CN108753052A - Aqueous imitative rose coating of one kind and preparation method thereof - Google Patents
Aqueous imitative rose coating of one kind and preparation method thereof Download PDFInfo
- Publication number
- CN108753052A CN108753052A CN201810316775.8A CN201810316775A CN108753052A CN 108753052 A CN108753052 A CN 108753052A CN 201810316775 A CN201810316775 A CN 201810316775A CN 108753052 A CN108753052 A CN 108753052A
- Authority
- CN
- China
- Prior art keywords
- rose
- sheet body
- aqueous
- coating
- parts
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D125/00—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by an aromatic carbocyclic ring; Coating compositions based on derivatives of such polymers
- C09D125/02—Homopolymers or copolymers of hydrocarbons
- C09D125/04—Homopolymers or copolymers of styrene
- C09D125/08—Copolymers of styrene
- C09D125/14—Copolymers of styrene with unsaturated esters
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/14—Paints containing biocides, e.g. fungicides, insecticides or pesticides
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/18—Fireproof paints including high temperature resistant paints
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/61—Additives non-macromolecular inorganic
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/63—Additives non-macromolecular organic
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/65—Additives macromolecular
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K2201/00—Specific properties of additives
- C08K2201/002—Physical properties
- C08K2201/003—Additives being defined by their diameter
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K2201/00—Specific properties of additives
- C08K2201/014—Additives containing two or more different additives of the same subgroup in C08K
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2201/00—Properties
- C08L2201/02—Flame or fire retardant/resistant
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2201/00—Properties
- C08L2201/08—Stabilised against heat, light or radiation or oxydation
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/02—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group
- C08L2205/025—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group containing two or more polymers of the same hierarchy C08L, and differing only in parameters such as density, comonomer content, molecular weight, structure
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
- C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
Abstract
A kind of aqueous imitative rose coating of disclosure of the invention and preparation method thereof, the aqueous imitative rose coating of one kind of the invention, including count in parts by weight following group are grouped as：150-350 parts of aqueous synthetic-resin emulsion, 10-25 parts of rose ethereal oil, 6% 80-150 parts of rose Protection glue; 500-700 parts of rose sheet body, 1-2.5 parts of cellulose, 30-70 parts of bentonite; 0.5-3 parts of pH adjusting agent; 3-7 parts of antifreezing agent, 2-5 parts of wetting agent, 2-5 parts of dispersant; 1-3 parts of fungicide; 0.5-4 parts of antifoaming agent, 1-5 parts of thickener, 5-100 parts of deionized water.The paint surface tension of the present invention is small, high surface activity, and defoaming power is strong, and chemical stabilization, no physiological activity is corrosion-free, safe.
Description
Technical field
The present invention relates to paint technology fields, and in particular to aqueous imitative rose coating of one kind and preparation method thereof.
Background technology
Rose (Rosarugosa) rose family rose, also known as dahurian rose flower, flower of hovering, assassin, punching rose.Rose
Have three outstanding persons in section))) rose, Chinese rose and rose are all rose in fact.In Chinese people be accustomed to flower diameter greatly,
The kind of Dan Sheng is known as Chinese rose, and the small referred to as rose to grow thickly can refine the title rose of essence.But they are referred to as in English
rose.The kind of formal registration at present, about 30000.Annual May opens rose in the natural environment, and China rose
November can be reached always from May.Chinese rose, rose are not only the difference in botany, spend rose available on the market at present
Mostly Chinese rose.The common kind of rose has red rose, Autumn Gold, purple rugose rose (Rosa rugosa var typica), rose white, black rose, green rose, Chinese red rose
With blue rose etc..Rose is planted extensively in the world, but is distributed in the Northern Hemisphere more, and rose also has more than 2000 years in China
Cultivation history originates in the north, there is plantation throughout the country at present, wherein with Shandong, Gansu, Beijing, Jiangsu, Henan, river
Based on the ground such as north, Sichuan, Liaoning, Heilungkiang, Taiwan, Shanxi, Xinjiang, Shaanxi, especially with Shandong Pingyin, the rose of Gansu misery
It is most notable.
Rose fragrant, there is antibacterial, anti-spasm, sterilize, promote the sexual maturity, purifying, is calm, mending body and other effects.It can prevent
Infectious disease, treatment skin adjust endocrine, promote human physiology and psychology activity.It can help for sleep, boost metabolism,
Cytothesis, blood circulation, can make health, beauty, and life is finer etc..The dining room that is the theme with rose, hotel, coffee
The young man's that the Room, KTV boxes, wedding room etc. are made widely known by more and more pursuit individual characteies pursues, and also there are many rose themes in market
The only similar smell of shape such as floor, wallpaper, tables and chairs unlike or rose scent the smells such as shower cream, shampoo, perfume
Similar profile unlike product.There is the product of the beautiful color of rose just seldom to see report, especially one again with Rose Essentielle
Money has the coating products that Rose Essentielle has red rose color again.The present inventor passes through in conjunction with market demand years of work experimental technology
A water paint product for having red rose color again with Rose Essentielle has been made in repetition test.The aqueous imitative rose coating
It uses rose ethereal oil, rose sheet body for main functional material, is aided with rose Protection glue, water, film forming matter, auxiliary agent is added
It is formed etc. refined, the color that has the characteristics that suffus an exquisite fragrance all around is true to nature.
Currently, lacking a kind of aqueous imitative rose coating and its preparation having rose bright-colored again with Rose Essentielle
Method.
Invention content
The purpose of the present invention is to provide a kind of aqueous imitative roses having rose bright-colored again with Rose Essentielle
Coating and preparation method thereof.
In order to achieve the above objectives, present invention employs following technical proposals：The aqueous imitative rose coating of one kind of the present invention,
Following group including counting in parts by weight is grouped as：
Further, the aqueous synthetic-resin emulsion is the common styrene-acrylic emulsion of coating industry；The rose
Essential oil is natural rose flower essential oil.
Further, the rose ethereal oil is the rose folk prescription essence of Guangzhou Sheng Yan Fine Chemical Co., Ltd production
Oil；The rose sheet body is that rose drying is crushed to sheet body, and the sheet body of the rose is 0.5-1mm roses
Sheet body, the sheet body of 1-2mm roses or the sheet body of 2-3mm roses；The bentonite is organically-modified sodium bentonite.
With excellent thickening and middle shearing density, rheological effect is good, and water conservation moisture retention is good.
Further, the wetting agent is the organic silicon polyether class surfactant of low molecular weight；The dispersion
Agent is polyether modified siloxane class high performance surface activating agent；The thickener be the common alkali soluble of coating industry rise class thickening
Agent；The mass ratio of the rose sheet body of the 0.5-1mm roses sheet body, 1-2mm roses sheet body and 2-3mm is 1：1-
1.5：1-1.5.
Further, the active ingredient of the rose sheet body Protection glue be aluminium-magnesium silicate, the mixture of lithium magnesium silicate,
The Protection glue produces for Guangdong Shi Naishi Industrial Co., Ltd.s；The 0.5-1mm roses sheet body, 1-2mm roses
The mass ratio of sheet body and 2-3mm rose sheet bodies is 1:1:2.
Further, the antifreezing agent is ethylene glycol；The antifoaming agent is organic silicon defoamer；Organic silicon defoamer
For the Taiwan Central Asia/wide spectrum antifoaming agent F111.Paint feature is that surface tension is small, high surface activity, and defoaming power is strong, defoams fast suds
Can be good, the fundamental property of bubbling system, diffusivity, good penetrability, chemical stabilization, no physiological activity, corrosion-free nothing are not influenced
Poison, no adverse side effect is not non-ignitable quick-fried, and safe, dosage is few, at low cost.Organic silicon defoamer and water and most organic matters
It is not miscible, most of frothing medias can be defoamed.Organic silicon defoamer has preferable thermal stability, can be at 5-150 DEG C
It is used in broad temperature range；Its chemical stability is preferable, difficult with other substance reactions, as long as configuration is appropriate, can acid, alkali,
It is used in salting liquid, lossless product quality.Organic silicon defoamer, with suds, broken big gun function, belongs to wide to all bubble systems
Compose antifoaming agent scope.Organic silicon defoamer is widely used in detergent, papermaking, paper pulp, sugaring, plating, chemical fertilizer, auxiliary agent, waste water
In the production processes such as processing.
Further, the organic silicon defoamer density is 0.88-0.94g/cm3, viscosity is in 300-800mPa.s
Organic silicon defoamer；The fungicide is the common wide-spectrum bactericide in market.
The preparation method of aqueous imitative rose coating of the present invention, includes the following steps：
(1) selection container prepares 3% bentonitic aqueous solution：Water is added in quantitative bentonite under 200-300r/min
In, mixing time be 5min to no powder particles, 1/10 cellulose is added, rotating speed is properly increased according to mill base state, stirring
Time is that 3min no longer changes to state, spare；
(2) container is selected, by mixing time in quantitative cellulose input water is 5min to molten at 200-300r/min
Liquid is added the pH adjusting agent activation hydrotropy of 1/10-1/3, rotating speed, mixing time is properly increased according to mill base state without powdered granule
For 5min to state not in variation until；
(3) selection container prepares 5% protection glue solution：Quantitative rose Protection glue is added under 200-300r/min
In water, mixing time is 5min to no powder particles, properly increases rotating speed according to mill base state, mixing time is 3min to state
No longer change, it is spare；
(4) cellulose solution dissolved, 3% bentonite solution and 5% protection glue solution are successively squeezed into Scattered Kettle
Middle mixing time is 2min, and remaining PH conditioning agents, aqueous synthetic-resin emulsion, rose anthosin is added under 600-900r/min
Oil, 6% rose Protection glue, rose sheet body, antifreezing agent, wetting agent, dispersant, fungicide, antifoaming agent, thickener and go from
Son, mixing time 10min；
(5) it is slowly added to the rose sheet body of the rose sheet body of 0.5-1mm, the rose sheet body of 1-2mm and 2-3mm,
Stirring to rose sheet body is uniformly dispersed；Stirring, which is maximum speed, must not be higher than 300r/min, and aqueous imitative rose coating is made.
Further, in step (1), the amount of coating will account for the 2/3-3/4 of vessel volume；Aqueous imitative rose coating
Form of construction work is with homochromy basecoat paint, specially spray gun bore 5mm, and pressure is 1.5-2 megapascal, is sprayed using right-angled intersection.
Further, in step (4), the preparation of rose sheet body：By fresh rose lobe 60 DEG C of drying in oven extremely
Water content 10-15% is sheared with slicer to the rose sheet body, the rose sheet body of 1-2mm and the rose of 2-3mm of 0.5-1mm
Rose sheet body is made in rare flower piece body.
Advantageous effect：The paint surface tension of the present invention is small, high surface activity, and defoaming power is strong, and it is good to defoam fast suds suppressing properties, no
The fundamental property of bubbling system is influenced, diffusivity, good penetrability, chemical stabilization, no physiological activity is corrosion-free nontoxic, invariably
Good side effect, non-ignitable not quick-fried, safe, dosage is few, at low cost.
Compared with prior art, the invention has the advantages that：(1) wetting agent used in has following features：Molecular weight is low,
More hydrophobic groups are in umbrella shape symmetrical structure, compared with traditional activated dose, soak, to permeate sex expression extremely excellent, efficient, are revolutions
The surfactant of new generation of property.Dynamic and static surface tension is extremely low, base containing polyether, and chemical property is inertia, is not involved in system
Chemical reaction, resistance to acid and alkali is good, and chemical property is stablized.
(2) it can effectively reduce the surface tension between solids and liquid, increase its spreading force.Wetting agent and dispersion
Agent is used cooperatively, and is reduced solid surface energy, is allowed the water to soak these color stuffing particles, is formed continuous phase in its surface of solids, is made
Solid powder is dispersed in water as stable suspension.
(3) organic silicon defoamer and water and most organic matters is not miscible, can be defoamed to most of frothing medias.It is organic
Silicon defoaming agent has preferable thermal stability, can be used in 5-150 DEG C of broad temperature range；Its chemical stability is preferable, difficult
It can be used in acid, alkali, salting liquid, lossless product quality with other substance reactions as long as configuration is appropriate.Organic silicon defoamer
To all bubble systems with suds, broken big gun function, belong to wide spectrum antifoaming agent scope.Organic silicon defoamer is widely used in washing
In the production processes such as agent, papermaking, paper pulp, sugaring, plating, chemical fertilizer, auxiliary agent, wastewater treatment.
(3) roseleaf and the creative of Rosa Damascana use mating protection glue again, and the present invention is made to see color shape in eye
And omnibearing stereo in smell, altitude simulation rose.Again be used cooperatively Protection glue stirring when protect roseleaf not by
It blends.
Specific implementation mode
By following embodiment, present invention be described in more detail, but should be noted that the scope of the present invention is not implemented by these
Any restrictions of example.
Embodiment 1
The aqueous imitative rose coating of one kind of invention, including count in parts by weight following group are grouped as：
The preparation method of aqueous imitative rose coating of the present invention, includes the following steps：
(1) selection container prepares 3% bentonitic aqueous solution：Quantitative bentonite is added to the water under 200r/min, is stirred
Mix the time be 5min to no powder particles, 1/10 cellulose is added, rotating speed is properly increased according to mill base state, mixing time is
3min no longer changes to state, spare.
(2) select container, at 300r/min by mixing time in quantitative cellulose input water be 5min to solution without
Powdered granule is added 1/3 pH adjusting agent activation hydrotropy, rotating speed is properly increased according to mill base state, mixing time be 5min extremely
State is not until variation.
(3) selection container prepares 5% protection glue solution：Water is added in quantitative rose Protection glue under 200r/min
In, mixing time is 5min to no powder particles, and rotating speed is properly increased according to mill base state, mixing time for 3min to state not
Change again, it is spare.
(4) cellulose solution dissolved, 3% bentonite solution and 5% protection glue solution are successively squeezed into Scattered Kettle
Middle mixing time is 2min, and remaining PH conditioning agents, aqueous synthetic-resin emulsion, rose ethereal oil, 6% is added under 900r/min
Rose Protection glue, rose sheet body, antifreezing agent, wetting agent, dispersant, fungicide, antifoaming agent, thickener and deionization, are stirred
It is 10min to mix the time；
(5) it is slowly added to the rose sheet body of the rose sheet body of 0.5-1mm, the rose sheet body of 1-2mm and 2-3mm,
Stirring to rose sheet body is uniformly dispersed；Stirring, which is maximum speed, must not be higher than 300r/min, and aqueous imitative rose coating is made；
(6) the aqueous imitative rose coating application mode of the present invention be with homochromy basecoat paint, specially spray gun bore 5mm,
Pressure is 2 megapascal, is sprayed using right-angled intersection.
Embodiment 2
The aqueous imitative rose coating of one kind of the present invention, including count in parts by weight following group are grouped as：
The preparation method of aqueous imitative rose coating of the present invention, includes the following steps：
(1) selection container prepares 3% bentonitic aqueous solution：Quantitative bentonite is added to the water under 300r/min, is stirred
Mix the time be 5min to no powder particles, 1/10 cellulose is added, rotating speed is properly increased according to mill base state, mixing time is
3min no longer changes to state, spare.
(2) select container, at 200r/min by mixing time in quantitative cellulose input water be 5min to solution without
Powdered granule is added 1/10 pH adjusting agent activation hydrotropy, rotating speed is properly increased according to mill base state, mixing time be 5min extremely
State is not until variation.
(3) selection container prepares 5% protection glue solution：Water is added in quantitative rose Protection glue under 200r/min
In, mixing time is 5min to no powder particles, and rotating speed is properly increased according to mill base state, mixing time for 3min to state not
Change again, it is spare.
(4) cellulose solution dissolved, 3% bentonite solution and 5% protection glue solution are successively squeezed into Scattered Kettle
Middle mixing time is 2min, and remaining PH conditioning agents, aqueous synthetic-resin emulsion, rose ethereal oil, 6% is added under 800r/min
Rose Protection glue, rose sheet body, antifreezing agent, wetting agent, dispersant, fungicide, antifoaming agent, thickener and deionization, are stirred
It is 10min to mix the time；
(5) it is slowly added to the rose sheet body of the rose sheet body of 0.5-1mm, the rose sheet body of 1-2mm and 2-3mm,
Stirring to rose sheet body is uniformly dispersed；Stirring, which is maximum speed, must not be higher than 300r/min, and aqueous imitative rose coating is made；
(6) the aqueous imitative rose coating application mode of the present invention be with homochromy basecoat paint, specially spray gun bore 5mm,
Pressure is 1.5 megapascal, is sprayed using right-angled intersection.
Embodiment 3
The aqueous imitative rose coating of one kind of the present invention, including count in parts by weight following group are grouped as：
The preparation method of aqueous imitative rose coating of the present invention, includes the following steps：
(1) selection container prepares 3% bentonitic aqueous solution：Water is added in quantitative bentonite under 200-300r/min
In, mixing time be 5min to no powder particles, 1/10 cellulose is added, rotating speed is properly increased according to mill base state, stirring
Time is that 3min no longer changes to state, spare.
(2) container is selected, by mixing time in quantitative cellulose input water is 5min to molten at 200-300r/min
Liquid is added 1/6 PH conditioning agents activation hydrotropy, properly increases rotating speed according to mill base state, mixing time is without powdered granule
5min is not until state is in variation.
(3) selection container prepares 5% protection glue solution：Water is added in quantitative rose Protection glue under 300r/min
In, mixing time is 5min to no powder particles, and rotating speed is properly increased according to mill base state, mixing time for 3min to state not
Change again, it is spare.
(4) cellulose solution dissolved, 3% bentonite solution and 5% protection glue solution are successively squeezed into Scattered Kettle
Middle mixing time is 2min, and remaining PH conditioning agents, aqueous synthetic-resin emulsion, rose ethereal oil, 6% is added under 900r/min
Rose Protection glue, rose sheet body, antifreezing agent, wetting agent, dispersant, fungicide, antifoaming agent, thickener and deionization, are stirred
It is 10min to mix the time；
(5) it is slowly added to the rose sheet body of the rose sheet body of 0.5-1mm, the rose sheet body of 1-2mm and 2-3mm,
Stirring to rose sheet body is uniformly dispersed；Stirring, which is maximum speed, must not be higher than 300r/min, and aqueous imitative rose coating is made；
The aqueous imitative rose coating application mode of the present invention is with homochromy basecoat paint, specially spray gun bore 5mm, and pressure is 1.5 million
Pa is sprayed using right-angled intersection.
Embodiment 4
The aqueous imitative rose coating of one kind of the present invention, including count in parts by weight following group are grouped as：
The aqueous synthetic-resin emulsion is the common styrene-acrylic emulsion of coating industry；The rose ethereal oil is natural
Rose ethereal oil, the rose ethereal oil are the rose folk prescription essential oil of Guangzhou Sheng Yan Fine Chemical Co., Ltd production.
The rose sheet body is that rose drying is crushed to sheet body, and the sheet body of the rose is 0.5-1mm
The sheet body of the sheet body of rose, the sheet body of 1.2mm roses or 2-3mm roses；The bentonite is organically-modified sodium base
Bentonite.With excellent thickening and middle shearing density, rheological effect is good, and water conservation moisture retention is good.
The wetting agent is the organic silicon polyether class surfactant of low molecular weight；The dispersant is polyether-modified
Type siloxane high performance surface activating agent；The thickener is that the common alkali soluble of coating industry rises class thickener；The 1mm
The mass ratio of the rose sheet body of rose sheet body, 1.2mm roses sheet body and 3mm is 1：1：1.5.
The active ingredient of the rose sheet body Protection glue is aluminium-magnesium silicate, the mixture of lithium magnesium silicate, the guarantor
Glue is protected to produce for Guangdong Shi Naishi Industrial Co., Ltd.s；1mm roses sheet body, 1.2mm roses sheet body and the 3mm roses
The mass ratio of flower piece body is 1:1:2.
The antifreezing agent is ethylene glycol；The antifoaming agent is organic silicon defoamer；Organic silicon defoamer be by silicone grease,
Emulsifier, waterproofing agent, thickening agent etc. are equipped with suitable quantity of water and are formed through machinery emulsification.Paint feature is that surface tension is small, high surface activity,
It is strong to defoam power, defoams that fast suds suppressing properties are good, does not influence the fundamental property of bubbling system, diffusivity, good penetrability, chemically surely
Fixed, no physiological activity is corrosion-free nontoxic, and no adverse side effect is not non-ignitable quick-fried, and safe, dosage is few, at low cost.Organosilicon
Antifoaming agent and water and most organic matters is not miscible, can be defoamed to most of frothing medias.Organic silicon defoamer has preferable
Thermal stability, can be used in 5-150 DEG C of broad temperature range；Its chemical stability is preferable, difficult and other substance reactions, only
It is appropriate to configure, and can be used in acid, alkali, salting liquid, lossless product quality.Organic silicon defoamer has both all bubble systems
There are suds, broken big gun function, belongs to wide spectrum antifoaming agent scope.Organic silicon defoamer be widely used in detergent, papermaking, paper pulp, sugaring,
In the production processes such as plating, chemical fertilizer, auxiliary agent, wastewater treatment.
The organic silicon defoamer density is 0.88g/cm3, viscosity 600mPa.s organic silicon defoamer；Described
Fungicide is the common wide-spectrum bactericide in market.
The preparation method of aqueous imitative rose coating of the present invention, includes the following steps：
(1) selection container prepares 3% bentonitic aqueous solution：Quantitative bentonite is added to the water under 280r/min, is stirred
Mix the time be 5min to no powder particles, 1/10 cellulose is added, rotating speed is properly increased according to mill base state, mixing time is
3min no longer changes to state, spare；The bentonite of 3% concentration is the concentration accumulated by many experiments.3% bentonite is molten
Solution got well state be sticky paste, if concentration it is excessive dissolving be not easy and viscosity be easy greatly very much a large amount of adhesions of chamber wall not
Easy next-step operation.The limited unfavorable subsequent production of excessive water as employed herein of water in the too small water increase formula used of concentration.
Rotating speed, which has no special requirements, only need to fully dissolve bentonite, as bentonitic addition viscosity can significantly increase so needs
Properly increase rotating speed.
(2) select container, at 280r/min by mixing time in quantitative cellulose input water be 5min to solution without
Powdered granule is added 1/10 pH adjusting agent activation hydrotropy, rotating speed is properly increased according to mill base state, mixing time be 5min extremely
State is not until variation；
(3) selection container prepares 5% protection glue solution：Water is added in quantitative rose Protection glue under 250r/min
In, mixing time is 5min to no powder particles, and rotating speed is properly increased according to mill base state, mixing time for 3min to state not
Change again, it is spare；
(4) cellulose solution dissolved, 3% bentonite solution and 5% protection glue solution are successively squeezed into Scattered Kettle
Middle mixing time is 2min, and remaining PH conditioning agents, aqueous synthetic-resin emulsion, rose ethereal oil, 6% is added under 600r/min
Rose Protection glue, rose sheet body, antifreezing agent, wetting agent, dispersant, fungicide, antifoaming agent, thickener and deionization, are stirred
It is 10min to mix the time.
(5) it is slowly added to the rose sheet body of the rose sheet body of 0.5-1mm, the rose sheet body of 1-2mm and 2-3mm,
Stirring to rose sheet body is uniformly dispersed；Stirring, which is maximum speed, must not be higher than 300r/min, and aqueous imitative rose coating is made；
Aqueous imitative rose coating application mode is with homochromy basecoat paint, specially spray gun bore 5mm, pressure 1.5
Megapascal is sprayed using right-angled intersection.
Embodiment 5
Embodiment 5 and embodiment 4 difference lies in：The aqueous imitative rose coating of one kind of the present invention, including by weight
Following group of number meter is grouped as：
The mass ratio of the rose sheet body of the 0.5mm roses sheet body, 2mm roses sheet body and 2.5mm is 1：
1.5：1.The mass ratio of the 0.5mm roses sheet body, 2mm roses sheet body and 2.5mm rose sheet bodies is 1:1:2.
The organic silicon defoamer density is 0.94g/cm3, viscosity 300mPa.s organic silicon defoamer；Described
Fungicide is the common wide-spectrum bactericide in market.
The preparation method of aqueous imitative rose coating of the present invention, includes the following steps：
In step (1), container is selected to prepare 3% bentonitic aqueous solution：Quantitative bentonite is added under 250r/min
Enter in water, mixing time be 5min to no powder particles, 1/10 cellulose is added, rotating speed is properly increased according to mill base state,
Mixing time is that 3min no longer changes to state, spare；
In step (2), container is selected, it is 5min that quantitative cellulose, which is put into mixing time in water, at 280r/min
To solution without powdered granule, 1/10 pH adjusting agent activation hydrotropy is added, rotating speed, mixing time are properly increased according to mill base state
For 5min to state not in variation until；
In step (3), container is selected to prepare 5% protection glue solution：Quantitative rose is protected under 280r/min
Glue is added to the water, mixing time be 5min to no powder particles, rotating speed, mixing time 3min are properly increased according to mill base state
No longer change to state, it is spare；
In step (4), the cellulose solution dissolved, 3% bentonite solution and 5% protection glue solution are successively beaten
It is 2min to enter mixing time in Scattered Kettle, and remaining PH conditioning agents, aqueous synthetic-resin emulsion, rose is added under 600-900r/min
Rare flower essential oil, 6% rose Protection glue, rose sheet body, antifreezing agent, wetting agent, dispersant, fungicide, antifoaming agent, thickener
And deionization, mixing time 10min.
In step (5), it is slowly added to the rose sheet body, the rose sheet body of 1-2mm and the rose of 2-3mm of 0.5-1mm
Rare flower piece body, stirring to rose sheet body are uniformly dispersed；Stirring, which is maximum speed, must not be higher than 300r/min, and aqueous imitative rose is made
Rare colored coating；Aqueous imitative rose coating application mode is with homochromy basecoat paint, specially spray gun bore 5mm, pressure 1.9
Megapascal is sprayed using right-angled intersection.
Embodiment 6
Embodiment 6 and embodiment 4 difference lies in：The rose sheet body is that rose drying is crushed to sheet body,
The sheet body of the rose is sheet body, the sheet body of 1mm roses or the sheet body of 2mm roses of 0.8mm roses.
The mass ratio of the rose sheet body of the 0.8mm roses sheet body, 1mm roses sheet body and 2mm is 1：1.2：
1.3。
The active ingredient of the rose sheet body Protection glue is aluminium-magnesium silicate, the mixture of lithium magnesium silicate, the guarantor
Glue is protected to produce for Guangdong Shi Naishi Industrial Co., Ltd.s；0.8mm roses sheet body, 1mm roses sheet body and the 2mm roses
The mass ratio of flower piece body is 1:1:2.
The organic silicon defoamer density is 0.92g/cm3, viscosity 800mPa.s organic silicon defoamer；Described
Fungicide is the common wide-spectrum bactericide in market.
The preparation method of aqueous imitative rose coating of the present invention, includes the following steps：
In step (4), the preparation of rose sheet body：By fresh rose lobe in 60 DEG C of drying in oven to water content
12%, it is sheared with slicer to the rose sheet body of the rose sheet body of 0.5-1mm, the rose sheet body of 1-2mm and 2-3mm,
Rose sheet body is made.
Aqueous imitative rose coating application mode is with homochromy basecoat paint, specially spray gun bore 5mm, pressure 1.8
Megapascal is sprayed using right-angled intersection.
Experiment 1
Aqueous imitative rose coating obtained is tested, all technical measured is shown in Table 1.
Table 1
By table 1 as can be seen that the aqueous imitative rose coating of the present invention can reach requirement.
The basic principles, main features and advantages of the present invention have been shown and described above.The technology of the industry
Personnel are it should be appreciated that the present invention is not limited to the above embodiments, and the above embodiments and description only describe this
The principle of invention, without departing from the spirit and scope of the present invention, various changes and improvements may be made to the invention, the present invention
Claimed range is delineated by the appended claims, the specification and equivalents thereof from the appended claims.
Claims (10)
1. a kind of aqueous imitative rose coating, it is characterised in that following group including counting in parts by weight is grouped as：
2. aqueous imitative rose coating according to claim 1, it is characterised in that：The aqueous synthetic-resin emulsion is
The common styrene-acrylic emulsion of coating industry；The rose ethereal oil is natural rose flower essential oil.
3. aqueous imitative rose coating according to claim 1, it is characterised in that：The rose ethereal oil is contained for Guangzhou
The rose folk prescription essential oil of beautiful Fine Chemical Co., Ltd's production；The rose sheet body is that rose drying is crushed to piece
Body, the sheet body of the rose are sheet body, the sheet body of 1-2mm roses or the piece of 2-3mm roses of 0.5-1mm roses
Body；The bentonite is organically-modified sodium bentonite.
4. aqueous imitative rose coating according to claim 1, it is characterised in that：The wetting agent is low molecular weight
Organic silicon polyether class surfactant；The dispersant is polyether modified siloxane class high performance surface activating agent；Described
Thickener is that the common alkali soluble of coating industry rises class thickener；The 0.5-1mm roses sheet body, 1-2mm rose sheet bodies
Mass ratio with the rose sheet body of 2-3mm is 1：1-1.5：1-1.5.
5. aqueous imitative rose coating according to claim 1, it is characterised in that：The rose sheet body Protection glue
Active ingredient is aluminium-magnesium silicate, and the mixture of lithium magnesium silicate, the Protection glue is the production of Guangdong Shi Naishi Industrial Co., Ltd.s；
The mass ratio of the 0.5-1mm roses sheet body, 1-2mm roses sheet body and 2-3mm rose sheet bodies is 1:1:2.
6. aqueous imitative rose coating according to claim 1, it is characterised in that：The antifreezing agent is ethylene glycol；Institute
The antifoaming agent stated is organic silicon defoamer；Organic silicon defoamer is the Taiwan Central Asia/wide spectrum antifoaming agent F111.
7. aqueous imitative rose coating according to claim 6, it is characterised in that：The organic silicon defoamer density is
0.88-0.94g/cm3, viscosity 300-800mPa.s organic silicon defoamer；The fungicide is the common wide spectrum in market
Fungicide.
8. the preparation method of aqueous imitative rose coating described in claim 1, it is characterised in that include the following steps：
(1) selection container prepares 3% bentonitic aqueous solution：Quantitative bentonite is added to the water under 200-300r/min, is stirred
Mix the time be 5min to no powder particles, 1/10 cellulose is added, rotating speed is properly increased according to mill base state, mixing time is
3min no longer changes to state, spare；
(2) select container, at 200-300r/min by mixing time in quantitative cellulose input water be 5min to solution without
Powdered granule is added the pH adjusting agent activation hydrotropy of 1/10-1/3, properly increases rotating speed according to mill base state, mixing time is
5min is not until state is in variation；
(3) selection container prepares 5% protection glue solution：Water is added in quantitative rose Protection glue under 200-300r/min
In, mixing time is 5min to no powder particles, and rotating speed is properly increased according to mill base state, mixing time for 3min to state not
Change again, it is spare；
(4) cellulose solution dissolved, 3% bentonite solution and 5% protection glue solution are successively squeezed into Scattered Kettle and is stirred
It is 2min to mix the time, and remaining PH conditioning agents, aqueous synthetic-resin emulsion, rose ethereal oil, 6% is added under 600-900r/min
Rose Protection glue, rose sheet body, antifreezing agent, wetting agent, dispersant, fungicide, antifoaming agent, thickener and deionization, are stirred
It is 10min to mix the time；
(5) it is slowly added to the rose sheet body of the rose sheet body of 0.5-1mm, the rose sheet body of 1-2mm and 2-3mm, is stirred
It is uniformly dispersed to rose sheet body；Stirring, which is maximum speed, must not be higher than 300r/min, and aqueous imitative rose coating is made.
9. the preparation method of aqueous imitative rose coating according to claim 8, it is characterised in that：In step (5), apply
The amount of material will account for the 2/3-3/4 of vessel volume；Aqueous imitative rose coating application mode is with homochromy basecoat paint, specially
Spray gun bore 5mm, pressure are 1.5-2 megapascal, are sprayed using right-angled intersection.
10. the preparation method of aqueous imitative rose coating according to claim 9, it is characterised in that：In step (4),
The preparation of rose sheet body：By fresh rose lobe in 60 DEG C of drying in oven to water content 10-15%, with slicer shear to
Rose sheet body is made in the rose sheet body of the rose sheet body of 0.5-1mm, the rose sheet body of 1-2mm and 2-3mm.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810316775.8A CN108753052A (en) | 2018-04-10 | 2018-04-10 | Aqueous imitative rose coating of one kind and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810316775.8A CN108753052A (en) | 2018-04-10 | 2018-04-10 | Aqueous imitative rose coating of one kind and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN108753052A true CN108753052A (en) | 2018-11-06 |
Family
ID=63981656
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201810316775.8A Pending CN108753052A (en) | 2018-04-10 | 2018-04-10 | Aqueous imitative rose coating of one kind and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN108753052A (en) |
Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101857747A (en) * | 2009-04-10 | 2010-10-13 | 王保瑞 | Method for preparing rose-jasmine aromatic coating |
| CN103819959A (en) * | 2014-01-24 | 2014-05-28 | 河北工程大学 | Light stone-imitating particulate matter and water-based stone-imitating coating prepared by adopting same |
| CN104098938A (en) * | 2014-08-01 | 2014-10-15 | 上海三银制漆有限公司 | New natural plant inorganic environment-friendly paint and preparation method thereof |
| CN104312351A (en) * | 2014-11-17 | 2015-01-28 | 广西启利新材料科技股份有限公司 | Sand-in-water colorful imitation stone paint |
| CN105801015A (en) * | 2016-03-17 | 2016-07-27 | 成都虹润制漆有限公司 | Textured paint and preparation method thereof |
| CN107286707A (en) * | 2017-06-22 | 2017-10-24 | 深圳市特塍装饰材料有限公司 | A kind of new natural plants inorganic environment-friendly coating and preparation method thereof |
-
2018
- 2018-04-10 CN CN201810316775.8A patent/CN108753052A/en active Pending
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101857747A (en) * | 2009-04-10 | 2010-10-13 | 王保瑞 | Method for preparing rose-jasmine aromatic coating |
| CN103819959A (en) * | 2014-01-24 | 2014-05-28 | 河北工程大学 | Light stone-imitating particulate matter and water-based stone-imitating coating prepared by adopting same |
| CN104098938A (en) * | 2014-08-01 | 2014-10-15 | 上海三银制漆有限公司 | New natural plant inorganic environment-friendly paint and preparation method thereof |
| CN104312351A (en) * | 2014-11-17 | 2015-01-28 | 广西启利新材料科技股份有限公司 | Sand-in-water colorful imitation stone paint |
| CN105801015A (en) * | 2016-03-17 | 2016-07-27 | 成都虹润制漆有限公司 | Textured paint and preparation method thereof |
| CN107286707A (en) * | 2017-06-22 | 2017-10-24 | 深圳市特塍装饰材料有限公司 | A kind of new natural plants inorganic environment-friendly coating and preparation method thereof |
Non-Patent Citations (1)
| Title |
|---|
| 申巨才等: "膏状仿瓷涂料", 《化学建材》 * |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN104353401B (en) | Condense multinuclear plants essential oil slow-release microcapsule and manufacture method, purposes again | |
| US20060039986A1 (en) | Functional material, process for producing functional material and functional member and environment modifying apparatus using the functional material | |
| CN102078268B (en) | Explosive salt and preparation method thereof | |
| TWI541025B (en) | W / O / W type emulsion with time stability and its manufacturing method | |
| CN101928641B (en) | Essence microcapsule with long-term effectiveness and preparation method thereof | |
| CN106063774B (en) | A kind of soft liquid talcum powder of corn | |
| CN109012133A (en) | A kind of microcapsules formaldehyde remover and preparation method thereof | |
| CN107801738A (en) | A kind of plant composition and preparation method thereof, application | |
| CN107467065A (en) | A kind of preparation method of long-acting slow release type solid chlorine dioxide air purifying preparation | |
| CN103232910A (en) | Transparent handmade soap and preparation method thereof | |
| CN103316616A (en) | Osmanthus essence nanocapsule and preparation method | |
| CN102653704A (en) | Preparation method of small peppermint essence soft capsule taking calcium alginate as wall material | |
| CN105838503A (en) | Slow aroma release type zein microcapsules and preparing method thereof | |
| CN104479866A (en) | Lavender essential oil microcapsule and preparation process thereof | |
| CN107517960A (en) | A kind of microballoon suspension seed-coating agent and preparation method thereof | |
| CN110352988A (en) | A kind of plant type air bacteriostatic agent and preparation method | |
| CN104892825A (en) | Lavender essential oil-loaded methyl methacrylate cross-linked polymer particles and preparation method thereof | |
| CN109260029A (en) | A kind of water-soluble nano essential oil micellar solution and preparation method thereof | |
| CN110130111A (en) | A kind of full biology base ultraviolet-resisting mosquito repellent microcapsules and preparation method thereof | |
| CN108753052A (en) | Aqueous imitative rose coating of one kind and preparation method thereof | |
| CN106387030B (en) | A kind of preparation method of sliver sea lettuce polysaccharide-chitosan compounding essential oil lotion | |
| CN105385502B (en) | A kind of preparation method of tea tree ethereal oil nanoparticle | |
| CN104651055A (en) | Polyurea microcapsule with aromatic smell and preparation method of polyurea microcapsule | |
| CN103920312B (en) | Method for preparing special foam-inhibiting defoaming agent for organic silicon wetting agent | |
| CN104472582A (en) | Plant-source pesticide for watermelon production |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20181106 |
|
| RJ01 | Rejection of invention patent application after publication |