CN108752754A - A kind of production method of plastic master batch - Google Patents
A kind of production method of plastic master batch Download PDFInfo
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- CN108752754A CN108752754A CN201810639374.6A CN201810639374A CN108752754A CN 108752754 A CN108752754 A CN 108752754A CN 201810639374 A CN201810639374 A CN 201810639374A CN 108752754 A CN108752754 A CN 108752754A
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L23/00—Compositions of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Compositions of derivatives of such polymers
- C08L23/02—Compositions of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Compositions of derivatives of such polymers not modified by chemical after-treatment
- C08L23/10—Homopolymers or copolymers of propene
- C08L23/14—Copolymers of propene
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
- C08K3/20—Oxides; Hydroxides
- C08K3/22—Oxides; Hydroxides of metals
- C08K2003/2227—Oxides; Hydroxides of metals of aluminium
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
- C08K3/20—Oxides; Hydroxides
- C08K3/22—Oxides; Hydroxides of metals
- C08K2003/2237—Oxides; Hydroxides of metals of titanium
- C08K2003/2241—Titanium dioxide
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/30—Sulfur-, selenium- or tellurium-containing compounds
- C08K2003/3045—Sulfates
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K2201/00—Specific properties of additives
- C08K2201/011—Nanostructured additives
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2201/00—Properties
- C08L2201/02—Flame or fire retardant/resistant
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2201/00—Properties
- C08L2201/06—Biodegradable
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
- C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
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- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Processes Of Treating Macromolecular Substances (AREA)
- Compositions Of Macromolecular Compounds (AREA)
Abstract
The invention discloses a kind of production methods of plastic master batch, plastic master batch component includes 20-30 parts of ternary polymerized polypropylene in parts by weight, 6-12 parts of polyester acid calcium, 4-10 parts of chlorinated paraffin, 3-9 parts of aluminium hydroxide, 2-6 parts of diatomite, 1-3 parts of white carbon, 1-5 parts of nano-titanium dioxide, 3-12 parts of blanc fixe, 4-10 parts of antimony oxide, 2-6 parts of acetylbutyrylcellulose, 8-18 parts of diamine propyl dimethyl silicone polymer, 4-10 parts of high efficiency water reducing agent polycarboxylic acids, production method of the present invention is simple, obtained plastics have good resistance to compression, it is wear-resisting, flame retardant property, deformation is less likely to occur, also there is biodegradability.
Description
Technical field
The present invention relates to plastic master batch preparing technical field, specially a kind of production method of plastic master batch.
Background technology
Filling-modified is an importance of polymer modification, on the one hand can reduce material cost, on the other hand also
Certain performances of material may be made to be improved（Such as heat resistance, dimensional stability）.It is filling-modified generally to use inorganic filler,
Mainly there are calcium carbonate, talcum powder, wollastonite, barium sulfate etc..And these fillers exist with powder form, in weighing, mix, make
Easy to produce a large amount of dust pollution during grain, deteriorate production environment, very big harm caused to health, and can pair plus
Construction equipment causes a degree of abrasion.And obtained plastic master batch comprehensive mechanical performance is poor.
Invention content
It is mentioned above in the background art to solve the purpose of the present invention is to provide a kind of production method of plastic master batch
Problem.
To achieve the above object, the present invention provides the following technical solutions：A kind of plastic master batch, plastic master batch component is by weight
Number includes 20-30 parts of ternary polymerized polypropylene, 6-12 parts of polyester acid calcium, 4-10 parts of chlorinated paraffin, 3-9 parts of aluminium hydroxide, silicon
2-6 parts of diatomaceous earth, 1-3 parts of white carbon, 1-5 parts of nano-titanium dioxide, 3-12 parts of blanc fixe, 4-10 parts of antimony oxide, acetic acid
2-6 parts of cellulose butyrate, 8-18 parts of diamine propyl dimethyl silicone polymer, 4-10 parts of high efficiency water reducing agent polycarboxylic acids.
Preferably, the preferred composition proportion of plastic master batch component include 25 parts of ternary polymerized polypropylene, 9 parts of polyester acid calcium,
7 parts of chlorinated paraffin, 6 parts of aluminium hydroxide, 4 parts of diatomite, 2 parts of white carbon, 3 parts of nano-titanium dioxide, 8 parts of blanc fixe, three oxygen
Change 7 parts of two antimony, 4 parts of acetylbutyrylcellulose, 13 parts of diamine propyl dimethyl silicone polymer, 7 parts of high efficiency water reducing agent polycarboxylic acids.
Preferably, a kind of production method of plastic master batch, includes the following steps：
A, it is added in stirred tank and stirs after mixing ternary polymerized polypropylene, polyester acid calcium, chlorinated paraffin, stir speed (S.S.) 300-
600 revs/min, diamine propyl dimethyl silicone polymer is added after stirring 5min, continues to stir 10min, obtains mixture A；
B, aluminium hydroxide, diatomite, white carbon, nano-titanium dioxide are sequentially added in mixture A, are added after being sufficiently mixed anti-
It answers in kettle, blanc fixe is added later, reaction kettle is heated to 60-80 DEG C, after heating 10min-18min, stop heating, slowly
It is cooled to room temperature, obtains mixture B；
C, antimony oxide, acetylbutyrylcellulose, high efficiency water reducing agent polycarboxylic acids are added in mixture B, at normal temperatures fully
Mixing, obtains mixture C；
D, mixture C is poured into master batch extruder and carries out extruding pelletization to get to plastic master batch.
Compared with prior art, the beneficial effects of the invention are as follows：Production method of the present invention is simple, and obtained plastics have tool
There are good resistance to compression, wear-resisting, flame retardant property, it is not easy to deform upon, also there is biodegradability；Wherein, add in the present invention
Blanc fixe, the antimony oxide added, can improve the flame retardant property of plastic master batch；White carbon, the nano-titanium dioxide of addition,
The elongation at break of plastic master batch can be improved.
Specific implementation mode
The following is a clear and complete description of the technical scheme in the embodiments of the invention, it is clear that described embodiment
Only a part of the embodiment of the present invention, instead of all the embodiments.Based on the embodiments of the present invention, the common skill in this field
The every other embodiment that art personnel are obtained without making creative work belongs to the model that the present invention protects
It encloses.
The present invention provides the following technical solutions：A kind of plastic master batch, plastic master batch component are total including ternary in parts by weight
Poly- polypropylene 20-30 parts, 6-12 parts of polyester acid calcium, 4-10 parts of chlorinated paraffin, 3-9 parts of aluminium hydroxide, 2-6 parts of diatomite, hard charcoal
1-3 parts black, 1-5 parts of nano-titanium dioxide, 3-12 parts of blanc fixe, 4-10 parts of antimony oxide, acetylbutyrylcellulose 2-6
Part, 8-18 parts of diamine propyl dimethyl silicone polymer, 4-10 parts of high efficiency water reducing agent polycarboxylic acids.
Embodiment one：
Plastic master batch component includes 20 parts of ternary polymerized polypropylene, 6 parts of polyester acid calcium, 4 parts of chlorinated paraffin, hydrogen-oxygen in parts by weight
Change 3 parts of aluminium, 2 parts of diatomite, 1 part of white carbon, 1 part of nano-titanium dioxide, 3 parts of blanc fixe, 4 parts of antimony oxide, acetic acid fourth
2 parts of acid cellulose, 8 parts of diamine propyl dimethyl silicone polymer, 4 parts of high efficiency water reducing agent polycarboxylic acids.
In the present embodiment, the production method of plastic master batch includes the following steps：
A, it is added in stirred tank and stirs after mixing ternary polymerized polypropylene, polyester acid calcium, chlorinated paraffin, stir speed (S.S.) 300
Rev/min, diamine propyl dimethyl silicone polymer is added after stirring 5min, continues to stir 10min, obtains mixture A；
B, aluminium hydroxide, diatomite, white carbon, nano-titanium dioxide are sequentially added in mixture A, are added after being sufficiently mixed anti-
It answers in kettle, blanc fixe is added later, reaction kettle is heated to 60 DEG C, after heating 10min, stop heating, slowly cool to room
Temperature obtains mixture B；
C, antimony oxide, acetylbutyrylcellulose, high efficiency water reducing agent polycarboxylic acids are added in mixture B, at normal temperatures fully
Mixing, obtains mixture C；
D, mixture C is poured into master batch extruder and carries out extruding pelletization to get to plastic master batch.
Embodiment two：
Plastic master batch component includes 30 parts of ternary polymerized polypropylene, 12 parts of polyester acid calcium, 10 parts of chlorinated paraffin, hydrogen in parts by weight
9 parts of aluminium oxide, 6 parts of diatomite, 3 parts of white carbon, 5 parts of nano-titanium dioxide, 12 parts of blanc fixe, 10 parts of antimony oxide, vinegar
6 parts of sour cellulose butyrate, 18 parts of diamine propyl dimethyl silicone polymer, 10 parts of high efficiency water reducing agent polycarboxylic acids.
In the present embodiment, the production method of plastic master batch includes the following steps：
A, it is added in stirred tank and stirs after mixing ternary polymerized polypropylene, polyester acid calcium, chlorinated paraffin, stir speed (S.S.) 600
Rev/min, diamine propyl dimethyl silicone polymer is added after stirring 5min, continues to stir 10min, obtains mixture A；
B, aluminium hydroxide, diatomite, white carbon, nano-titanium dioxide are sequentially added in mixture A, are added after being sufficiently mixed anti-
It answers in kettle, blanc fixe is added later, reaction kettle is heated to 80 DEG C, after heating 18min, stop heating, slowly cool to room
Temperature obtains mixture B；
C, antimony oxide, acetylbutyrylcellulose, high efficiency water reducing agent polycarboxylic acids are added in mixture B, at normal temperatures fully
Mixing, obtains mixture C；
D, mixture C is poured into master batch extruder and carries out extruding pelletization to get to plastic master batch.
Embodiment three：
Plastic master batch component includes 22 parts of ternary polymerized polypropylene, 7 parts of polyester acid calcium, 5 parts of chlorinated paraffin, hydrogen-oxygen in parts by weight
Change 4 parts of aluminium, 2 parts of diatomite, 2 parts of white carbon, 2 parts of nano-titanium dioxide, 5 parts of blanc fixe, 6 parts of antimony oxide, acetic acid fourth
3 parts of acid cellulose, 10 parts of diamine propyl dimethyl silicone polymer, 6 parts of high efficiency water reducing agent polycarboxylic acids.
In the present embodiment, the production method of plastic master batch includes the following steps：
A, it is added in stirred tank and stirs after mixing ternary polymerized polypropylene, polyester acid calcium, chlorinated paraffin, stir speed (S.S.) 350
Rev/min, diamine propyl dimethyl silicone polymer is added after stirring 5min, continues to stir 10min, obtains mixture A；
B, aluminium hydroxide, diatomite, white carbon, nano-titanium dioxide are sequentially added in mixture A, are added after being sufficiently mixed anti-
It answers in kettle, blanc fixe is added later, reaction kettle is heated to 65 DEG C, after heating 11min, stop heating, slowly cool to room
Temperature obtains mixture B；
C, antimony oxide, acetylbutyrylcellulose, high efficiency water reducing agent polycarboxylic acids are added in mixture B, at normal temperatures fully
Mixing, obtains mixture C；
D, mixture C is poured into master batch extruder and carries out extruding pelletization to get to plastic master batch.
Example IV：
Plastic master batch component includes 28 parts of ternary polymerized polypropylene, 10 parts of polyester acid calcium, 8 parts of chlorinated paraffin, hydrogen in parts by weight
8 parts of aluminium oxide, 5 parts of diatomite, 3 parts of white carbon, 4 parts of nano-titanium dioxide, 10 parts of blanc fixe, 9 parts of antimony oxide, acetic acid
5 parts of cellulose butyrate, 16 parts of diamine propyl dimethyl silicone polymer, 9 parts of high efficiency water reducing agent polycarboxylic acids.
In the present embodiment, the production method of plastic master batch includes the following steps：
A, it is added in stirred tank and stirs after mixing ternary polymerized polypropylene, polyester acid calcium, chlorinated paraffin, stir speed (S.S.) 500
Rev/min, diamine propyl dimethyl silicone polymer is added after stirring 5min, continues to stir 10min, obtains mixture A；
B, aluminium hydroxide, diatomite, white carbon, nano-titanium dioxide are sequentially added in mixture A, are added after being sufficiently mixed anti-
It answers in kettle, blanc fixe is added later, reaction kettle is heated to 75 DEG C, after heating 16min, stop heating, slowly cool to room
Temperature obtains mixture B；
C, antimony oxide, acetylbutyrylcellulose, high efficiency water reducing agent polycarboxylic acids are added in mixture B, at normal temperatures fully
Mixing, obtains mixture C；
D, mixture C is poured into master batch extruder and carries out extruding pelletization to get to plastic master batch.
Embodiment five：
Plastic master batch component includes 25 parts of ternary polymerized polypropylene, 9 parts of polyester acid calcium, 7 parts of chlorinated paraffin, hydrogen-oxygen in parts by weight
Change 6 parts of aluminium, 4 parts of diatomite, 2 parts of white carbon, 3 parts of nano-titanium dioxide, 8 parts of blanc fixe, 7 parts of antimony oxide, acetic acid fourth
4 parts of acid cellulose, 13 parts of diamine propyl dimethyl silicone polymer, 7 parts of high efficiency water reducing agent polycarboxylic acids.
In the present embodiment, the production method of plastic master batch includes the following steps：
A, it is added in stirred tank and stirs after mixing ternary polymerized polypropylene, polyester acid calcium, chlorinated paraffin, stir speed (S.S.) 300-
600 revs/min, diamine propyl dimethyl silicone polymer is added after stirring 5min, continues to stir 10min, obtains mixture A；
B, aluminium hydroxide, diatomite, white carbon, nano-titanium dioxide are sequentially added in mixture A, are added after being sufficiently mixed anti-
It answers in kettle, blanc fixe is added later, reaction kettle is heated to 60-80 DEG C, after heating 10min-18min, stop heating, slowly
It is cooled to room temperature, obtains mixture B；
C, antimony oxide, acetylbutyrylcellulose, high efficiency water reducing agent polycarboxylic acids are added in mixture B, at normal temperatures fully
Mixing, obtains mixture C；
D, mixture C is poured into master batch extruder and carries out extruding pelletization to get to plastic master batch.
Experimental example：
It is tested for the property using plastic master batch made from various embodiments of the present invention, obtains data such as following table：
| Compression strength（MPA） | Elongation at break（%） | |
| Embodiment one | 85 | 245 |
| Embodiment two | 88 | 250 |
| Embodiment three | 87 | 252 |
| Example IV | 85 | 252 |
| Embodiment five | 90 | 255 |
Production method of the present invention is simple, and obtained plastics are with good resistance to compression, wear-resisting, flame retardant property, it is not easy to occur
Deformation also has biodegradability；Wherein, blanc fixe, the antimony oxide added in the present invention, can improve plastic master
The flame retardant property of grain；White carbon, the nano-titanium dioxide of addition, can improve the elongation at break of plastic master batch.
It although an embodiment of the present invention has been shown and described, for the ordinary skill in the art, can be with
Understanding without departing from the principles and spirit of the present invention can carry out these embodiments a variety of variations, modification, replace
And modification, the scope of the present invention is defined by the appended.
Claims (3)
1. a kind of plastic master batch, it is characterised in that：Plastic master batch component includes ternary polymerized polypropylene 20-30 in parts by weight
Part, 6-12 parts of polyester acid calcium, 4-10 parts of chlorinated paraffin, 3-9 parts of aluminium hydroxide, 2-6 parts of diatomite, 1-3 parts of white carbon, nanometer two
1-5 parts of titanium oxide, 3-12 parts of blanc fixe, 4-10 parts of antimony oxide, 2-6 parts of acetylbutyrylcellulose, diamine propyl poly- two
8-18 parts of methylsiloxane, 4-10 parts of high efficiency water reducing agent polycarboxylic acids.
2. a kind of plastic master batch according to claim 1, it is characterised in that：The preferred composition proportion packet of plastic master batch component
Include 25 parts of ternary polymerized polypropylene, 9 parts of polyester acid calcium, 7 parts of chlorinated paraffin, 6 parts of aluminium hydroxide, 4 parts of diatomite, 2 parts of white carbon,
3 parts of nano-titanium dioxide, 8 parts of blanc fixe, 7 parts of antimony oxide, 4 parts of acetylbutyrylcellulose, diamine propyl poly dimethyl
13 parts of siloxanes, 7 parts of high efficiency water reducing agent polycarboxylic acids.
3. a kind of production method of plastic master batch, it is characterised in that：Include the following steps：
A, it is added in stirred tank and stirs after mixing ternary polymerized polypropylene, polyester acid calcium, chlorinated paraffin, stir speed (S.S.) 300-
600 revs/min, diamine propyl dimethyl silicone polymer is added after stirring 5min, continues to stir 10min, obtains mixture A；
B, aluminium hydroxide, diatomite, white carbon, nano-titanium dioxide are sequentially added in mixture A, are added after being sufficiently mixed anti-
It answers in kettle, blanc fixe is added later, reaction kettle is heated to 60-80 DEG C, after heating 10min-18min, stop heating, slowly
It is cooled to room temperature, obtains mixture B；
C, antimony oxide, acetylbutyrylcellulose, high efficiency water reducing agent polycarboxylic acids are added in mixture B, at normal temperatures fully
Mixing, obtains mixture C；
D, mixture C is poured into master batch extruder and carries out extruding pelletization to get to plastic master batch.
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| CN201810639374.6A CN108752754A (en) | 2018-06-20 | 2018-06-20 | A kind of production method of plastic master batch |
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| CN201810639374.6A CN108752754A (en) | 2018-06-20 | 2018-06-20 | A kind of production method of plastic master batch |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109719977A (en) * | 2019-03-20 | 2019-05-07 | 无锡市宏佳华新材料有限公司 | PP material plate processing technology |
| CN111944227A (en) * | 2020-08-17 | 2020-11-17 | 东莞市赛美塑胶制品有限公司 | Plastic defoaming master batch and preparation method thereof |
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| CN102604228A (en) * | 2012-03-20 | 2012-07-25 | 广州市聚赛龙工程塑料有限公司 | Multi-functional plastic masterbatch and preparation method thereof |
| CN104927205A (en) * | 2014-03-21 | 2015-09-23 | 荆春芳 | Enhanced plastic masterbatch |
| CN107936327A (en) * | 2017-12-07 | 2018-04-20 | 扬州市泽龙塑业有限公司 | A kind of preparation method of the strong thermoplastic plastic parent particles of stretch-resistance |
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2018
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| CN102443208A (en) * | 2011-10-28 | 2012-05-09 | 泰安现代塑料有限公司 | Mining flame retardant plastic geogrid master batch |
| CN102604228A (en) * | 2012-03-20 | 2012-07-25 | 广州市聚赛龙工程塑料有限公司 | Multi-functional plastic masterbatch and preparation method thereof |
| CN104927205A (en) * | 2014-03-21 | 2015-09-23 | 荆春芳 | Enhanced plastic masterbatch |
| CN107936327A (en) * | 2017-12-07 | 2018-04-20 | 扬州市泽龙塑业有限公司 | A kind of preparation method of the strong thermoplastic plastic parent particles of stretch-resistance |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109719977A (en) * | 2019-03-20 | 2019-05-07 | 无锡市宏佳华新材料有限公司 | PP material plate processing technology |
| CN111944227A (en) * | 2020-08-17 | 2020-11-17 | 东莞市赛美塑胶制品有限公司 | Plastic defoaming master batch and preparation method thereof |
| CN111944227B (en) * | 2020-08-17 | 2022-07-15 | 东莞市赛美塑胶制品有限公司 | Plastic defoaming master batch and preparation method thereof |
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Application publication date: 20181106 |