floats to the lower surface fold B (3-43) on upper layer, and finally from fold B
It is detached from disk body (3-45) at (3-43) and floats up, is finally discharged and collects from oil export (3-5).
Embodiment 7：With reference to the structural schematic diagram that Fig. 3 and Fig. 7 is the embodiment of the present invention 7, present embodiment discloses a kind of energy
The gleditsia sinensis knockout tower of automatic row's gleditsia sinensis, including tank body B3, the tank body B3 are in barreled structure, which is provided with oil export 3-5, soap oil
The inner cavity in separator 3, the oil export 3-5 is arranged in separator disk 3-4 and row gleditsia sinensis pipe 3-8, the soap oil separator disk 3-4
It is arranged on the top of separator 3, row's gleditsia sinensis pipe 3-8 is disposed relative to the lower part of the separator 3 of oil export 3-5,
The preferably described row's gleditsia sinensis pipe 3-8 of the present embodiment is in the form of a column structure, and gleditsia sinensis accumulated amount controller and drawing liquid are equipped on the column structure
Pump, the gleditsia sinensis accumulated amount controller include control device 3-6 and at least one set of light sensitive component, and the light sensitive component includes the dress that shines
3-1 and photosensitive device 3-7 are set, and light sensitive component is arranged in the inside of the column structure, as needed, the control device 3-
6 may also be arranged on the inside of the column structure, and the preferred control device 3-6 of the present embodiment is arranged in the outside of column structure, such as
This, facilitates maintenance conditions；The drawing liquid pump is arranged in the end of row's gleditsia sinensis pipe 3-8, and is connected with motor at the drawing liquid pump,
The control device 3-6 is electrically connected between the light sensitive component and the motor namely control device 3-6 and the light sensation member
Part and the motor constitute a control loop, and photoreceptor signal can be fed back to control by the photosensitive device 3-7 in the light sensitive component
Device 3-6 processed controls drawing liquid pump and is turned on and off to control electric motor starting or stopping, specifically, feeling in photosensitive device 3-7
When knowing the light that light-emitting device 3-1 is sent out, generates a trigger signal and control device 3-6, control device 3-6 is given to be touched according to this
It signals to start motor rotation, and then controls drawing liquid pump and open；Do not perceive what light-emitting device 3-1 was sent out in photosensitive device 3-7
When light, generates an interrupt signal and control device 3-6, control device 3-6 is given to stop motor rotation according to the interrupt signal, into
And drawing liquid pump closing is controlled, in the present embodiment, the light-emitting device 3-1 includes illuminator, and the photosensitive device 3-7 includes photosensitive
Element.
Preferably, it is equipped with four groups of light sensitive components, every group of sense side by side in vertical direction of the present embodiment in row gleditsia sinensis pipe 3-8
Optical element is arranged on the madial wall of row's gleditsia sinensis pipe 3-8 column structures, and the light-emitting device 3-1 in every group of light sensitive component
It is in the same horizontal position with the photosensitive device 3-7, it can be to the gleditsia sinensis amount in row gleditsia sinensis pipe 3-8 using four groups of light sensitive components
It is measured in real time, that is, can detect that gleditsia sinensis accumulates in height or accumulation in row's gleditsia sinensis pipe 3-8 by four groups of light sensitive components
Amount, and then the gleditsia sinensis in the row of accumulating in gleditsia sinensis pipe 3-8 can be discharged in time by starting drawing liquid pump.
Preferably, in the present embodiment, its physical life is reduced in order to avoid light sensitive component is immersed in gleditsia sinensis for a long time
With increase detection error, preferably casing, the tube body 3-2 of the casing are equipped on the madial wall of the column structure of row gleditsia sinensis pipe 3-8
Top be transparent material, the light-emitting device 3-1 and/or the photosensitive device 3-7 can be fixed in the casing；Certainly, root
According to needs, multiple through-holes that can be by divergence of beam to outside are may also set up at the top of casing pipe 3-2.
In the present embodiment, when light-emitting device 3-1 is arranged in the casing, it can be realized using the casing and model is scattered to light
The control enclosed, in this way, detection error can be reduced.
Preferably, the separator disk disk body 3-45 of the soap oil separator disk 3-4 is in umbrella-shaped structure.
In use, by soap oil separator disk 3-4 the gleditsia sinensis heavier relative to oil is entered in row's gleditsia sinensis pipe 3-8, due to
It is equipped with light sensitive component in row's gleditsia sinensis pipe 3-8, therefore, when gleditsia sinensis accumulation is a certain amount of, light sensitive component can be flooded so that light
Photosensitive device 3-7 in sensing unit can not perceive light caused by light-emitting device 3-1, be touched at this point, light sensitive component generates one
It signals and is sent to control device 3-6, control device 3-6 starts motor rotation after receiving the trigger signal, and then drives and take out
Liquid pump works, and in time pumps out gleditsia sinensis in row gleditsia sinensis pipe 3-8；With the discharge of gleditsia sinensis burden, photosensitive element is exposed,
At this point, photosensitive device 3-7 can perceive caused by light-emitting device 3-1 bright again, while an interrupt signal is generated and will be in this
Break signal is sent to control device 3-6, and control device 3-6 controls motor stalls after receiving the interrupt signal, and then controls
Drawing liquid pump is stopped.
Further, in the present embodiment, excellent in order to adjust the working condition of drawing liquid pump according to the burden of gleditsia sinensis
It is that variable-frequency motor then starts variable-frequency motor in use, when light sensitive component detects that the burden of gleditsia sinensis is more to select the motor
High gear so that drawing liquid pump can quickly will row gleditsia sinensis pipe 3-8 in gleditsia sinensis pump out；When light sensitive component detects the product of gleditsia sinensis
When storage is less, then start the low gear of variable-frequency motor, is pumped out the gleditsia sinensis arranged in gleditsia sinensis pipe 3-8 by drawing liquid pump, specifically
, it selects and is equipped with four groups of light sensitive components in the vertical direction in the row of being located at gleditsia sinensis pipe 3-8 side by side, when gleditsia sinensis floods the light sensation of the bottom
When element, trigger signal can not be generated, when gleditsia sinensis floods the light sensitive component of layer second from the bottom, low speed triggering letter can be generated at this time
Number give control device 3-6, control device 3-6 according to the low speed trigger signal control variable-frequency motor slow rotation, and then drive take out
Liquid pump at the uniform velocity works, when gleditsia sinensis flood layer light sensitive component third from the bottom or flood layer light sensitive component third from the bottom have certain time or
When flooding the light sensitive component of fourth from the last layer, high speed trigger signal can be generated at this time and gives control device 3-6, control device 3-6 roots
According to high speed trigger signal control variable-frequency motor block speed rotation, and then the work of drawing liquid pump block speed is driven, certainly, above is this implementation
A kind of preferred specific working mode of example, as needed, the also working frequency of replaceable variable-frequency motor.
Further, in the present embodiment, in order to preferably realize that soap oil detaches, it is preferably provided with multigroup soap oil separator disk 3-
4, multigroup group of soap oil separator disk 3-4 are fixed on the inner cavity of the tank body B3 by materail tube 3-48, and the materail tube 3-48 is in " L "
Shape structure, and the tank body B3 is extended as material inlet 3-3 in one free end, is fixed with one end of soap oil separator disk 3-4
Equipped with bleed opening 3-47.
Embodiment 8：With reference to the structural schematic diagram that Fig. 8~10 are the embodiment of the present invention 8, present embodiment discloses a kind of gleditsia sinensis
Exsolution apparatus, it is characterised in that：Including tank body C (4), tank body C (4) top is equipped with solvent vapo(u)r and exports (4-4), and bottom is set
There are gleditsia sinensis discharge pipe (4-6), the tank body C (4) to be equipped with heating and mixing device,
The heating and mixing device includes：Containing molten gleditsia sinensis inlet tube (4-2), steam inlet (4-1) and outer cover (4-3), institute
It states outer cover (4-3) and is set in the heating room (4-9) for forming strip on the outside of tank body C (4), the tank body C at heating room (4-9)
(4) surface is equipped with spray-hole (4-8), described to be connected to heating room (4-9) containing molten gleditsia sinensis inlet tube (4-2), the steam inlet
(4-1) is connected to containing molten gleditsia sinensis inlet tube (4-2), i.e., steam can be entered by steam inlet (4-1) and contain molten gleditsia sinensis inlet tube
It in (4-2), and is mixed, and is heated containing in molten gleditsia sinensis inlet tube (4-21) with containing the liquid in molten gleditsia sinensis inlet tube (4-2)
Liquid, and from spray-hole (4-8) enter tank body C (4) inner cavity.
As an improvement, the liquid outlet height of the gleditsia sinensis discharge pipe (4-6) is higher than the liquid level in tank body C (4).
In actual use：Enter tank body C by containing molten gleditsia sinensis inlet tube (4-2) by the isolated molten gleditsia sinensis that contains of gleditsia sinensis
(4), described containing steam inlet (4-1) is connected on molten gleditsia sinensis inlet tube (4-2), steam, which enters, contains molten gleditsia sinensis inlet tube (4-2)
Mixed afterwards with containing molten gleditsia sinensis, and molten gleditsia sinensis liquid will be contained and heated, at this point, the solvent contained in gleditsia sinensis can be gasified, from
When spray-hole (4-8) sprays, solvent vapo(u)r realizes that solvent is collected from solvent vapo(u)r outlet (4-4) discharge, and gleditsia sinensis or liquid
Body retains in tank body C (4) lower part, since the liquid outlet of gleditsia sinensis discharge pipe (4-6) is higher than the liquid levels in tank body C (4), only
Have when the liquid in tank body C (4) is higher than the liquid outlet of gleditsia sinensis discharge pipe (4-6), gleditsia sinensis can be just discharged, is realized unpowered molten
Agent seperator gleditsia sinensis is collected.
As an improvement, steam inlet (4-1) and containing the molten gleditsia sinensis inlet tube junction (4-2) with heat room (4-9) between
At least one set of barrier piece (4-7) is equipped in tube body containing molten gleditsia sinensis inlet tube (4-2).
In actual use：Containing barrier piece (4-7) is equipped in molten gleditsia sinensis inlet tube (4-2), can adequately make steam with
The mixing of liquid, it is more thorough to being heated containing the solvent in molten gleditsia sinensis liquid, improve the rate of recovery of solvent.
As an improvement, the corresponding outer cover (4-3) of spray-hole (4-8) is equipped with adjusting bolt (4-5), by screwing the adjusting
Bolt (4-5) can adjust the size of spray-hole (4-8), i.e. the end of adjusting bolt (4-5) is tapered, and can be fastened on injection
At hole (4-8), and spray-hole (4-8) can be blocked.
In actual use：Spray-hole (4-8) size can be adjusted, it is easy to use, it is adaptable.
The above content is combining, specific embodiment is made for the present invention to be further described, and it cannot be said that this hair
Bright specific implementation is confined to these explanations.For those of ordinary skill in the art to which the present invention belongs, it is not taking off
Under the premise of from present inventive concept, a number of simple deductions or replacements can also be made, all shall be regarded as belonging to the protection of the present invention
Range.
Claims (7)
1. a kind of gleditsia sinensis knockout tower of static separation soap oil, it is characterised in that：Including tank body B (3), the tank body B (3) is equipped with
Oil export (3-5), row's gleditsia sinensis pipe (3-8) and material inlet (3-3), the oil export (3-5) are located at the top of (3) tank body B, arrange
Gleditsia sinensis pipe (3-8) is located at the lower part of (3) tank body B, and at least one set of soap oil is equipped between oil export (3-5) and row's gleditsia sinensis pipe (3-8)
Separator disk (3-4), the soap oil separator disk (3-4) include separator disk disk body (3-45), and the separator disk disk body (3-45) is in umbrella
Shape, surface are equipped with fold, i.e. fold A (3-42) and fold B (3-43), fold A (3-42) folding downwards, fold B (3-43) to
Upper folding, fold A (3-42) and fold B (3-43) are arranged alternately, and the axle center of the separator disk disk body (3-45) is equipped with materail tube (3-
48), at least one end of the materail tube (3-48) is open end, and open end is feed inlet (3-41), the feed inlet (3-
41) it is connect with material inlet (3-3), materail tube (3-48) tube surfaces are equipped with bleed opening (3-47), the bleed opening (3-
47) it is located in the umbrella that separator disk disk body (3-45) is covered.
2. the gleditsia sinensis knockout tower of static separation soap oil as described in claim 1, it is characterised in that：It is equipped at bleed opening (3-47)
Baffle (3-46).
3. the gleditsia sinensis knockout tower of static separation soap oil as claimed in claim 2, it is characterised in that：The baffle (3-46) is in ring
Shape, i.e. baffle (3-46) are the ring-type being set on the outside of materail tube (3-48).
4. the gleditsia sinensis knockout tower of static separation soap oil as claimed in claim 1,2 or 3, it is characterised in that：Fold A (3-42) and
Fold B (3-43) is V-type or arc.
5. the gleditsia sinensis knockout tower of static separation soap oil as claimed in claim 1,2 or 3, it is characterised in that：Equipped with 2~10 groups of soaps
Oil separation disc (3-4).
6. a kind of mixed cotton seed oil refining method, it is characterised in that：Including at least gleditsia sinensis separating step, gleditsia sinensis separating step be by
The liquid obtained after alkali refining carries out the separation of soap and oil using gleditsia sinensis separator, collects oil and gleditsia sinensis after separation, the soap
Angle separator has used the oily alkali static mixing device as described in claims 1 to 3 to carry out oily alkali mixing.
7. mixed cotton seed oil refining method as claimed in claim 6, it is characterised in that：Also include gleditsia sinensis precipitation step, gleditsia sinensis
Precipitation is that the gleditsia sinensis that gleditsia sinensis separates and collects is pumped into gleditsia sinensis exsolution apparatus, carries out gleditsia sinensis carrying out precipitation treatment, recycling design and gleditsia sinensis.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810468843.2A CN108753450B (en) | 2018-05-16 | 2018-05-16 | Chinese honeylocust separation tower and method for preparing refined cottonseed oil from mixed cottonseed oil by using same |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810468843.2A CN108753450B (en) | 2018-05-16 | 2018-05-16 | Chinese honeylocust separation tower and method for preparing refined cottonseed oil from mixed cottonseed oil by using same |
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| CN108753450B CN108753450B (en) | 2023-08-22 |
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