CN108729887A - Adhesive film stablizes gravel packing zone sand-preventing process - Google Patents

Adhesive film stablizes gravel packing zone sand-preventing process Download PDF

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Publication number
CN108729887A
CN108729887A CN201710264258.6A CN201710264258A CN108729887A CN 108729887 A CN108729887 A CN 108729887A CN 201710264258 A CN201710264258 A CN 201710264258A CN 108729887 A CN108729887 A CN 108729887A
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Prior art keywords
sand
adhesive film
gravel packing
packing zone
alcohol
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CN201710264258.6A
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CN108729887B (en
Inventor
宋金波
李常友
熊伟
孙秀钊
董海生
武明鸣
高雪峰
梅明霞
王冰
王东
张锡娟
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China Petroleum and Chemical Corp
Sinopec Research Institute of Petroleum Engineering Shengli Co
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China Petroleum and Chemical Corp
Sinopec Research Institute of Petroleum Engineering Shengli Co
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    • EFIXED CONSTRUCTIONS
    • E21EARTH OR ROCK DRILLING; MINING
    • E21BEARTH OR ROCK DRILLING; OBTAINING OIL, GAS, WATER, SOLUBLE OR MELTABLE MATERIALS OR A SLURRY OF MINERALS FROM WELLS
    • E21B43/00Methods or apparatus for obtaining oil, gas, water, soluble or meltable materials or a slurry of minerals from wells
    • E21B43/02Subsoil filtering
    • E21B43/04Gravelling of wells
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D177/00Coating compositions based on polyamides obtained by reactions forming a carboxylic amide link in the main chain; Coating compositions based on derivatives of such polymers
    • C09D177/06Polyamides derived from polyamines and polycarboxylic acids

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Mining & Mineral Resources (AREA)
  • Geology (AREA)
  • Environmental & Geological Engineering (AREA)
  • Organic Chemistry (AREA)
  • Physics & Mathematics (AREA)
  • Wood Science & Technology (AREA)
  • Fluid Mechanics (AREA)
  • Materials Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Geochemistry & Mineralogy (AREA)
  • Sealing Material Composition (AREA)
  • Adhesives Or Adhesive Processes (AREA)

Abstract

The invention discloses a kind of adhesive films to stablize gravel packing zone sand-preventing process, includes the following steps:(1)After gravel filling sand prevention EP (end of program), prepad fluid is injected immediately, for cleaning filling layer and oil reservoir;(2)Pump note alcohol-soluble film forming agent, adhesive film is generated for being precipitated automatically in gravel packing zone pore water wet structure;The alcohol-soluble film forming agent be amide resin ethanol solution, a concentration of 3~20%;(3)It injects water or gravel filling and is replaced with water-base carrier fluid and enter bottom, dosage is 3 times or more of alcohol-soluble film forming agent dosage, promote film spreading by water driving force and film forming agent intrinsic viscosity, after ultra-thin adhesive film, the particle of intrusion filling layer is adhered to around back-up sand, it will not migrate and then block filling layer hole, to keep the high osmosis and stability of filling layer for a long time.The technique of the present invention neither injures reservoir permeability, keeps compared with high flow conductivity, and significantly improves filling sand body stability, facilitates construction.

Description

Adhesive film stablizes gravel packing zone sand-preventing process
Technical field
The present invention relates to a kind of adhesive films to stablize gravel packing zone sand-preventing process, belongs to petroleum works technical field.
Background technology
Reservoir fine migration (as shown in Figure 1) is adjoint in each stage of petroleum production engineering, when fluid-flow rate is big in reservoir When the maximum critical flow velocity of fine migration in hole, a series of serious problems from stratum to ground can be caused, such as:Reservoir Productivity decline is rapid, filter sand blockage, holddown, ground solid pollutant increase etc..The big pump extract of block since the Shengli Oil Field Since pilot, since fine migration blocks oil well productivity decline rapid (as shown in Figure 2) caused by gravel packing zone in reservoir Problem is more prominent, and it is equally prominent to block the problem of oil well productivity caused by sand screen declines after reservoir particle inflow pit shaft.It can See, it is the key that extend oil well productivity, improve the sand control life effectively to control reservoir fine migration and block gravel packing zone.
Widely used cationic polymer presses down sand agent due to the limitation in structure and performance in sand control pack technique at present The requirement that current big pump extract, long-acting sand control and acidification control fine migration is not adapted to:One, cationic polymer Suppression sand agent water solubility can be dissolved into water flooding again with the extension of production time, remain in the active ingredient of hole table wall by ground Layer salinity and shear action influence can be denaturalized chain rupture, and successively decreasing, which causes to press down rapidly grittiness, to fall sharply;Secondly, remain in hole and micro- The cationic polymer of grain table wall only leans on Electrostatic Absorption and hydrogen bond action suppression grittiness can faint, resistance to erosion discharge capacity only 900ml/h;Its Three, cationic polymer can be caused in middle low permeability reservoir improper use by reservoir damage.It is although pre-coated with from consolidated proppants Machine film, but only meet itself consolidation under the conditions of underground and generate intensity, this precoating organic film does not have viscosity property, because without The formation fines of intrusion filling layer can be adhered to.Therefore, it is necessary to provide a kind of new adhesive film stabilization gravel packing zone sand control work Skill.
Invention content
For the above-mentioned prior art, the present invention provides a kind of adhesive films to stablize gravel packing zone sand-preventing process, the technique Adhesive film can be generated in gravel packing zone pore surface, stablize filling sand body, effectively solve reservoir fine migration and block gravel Oil well productivity caused by filling layer declines rapid problem, significantly improves sand control pack effect, and popularizing application prospect is wide.
The present invention is achieved by the following technical solutions:
A kind of adhesive film stabilization gravel packing zone sand-preventing process, steps are as follows:
(1) after gravel filling sand prevention EP (end of program), prepad fluid is injected immediately, for cleaning filling layer and oil reservoir;It is described Prepad fluid is made of microemulsion, hydrogen chloride and water, wherein and microemulsion accounts for 1.5~1.9%, and hydrogen chloride accounts for 13.3~22.5%, Surplus is water (by weight percentage);
The microemulsion be by the group of following parts by weight be grouped as (i.e.:Patent No. 200610009675.8 authorizes public affairs Accuse the microemulsion described in number document for being CN 100336891C):
Further, the injection rate of the prepad fluid, is calculate by the following formula determination:
In formula, ri--- design radial (unit:m);rw--- wellbore radius (unit:m);The average hole of φ --- oil reservoir Porosity;H --- core intersection (unit:m);
The design radial, depending on sand control sand production situation, usually 2.0~3.0m;
(2) pump note alcohol-soluble film forming agent generates adhesive film (alcohol for being precipitated automatically in gravel packing zone pore water wet structure Insoluble film former injection rate is 1~4 times of prepad fluid dosage, and injection pressure is less than the 80% of formation fracture pressure), keep filling Sand body stability, while effectively oil well productivity decline caused by solution reservoir fine migration blocking gravel packing zone is rapidly asked Topic;
The alcohol-soluble film forming agent is the ethanol solution of amide resin (weight concentration of amide resin is 3~20%) (3% is that can be resistant to wash away the minimum concentration that discharge capacity reaches 7000ml/h, 20% be clay content more than 10% loose sand Layer SC service ceiling, experiment finds that concentration transfinites and deposits the influence of influence in-place permeability after precipitation, takes into account economy and finally determines Upper concentration 20%);The amide resin is selected from 650 amide resin of low molecule, 600 amide resins, V115 amide resins, V125 Amide resin, 3650 amide resins, 3155 amide resins (amide resin of these models can conventional market be commercially available);
Further, for the unconsolidated sandstone formation of clay content 5-10%, a concentration of the 3~10% of amide resin;It is right It is more than 10% unconsolidated sandstone formation in clay content, the weight concentration of amide resin is 10~20%;
Further, when injecting alcohol-soluble film forming agent, disposable injection or the injection of multistage plug;When multistage plug injects, slug It is designed as alcohol-soluble film forming agent and replaces injection, general 3 slugs in equal volume with water;
(3) injection water (such as oilfield sewage) or gravel filling water-base carrier fluid replace and enter bottom, and dosage is that alcohol is molten Property film forming agent dosage 3 times (volume multiples) more than (it is excessive, alcohol-soluble film forming agent can be made to be precipitated complete, to effective profit With), promote film spreading to invade the particle of filling layer after ultra-thin adhesive film by water driving force and film forming agent intrinsic viscosity Be adhered to around back-up sand, will not migrate so that block filling layer hole, to for a long time keep filling layer high osmosis and Stability.
The adhesive film of the present invention stablizes gravel packing zone sand-preventing process, washes away discharge capacity and reaches 7000ml/h, outlet sand content < 0.5g/L (evaluation method uses in Q/SH1020 2377-2015 5.5);It is applicable in reservoir and permeates > 10md, rock core infiltration retains Rate > 90% (evaluation method uses in Q/SLCG0097-2014 4.7);Extend sand control measure oil-water well term of validity > half a year.
The adhesive film of the present invention stablizes gravel packing zone sand-preventing process, and section plug pump note technique promotes to generate adhesive film (film-forming state is precipitated in alcohol-soluble film forming agent water as shown in figure 4, adhesive film fixation in situ particle displaing micro picture is as shown in Figure 5.Alcohol When insoluble film former selects a concentration of 10% ethanol solution of 650 amide resins, adhesive film stablizes gravel packing zone corpuscular property Energy tables of data is as shown in table 1, and the influence tables of data to in-place permeability is as shown in table 2), reservoir permeability is neither injured, is kept Compared with high flow conductivity, but significantly improve filling sand body stability, facilitate construction, have safety and environmental protection, construction is simple, film forming soon, The features such as resistance to erosion ability is strong is the new process that mid-late oilfield development extends sand control filling stable production period, promotes and applies valence It is worth big, strong applicability.
1 adhesive film of table stablizes gravel packing zone particle performance data table
(evaluation method uses in Q/SH1020 2377-2015 5.5)
Influence tables of data of the 2 alcohol-soluble film forming agent of table to in-place permeability
(evaluation method uses in Q/SLCG0097-2014 4.7)
Description of the drawings
Fig. 1:Liquid stream promotes fine migration schematic diagram in hole.
Fig. 2:Fine migration blocks pore throat, and oil well productivity is caused to decline schematic diagram.
Fig. 3:The apparent gap adhesive film particle that adherency is migrated in situ, remains the unobstructed schematic diagram of filling layer pore throat.
Fig. 4:Film-forming state is precipitated in alcohol-soluble film forming agent water.
Fig. 5:Adhesive film fixation in situ particle displaing micro picture.
Specific implementation mode:
With reference to embodiment, the present invention is further illustrated.
Involved instrument, reagent, material etc., are existing in the prior art unless otherwise noted in following embodiments Conventional instrument, reagent, material etc., can be obtained by regular commercial sources.Involved experimental method in following embodiments, inspection Survey method etc. is unless otherwise noted existing routine experiment method in the prior art, detection method etc..
1 adhesive film of embodiment stablizes gravel packing zone sand-preventing process
Steps are as follows:
(1) after gravel filling sand prevention EP (end of program), prepad fluid is injected immediately, for cleaning filling layer and oil reservoir;It is described Prepad fluid is made of microemulsion, hydrogen chloride and water, wherein microemulsion accounts for 1.7%, and hydrogen chloride accounts for 18.5%, and surplus is that water (is pressed Weight percent meter);
The microemulsion be by the group of following parts by weight be grouped as (i.e.:Patent No. 200610009675.8 authorizes public affairs Accuse the microemulsion described in number document for being CN 100336891C):
The injection rate of the prepad fluid, is calculate by the following formula determination:
In formula, ri--- design radial (unit:m);rw--- wellbore radius (unit:m);The average hole of φ --- oil reservoir Porosity;H --- core intersection (unit:m);
The design radial is 2.0~3.0m;
(2) (alcohol-soluble film forming agent injection rate is 1~4 times of prepad fluid dosage to pump note alcohol-soluble film forming agent, and injection pressure is small In the 80% of formation fracture pressure), adhesive film is generated for being precipitated automatically in gravel packing zone pore water wet structure, keeps filling Sand body stability, while effectively oil well productivity decline caused by solution reservoir fine migration blocking gravel packing zone is rapidly asked Topic;
The alcohol-soluble film forming agent is the ethanol solution of amide resin (weight concentration of amide resin is 3~20%);Institute It states amide resin and is selected from 650 amide resin of low molecule, 600, V115, V125,3650,3155;
(3) injection water (such as oilfield sewage) or gravel filling water-base carrier fluid replace and enter bottom, and dosage is that alcohol is molten Property film forming agent dosage 3 times (volume multiples) more than (excess), promote film paving by water driving force and film forming agent intrinsic viscosity Exhibition, after ultra-thin adhesive film, the particle for invading filling layer is adhered to around back-up sand, will not be migrated and then be blocked filling layer hole Gap (as shown in Figure 3), to keep the high osmosis and stability of filling layer for a long time.
Application example
1. selecting well
Well selection criterion:
(1) heavy oil wells in the loose sand reservoir oil area of clay content 5~30% or general thin oil well and gas well;
(2) 3~20 meters of well section of construction is more than that time core intersection carries out incremental extrusion using mechanical coupling segment tool;
(3) it is greater than 40% containing saturation degree, if saturation degree is low, considers economic return;
(4) well temperature range is applicable within 160 DEG C.
2. detail design
According to the completion basic data of oil well, perforation situation (including perforated interval, the depth, core intersection etc.), oil reservoir hole The data such as porosity, permeability, hydrocarbon saturation, clay content, Extra-fine sand content, well-designed, format and specification and gravel Filling anti-sand design is similar.
3. working procedure and operational method:
(1) construction operation prepares
A. former well casing column and pump are taken out in erection of derrick, kill-job;
B. sand-flushing pipe column is descended to visit sand face, if any sand, well-flushing takes out sand-flushing pipe column to artificial bottom of a well after sand washing operation;
C. plain tubing of the tripping in pen tip is to 15~30m of oil reservoir top;
D. 250 model well head is installed, adhesive film is carried out and stablizes the preparation of gravel packing zone sand control.
(2) adhesive film stablizes the construction of gravel packing zone sand control
A. surface line pressure testing 25MPa is connected, does not pierce and does not leak for qualification, lower step construction can be carried out;
B. pad stage is injected, injection displacement control is in 500~1000L/min, and volume is according to detail design;
C. it injects the stage of alcohol-soluble film forming agent, injection displacement control is in 500~1000L/min, it is necessary to according to oil reservoir reality Border situation implements disposable injection or the injection of multistage plug, if multistage plug injects, it is dirty with oil field that slug is designed as alcohol-soluble film forming agent Water alternately injects in equal volume, and general 3 slugs can fully meet construction requirement;
D. 3 times or more the oilfield sewages or gravel filling water-base carrier fluid of alcohol-soluble film forming agent volume are directly injected into.
(3) operation after constructing.
Advantage of the invention is that:After adhesive film stablizes the construction of gravel packing zone sand control, does not have to closing well and wait for, it directly can be with Lower pump is gone into operation, to save the activity duration.
Although above-mentioned be described the specific implementation mode of the present invention in conjunction with the embodiments, not the present invention is protected The limitation of range, those skilled in the art should understand that, based on the technical solutions of the present invention, those skilled in the art The various modifications or changes that can be made need not be made the creative labor still within protection scope of the present invention.

Claims (7)

1. a kind of adhesive film stablizes gravel packing zone sand-preventing process, it is characterised in that:Include the following steps:
(1) after gravel filling sand prevention EP (end of program), prepad fluid is injected immediately, for cleaning filling layer and oil reservoir;It is described preposition Liquid is made of microemulsion, hydrogen chloride and water, wherein microemulsion accounts for 1.5~1.9%, and hydrogen chloride accounts for 13.3~22.5%, surplus For water;
(2) pump note alcohol-soluble film forming agent generates adhesive film for being precipitated automatically in gravel packing zone pore water wet structure;
The alcohol-soluble film forming agent is the ethanol solution of amide resin, and the weight concentration of amide resin is 3~20%;
The amide resin be selected from 650 amide resin of low molecule, 600 amide resins, V115 amide resins, V125 amide resins, 3650 amide resins, 3155 amide resins;
(3) inject water or gravel filling water-base carrier fluid and replace and enter bottom, dosage be 3 times of alcohol-soluble film forming agent dosage with On.
2. adhesive film according to claim 1 stablizes gravel packing zone sand-preventing process, it is characterised in that:The step (1) In, the microemulsion is grouped as by the group of following parts by weight:
3. adhesive film according to claim 1 stablizes gravel packing zone sand-preventing process, it is characterised in that:The step (1) In, the injection rate of the prepad fluid is calculate by the following formula determination:
In formula, ri--- design radial;rw--- wellbore radius;The average pore of φ --- oil reservoir;H --- core intersection.
4. adhesive film according to claim 3 stablizes gravel packing zone sand-preventing process, it is characterised in that:The design radial For 2.0~3.0m.
5. adhesive film according to claim 1 stablizes gravel packing zone sand-preventing process, it is characterised in that:The step (2) In, alcohol-soluble film forming agent injection rate is 1~4 times of prepad fluid dosage, and injection pressure is less than the 80% of formation fracture pressure.
6. adhesive film according to claim 1 stablizes gravel packing zone sand-preventing process, it is characterised in that:The step (2) In, for the unconsolidated sandstone formation of clay content 5-10%, a concentration of the 3~10% of amide resin;Clay content is more than The weight concentration of 10% unconsolidated sandstone formation, amide resin is 10~20%.
7. adhesive film according to claim 1 stablizes gravel packing zone sand-preventing process, it is characterised in that:The step (2) In, when injecting alcohol-soluble film forming agent, disposable injection or the injection of multistage plug;Multistage plug inject when, slug be designed as alcohol-soluble at Film replaces injection with water in equal volume.
CN201710264258.6A 2017-04-21 2017-04-21 Sand prevention process for viscous membrane stable gravel packing layer Active CN108729887B (en)

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Cited By (2)

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Publication number Priority date Publication date Assignee Title
CN113494275A (en) * 2020-03-18 2021-10-12 中国海洋石油集团有限公司 Water control well completion structure for controlling axial channeling by utilizing particle migration
CN115341879A (en) * 2022-10-17 2022-11-15 中国石油大学(华东) Composite sand control construction design method for sand production oil and gas well

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Publication number Priority date Publication date Assignee Title
CN113494275A (en) * 2020-03-18 2021-10-12 中国海洋石油集团有限公司 Water control well completion structure for controlling axial channeling by utilizing particle migration
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CN115341879B (en) * 2022-10-17 2023-01-13 中国石油大学(华东) Composite sand control construction design method for sand production oil and gas well

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