CN108716818A - A kind of efficient freeze-drying apparatus for polypeptide - Google Patents
A kind of efficient freeze-drying apparatus for polypeptide Download PDFInfo
- Publication number
- CN108716818A CN108716818A CN201810634599.2A CN201810634599A CN108716818A CN 108716818 A CN108716818 A CN 108716818A CN 201810634599 A CN201810634599 A CN 201810634599A CN 108716818 A CN108716818 A CN 108716818A
- Authority
- CN
- China
- Prior art keywords
- babinet
- polypeptide
- drying apparatus
- driving device
- condenser pipe
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 229920001184 polypeptide Polymers 0.000 title claims abstract description 31
- 102000004196 processed proteins & peptides Human genes 0.000 title claims abstract description 31
- 108090000765 processed proteins & peptides Proteins 0.000 title claims abstract description 31
- 238000004108 freeze drying Methods 0.000 title claims abstract description 23
- 238000012360 testing method Methods 0.000 claims abstract description 19
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 13
- 230000000694 effects Effects 0.000 abstract description 13
- 238000001816 cooling Methods 0.000 abstract description 6
- 238000003912 environmental pollution Methods 0.000 abstract description 4
- 230000003631 expected effect Effects 0.000 abstract description 4
- 230000007613 environmental effect Effects 0.000 description 6
- 238000000034 method Methods 0.000 description 5
- 230000015556 catabolic process Effects 0.000 description 4
- 238000013461 design Methods 0.000 description 3
- 238000004134 energy conservation Methods 0.000 description 3
- 238000012423 maintenance Methods 0.000 description 3
- 238000004519 manufacturing process Methods 0.000 description 3
- 238000005516 engineering process Methods 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 230000015572 biosynthetic process Effects 0.000 description 1
- 238000009833 condensation Methods 0.000 description 1
- 230000005494 condensation Effects 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 235000013399 edible fruits Nutrition 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 238000001727 in vivo Methods 0.000 description 1
- 238000004064 recycling Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
Classifications
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F26—DRYING
- F26B—DRYING SOLID MATERIALS OR OBJECTS BY REMOVING LIQUID THEREFROM
- F26B5/00—Drying solid materials or objects by processes not involving the application of heat
- F26B5/04—Drying solid materials or objects by processes not involving the application of heat by evaporation or sublimation of moisture under reduced pressure, e.g. in a vacuum
- F26B5/06—Drying solid materials or objects by processes not involving the application of heat by evaporation or sublimation of moisture under reduced pressure, e.g. in a vacuum the process involving freezing
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F26—DRYING
- F26B—DRYING SOLID MATERIALS OR OBJECTS BY REMOVING LIQUID THEREFROM
- F26B25/00—Details of general application not covered by group F26B21/00 or F26B23/00
- F26B25/06—Chambers, containers, or receptacles
Landscapes
- Engineering & Computer Science (AREA)
- Mechanical Engineering (AREA)
- General Engineering & Computer Science (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Molecular Biology (AREA)
- Drying Of Solid Materials (AREA)
Abstract
The invention discloses a kind of efficient freeze-drying apparatus for polypeptide, including babinet and test tube holder, it is wound with condenser pipe on the outside of the test tube holder, one end of the condenser pipe connects outside condenser, it is connected by motor and control module between the compressor and condenser pipe, temperature control tube is arranged in the motor lower end, the temperature control tube extends at the air extractor being arranged in babinet, the air extractor includes evacuating plate, the evacuating plate is connected by the discharge port of conduit and vacuum pump, the feed inlet of the vacuum pump other end connects driving device, the driving device is also connected with circulating fan.The temperature of condenser pipe is reduced by compressor, realize the effect of polypeptide freeze-drying, it arranges in pairs or groups and uses with the air extractor of babinet lower end, when expected effect is not achieved in effect, start circulating fan and motor, it is delivered in babinet again after gas in babinet is carried out cooling down, realizes the reducing temperature twice of gas, prevent compressor recycles caused environmental pollution.
Description
Technical field
The present invention relates to chemical fields, and in particular to a kind of efficient freeze-drying apparatus for polypeptide.
Background technology
With the increasingly promotion of science and technology, there are many freeze dryers and freeze-drying apparatus at present, but these freeze-drying apparatus cannot root
It is targetedly lyophilized according to the characteristic of polypeptide, it is then very improper for polypeptide freeze-drying, while due to drop during freeze-drying
Temp effect is excessively apparent, and is not easily controlled, and can lead to polypeptide breakdown, while there is also the method for some Physical temperature-lowerings, and one
Denier cooling is not that can uniformly lead to very much the experiment of polypeptide next process, therefore urgently those skilled in the art solve this and ask
Topic.
Invention content
To solve the above problems, the invention discloses a kind of efficient freeze-drying apparatus for polypeptide, its object is to solve
The problem of polypeptide is lyophilized.
In order to reach object above, the present invention provides the following technical solutions：A kind of efficient freeze-drying apparatus for polypeptide, packet
Babinet is included, the test tube holder for holding test tube is equipped in the babinet, is wound with condenser pipe on the outside of the test tube holder, institute
One end connection outside condenser for stating condenser pipe, is connected between the compressor and condenser pipe by motor and control module, institute
Motor lower end setting temperature control tube is stated, the temperature control tube extends at the air extractor being arranged in babinet, and the air extractor includes
Evacuating plate, the evacuating plate are connected by the discharge port of conduit and vacuum pump, and the feed inlet connection of the vacuum pump other end is driven
Dynamic device, the driving device are also connected with circulating fan, are connected by circuit between the circulating fan and driving device.This sets
It is simple in structure clear to count, and is closely connected and does not influence each other between each component, required part replacement is convenient, is easy to product in the future and exists
Polypeptide can be put in test tube, then be placed in examination by the maintenance during use by the way that test tube holder is arranged in babinet
On pipe holder, the temperature of condenser pipe is reduced by compressor, is realized the effect of polypeptide freeze-drying, is taken with the air extractor of babinet lower end
With use, when expected effect is not achieved in effect, starts circulating fan and motor, the gas in babinet is cooled down
It is delivered in babinet again after cooling, realizes the reducing temperature twice of gas, prevent compressor recycles caused environmental pollution, together
When can play the role of environmental protection.
As an improvement of the present invention, pure water collection device, the pure water collection are additionally provided on the outside of the babinet
Device includes collecting box, and collecting pipe is equipped between the collecting box and babinet, and the collecting pipe uses inverted L shape collecting pipe.In case
External setting pure water collection device, can be after being lyophilized process, and the gas water resource of box house is recycled, symbol
Close the theory of energy conservation and environmental protection production.
As an improvement of the present invention, the driving device uses motor.
As an improvement of the present invention, the inside of the babinet is additionally provided with temperature sensor and humidity sensor.In case
Temperature sensor and humidity sensor are set in vivo, and the temperature in guard box body can reach the effect of polypeptide, be easy control
System, avoids polypeptide breakdown.
As an improvement of the present invention, the temperature sensor and the external display instrument of humidity sensor connecting box, institute
It states and is connected by circuit between display instrument and temperature sensor and humidity sensor.
The opposite and prior art, the invention has the advantages that：
1）The design structure is simply clear, is closely connected and does not influence each other between each component, and required part replacement is convenient, is easy to
Polypeptide can be put in test tube by the maintenance of product in use in the future by the setting test tube holder in babinet,
It is placed in again on test tube holder, the temperature of condenser pipe is reduced by compressor, the effect of polypeptide freeze-drying is realized, with babinet lower end
Air extractor collocation uses, and when expected effect is not achieved in effect, starts circulating fan and motor, by the gas in babinet
Body is delivered in babinet again after carrying out cooling down, realizes the reducing temperature twice of gas, prevents recycling for compressor caused
Environmental pollution, while environmental protection can be played the role of；
2）Pure water collection device is set outside the enclosure, can be after process be lyophilized, the gas water resource of box house carries out
It recycles, meets the theory of energy conservation and environmental protection production；
3）Temperature sensor and humidity sensor are set in babinet, and the temperature in guard box body can reach the freeze-drying effect of polypeptide
Fruit is easy to control, and avoids polypeptide breakdown；
4）The design scheme cost is relatively low, is convenient for the popularization and use in market.
Description of the drawings
Fig. 1 is a kind of efficient freeze-drying apparatus overall structure diagram for polypeptide of the invention；
Reference numerals list：1, babinet；2, test tube holder；3, condenser pipe；4, compressor；5, motor；6, control module；7, temperature control
Pipe；8, air extractor；801, evacuating plate；802, conduit；803, vacuum pump；9, driving device；10, circulating fan；11, pure water is received
Acquisition means；1101, collecting box；1102, collecting pipe；12, temperature sensor；13, humidity sensor；14, display instrument；15, circuit.
Specific implementation mode
In order to make technical problems, technical solutions and advantages to be solved be more clearly understood, tie below
Accompanying drawings and embodiments are closed, the present invention will be described in further detail.It should be appreciated that specific embodiment described herein is only
To explain the present invention, it is not intended to limit the present invention.
It should be noted that when element is referred to as " being fixed on " or " being set to " another element, it can be directly another
On one element or it is connected on another element.When an element is known as " being connected to " another element, it can
To be directly to another element or be indirectly connected on another element.
It is to be appreciated that term " length ", " width ", "upper", "lower", "front", "rear", "left", "right", "vertical",
The orientation or positional relationship of the instructions such as "horizontal", "top", "bottom" "inner", "outside" is that orientation based on ... shown in the drawings or position are closed
System, is merely for convenience of description of the present invention and simplification of the description, not indicating or implying the indicated device or element must have
Specific orientation, with specific azimuth configuration and operation, therefore be not considered as limiting the invention.
In addition, term " first ", " second " are used for description purposes only, it is not understood to indicate or imply relative importance
Or implicitly indicate the quantity of indicated technical characteristic.Define " first " as a result, the feature of " second " can be expressed or
Implicitly include one or more this feature.In the description of the present invention, the meaning of " plurality " is two or more,
Unless otherwise specifically defined.
Embodiment 1：Referring to Fig. 1, now a kind of efficient freeze-drying apparatus for polypeptide provided by the invention is illustrated, is wrapped
Babinet 1 is included, the test tube holder 2 for holding test tube is equipped in the babinet 1, the outside of the test tube holder 2 is wound with condensation
One end of pipe 3, the condenser pipe 3 connects outside condenser 4, passes through motor 5 and control between the compressor 4 and condenser pipe 3
Module 6 connects, and temperature control tube 7 is arranged in 5 lower end of the motor, and the temperature control tube 7 extends at the air extractor 8 being arranged in babinet 1,
The air extractor 8 includes evacuating plate 801, and the evacuating plate 801 is connect by conduit 802 with the discharge port of vacuum pump 803, institute
The feed inlet connection driving device 9 of 803 other end of vacuum pump is stated, the driving device 9 is also connected with circulating fan 10, the cycle
It is connected by circuit 15 between wind turbine 10 and driving device 9.The design structure is simply clear, is closely connected between each component and not
It influences each other, required part replacement is convenient, is easy to the maintenance of product in use in the future, by being arranged in babinet
Polypeptide can be put in test tube by test tube holder, then be placed on test tube holder, and the temperature of condenser pipe is reduced by compressor,
The effect for realizing polypeptide freeze-drying is arranged in pairs or groups with the air extractor of babinet lower end and is used, when expected effect is not achieved in effect,
Start circulating fan and motor, is delivered in babinet again after the gas in babinet is carried out cooling down, realizes the secondary of gas
Cooling, prevents the caused environmental pollution that recycles of compressor, while can play the role of environmental protection；It is set in babinet
Temperature control tube is set, temperature control tube can be controlled by control module, then achieve effective control babinet temperature when too high or too low for temperature
The effect of degree.
Embodiment 2：Referring to Fig. 1, as an improvement of the present invention, the outside of the babinet 1 is additionally provided with pure water collection
Device 11, the pure water collection device 11 include collecting box 1101, and collecting pipe is equipped between the collecting box 1101 and babinet 1
1102, the collecting pipe 1102 uses inverted L shape collecting pipe.Pure water collection device is set outside the enclosure, it can be in freeze-drying process knot
The gas water resource of Shu Hou, box house are recycled, and meet the theory of energy conservation and environmental protection production.
Embodiment 3：Referring to Fig. 1, as an improvement of the present invention, the driving device 9 uses motor.
Embodiment 4：Referring to Fig. 1, as an improvement of the present invention, the inside of the babinet 1 is additionally provided with temperature sensor
12 with humidity sensor 13.Temperature sensor and humidity sensor are set in babinet, and the temperature in guard box body can reach
The effect of polypeptide, is easy to control, and avoids polypeptide breakdown.
Embodiment 5：Referring to Fig. 1, as an improvement of the present invention, the temperature sensor 12 connects with humidity sensor 13
The display instrument 14 outside babinet 1 is connect, is connected by circuit between the display instrument 14 and temperature sensor 12 and humidity sensor 13.
At least one of embodiment 2,3,4,5 technical characteristics can also be combined formation by the present invention with embodiment 1
New embodiment.
Humidity sensor, temperature sensor and display instrument are the prior arts, the logic judgment of itself and execution function
Belong to the prior art, be not the innovative point of the present invention, the present invention is only made as the module that hardware connects
With and the direct connection relation of other components be only the inventive point to be protected of the invention.
The technical means disclosed in the embodiments of the present invention is not limited only to the technological means disclosed in the above embodiment, further includes
By the above technical characteristic arbitrarily the formed technical solution of combination.It should be pointed out that for those skilled in the art
For, various improvements and modifications may be made without departing from the principle of the present invention, these improvements and modifications are also considered as
Protection scope of the present invention.
Claims (5)
1. a kind of efficient freeze-drying apparatus for polypeptide, including babinet, it is characterised in that：It is equipped in the babinet for holding examination
The test tube holder of pipe, condenser pipe is wound on the outside of the test tube holder, and one end of the condenser pipe connects outside condenser, institute
It states and is connected by motor and control module between compressor and condenser pipe, temperature control tube, the temperature control tube is arranged in the motor lower end
It extends at the air extractor being arranged in babinet, the air extractor includes evacuating plate, and the evacuating plate passes through conduit and vacuum
The discharge port of pump connects, and the feed inlet of the vacuum pump other end connects driving device, and the driving device is also connected with circulated air
Machine is connected between the circulating fan and driving device by circuit.
2. a kind of efficient freeze-drying apparatus for polypeptide according to claim 1, it is characterised in that：The outside of the babinet
It is additionally provided with pure water collection device, the pure water collection device includes collecting box, is equipped with and collects between the collecting box and babinet
Pipe, the collecting pipe use inverted L shape collecting pipe.
3. a kind of efficient freeze-drying apparatus for polypeptide according to claim 1, it is characterised in that：The driving device is adopted
Use motor.
4. a kind of efficient freeze-drying apparatus for polypeptide according to claim 3, it is characterised in that：The inside of the babinet
It is additionally provided with temperature sensor and humidity sensor.
5. a kind of efficient freeze-drying apparatus for polypeptide according to claim 4, it is characterised in that：The temperature sensor
The external display instrument with humidity sensor connecting box, passes through circuit between the display instrument and temperature sensor and humidity sensor
Connection.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810634599.2A CN108716818A (en) | 2018-06-20 | 2018-06-20 | A kind of efficient freeze-drying apparatus for polypeptide |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810634599.2A CN108716818A (en) | 2018-06-20 | 2018-06-20 | A kind of efficient freeze-drying apparatus for polypeptide |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN108716818A true CN108716818A (en) | 2018-10-30 |
Family
ID=63913349
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201810634599.2A Pending CN108716818A (en) | 2018-06-20 | 2018-06-20 | A kind of efficient freeze-drying apparatus for polypeptide |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN108716818A (en) |
Citations (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20050155373A1 (en) * | 2002-09-10 | 2005-07-21 | Tokyo Electron Limited | Processing apparatus and processing apparatus maintenance method |
| CN2888374Y (en) * | 2006-01-17 | 2007-04-11 | 上海东富龙科技有限公司 | Vacuum refrigerating drying machine |
| CN204043318U (en) * | 2014-09-04 | 2014-12-24 | 苏州禾川化学技术服务有限公司 | A kind of baking oven automatically |
| CN204923696U (en) * | 2015-08-28 | 2015-12-30 | 合肥国肽生物科技有限公司 | Be used for quick freeze -drying device of polypeptide |
| CN205747691U (en) * | 2016-05-27 | 2016-11-30 | 江苏博莱客冷冻科技发展有限公司 | Energy-conservation radiation freeze-drier |
| CN106871583A (en) * | 2017-03-30 | 2017-06-20 | 北京科技大学 | Heat-pump-type vacuum refrigeration hot air convection joint food medicinal material dryer |
| CN207035701U (en) * | 2017-06-05 | 2018-02-23 | 天津禹王生物医药科技有限公司 | A kind of vacuum freeze drier |
| US20180120026A1 (en) * | 2016-11-01 | 2018-05-03 | Steven Finley | Methods for measuring pressure in freeze drying systems |
| CN208567313U (en) * | 2018-06-20 | 2019-03-01 | 南京肽业生物科技有限公司 | A kind of efficient freeze-drying apparatus for polypeptide |
-
2018
- 2018-06-20 CN CN201810634599.2A patent/CN108716818A/en active Pending
Patent Citations (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20050155373A1 (en) * | 2002-09-10 | 2005-07-21 | Tokyo Electron Limited | Processing apparatus and processing apparatus maintenance method |
| CN2888374Y (en) * | 2006-01-17 | 2007-04-11 | 上海东富龙科技有限公司 | Vacuum refrigerating drying machine |
| CN204043318U (en) * | 2014-09-04 | 2014-12-24 | 苏州禾川化学技术服务有限公司 | A kind of baking oven automatically |
| CN204923696U (en) * | 2015-08-28 | 2015-12-30 | 合肥国肽生物科技有限公司 | Be used for quick freeze -drying device of polypeptide |
| CN205747691U (en) * | 2016-05-27 | 2016-11-30 | 江苏博莱客冷冻科技发展有限公司 | Energy-conservation radiation freeze-drier |
| US20180120026A1 (en) * | 2016-11-01 | 2018-05-03 | Steven Finley | Methods for measuring pressure in freeze drying systems |
| CN106871583A (en) * | 2017-03-30 | 2017-06-20 | 北京科技大学 | Heat-pump-type vacuum refrigeration hot air convection joint food medicinal material dryer |
| CN207035701U (en) * | 2017-06-05 | 2018-02-23 | 天津禹王生物医药科技有限公司 | A kind of vacuum freeze drier |
| CN208567313U (en) * | 2018-06-20 | 2019-03-01 | 南京肽业生物科技有限公司 | A kind of efficient freeze-drying apparatus for polypeptide |
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