CN108740071A - A kind of preparation method of Zhuge's vegetable seed oil microcapsule - Google Patents
A kind of preparation method of Zhuge's vegetable seed oil microcapsule Download PDFInfo
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- CN108740071A CN108740071A CN201810554590.0A CN201810554590A CN108740071A CN 108740071 A CN108740071 A CN 108740071A CN 201810554590 A CN201810554590 A CN 201810554590A CN 108740071 A CN108740071 A CN 108740071A
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- zhuge
- seed oil
- vegetable seed
- preparation
- emulsion
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Classifications
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23D—EDIBLE OILS OR FATS, e.g. MARGARINES, SHORTENINGS, COOKING OILS
- A23D9/00—Other edible oils or fats, e.g. shortenings, cooking oils
- A23D9/007—Other edible oils or fats, e.g. shortenings, cooking oils characterised by ingredients other than fatty acid triglycerides
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23D—EDIBLE OILS OR FATS, e.g. MARGARINES, SHORTENINGS, COOKING OILS
- A23D9/00—Other edible oils or fats, e.g. shortenings, cooking oils
- A23D9/02—Other edible oils or fats, e.g. shortenings, cooking oils characterised by the production or working-up
- A23D9/04—Working-up
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- Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Manufacturing Of Micro-Capsules (AREA)
- Medicines Containing Plant Substances (AREA)
Abstract
The preparation method of Zhuge's vegetable seed oil microcapsule, including：(1) emulsion of microcapsules is prepared:Using lactalbumin and maltodextrin as wall material, it is compound wall materials to weigh WP and MD by quality proportioning, places it in magnetic stirring apparatus and is successively dissolved in distilled water, after it is completely dissolved, is stirred in high speed disperser, and Zhuge's vegetable seed oil emulsion is made, spare；(2) Zhuge's vegetable seed oil microcapsule is prepared:Emulsion is placed in spray dryer, Spray Drying Spray is carried out according to the condition of setting, after the completion of dry, microscapsule powder is collected with self-sealing plastic bag, is placed in refrigerator preservation to get Zhuge's vegetable seed oil microcapsule.The method of the present invention solves the problems, such as that Pueraria lobota rapeseed oil is easy to happen oxidative rancidity in storage, to keep the quality of Zhuge's rapeseed oil to create condition.Suitable for the area rich in Orychophragmus violaceus, the utilization rate of Orychophragmus violaceus resource is improved, is people's health service.
Description
Technical field
The present invention relates to rapeseed oils, are directed to microcapsules, it particularly relates to the preparation of Zhuge's vegetable seed oil microcapsule.
Background technology
Orychophragmus violaceus（Orychophragmus violaceus）It is Cruciferae, Orychophragmus, brassicaceae, alias two
Pale blue.Orychophragmus violaceus contains the multivitamins such as protein, carbohydrate, crude fibre and vitamin (B, C), carrotene, citrin, fat
Fat content is again very low, is most excellent Weight-reducing health dish.Contain flavone compound in cauline leaf, has and inhibit tumour, protection
The effects that liver, prevention and cure of cardiovascular disease.It contains eight kinds of amino acid of needed by human body.Moreover, Orychophragmus violaceus is wide in China's distribution
It is general, it is resourceful, it is a kind of vegetables new seed source with very great development potentiality.Orychophragmus violaceus is a kind of common open country of north of China
Dish, tender leaf and stem are edible, and seed collection, which gets up, can be used for extracting oil.Oil content is that good oil plant is made up to 50% or more in seed
Object.Contain abundant unsaturated fatty acid linoleic acid in Zhuge's rapeseed oil, it is beneficial to the National People's Congress.Human body is reduced because linoleic acid has
The function of interior serum cholesterol and triglycerides, and blood vessel can be softened and prevent thrombosis, it is the good of cardiovascular patient
Drug.But Zhuge's rapeseed oil is easy to happen oxidative rancidity in storage, to just influence Zhuge's rapeseed oil quality and
It is edible.
The patent application of grease microcapsule involved in Chinese patent database has No. ZL2014107929771《It is a kind of acidproof
Type microalgae DHA grease microscapsule powder》, No. ZL2015101068294《High stability algae oil DHA microscapsule powders and its preparation
Method》, No. 2016101984350《A kind of preparation method of high temperature resistant type microalgae DHA grease microscapsule powder》,
No. 2017107587710《A kind of DHA grease microscapsule powder and preparation method thereof containing polypeptide》Deng although related at present
In the report of Zhuge's rapeseed oil, but have no relevant patent application.
Invention content
The present invention is intended to provide a kind of preparation method of Zhuge's vegetable seed oil microcapsule, using microcapsules technology by Zhuge's vegetable seed
Oil wraps up, and to completely cut off extraneous poor environment, reduces Zhuge's rapeseed oil oxidizable rancid problem in storage, keeps
The quality of Zhuge's rapeseed oil.
The preparation method for Zhuge's vegetable seed oil microcapsule that inventor provides includes the preparation of emulsion and the preparation of microcapsules
Two steps, specific way are：
(1) emulsion of microcapsules is prepared
With lactalbumin（Whey protein, WP）And maltodextrin (Maltodetrin, MD) is used as wall material, matches by quality
It is compound wall materials than weighing WP and MD for 1~2: 1, places it in magnetic stirring apparatus and be successively dissolved in a certain amount of distilled water
Emulsification is proportionally added into Zhuge's rapeseed oil after it is completely dissolved, and stirs, emulsifies, Zhuge obtained in high speed disperser
Zhuge's rapeseed oil is wrapped in compound wall materials by vegetable seed oil emulsion, spare；
(2) Zhuge's vegetable seed oil microcapsule is prepared
Emulsion prepared by back is placed in spray dryer, Spray Drying Spray is carried out according to the preparation condition of setting, does
After the completion of dry, microscapsule powder is collected with self-sealing plastic bag, is placed in refrigerator and carries out preservation to get the micro- glue of Zhuge's rapeseed oil
Capsule.
In (1) step of the above method, the dosage of the distilled water is 5 times of the quality of WP and MD, the temperature of distilled water
It it is 55 DEG C~60 DEG C, the emulsification times are 5 ~ 10min；The dosage of Zhuge's rapeseed oil and the mass ratio of WP and MD, that is, core wall
Than being 1: 2~3, the rotary speed of the high speed disperser is 8r/min.
In (2) step of the above method, it is 100% that the preparation condition of the setting, which is compressed air speed, be spray-dried into
Air temperature is 150 DEG C~180 DEG C, and leaving air temp is that 40 DEG C~50 DEG C sample introduction revolution speeds are 8r/min；The preservation temperature of the refrigerator
Degree is 4 DEG C；The solid content of Zhuge's vegetable seed oil microcapsule is 20%, under this condition the packet of Zhuge's vegetable seed oil microcapsule
It is 88.78% to bury rate.
It is micro- to prepare Zhuge's rapeseed oil by experiment to spray drying for the preparation method of Zhuge's vegetable seed oil microcapsule of the present invention
The technique of capsule optimizes, to solve the problems, such as that Pueraria lobota rapeseed oil is easy to happen oxidative rancidity in storage, to protect
The quality for holding Zhuge's rapeseed oil creates condition.The present invention is suitable for the area rich in Orychophragmus violaceus, improves the profit of Orychophragmus violaceus resource
It is people's health service with rate.
Specific implementation mode
Embodiment 1 prepares Zhuge's vegetable seed oil microcapsule
Two steps of preparation of preparation and microcapsules including emulsion, specific way are：With through ultrasonic wave assisted extraction method
Obtained Zhuge's vegetable seed crude oil is raw material.
(1) emulsion of microcapsules is prepared
The lactalbumin produced with thousand will commerce and trade company of Henan（Whey protein, WP）And maltodextrin (Maltodetrin,
MD it) is used as wall material, WP and MD is weighed as compound wall materials at 2: 1 in mass ratio, places it in Gongyi City and give the limited public affairs of magnificent instrument
It takes charge of in the DF-101S type magnetic stirring apparatus of production and is successively dissolved in the distilled water that temperature is 55 DEG C~60 DEG C, the use of distilled water
Amount is 5 times of the quality of WP, MD and core material;After it is completely dissolved, by the mass ratio of the dosage and WP and MD of Zhuge's rapeseed oil
I.e. core wall ratio is 1: 3 addition Zhuge's rapeseed oil, and in the XHF-D type high speeds of NingBo XinZhi Biology Science Co., Ltd's production
It is stirred in disperser, emulsifies 5~10min, the rotary speed of high speed disperser is 8r/min, Zhuge's rapeseed oil emulsification obtained
Zhuge's rapeseed oil is wrapped in compound wall materials by liquid, spare；
(2) Zhuge's vegetable seed oil microcapsule is prepared
Emulsion prepared by back is placed in the B-290 type spray dryers of BUCHI Co., Ltds of Sweden product, according to setting
Preparation condition：Compressed air speed be 100%, spray drying EAT be 150 DEG C~180 DEG C, leaving air temp be 40 DEG C~
50 DEG C, sample introduction revolution speed is 8 r/min, and the storage temperature of the refrigerator is 4 DEG C of progress Spray Drying Sprays, after the completion of dry,
Microscapsule powder is collected with self-sealing plastic bag, is placed in refrigerator and carries out preservation to get Zhuge's vegetable seed oil microcapsule, solid content
Content is 20%, and the embedding rate of Zhuge's vegetable seed oil microcapsule is 88.78%.
Embodiment 2
(1) emulsion of microcapsules is prepared
The lactalbumin produced with thousand will commerce and trade company of Henan（Whey protein, WP）And maltodextrin (Maltodetrin,
MD it) is used as wall material, WP and MD is weighed as compound wall materials at 2: 1 in mass ratio, places it in Gongyi City and give the limited public affairs of magnificent instrument
It takes charge of in the DF-101S type magnetic stirring apparatus of production and is successively dissolved in the distilled water that temperature is 55 DEG C~60 DEG C, the use of distilled water
Amount is 5 times of the quality of WP, MD and core material;After it is completely dissolved, by the mass ratio of the dosage and WP and MD of Zhuge's rapeseed oil,
I.e. core wall ratio is 1: 2 addition Zhuge's rapeseed oil, and in the XHF-D type high speeds of NingBo XinZhi Biology Science Co., Ltd's production
It is stirred in disperser, emulsifies 5~10min, the rotary speed of high speed disperser is 8r/min, Zhuge's rapeseed oil emulsification obtained
Zhuge's rapeseed oil is wrapped in compound wall materials by liquid, spare；
(2) Zhuge's vegetable seed oil microcapsule is prepared
Emulsion prepared by back is placed in the B-290 type spray dryers of BUCHI Co., Ltds of Sweden product, according to setting
Preparation condition：Compressed air speed be 100%, spray drying EAT be 150 DEG C~180 DEG C, leaving air temp be 40 DEG C~
50 DEG C, sample introduction revolution speed is 8r/min, and the storage temperature of the refrigerator is 4 DEG C of progress Spray Drying Sprays, after the completion of dry, is used
Self-sealing plastic bag collects microscapsule powder, is placed in refrigerator and carries out preservation to get Zhuge's vegetable seed oil microcapsule, solid content contains
Amount is 20%, and the embedding rate of Zhuge's vegetable seed oil microcapsule is 83.60%.
Embodiment 3
(1) emulsion of microcapsules is prepared
The lactalbumin produced with thousand will commerce and trade company of Henan（Whey protein, WP）And maltodextrin (Maltodetrin,
MD it) is used as wall material, WP and MD is weighed as compound wall materials at 1: 1 in mass ratio, places it in Gongyi City and give the limited public affairs of magnificent instrument
It takes charge of in the DF-101S type magnetic stirring apparatus of production and is successively dissolved in the distilled water that temperature is 55 DEG C~60 DEG C, the use of distilled water
Amount is 4 times of the quality of WP, MD and core material;After it is completely dissolved, by the mass ratio of the dosage and WP and MD of Zhuge's rapeseed oil
I.e. core wall ratio is 1: 3 addition Zhuge's rapeseed oil, and in the XHF-D type high speeds of NingBo XinZhi Biology Science Co., Ltd's production
It is stirred in disperser, emulsifies 5~10min, the rotary speed of high speed disperser is 8r/min, Zhuge's rapeseed oil emulsification obtained
Zhuge's rapeseed oil is wrapped in compound wall materials by liquid, spare；
(2) Zhuge's vegetable seed oil microcapsule is prepared
Emulsion prepared by back is placed in the B-290 type spray dryers of BUCHI Co., Ltds of Sweden product, according to setting
Preparation condition：Compressed air speed be 100%, spray drying EAT be 150 DEG C~180 DEG C, leaving air temp be 40 DEG C~
50 DEG C, sample introduction revolution speed is 8 r/min, and the storage temperature of the refrigerator is4DEG C Spray Drying Spray is carried out, after the completion of dry,
Microscapsule powder is collected with self-sealing plastic bag, is placed in refrigerator and carries out preservation to get Zhuge's vegetable seed oil microcapsule, solid content
Content is 25%, and the embedding rate of Zhuge's vegetable seed oil microcapsule is 79.59%.
Claims (3)
1. the preparation method of Zhuge's vegetable seed oil microcapsule, feature includes the preparation of emulsion and two steps of preparation of microcapsules
Suddenly, specific way is：
(1) emulsion of microcapsules is prepared
Using lactalbumin and maltodextrin as wall material, weighs WP and MD as compound wall materials at 1~2: 1 in mass ratio, incite somebody to action
It, which is placed in magnetic stirring apparatus, is successively dissolved in a certain amount of distilled water, after it is completely dissolved, is proportionally added into Orychophragmus violaceus
Seed oil, and stir, emulsify in high speed disperser, Zhuge's vegetable seed oil emulsion is made, it is spare；
(2) Zhuge's vegetable seed oil microcapsule is prepared
Emulsion prepared by back is placed in spray dryer, Spray Drying Spray is carried out according to the preparation condition of setting, does
After the completion of dry, microscapsule powder is collected with self-sealing plastic bag, is placed in refrigerator and carries out preservation to get the micro- glue of Zhuge's rapeseed oil
Capsule.
2. the preparation method of Zhuge's vegetable seed oil microcapsule as described in claim 1, it is characterised in that in (1) step of method,
The dosage of the distilled water is 5 times of the quality of WP and MD, and the temperature of distilled water is 55 DEG C~60 DEG C, the emulsification times are 5 ~
10min；The dosage of Zhuge's rapeseed oil is 1: 2~3 with the mass ratio of WP and MD, that is, core wall ratio, the rotation of the high speed disperser
Rotary speed is 8r/min.
3. the preparation method of Zhuge's vegetable seed oil microcapsule as described in claim 1, it is characterised in that in (2) step of method,
The preparation condition of the setting is that compressed air speed is 100%, and spray drying temperature is 150 DEG C~180 DEG C, sample introduction revolution speed
For 8 r/min；The storage temperature of the refrigerator is 4 DEG C；The solid content of Zhuge's vegetable seed oil microcapsule is 20%.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810554590.0A CN108740071A (en) | 2018-06-01 | 2018-06-01 | A kind of preparation method of Zhuge's vegetable seed oil microcapsule |
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| CN201810554590.0A CN108740071A (en) | 2018-06-01 | 2018-06-01 | A kind of preparation method of Zhuge's vegetable seed oil microcapsule |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114271499A (en) * | 2021-12-29 | 2022-04-05 | 江南大学 | Microcapsule powder with high embedding rate and preparation method thereof |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1554734A (en) * | 2003-12-26 | 2004-12-15 | 颜怀玮 | Method for producing medicinal food and plant orychophiagmus violaceus |
| CN104757531A (en) * | 2014-11-05 | 2015-07-08 | 四川省植物工程研究院 | Chinese prickly ash seed oil micro capsule and preparation method thereof |
-
2018
- 2018-06-01 CN CN201810554590.0A patent/CN108740071A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1554734A (en) * | 2003-12-26 | 2004-12-15 | 颜怀玮 | Method for producing medicinal food and plant orychophiagmus violaceus |
| CN104757531A (en) * | 2014-11-05 | 2015-07-08 | 四川省植物工程研究院 | Chinese prickly ash seed oil micro capsule and preparation method thereof |
Non-Patent Citations (1)
| Title |
|---|
| 吴克刚等: "《食品微胶囊技术》", 31 July 2006, 中国轻工业出版社 * |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114271499A (en) * | 2021-12-29 | 2022-04-05 | 江南大学 | Microcapsule powder with high embedding rate and preparation method thereof |
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Application publication date: 20181106 |