CN108689563A - A kind of sulfonation process for treating waste sludge resulted - Google Patents
A kind of sulfonation process for treating waste sludge resulted Download PDFInfo
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- CN108689563A CN108689563A CN201810856547.XA CN201810856547A CN108689563A CN 108689563 A CN108689563 A CN 108689563A CN 201810856547 A CN201810856547 A CN 201810856547A CN 108689563 A CN108689563 A CN 108689563A
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F11/00—Treatment of sludge; Devices therefor
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F11/00—Treatment of sludge; Devices therefor
- C02F11/02—Biological treatment
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F11/00—Treatment of sludge; Devices therefor
- C02F11/12—Treatment of sludge; Devices therefor by de-watering, drying or thickening
- C02F11/121—Treatment of sludge; Devices therefor by de-watering, drying or thickening by mechanical de-watering
- C02F11/122—Treatment of sludge; Devices therefor by de-watering, drying or thickening by mechanical de-watering using filter presses
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F11/00—Treatment of sludge; Devices therefor
- C02F11/12—Treatment of sludge; Devices therefor by de-watering, drying or thickening
- C02F11/14—Treatment of sludge; Devices therefor by de-watering, drying or thickening with addition of chemical agents
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F9/00—Multistage treatment of water, waste water or sewage
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/02—Treatment of water, waste water, or sewage by heating
- C02F1/04—Treatment of water, waste water, or sewage by heating by distillation or evaporation
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/24—Treatment of water, waste water, or sewage by flotation
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/40—Devices for separating or removing fatty or oily substances or similar floating material
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/44—Treatment of water, waste water, or sewage by dialysis, osmosis or reverse osmosis
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/44—Treatment of water, waste water, or sewage by dialysis, osmosis or reverse osmosis
- C02F1/441—Treatment of water, waste water, or sewage by dialysis, osmosis or reverse osmosis by reverse osmosis
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/46—Treatment of water, waste water, or sewage by electrochemical methods
- C02F1/461—Treatment of water, waste water, or sewage by electrochemical methods by electrolysis
- C02F1/463—Treatment of water, waste water, or sewage by electrochemical methods by electrolysis by electrocoagulation
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- Engineering & Computer Science (AREA)
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
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- Water Supply & Treatment (AREA)
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Abstract
The invention discloses a kind of sulfonation process for treating waste sludge resulted, include the following steps, by lignosulfonate mud after carrying out fluidized reaction;By the fine sand removal in lignosulfonate mud;After carrying out equal qualitative response in the first homogeneous tank again;It is separated by solid-liquid separation again;Isolated solid phase enters in the second homogeneous tank after progress second homogenate reaction, then carries out the liquid phase that press filtration obtains and enter in buffer storage;Liquid phase in buffer storage enters air-flotation process in micro-nano air-flotation process unit, then liquid phase enters back into high-voltage pulse electric flocculation processing unit be electrochemically reacted after;Liquid phase, which enters in double film filters, carries out double medium filtration, and filtered part clear water, which enters, is used for medicament configuration in dispensing canister, and a small amount of concentrated water for filtering generation enters in MVR vaporising devices and is evaporated crystallization.The present invention provides a kind of new technique for lignosulfonate mud processing, and technique is simplified, energy saving, treatment effeciency is high, and reaches the standard of discharge after enabling to lignosulfonate mud to handle.
Description
Technical field
The present invention relates to php slurry processing technology fields, more particularly, to a kind of sulfonation process for treating waste sludge resulted.
Background technology
Three-sulfonated mud system also becomes lignosulfonate mud system, is a kind of function admirable, the price that oil field at home generally uses
Cheap high temperature resistant type mud system is mainly used for deep drilling process when drilling depth reaches 2000-3000m or more, mesh
There is an a large amount of use in preceding oil field each at home, three-sulfonated mud system be exactly added in mud system sulfonated phenol formaldehyde resin,
The mud system that the substances such as sulfonated lignite, sulfonation tannin extract are formed.
Generated waste liquid of drilling becomes sulfonation discarded slurry, sulfonation discarded slurry to lignosulfonate mud system in use
Be mainly characterized by that water-soluble COD value is high, and coloration is big;Also contain a large amount of inorganic salts in sulfonation discarded slurry, high molecular weight
Organic compound, the heavy metal ion such as mercury, arsenic, cadmium, chromium, lead and petroleum hydrocarbon class pollutant, present sulfonation discarded slurry is all
It can not be effectively treated and reach discharge standard so that the discharge of present sulfonation discarded slurry causes local water quality, edaphic condition
It causes seriously to pollute, serious destruction is caused to local ecological environment and the ecological balance.
Invention content
For the above problem in the prior art, the present invention proposes a kind of sulfonation process for treating waste sludge resulted, solves
Sulfonation discarded slurry can not be effectively treated now, discharge standard is not achieved, water quality, edaphic condition is caused to cause serious dirt
It dye and the technical problems such as does great damage to local environment and the ecological balance.
The technical scheme is that:A kind of sulfonation process for treating waste sludge resulted, includes the following steps,
1) lignosulfonate mud is sent by grabbing device in fluidizer, by lignosulfonate mud according to 1 in fluidizer:1
~3 ratio is diluted with water, and adds suitable biological surface cleaning agent, and controlling reaction temperature is not less than 30 DEG C, fluidized reaction
15~25min;Lignosulfonate mud is first subjected to fluidized reaction, fluidized reaction can effectively go the organic pollution in lignosulfonate mud
It removes, it is best to the removal effect of organic pollution compared to microbiological treatment and other processing methods, fluidized reaction.
2) after reaction finishes, lignosulfonate mud is pumped into screening plant, the fine sand in lignosulfonate mud is removed;
By subsequent equipment damage, in addition fine sand removal in lignosulfonate mud is prevented on the one hand so that preventing fine sand by line clogging
On the one hand it is so that the effect of subsequent electrochemical reaction is more preferable, effective mitigate detaches burden so that entire technique is to sulfonation
The effect of mud conditioning is more preferable.
3) it carries out the lignosulfonate mud after desanding operation to enter in the first homogeneous tank, while adding successively in the first homogeneous tank
Enter suitable gel breaker, heavy metal chelant carries out equal qualitative response;It in this way can will be in lignosulfonate mud
4) the lignosulfonate mud that finishes of qualitative response is entered in centrifugal device and is separated by solid-liquid separation, isolated liquid phase into
Enter into buffer storage;
5) isolated solid phase enters in the second homogeneous tank, while suitable microorganism is added in the second homogeneous tank
Degradation agent carries out second homogenate reaction;Second homogenate reaction and secondary cleaning are carried out to the solid phase after separation so that separation row
The mud cake gone out not can cause environmental pollution.
6) solid phase after progress second homogenate reaction, which enters, carries out press filtration in filter-pressing device, the liquid phase that press filtration obtains enters
Into buffer storage;Liquid phase carries out precipitation caching in buffer storage, and then clear liquid is entered in micro-nano air flotation device and carried out
Air-flotation process will further ensure the clean-up performance of liquid phase in this way, not only so that subsequently more preferable to the treatment effect of liquid phase,
Follow-up precision equipment is avoided to be damaged.
7) liquid phase in buffer storage enters in the micro-nano air-flotation process unit in electric flocculation air-floating apparatus at air supporting
Reason, while a small amount of oil phase is removed by mud-scraping apparatus;Then liquid phase enter back into high-voltage pulse electric flocculation processing unit into
Row electrochemical reaction realizes the pollutant in liquid phase comprehensive decomposition and separation, the bed mud row in electric flocculation air-floating apparatus
Enter into sludge concentration tank;Liquid phase can disposably be carried out to electrolytic oxidation reaction in this way, electroreduction reacts, electrolytic flocculation is anti-
It answers, electrofloatation reaction, comprehensive separation and decomposition can be carried out to pollutant in this way,
8) liquid phase finished is reacted in electric flocculation air-floating apparatus enter in double film filters carry out double medium filtration, mistake
Part clear water after filter, which enters, is used for medicament configuration in dispensing canister, a small amount of concentrated water for filtering generation enters MVR vaporising devices
In be evaporated crystallization, the standard of environmental emission can not only be reached by handling liquid phase in this way, additionally it is possible to see the liquid phase after processing
It recycles in the art.
Further, the reaction temperature in the step 1) is 30~50 DEG C.Enable to fluidized reaction to sulfonation in this way
The treatment effect of mud is more preferable, in addition can also ensure that the energy consumption of entire process is lower in this way.
Further, the fluidized reaction time is 18~22min, while ensureing fluidization treatment effect, it is ensured that
The efficiency of fluidization treatment.
Further, the gel breaker in the step 3) is aluminium polychloride, bodied ferric sulfate or polymeric aluminium ferrum silicate
In it is one or more;
Further, the heavy metal chelant in the step 3) is xanthic acid esters or dithiocarbamates
Derivative.
Further, ceramic membrane and anti-pollution RO films are set in double film filters in the step 8).
Compared with prior art, the beneficial effects of the invention are as follows:
The present invention is optimized by the equipment to entire technological process, not only so that through the invention can be by sulphur
Change mud to be effectively treated, the liquid phase after handling can directly reach the standard of discharge, and entire technological process is opposite
More simplify, entire processing operation process is also relatively simple, and treatment effeciency is high and to the good energy-conserving effect of entire technique;Therefore,
The present invention fundamentally solves the problems, such as that lignosulfonate mud causes seriously to pollute to soil and water quality.
Description of the drawings
Fig. 1 is the process flow chart of the present invention.
Specific implementation mode
The technical solution in the present invention is further illustrated with reference to the accompanying drawings and embodiments.
Embodiment 1
1, a kind of sulfonation process for treating waste sludge resulted, which is characterized in that include the following steps,
1) lignosulfonate mud is sent by grabbing device in fluidizer 1, by lignosulfonate mud according to 1 in fluidizer 1:
1~3 ratio is diluted with water, and adds suitable biological surface cleaning agent, and controlling reaction temperature is 30 DEG C, fluidized reaction
18min;
2) after reaction finishes, lignosulfonate mud is pumped into screening plant 2, the fine sand in lignosulfonate mud is gone
It removes;
3) carry out desanding operation after lignosulfonate mud enter in the first homogeneous tank 3, while in the first homogeneous tank 3 according to
It is secondary that suitable aluminium polychloride, the equal qualitative response of sawdust cellulose xanthate progress is added;
4) lignosulfonate mud that qualitative response finishes, which enters in centrifugal device 4, is separated by solid-liquid separation, isolated liquid phase
It enters in buffer storage 7;
5) isolated solid phase enters in the second homogeneous tank 5, while suitable micro- life is added in the second homogeneous tank 5
Object degradation agent carries out second homogenate reaction;
6) solid phase after second homogenate reaction is carried out to enter and carries out press filtration in filter-pressing device 6, the liquid phase that press filtration obtains into
Enter into buffer storage 7;
7) liquid phase in buffer storage 7 enters air supporting in the micro-nano air-flotation process unit 8 in electric flocculation air-floating apparatus
Processing, while a small amount of oil phase is removed by mud-scraping apparatus;Then liquid phase enters back into high-voltage pulse electric flocculation processing unit 9
It is electrochemically reacted, comprehensive decomposition and separation, the bed mud in electric flocculation air-floating apparatus is realized to the pollutant in liquid phase
It is drained into sludge concentration tank 13;
8) liquid phase finished reacted in electric flocculation air-floating apparatus enter in double film filters 10 carry out double medium filtration,
Filtered part clear water, which enters, is used for medicament configuration in dispensing canister 12, a small amount of concentrated water for filtering generation enters MVR evaporations
Crystallization is evaporated in device 11.
Embodiment 2
1, a kind of sulfonation process for treating waste sludge resulted, which is characterized in that include the following steps,
1) lignosulfonate mud is sent by grabbing device in fluidizer 1, by lignosulfonate mud according to 1 in fluidizer 1:
1~3 ratio is diluted with water, and adds suitable biological surface cleaning agent, and controlling reaction temperature is 40 DEG C, fluidized reaction
20min;
2) after reaction finishes, lignosulfonate mud is pumped into screening plant 2, the fine sand in lignosulfonate mud is gone
It removes;
3) carry out desanding operation after lignosulfonate mud enter in the first homogeneous tank 3, while in the first homogeneous tank 3 according to
It is secondary that suitable bodied ferric sulfate, the equal qualitative response of sodium diethyldithiocarbamate progress is added;
4) lignosulfonate mud that qualitative response finishes, which enters in centrifugal device 4, is separated by solid-liquid separation, isolated liquid phase
It enters in buffer storage 7;
5) isolated solid phase enters in the second homogeneous tank 5, while suitable micro- life is added in the second homogeneous tank 5
Object degradation agent carries out second homogenate reaction;
6) solid phase after second homogenate reaction is carried out to enter and carries out press filtration in filter-pressing device 6, the liquid phase that press filtration obtains into
Enter into buffer storage 7;
7) liquid phase in buffer storage 7 enters air supporting in the micro-nano air-flotation process unit 8 in electric flocculation air-floating apparatus
Processing, while a small amount of oil phase is removed by mud-scraping apparatus;Then liquid phase enters back into high-voltage pulse electric flocculation processing unit 9
It is electrochemically reacted, comprehensive decomposition and separation, the bed mud in electric flocculation air-floating apparatus is realized to the pollutant in liquid phase
It is drained into sludge concentration tank 13;
8) liquid phase finished reacted in electric flocculation air-floating apparatus enter in double film filters 10 carry out double medium filtration,
Filtered part clear water, which enters, is used for medicament configuration in dispensing canister 12, a small amount of concentrated water for filtering generation enters MVR evaporations
Crystallization is evaporated in device 11.
Embodiment 3
1, a kind of sulfonation process for treating waste sludge resulted, which is characterized in that include the following steps,
1) lignosulfonate mud is sent by grabbing device in fluidizer 1, by lignosulfonate mud according to 1 in fluidizer 1:
1~3 ratio is diluted with water, and adds suitable biological surface cleaning agent, 50 DEG C of controlling reaction temperature position, fluidized reaction
22min;
2) after reaction finishes, lignosulfonate mud is pumped into screening plant 2, the fine sand in lignosulfonate mud is gone
It removes;
3) carry out desanding operation after lignosulfonate mud enter in the first homogeneous tank 3, while in the first homogeneous tank 3 according to
It is secondary that suitable polymeric aluminium ferrum silicate, the equal qualitative response of sodium diethyldithiocarbamate progress is added;
4) lignosulfonate mud that qualitative response finishes, which enters in centrifugal device 4, is separated by solid-liquid separation, isolated liquid phase
It enters in buffer storage 7;
5) isolated solid phase enters in the second homogeneous tank 5, while suitable micro- life is added in the second homogeneous tank 5
Object degradation agent carries out second homogenate reaction;
6) solid phase after second homogenate reaction is carried out to enter and carries out press filtration in filter-pressing device 6, the liquid phase that press filtration obtains into
Enter into buffer storage 7;
7) liquid phase in buffer storage 7 enters air supporting in the micro-nano air-flotation process unit 8 in electric flocculation air-floating apparatus
Processing, while a small amount of oil phase is removed by mud-scraping apparatus;Then liquid phase enters back into high-voltage pulse electric flocculation processing unit 9
It is electrochemically reacted, comprehensive decomposition and separation, the bed mud in electric flocculation air-floating apparatus is realized to the pollutant in liquid phase
It is drained into sludge concentration tank 13;
8) liquid phase finished reacted in electric flocculation air-floating apparatus enter in double film filters 10 carry out double medium filtration,
Filtered part clear water, which enters, is used for medicament configuration in dispensing canister 12, a small amount of concentrated water for filtering generation enters MVR evaporations
Crystallization is evaporated in device 11.
The foregoing is merely illustrative of the preferred embodiments of the present invention, is not intended to limit the invention, all essences in the present invention
With within principle, any modification, equivalent replacement, improvement and so on should all be included in the protection scope of the present invention god.
Claims (6)
1. a kind of sulfonation process for treating waste sludge resulted, which is characterized in that include the following steps,
1) lignosulfonate mud is sent by grabbing device in fluidizer, by lignosulfonate mud according to 1 in fluidizer:1~3
Ratio is diluted with water, and adds suitable biological surface cleaning agent, and controlling reaction temperature is not less than 30 DEG C, and fluidized reaction 15~
25min;
2) after reaction finishes, lignosulfonate mud is pumped into screening plant, the fine sand in lignosulfonate mud is removed;
3) it carries out the lignosulfonate mud after desanding operation to enter in the first homogeneous tank, while sequentially adding in the first homogeneous tank suitable
Gel breaker, the heavy metal chelant of amount carry out equal qualitative response;
4) lignosulfonate mud that qualitative response finishes, which enters in centrifugal device, is separated by solid-liquid separation, and isolated liquid phase enters
In buffer storage;
5) isolated solid phase enters in the second homogeneous tank, while suitable microbial degradation is added in the second homogeneous tank
Agent carries out second homogenate reaction;
6) solid phase after progress second homogenate reaction, which enters, carries out press filtration in filter-pressing device, the liquid phase that press filtration obtains enters slow
In cryopreservation device;
7) liquid phase in buffer storage enters air-flotation process in the micro-nano air-flotation process unit in electric flocculation air-floating apparatus, together
When a small amount of oil phase is removed by mud-scraping apparatus;Then liquid phase, which enters back into, carries out electrification in high-voltage pulse electric flocculation processing unit
Reaction is learned, realizes that comprehensive decomposition and separation, the bed mud in electric flocculation air-floating apparatus are drained into dirt to the pollutant in liquid phase
In mud thickener;
8) liquid phase finished is reacted in electric flocculation air-floating apparatus enter in double film filters and carry out double medium filtration, after filtering
Part clear water enter in dispensing canister be used for medicament configuration, filter generation a small amount of concentrated water enter in MVR vaporising devices into
Row evaporative crystallization.
2. a kind of sulfonation process for treating waste sludge resulted as described in claim 1, it is characterised in that:Reaction in the step 1)
Temperature is 30~50 DEG C.
3. a kind of sulfonation process for treating waste sludge resulted as described in claim 1, it is characterised in that:The fluidized reaction time is
18~22min.
4. a kind of sulfonation process for treating waste sludge resulted as described in claim 1, it is characterised in that:Broken glue in the step 3)
Agent is one or more in aluminium polychloride, bodied ferric sulfate or polymeric aluminium ferrum silicate.
5. a kind of sulfonation process for treating waste sludge resulted as described in claim 1, it is characterised in that:A huge sum of money in the step 3)
It is xanthic acid esters or dithiocarbamates derivative to belong to chelating agent.
6. a kind of sulfonation process for treating waste sludge resulted as described in claim 1, it is characterised in that:Double films in the step 8)
Ceramic membrane and anti-pollution RO films are set in filter device.
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Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN111003910A (en) * | 2019-12-31 | 2020-04-14 | 西安华盛坤泰能源环保科技有限公司 | Method for treating waste sulfonated mud from drilling |
CN111870862A (en) * | 2020-07-29 | 2020-11-03 | 沈阳有研矿物化工有限公司 | Harmless treatment method for waste salt in production of alkylxanthate beneficiation reagent |
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EP0682965A1 (en) * | 1994-05-18 | 1995-11-22 | Centre de Prétraitement Régional (CPR) S.N.C. | Process and installation for the treatment and utilisation of fatty wastes |
US20090084148A1 (en) * | 2005-07-14 | 2009-04-02 | Capensis Investments 497 (Proprietary) Limited | Treatment of organic matter sludges |
CN101863605A (en) * | 2010-05-28 | 2010-10-20 | 东营顺通化工(集团)有限公司 | Waste drilling mud harmless treating process |
CN102267785A (en) * | 2011-07-11 | 2011-12-07 | 中国水电顾问集团中南勘测设计研究院 | Renewable water treatment device and method by use of micro-polluted water bodies as sources |
JP2014000495A (en) * | 2012-06-15 | 2014-01-09 | Universal Engineering Co Ltd | Sewage treatment apparatus, and sewage treatment method using the same |
CN203530059U (en) * | 2013-09-04 | 2014-04-09 | 北京联众华禹环保科技有限公司 | Treatment system of waste drilling mud filtrate |
CN204958662U (en) * | 2015-08-20 | 2016-01-13 | 湖北水云涧环保工程有限公司 | Proprietary effluent treatment plant of papermaking trade |
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2018
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EP0682965A1 (en) * | 1994-05-18 | 1995-11-22 | Centre de Prétraitement Régional (CPR) S.N.C. | Process and installation for the treatment and utilisation of fatty wastes |
US20090084148A1 (en) * | 2005-07-14 | 2009-04-02 | Capensis Investments 497 (Proprietary) Limited | Treatment of organic matter sludges |
CN101863605A (en) * | 2010-05-28 | 2010-10-20 | 东营顺通化工(集团)有限公司 | Waste drilling mud harmless treating process |
CN102267785A (en) * | 2011-07-11 | 2011-12-07 | 中国水电顾问集团中南勘测设计研究院 | Renewable water treatment device and method by use of micro-polluted water bodies as sources |
JP2014000495A (en) * | 2012-06-15 | 2014-01-09 | Universal Engineering Co Ltd | Sewage treatment apparatus, and sewage treatment method using the same |
CN203530059U (en) * | 2013-09-04 | 2014-04-09 | 北京联众华禹环保科技有限公司 | Treatment system of waste drilling mud filtrate |
CN204958662U (en) * | 2015-08-20 | 2016-01-13 | 湖北水云涧环保工程有限公司 | Proprietary effluent treatment plant of papermaking trade |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN111003910A (en) * | 2019-12-31 | 2020-04-14 | 西安华盛坤泰能源环保科技有限公司 | Method for treating waste sulfonated mud from drilling |
CN111870862A (en) * | 2020-07-29 | 2020-11-03 | 沈阳有研矿物化工有限公司 | Harmless treatment method for waste salt in production of alkylxanthate beneficiation reagent |
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