CN108707430A - A kind of white sand adhesive waterproof coil and preparation method thereof - Google Patents

A kind of white sand adhesive waterproof coil and preparation method thereof Download PDF

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Publication number
CN108707430A
CN108707430A CN201810314027.6A CN201810314027A CN108707430A CN 108707430 A CN108707430 A CN 108707430A CN 201810314027 A CN201810314027 A CN 201810314027A CN 108707430 A CN108707430 A CN 108707430A
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CN
China
Prior art keywords
white sand
adhesive waterproof
waterproof coil
mixture
tackifier
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Pending
Application number
CN201810314027.6A
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Chinese (zh)
Inventor
吴红华
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Individual
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Individual
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Priority to CN201810314027.6A priority Critical patent/CN108707430A/en
Publication of CN108707430A publication Critical patent/CN108707430A/en
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    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
    • C09J7/00—Adhesives in the form of films or foils
    • C09J7/20—Adhesives in the form of films or foils characterised by their carriers
    • C09J7/21—Paper; Textile fabrics
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D195/00—Coating compositions based on bituminous materials, e.g. asphalt, tar, pitch
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
    • C09D7/40—Additives
    • C09D7/60—Additives non-macromolecular
    • C09D7/61—Additives non-macromolecular inorganic
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
    • C09D7/40—Additives
    • C09D7/65—Additives macromolecular
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2201/00—Properties
    • C08L2201/08—Stabilised against heat, light or radiation or oxydation
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2205/00—Polymer mixtures characterised by other features
    • C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
    • C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
    • C09J2301/00—Additional features of adhesives in the form of films or foils
    • C09J2301/30—Additional features of adhesives in the form of films or foils characterized by the chemical, physicochemical or physical properties of the adhesive or the carrier
    • C09J2301/312—Additional features of adhesives in the form of films or foils characterized by the chemical, physicochemical or physical properties of the adhesive or the carrier parameters being the characterizing feature
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
    • C09J2400/00—Presence of inorganic and organic materials
    • C09J2400/10—Presence of inorganic materials
    • C09J2400/14—Glass
    • C09J2400/143—Glass in the substrate
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
    • C09J2400/00—Presence of inorganic and organic materials
    • C09J2400/20—Presence of organic materials
    • C09J2400/26—Presence of textile or fabric
    • C09J2400/263—Presence of textile or fabric in the substrate
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
    • C09J2467/00—Presence of polyester
    • C09J2467/006—Presence of polyester in the substrate

Abstract

A kind of white sand adhesive waterproof coil and preparation method thereof, one Hermetical stirring tank is heated to 160 ~ 200 DEG C, then pitch is added into the Hermetical stirring tank, rubber oil is added to stir 10 ~ 20 minutes, then the temperature of the inner cavity of the Hermetical stirring tank is adjusted to 160 ~ 180 DEG C, add sbR, stirring 40 ~ after sixty minutes, temperature is adjusted to 180 ~ 200 DEG C, it is subsequently added into rubber powder and tackifier, stirring obtains mixture in 3 ~ 4 hours, it is added after being ground to the mixture using colloid mill to an auger tank, put into mountain flour, under the conditions of 160 ~ 180 DEG C, it is mixed 1 ~ 1.5 hour, up to semi-finished product mixture；The semi-finished product mixture is coated in the both side surface of base material, then a side surface coats adhesives, and another side surface applies white sand, up to white sand adhesive waterproof coil after cooling molding.Product produced by the present invention has good self-adhesion and bending property, and ageing-resistant, 70-90 DEG C of high temperature, low temperature -0 ~ -20 DEG C degree is easy construction, pollution-free.

Description

A kind of white sand adhesive waterproof coil and preparation method thereof
Technical field
The invention belongs to technical field of polymer materials, and in particular to a kind of white sand adhesive waterproof coil and its preparation side Method.
Background technology
Self-adhesion SBS modified pitch Shamian Island water-proof coiled material products are mixed with raw material such as pitches, and tank body is mixed It is to be heated to 230 DEG C -250 DEG C of temperature with boiler to carry out heat conducting oil pipe circulating-heating, is heated to 160 DEG C of -200 DEG C of degree Proportionally the raw material such as input pitch carry out whip modified mixing in 3 hours under the high temperature conditions.
The raw material that mix carry out colloid mill grinding, and grinding makes raw material mixed performance uniform again, after grinding by Bitumenpump squeezes into stirred autoclave, then talcum powder is added to reaction kettle and is stirred mixing, the time at 1-2 hours, temperature It at 180 DEG C -200 DEG C, is stirred as qualified dip-coating material, there is bitumenpump to squeeze into coil production line painting oil sump and use oiling, Oiling uses polyester felt or glass fibrofelt for carcass, lower surface apply 3 mm of thickness mixtures being modified, be covered with again silicone oil every From membrane material, upper surface applies 3-6 millimeters of yellow sands of last layer, shapes, and cools down after setting is good, cooling is by traction cooling Become self-adhesion yellow sand face waterproof roll after roller molding.
The shortcomings that existing self-adhesion SBS modified pitch Shamian Island water-proof coiled material product is that Cohesion reliability stability is uneven.
Invention content
Present invention aims at a kind of white sand adhesive waterproof coils of offer and preparation method thereof.
To achieve the above object, technical solution provided by the invention is：A kind of white sand adhesive waterproof coil, the white sand self-adhesion The surface of the base material of waterproof roll is coated with mixture, the material of salt and spice ratio containing following masses：
Pitch 45 ~ 55%；
Rubber oil 10 ~ 15%；
Butadiene-styrene rubber 3 ~ 6%；
Rubber powder 11 ~ 42%；
Tackifier 2 ~ 5%；
Mountain flour 11 ~ 18%.
Preferably technical solution is：The tackifier are selected from rosin, rosin, terpene resin, C5 Petropols.
To achieve the above object, technical solution provided by the invention is：A kind of preparation method of white sand adhesive waterproof coil, The material of salt and spice ratio containing following masses：
Pitch 45 ~ 55%；
Rubber oil 10 ~ 15%；
Butadiene-styrene rubber 3 ~ 6%；
Rubber powder 11 ~ 42%；
Tackifier 2 ~ 5%；
Mountain flour 11 ~ 18%；
Preparation method includes：One Hermetical stirring tank is heated to 160 ~ 200 DEG C, is then added into the Hermetical stirring tank Pitch adds rubber oil and stirs 10 ~ 20 minutes, the temperature of the inner cavity of the Hermetical stirring tank is then adjusted to 160 ~ 180 DEG C, add sbR, stirring 40 ~ after sixty minutes, temperature is adjusted to 180 ~ 200 DEG C, is subsequently added into rubber powder and tackifier, stirring 3 ~ 4 Hour obtains mixture, is added after being ground to the mixture using colloid mill to an auger tank, throws Enter mountain flour, under the conditions of 160 ~ 180 DEG C, is mixed 1 ~ 1.5 hour to get semi-finished product mixture；The semi-finished product are mixed Material is coated in the both side surface of base material, and then a side surface coats adhesives, and another side surface applies white sand, after cooling molding Up to white sand adhesive waterproof coil.
Preferably technical solution is：The tackifier are selected from rosin, rosin, terpene resin, C5 Petropols.
Since above-mentioned technical proposal is used, the present invention this have the advantage that compared with prior art：
Product produced by the present invention have good self-adhesion and bending property, ageing-resistant, 70-90 DEG C of high temperature, low temperature -0 ~ - 20 DEG C of degree, it is easy construction, pollution-free.
Specific implementation mode
Illustrate that embodiments of the present invention, those skilled in the art can be by this explanations by particular specific embodiment below Content disclosed by book understands other advantages and effect of the present invention easily.
Embodiment 1：A kind of white sand adhesive waterproof coil and preparation method thereof
A kind of preparation method of white sand adhesive waterproof coil, the material of salt and spice ratio containing following masses：
Pitch 45%；
Rubber oil 15%；
Butadiene-styrene rubber 6%；
Rubber powder 19%；
Tackifier 3%；
Mountain flour 12%.
The tackifier are selected as terpene resin.
Preparation method includes：One Hermetical stirring tank is heated to 160 DEG C, is then added into the Hermetical stirring tank Pitch adds rubber oil and stirs 20 minutes, the temperature of the inner cavity of the Hermetical stirring tank is then adjusted to 180 DEG C, then add Entering sbR, temperature after sixty minutes, is adjusted to 200 DEG C by stirring, is subsequently added into rubber powder and tackifier, and stirring obtains mixture in 3 hours, It is added after being ground to the mixture using colloid mill to an auger tank, mountain flour is put into, in 170 DEG C of items Under part, 1 hour is mixed to get semi-finished product mixture；The semi-finished product mixture is coated in the both side surface of base material, so Latter side surface coats adhesives, and another side surface applies white sand, up to white sand adhesive waterproof coil after cooling molding.Half at When product mixture coats：Semi-finished product mixture is first flowed into coil production line and applies oil sump using oiling, using polyester felt or glass Dimension felt is carcass, and upper and lower surface applies the semi-finished product mixture being modified, adjusts thickness appropriate, bottom surface according to oiling and immersion oil Coated with tack mixture, upper surface applies white sand, is molded into coiled material carrying out chilling roll cooling, coiled material cutting is special being subject to Cutting is carried out as the coiled material of 50 centimeters of wide cut with equipment.
Embodiment 2：A kind of white sand adhesive waterproof coil and preparation method thereof
A kind of preparation method of white sand adhesive waterproof coil, the material of salt and spice ratio containing following masses：
Pitch 50%；
Rubber oil 12%；
Butadiene-styrene rubber 4%；
Rubber powder 20%；
Tackifier 3%；
Mountain flour 11%；
The tackifier are by rosin and terpene resin according to 1：It is formed after 1 mass ratio mixing.
Preparation method includes：One Hermetical stirring tank is heated to 180 DEG C, is then added into the Hermetical stirring tank Pitch adds rubber oil and stirs 15 minutes, the temperature of the inner cavity of the Hermetical stirring tank is then adjusted to 170 DEG C, then add Entering sbR, after stirring 50 minutes, temperature is adjusted to 190 DEG C, is subsequently added into rubber powder and tackifier, stirring obtains mixture in 3 hours, It is added after being ground to the mixture using colloid mill to an auger tank, mountain flour is put into, in 170 DEG C of items Under part, 1.5 hours are mixed to get semi-finished product mixture；The semi-finished product mixture is coated in the both side surface of base material, Then a side surface coats adhesives, and another side surface applies white sand, up to white sand adhesive waterproof coil after cooling molding.Half When finished product mixture coats：Semi-finished product mixture is first flowed into coil production line and applies oil sump using oiling, using polyester felt or glass Fibrofelt is carcass, and upper and lower surface applies the semi-finished product mixture being modified, adjusts thickness appropriate, bottom according to oiling and immersion oil Face applies white sand coated with tack mixture, upper surface, is molded into coiled material carrying out chilling roll cooling, is being subject to coiled material cutting Special equipment carries out cutting as the coiled material of 50 centimeters of wide cut.
Embodiment 3：A kind of white sand adhesive waterproof coil and preparation method thereof
A kind of preparation method of white sand adhesive waterproof coil, the material of salt and spice ratio containing following masses：
Pitch 55%；
Rubber oil 10%；
Butadiene-styrene rubber 3%；
Rubber powder 12%；
Tackifier 2%；
Mountain flour 18%；
The tackifier are selected as terpene resin
Preparation method includes：One Hermetical stirring tank is heated to 200 DEG C, drip is then added into the Hermetical stirring tank Blueness adds rubber oil and stirs 10 minutes, the temperature of the inner cavity of the Hermetical stirring tank is then adjusted to 180 DEG C, is added Temperature after forty minutes, is adjusted to 200 DEG C by sbR, stirring, is subsequently added into rubber powder and tackifier, and stirring obtains mixture in 3 hours, adopts It is added after being ground to the mixture with colloid mill to an auger tank, mountain flour is put into, in 180 DEG C of conditions Under, 1 hour is mixed to get semi-finished product mixture；The semi-finished product mixture is coated in the both side surface of base material, then One side surface coats adhesives, and another side surface applies white sand, up to white sand adhesive waterproof coil after cooling molding.Semi-finished product When mixture coats：Semi-finished product mixture is first flowed into coil production line and applies oil sump using oiling, is tieed up using polyester felt or glass Felt is carcass, and upper and lower surface applies the semi-finished product mixture being modified, adjusts thickness appropriate according to oiling and immersion oil, and bottom surface is covered With tack mixture, upper surface applies white sand, is molded into coiled material carrying out chilling roll cooling, coiled material cutting is special being subject to Equipment carries out cutting as the coiled material of 50 centimeters of wide cut.
The above-described embodiments merely illustrate the principles and effects of the present invention, and is not intended to limit the present invention.It is any ripe The personage for knowing this technology can all carry out modifications and changes to above-described embodiment without violating the spirit and scope of the present invention.Cause This, institute is complete without departing from the spirit and technical ideas disclosed in the present invention by those of ordinary skill in the art such as At all equivalent modifications or change, should by the present invention claim be covered.

Claims (4)

1. the surface of a kind of white sand adhesive waterproof coil, the base material of the white sand adhesive waterproof coil is coated with mixture, feature It is：The material of salt and spice ratio containing following masses：
Pitch 45 ~ 55%；
Rubber oil 10 ~ 15%；
Butadiene-styrene rubber 3 ~ 6%；
Rubber powder 11 ~ 42%；
Tackifier 2 ~ 5%；
Mountain flour 11 ~ 18%.
2. white sand adhesive waterproof coil according to claim 1, it is characterised in that：The tackifier are selected from rosin, rosin Fat, terpene resin, C5 Petropols.
3. a kind of preparation method of white sand adhesive waterproof coil, it is characterised in that：Salt and spice ratio containing following masses Material：
Pitch 45 ~ 55%；
Rubber oil 10 ~ 15%；
Butadiene-styrene rubber 3 ~ 6%；
Rubber powder 11 ~ 42%；
Tackifier 2 ~ 5%；
Mountain flour 11 ~ 18%；
Preparation method includes：One Hermetical stirring tank is heated to 160 ~ 200 DEG C, is then added into the Hermetical stirring tank Pitch adds rubber oil and stirs 10 ~ 20 minutes, the temperature of the inner cavity of the Hermetical stirring tank is then adjusted to 160 ~ 180 DEG C, add sbR, stirring 40 ~ after sixty minutes, temperature is adjusted to 180 ~ 200 DEG C, is subsequently added into rubber powder and tackifier, stirring 3 ~ 4 Hour obtains mixture, is added after being ground to the mixture using colloid mill to an auger tank, throws Enter mountain flour, under the conditions of 160 ~ 180 DEG C, is mixed 1 ~ 1.5 hour to get semi-finished product mixture；The semi-finished product are mixed Material is coated in the both side surface of base material, and then a side surface coats adhesives, and another side surface applies white sand, after cooling molding Up to white sand adhesive waterproof coil.
4. the preparation method of white sand adhesive waterproof coil according to claim 1, it is characterised in that：The tackifier are selected from Rosin, rosin, terpene resin, C5 Petropols.
CN201810314027.6A 2018-04-10 2018-04-10 A kind of white sand adhesive waterproof coil and preparation method thereof Pending CN108707430A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201810314027.6A CN108707430A (en) 2018-04-10 2018-04-10 A kind of white sand adhesive waterproof coil and preparation method thereof

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201810314027.6A CN108707430A (en) 2018-04-10 2018-04-10 A kind of white sand adhesive waterproof coil and preparation method thereof

Publications (1)

Publication Number Publication Date
CN108707430A true CN108707430A (en) 2018-10-26

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CN201810314027.6A Pending CN108707430A (en) 2018-04-10 2018-04-10 A kind of white sand adhesive waterproof coil and preparation method thereof

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110872433A (en) * 2019-12-04 2020-03-10 泰安乐邦环保科技有限公司 Waterproof coiled material prepared from coating waste residues and preparation method thereof
CN116218239A (en) * 2022-12-06 2023-06-06 渭南科顺新型材料有限公司 Environment-friendly self-adhesive modified asphalt waterproof coiled material and manufacturing method thereof

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102559135A (en) * 2012-02-09 2012-07-11 深圳市卓宝科技股份有限公司 Asphalt self-adhesive and high-polymer self-adhesion rubber waterproof coiled material prepared from asphalt self-adhesive
CN104057668A (en) * 2014-06-11 2014-09-24 胜利油田大明新型建筑防水材料有限责任公司 Preparation method for self-adhesive modified asphalt waterproof coiled material with cement reactivity
KR101757190B1 (en) * 2016-12-15 2017-07-27 (주)리뉴시스템 A Production Method Of Rubberized Asphalt Waterproofing Material With High Viscosity And Self-adhesiveness

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102559135A (en) * 2012-02-09 2012-07-11 深圳市卓宝科技股份有限公司 Asphalt self-adhesive and high-polymer self-adhesion rubber waterproof coiled material prepared from asphalt self-adhesive
CN104057668A (en) * 2014-06-11 2014-09-24 胜利油田大明新型建筑防水材料有限责任公司 Preparation method for self-adhesive modified asphalt waterproof coiled material with cement reactivity
KR101757190B1 (en) * 2016-12-15 2017-07-27 (주)리뉴시스템 A Production Method Of Rubberized Asphalt Waterproofing Material With High Viscosity And Self-adhesiveness

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* Cited by examiner, † Cited by third party
Title
张能武 等: "《材料员岗位技能必读》", 30 April 2014, 湖南科学技术出版社 *

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110872433A (en) * 2019-12-04 2020-03-10 泰安乐邦环保科技有限公司 Waterproof coiled material prepared from coating waste residues and preparation method thereof
CN116218239A (en) * 2022-12-06 2023-06-06 渭南科顺新型材料有限公司 Environment-friendly self-adhesive modified asphalt waterproof coiled material and manufacturing method thereof

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Application publication date: 20181026