CN108693020A - A kind of padded coaming expansive force and saturation test method - Google Patents

A kind of padded coaming expansive force and saturation test method Download PDF

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Publication number
CN108693020A
CN108693020A CN201710223918.6A CN201710223918A CN108693020A CN 108693020 A CN108693020 A CN 108693020A CN 201710223918 A CN201710223918 A CN 201710223918A CN 108693020 A CN108693020 A CN 108693020A
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Prior art keywords
expansive force
sample
test
water
experiment
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CN201710223918.6A
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刘月妙
谢敬礼
曹胜飞
高玉峰
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Beijing Research Institute of Uranium Geology
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Beijing Research Institute of Uranium Geology
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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N3/00Investigating strength properties of solid materials by application of mechanical stress
    • G01N3/02Details
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N15/00Investigating characteristics of particles; Investigating permeability, pore-volume or surface-area of porous materials
    • G01N15/08Investigating permeability, pore-volume, or surface area of porous materials
    • G01N15/0806Details, e.g. sample holders, mounting samples for testing
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N3/00Investigating strength properties of solid materials by application of mechanical stress
    • G01N3/08Investigating strength properties of solid materials by application of mechanical stress by applying steady tensile or compressive forces
    • G01N3/18Performing tests at high or low temperatures

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  • Chemical & Material Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Biochemistry (AREA)
  • Physics & Mathematics (AREA)
  • General Physics & Mathematics (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Dispersion Chemistry (AREA)
  • Investigation Of Foundation Soil And Reinforcement Of Foundation Soil By Compacting Or Drainage (AREA)
  • Investigating Strength Of Materials By Application Of Mechanical Stress (AREA)

Abstract

The invention belongs to the expansion of high-level waste geology treatment padded coaming and permeability test research fields, and in particular to a kind of padded coaming expansive force and saturation experimental rig and method;The purpose of the present invention is, for prior art deficiency, a kind of bentonitic expansion of acquisition padded coaming and permeance property parameter are provided, a kind of padded coaming expansive force and saturation test method that parameter foundation is provided are designed for Deep Geological Disposal of High-level Radioactive Wastes library and engineering barrier;The beneficial effects of the invention are as follows:(1) bentonitic expansive force measures under the conditions of capable of realizing constant volume;(2) expansive force of sample and permeance property test under different temperatures and exhaust conditions may be implemented;(3) expansive force and saturation permeability coefficient can be carried out simultaneously to same sample to test, easy to operate, measure convenient, test result precision is high.

Description

A kind of padded coaming expansive force and saturation test method
Technical field
The invention belongs to the expansion of high-level waste geology treatment padded coaming and permeability test research fields, and in particular to a kind of Padded coaming expansive force and saturation test method.
Background technology
Important component of the padded coaming as multibarrier system in disposition library, plays engineering barrier and hydraulics screen The effect of barrier.In high level radioactive waste repository, the bentonite as padded coaming should be closed between disposition library country rock and dedicated waste tanks Gap and near field country rock crack, alleviate effect of the pressure from surrounding rock to dedicated waste tanks in stratum again, therefore both needed certain Expansive force need to have certain dilatancy ability again, it is necessary to the bentonitic expansion character of padded coaming is ground Study carefully.
Underground water is the load that the principal element for causing dedicated waste tanks to corrode and high-level waste are leaked to disposition library free surrounding space Body.Padded coaming plays the weight of hydraulics barrier as last road artificial barrier being filled between dedicated waste tanks and geologic body Act on, prevent underground water (corrosive deposit may be contained) flow to dedicated waste tanks surface, while prevent dedicated waste tanks water soluble compounds and In Nuclides Leakage to country rock, it is therefore necessary to grasp the bentonitic Penetration Signature of padded coaming.
Expansive force is that the soil body fully absorbs water in the case where not allowing lateral deformation, its holding is made not occur vertically to expand required apply Maximum pressure value.I.e. expansive force is the maximum internal stress that soil body sample is generated in constancy of volume due to water swelling.It is swollen It is measured there are mainly three types of bentonitic expansive force test methods in expansive force experiment, is free wxpansion-compression test method, load respectively Expansion-compression test method(s) and constant volume test method(s), experimental measured result and theory analysis, constant volume test method(s) measure Expansive force is more moderate.
Padded coaming is a kind of unsaturated soil with high-expansion, and permeance property generally refers to unsaturation permeability It can be with saturation performance.In high level radioactive waste repository operational process, the padded coaming starting stage is in unsaturated state, if Reach saturation after dry year.For the padded coaming of low osmotic medium, using its infiltration of conventional soil test normative testing Coefficient, time-consuming, low precision, it is difficult to meet testing requirement.
The present invention is directed to the padded coaming bentonite of highly expanded and low osmotic medium, is oozed using the high-temperature expansion of independent research The saturating instrument testing equipment (patent No.:ZL200920154214.9), establish a kind of while expansive force and saturation can be measured The test method of coefficient.
Invention content
The object of the present invention is in view of the shortcomings of the prior art, provide that a kind of acquisitions padded coaming is bentonitic to be expanded and ooze Saturating performance parameter, for Deep Geological Disposal of High-level Radioactive Wastes library and engineering barrier design provide parameter foundation a kind of padded coaming expansion Power and saturation test method.
The technical scheme is that:
A kind of padded coaming expansive force and saturation test method, include the following steps:
Step 1, sample preparation
Step 1.1 is calculated and is weighed the bentonite of corrresponding quality by parameters such as scheduled dry density and volumes, poured into compacting Mold;
Step 1.2 prepares test specimen using uniaxial static(al) pressing mode, at the same measure the quality of test specimen, height and Diameter calculates the true dry density of test specimen;
Step 2, sample installation
Permeable stone is placed in the groove of balancing gate pit by step 2.1, is sequentially placed test specimen and permeable stone;
Pressure sensor and balancing gate pit are fastenedly connected by step 2.2, are integrally put into experiment casing;
The inlet tube and outlet tube in each channel is connected on the corresponding water-in and water-out pipe fitting in balancing gate pit by step 2.3.
Step 3, sample test
Step 3.1 opens data collecting system, all test parameters of start recording in advance;
Step 3.2 sets experiment casing to room temperature environment, opens loading device, and setting intake pressure is 0.01MPa, note Expansive force versus time curve is recorded, when expansive force remains unchanged in 24 hours, the expansive force recorded at this time is the sample Maximum swelling power;
After step 3.3 reaches maximum swelling power, setting intake pressure is 1MPa and keeps pressure stability, proceeds by saturation Permeability test opens water outlet measuring equipment, while recording the water-in and water-out pressure and water of sample, after water yield stabilization, foundation Darcy's law calculates its infiltration coefficient;
Similarly, the temperature of experiment casing can be arranged, testing experiment sample is not after expansive force changes and stablizes in step 3.4 Expansive force under the conditions of synthermal;Also the temperature of experiment casing can be set, and measuring and calculation test specimen exists after water yield stabilization Saturation permeability coefficient under condition of different temperatures;
After step 3.5 is to be tested, dismantling experiment, the microstructure change of the front and back sample of analysis experiment.
The beneficial effects of the invention are as follows:
(1) a kind of padded coaming expansive force of the invention and saturation test method, under the conditions of capable of realizing constant volume Bentonitic expansive force measures;
(2) a kind of padded coaming expansive force of the invention and saturation test method, may be implemented different temperatures and row The expansive force of sample and permeance property test under the conditions of gas;
(3) a kind of padded coaming expansive force of the invention and saturation test method, can carry out same sample simultaneously Expansive force and saturation permeability coefficient test, easy to operate, measure convenient, test result precision is high.
Description of the drawings
Fig. 1 is a kind of padded coaming expansive force and the test device schematic diagram of saturation test method.
In figure:1- loading devices, 2- permeable stones, 3- test specimens, the balancing gate pits 4-, 5- sensors, 6- experiment casings, 7- go out Water measuring equipment.
Specific implementation mode
The present invention is further introduced with embodiment below in conjunction with the accompanying drawings:
A kind of padded coaming expansive force and saturation test method, include the following steps:
Step 1, sample preparation
Step 1.1 is calculated and is weighed the bentonite of corrresponding quality by parameters such as scheduled dry density and volumes, poured into compacting Mold;
Step 1.2 prepares test specimen 3 using uniaxial static(al) pressing mode, while measuring the quality of test specimen 3, height And diameter, calculate the true dry density of test specimen 3;
Step 2, sample installation
Permeable stone 2 is placed in the groove of balancing gate pit 4 by step 2.1, is sequentially placed test specimen 3 and permeable stone 2;
Pressure sensor 5 and balancing gate pit 4 are fastenedly connected by step 2.2, are integrally put into experiment casing 6;
The inlet tube and outlet tube in each channel is connected on 4 corresponding water-in and water-out pipe fitting of balancing gate pit by step 2.3.
Step 3, sample test
Step 3.1 opens data collecting system, all test parameters of start recording in advance;
Step 3.2 sets experiment casing to room temperature environment, opens loading device 1, and setting intake pressure is 0.01MPa, Expansive force versus time curve is recorded, when expansive force remains unchanged in 24 hours, the expansive force recorded at this time is the examination The maximum swelling power of sample;
After step 3.3 reaches maximum swelling power, setting intake pressure is 1MPa and keeps pressure stability, proceeds by saturation Permeability test opens water outlet measuring equipment 7, while recording the water-in and water-out pressure and water of sample, after water yield stabilization, according to Its infiltration coefficient is calculated according to Darcy's law;
Similarly, the temperature of experiment casing 6 can be arranged, testing experiment sample 3 exists after expansive force changes and stablizes in step 3.4 Expansive force under condition of different temperatures;Also can the temperature of experiment casing 6, measuring and calculation test sample be set after water yield stabilization Saturation permeability coefficient of the product 3 under condition of different temperatures;
After step 3.5 is to be tested, dismantling experiment, the microstructure change of the front and back sample of analysis experiment.
Specific embodiment:
Step 1, sample preparation
Step 1.1 presses scheduled dry density (such as 1.7g/cm3) and volume (such as Φ 50mm × 10mm) parameter, it calculates simultaneously The bentonite for weighing corrresponding quality, pours into compaction tool;
Step 1.2 prepares test specimen 3 using uniaxial static(al) pressing mode, while measuring the quality of test specimen 3, height And diameter, calculate the true dry density of test specimen 3;
Step 2, sample installation
Permeable stone 2 is placed in the groove of balancing gate pit 4 by step 2.1, is sequentially placed test specimen 3 and permeable stone 2;
Pressure sensor 5 and balancing gate pit 4 are fastenedly connected by step 2.2, are integrally put into experiment casing 6;
The inlet tube and outlet tube in each channel is connected on 4 corresponding water-in and water-out pipe fitting of balancing gate pit by step 2.3.
Step 3, sample test
Step 3.1 opens data collecting system, all test parameters of start recording in advance;
Step 3.2 sets experiment casing to room temperature environment (such as 20 DEG C), opens loading device 1, and setting intake pressure is 0.01MPa records expansive force versus time curve, when expansive force remains unchanged in 24 hours, records expansion at this time Power is the maximum swelling power of the sample;
After step 3.3 reaches maximum swelling power, setting intake pressure is 1MPa and keeps pressure stability, proceeds by saturation Permeability test opens water outlet measuring equipment 7, while recording the water-in and water-out pressure and water of sample, after water yield stabilization, according to Its infiltration coefficient is calculated according to Darcy's law;
Step 3.4 similarly, can reset the temperature (such as 30 DEG C) of experiment casing 6, test after expansive force changes and stablizes Expansive force of the test specimen 3 under the conditions of 30 DEG C, when expansive force when remaining unchanged within 24 hours, the expansive force recorded at this time is 30 Maximum swelling power under the conditions of DEG C;Meanwhile the experiment of the saturation under the conditions of 30 DEG C is proceeded by, water outlet measuring equipment 7 is opened, After water yield stabilization, its infiltration coefficient under the conditions of 30 DEG C is calculated according to Darcy's law;Can be pushed into successively with class 40 DEG C, 50 DEG C, 60 DEG C, 70 DEG C, 80 DEG C and 90 DEG C etc., can get the expansive force and infiltration coefficient under condition of different temperatures.
After step 3.5 is to be tested, dismantling experiment, the microstructure change of the front and back sample of analysis experiment.

Claims (1)

1. a kind of padded coaming expansive force and saturation test method, it is characterised in that:Include the following steps:
Step 1, sample preparation
Step 1.1 is calculated and is weighed the bentonite of corrresponding quality by parameters such as scheduled dry density and volumes, poured into compacting mould Tool;
Step 1.2 prepares test specimen (3) using uniaxial static(al) pressing mode, while measuring the quality of test specimen (3), height And diameter, calculate the true dry density of test specimen (3);
Step 2, sample installation
Permeable stone (2) is placed in the groove of balancing gate pit (4) by step 2.1, is sequentially placed test specimen (3) and permeable stone (2);
Pressure sensor (5) and balancing gate pit (4) are fastenedly connected by step 2.2, are integrally put into experiment casing (6);
The inlet tube and outlet tube in each channel is connected on the corresponding water-in and water-out pipe fitting in balancing gate pit (4) by step 2.3.
Step 3, sample test
Step 3.1 opens data collecting system, all test parameters of start recording in advance;
Step 3.2 sets experiment casing to room temperature environment, opens loading device (1), and setting intake pressure is 0.01MPa, note Expansive force versus time curve is recorded, when expansive force remains unchanged in 24 hours, the expansive force recorded at this time is the sample Maximum swelling power;
After step 3.3 reaches maximum swelling power, setting intake pressure is 1MPa and keeps pressure stability, proceeds by saturation Experiment opens water outlet measuring equipment (7), while recording the water-in and water-out pressure and water of sample, after water yield stabilization, foundation Darcy's law calculates its infiltration coefficient;
Step 3.4 similarly, can be after expansive force changes and stablizes, and the temperature of setting experiment casing (6), testing experiment sample (3) exists Expansive force under condition of different temperatures;Also can be after water yield stabilization, the temperature of setting experiment casing (6), measuring and calculation experiment Saturation permeability coefficient of the sample (3) under condition of different temperatures;
After step 3.5 is to be tested, dismantling experiment, the microstructure change of the front and back sample of analysis experiment.
CN201710223918.6A 2017-04-07 2017-04-07 A kind of padded coaming expansive force and saturation test method Pending CN108693020A (en)

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Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109655599A (en) * 2018-12-04 2019-04-19 三峡大学 A kind of bentonite inflated power of high-pressure solid-infiltration coupling test instrument and its application method
CN111610313A (en) * 2020-07-03 2020-09-01 核工业北京地质研究院 Device and method for testing combined joint healing effect of buffer material building blocks
CN111610315A (en) * 2020-07-03 2020-09-01 核工业北京地质研究院 Bentonite building block single seam healing effect testing device and method
CN111610314A (en) * 2020-07-03 2020-09-01 核工业北京地质研究院 Device and method for testing healing effect of buffer backfill material of high-level disposal warehouse
CN112036028A (en) * 2020-08-28 2020-12-04 东华理工大学 Method for evaluating disposal reservoir stability based on clay bentonite buffer backfill system homogenization model
CN113686754A (en) * 2021-09-14 2021-11-23 中国科学院武汉岩土力学研究所 Sample penetration testing method based on irradiation-stress coupling effect

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0064753A1 (en) * 1981-05-12 1982-11-17 Georg Fischer Aktiengesellschaft Sand testing apparatus
CN201408187Y (en) * 2009-05-14 2010-02-17 核工业北京地质研究院 Microcomputer-controlled high-temperature expansion and penetrability determinator
CN201945541U (en) * 2011-01-13 2011-08-24 东华理工大学 Osmosis-expansion force coupling test device for clay
CN102221600A (en) * 2011-06-03 2011-10-19 同济大学 Expansion force and saturated permeation multifunctional tester

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0064753A1 (en) * 1981-05-12 1982-11-17 Georg Fischer Aktiengesellschaft Sand testing apparatus
CN201408187Y (en) * 2009-05-14 2010-02-17 核工业北京地质研究院 Microcomputer-controlled high-temperature expansion and penetrability determinator
CN201945541U (en) * 2011-01-13 2011-08-24 东华理工大学 Osmosis-expansion force coupling test device for clay
CN102221600A (en) * 2011-06-03 2011-10-19 同济大学 Expansion force and saturated permeation multifunctional tester

Cited By (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109655599A (en) * 2018-12-04 2019-04-19 三峡大学 A kind of bentonite inflated power of high-pressure solid-infiltration coupling test instrument and its application method
CN111610313A (en) * 2020-07-03 2020-09-01 核工业北京地质研究院 Device and method for testing combined joint healing effect of buffer material building blocks
CN111610315A (en) * 2020-07-03 2020-09-01 核工业北京地质研究院 Bentonite building block single seam healing effect testing device and method
CN111610314A (en) * 2020-07-03 2020-09-01 核工业北京地质研究院 Device and method for testing healing effect of buffer backfill material of high-level disposal warehouse
CN111610314B (en) * 2020-07-03 2022-07-22 核工业北京地质研究院 Device and method for testing healing effect of buffer backfill material of high-level disposal warehouse
CN111610313B (en) * 2020-07-03 2022-07-22 核工业北京地质研究院 Buffer material building block combination joint healing effect testing device and method
CN112036028A (en) * 2020-08-28 2020-12-04 东华理工大学 Method for evaluating disposal reservoir stability based on clay bentonite buffer backfill system homogenization model
CN112036028B (en) * 2020-08-28 2023-05-09 东华理工大学 High-level waste disposal warehouse bentonite homogenization model and stability evaluation method
CN113686754A (en) * 2021-09-14 2021-11-23 中国科学院武汉岩土力学研究所 Sample penetration testing method based on irradiation-stress coupling effect

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Application publication date: 20181023