CN108686595A - A kind of haloflex reaction kettle enamel method for repairing and mending and component - Google Patents

A kind of haloflex reaction kettle enamel method for repairing and mending and component Download PDF

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Publication number
CN108686595A
CN108686595A CN201810526840.XA CN201810526840A CN108686595A CN 108686595 A CN108686595 A CN 108686595A CN 201810526840 A CN201810526840 A CN 201810526840A CN 108686595 A CN108686595 A CN 108686595A
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China
Prior art keywords
reaction kettle
repairing
turnbuckle
haloflex
kettle body
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CN201810526840.XA
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Chinese (zh)
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CN108686595B (en
Inventor
徐建华
孙振宇
李垂祥
栾京民
李树军
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Weifang Master Chemical Co Ltd
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Weifang Master Chemical Co Ltd
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/02Apparatus characterised by being constructed of material selected for its chemically-resistant properties

Abstract

The present invention discloses a kind of haloflex reaction kettle enamel method for repairing and mending of offer and component, belongs to haloflex preparation field, specific steps include:Select the specification of anti-corrosion repairing plate, teflon gasket, turnbuckle, butterfly spring;1. the central punch of failure area in reaction kettle body internal jacket, penetrates reaction kettle body external jacket;On reaction kettle body external jacket, by the centre bore of brill 1. centered on, trepanning is 2.;It will be with hole 2. chuck distance sleeve of corresponding size and the welding of reaction kettle body internal jacket outer wall and reaction kettle body external jacket;By anti-corrosion repairing plate, teflon gasket is packaged, disk spring is set on turnbuckle, screws on locking nut in turnbuckle.The present invention utilizes the pretightning force of disk spring, and creep caused by offsetting the operation of teflon gasket long term high temperature is thinning, the defect that sealing performance is deteriorated;Reaction kettle is reduced because repairing point failure again, and causing problem to be extended to can not retrieve, until the problem of reaction kettle is scrapped.

Description

A kind of haloflex reaction kettle enamel method for repairing and mending and component
Technical field
The invention belongs to haloflex preparation fields, and in particular to a kind of haloflex reaction kettle enamel repairing side Method and component.
Background technology
Repairing after existing haloflex reaction kettle enamel damage, the damage of small area are attacked in kettle internal drilling Silk, repair piece is fastened on corrosion-resistant bolt on autoclave body.The failure area of larger area is repaired, and the feelings perforated especially occurs Under condition, then using the hole penetrated, the method tensed from outside with bolt.Need experienced maintenance personal, running check fastening. The maintenance personal to lack experience, it is easy to which spot failure is magnified.In general, the short reason of repairing point service life is exactly to use Gasket is tetrafluoro material, needs frequent follow-up investigations and firm.It frequently occurs repairing point to be difficult to check, is not to check after repairing Frequently, cause to influence to produce;Otherwise it just checks not in place, is difficult to find when leaking, the enamel for causing whole value expensive The heavy losses that reaction kettle is scrapped.
Invention content
The present invention provides a kind of haloflex reaction kettle enamel method for repairing and mending and component, this hair to solve Problems Existing The bright reaction kettle that substantially reduces is because repairing point failure again, and causing problem to be extended to can not retrieve, up to what reaction kettle was scrapped asks Topic.After present invention repairing is finished and come into operation, hand inspection is not needed.
The technical solution adopted by the present invention to solve the technical problems is:
On the one hand the present invention provides a kind of haloflex reaction kettle enamel method for repairing and mending, includes the following steps:
1, the specification of anti-corrosion repairing plate, teflon gasket, turnbuckle, butterfly spring is selected;
2,1. the central punch of the failure area in reaction kettle body internal jacket, penetrates reaction kettle body external jacket;
3, on reaction kettle body external jacket, centre bore 1. centered on, trepanning is 2.;
It 4, will be with the hole 2. matched chuck distance sleeve of size and the weldering of reaction kettle body internal jacket outer wall and reaction kettle body external jacket It connects, keeps pressing container pressure grade, suppress and do not leak;
5, turnbuckle is threadedly secured on anti-corrosion repairing plate in the upper teflon gasket of turnbuckle other end set, and from Reaction kettle body inner wall is pierced by, and disk spring is set on turnbuckle, screws on locking nut in turnbuckle, is twisted with torque wrench Tightly, you can come into operation.
Preferably, the format diameter of the corrosion-resistant plate is bigger 90~110mm than failure area diameter.Since the present invention is suitable In production technology for internal pressure less than 0.8MPa, glassed steel reaction vessels internal pressure is less than 0.8MPa, in long-term life Production use during can make damaged part generate a tension, the elastic force of glassed steel reaction vessels internal pressure combination butterfly spring with Service life, the format diameter 90~110mm service lifes bigger than failure area diameter and cost of corrosion-resistant plate just can reach Most preferably.
Preferably, the outer diameter of the teflon gasket is smaller 8~12mm than anti-corrosion repairing board diameter, polytetrafluoroethylene (PTFE) pad The size of piece internal diameter is at least consistent with the diameter of failure area, and teflon gasket thickness takes 5~8mm.
Preferably, the specification of the turnbuckle takes M12~M30.
Preferably, the butterfly spring matches with turnbuckle.
Preferably, the hole is 2. longer 30mm than the diameter of the butterfly spring of selection.Since hole is 2. big with chuck distance sleeve It is small to match, therefore the diameter of distance sleeve is longer 30mm than the diameter of the butterfly spring of selection, is because butterfly spring is sleeved on drawing On tight bolt and it is tightly attached to failure area, a certain distance one side disk spring is equipped between butterfly spring and set distance sleeve There is buffering of enough pretightning forces convenient for sealing when, later stage failure area is on the other hand convenient for repair the timely hair after breakage again It now and handles, it is preferred that the turnbuckle is threadedly secured on corrosion-resistant plate.
Preferably, the locking nut is tightened according to bolt required standard torque.
A kind of haloflex reaction kettle enamel method for repairing and mending provided by the invention is interior suitable for glassed steel reaction vessels Pressure vessel, when longtime running, because teflon gasket is because of high-temerature creep, when size is thinning, because disk spring have it is enough Pretightning force, it is sufficient to meet the seal request of anti-corrosion repair piece, even if teflon gasket sealing performance declines, leaks, It from disk spring, can also find in time, convenient for handling at once, there is no hidden danger.
A kind of haloflex reaction kettle enamel method for repairing and mending is less than suitable for glassed steel reaction vessels internal pressure In the production technology of 0.8MPa.
On the other hand, the present invention provides a kind of haloflex reaction kettle enamel repairing component, including:Anti-corrosion repairing Plate, teflon gasket, reaction kettle inner body chuck, reaction kettle external jacket, it is characterised in that:It is fixed on the anti-corrosion repairing plate Turnbuckle, is cased with teflon gasket on the turnbuckle, outside the reaction kettle body internal jacket outer wall and reaction kettle body Chuck distance sleeve is welded between chuck, the turnbuckle is located at across reaction kettle internal jacket inside chuck distance sleeve, institute Tightening retaining nuts on turnbuckle are stated, butterfly spring is equipped between the turnbuckle and tightening retaining nuts.
Preferably, the anti-corrosion repairing plate and teflon gasket are located at reaction kettle internal jacket inner wall.
Compared with prior art, beneficial effects of the present invention are:
1. a kind of haloflex reaction kettle enamel method for repairing and mending provided by the invention and component, provide it is various study for a second time courses one has flunked component, Each specification studied for a second time courses one has flunked between component cooperates, on the one hand easy to implement, easy to operate, does not need experienced repair Personnel's running check fastens, and mitigates labour, on the other hand can rise and repairing is effectively performed, improves the service life after repairing;
2. a kind of haloflex reaction kettle enamel method for repairing and mending provided by the invention and component, can in advance be stored up with seriation Standby various specifications study for a second time courses one has flunked component, and repair is implemented in failure at once, and go wrong the phenomenon that repairing a couple of days before breaking away from, and improves Repairing efficiency reduces production cost loss;
3. a kind of haloflex reaction kettle enamel method for repairing and mending provided by the invention and component, increase set distance sleeve with Reaction kettle body internal jacket outer wall and the welding of reaction kettle body external jacket, are easy to check, without needing ability after fastening as before It checks, reduces the process of inspection, mitigate labour, improve working efficiency;Increase reliability and the safety of repairing;
4. a kind of haloflex reaction kettle enamel method for repairing and mending provided by the invention and component are twisted and are locked in turnbuckle Increase butterfly spring between tight nut, disk spring there are enough pretightning forces, it is sufficient to meet the seal request of anti-corrosion repair piece, separately Outside, it when the decline of teflon gasket sealing performance leaks, from disk spring, can find in time, convenient for handling at once, There is no hidden danger, there is leakage and is easy to find immediately in repairing point, avoids corrosion sudden enlargement, caused by finding not in time, Light then serious equipment fault loss, it is heavy then serious safety production accident occurs;
5. a kind of haloflex reaction kettle enamel method for repairing and mending provided by the invention and component, maintenance cost is cheap, cost It is low, reliability and safe in conventional repair mode.
Description of the drawings
Fig. 1 is the structural schematic diagram of present invention repairing component.
In figure:1 is anti-corrosion repairing plate, and 2 be teflon gasket, and 3 be turnbuckle, and 4 locking nuts, 5 be butterfly-type bullet Spring, 6 be reaction kettle inner body chuck, and 7 be chuck distance sleeve, and 8 be reaction kettle external jacket.
Specific implementation mode
With reference to embodiment, present disclosure is further illustrated.It should be appreciated that the implementation of the present invention is not limited to In the following examples, the accommodation in any form and/or change made to the present invention fall within the scope of the present invention.
In the present invention, if not refering in particular to, all parts, percentage are unit of weight, and all equipment and raw material etc. are equal It is commercially available or the industry is common.If without specializing, the method that embodiment uses is technology generally in the art.
To solve prior art problem, the embodiment of the present invention provides a kind of haloflex reaction kettle enamel method for repairing and mending And component, it is described in detail below.
Embodiment 1
On the one hand the present embodiment provides a kind of haloflex reaction kettle enamel method for repairing and mending, include the following steps:
1. selecting the specification of anti-corrosion repairing plate 1, teflon gasket 2, turnbuckle 3, butterfly spring 5;
The format diameter of the corrosion-resistant plate 1 is bigger than failure area by 100;The outer diameter of teflon gasket 2 is than anti-corrosion repairing The size of the small 10mm of 1 diameter of plate, 2 internal diameter of teflon gasket are consistent with the diameter of failure area, polytetrafluoroethylene (PTFE) pad 2 thickness of piece takes 8mm;The specification of turnbuckle 3 takes M12;
2. the central punch of the failure area in reaction kettle body internal jacket 6 is 1., reaction kettle body external jacket 8 is penetrated;
3. on reaction kettle body external jacket 8, by the centre bore of brill 1. centered on, 2., hole is 2. than the butterfly spring of selection 5 for trepanning The long 30mm of diameter;
4. will be with the hole 2. matched chuck distance sleeve of size 7 and 6 outer wall of reaction kettle body internal jacket and reaction kettle body external jacket 8 Welding keeps pressing container pressure grade, suppresses and do not leak;
5. by anti-corrosion repairing plate 1, teflon gasket 2 is packaged, is pierced by from reaction kettle body inner wall, disk spring 5 is set to drawing On tight bolt 3, locking nut 4 is screwed in turnbuckle 3, is tightened with torque wrench, locking nut 4 is turned round according to bolt required standard Square, which is tightened, to come into operation.
It is internal pressure vessel that method provided in this embodiment, which is suitable for glassed steel reaction vessels, is suitable for inside glassed steel reaction vessels In the production technology of pressure 0.7MPa.
On the other hand, the present embodiment also provides a kind of haloflex reaction kettle enamel repairing component, including:It is anti-corrosion to repair Mend plate, teflon gasket, reaction kettle inner body chuck, reaction kettle external jacket, it is characterised in that:It is solid on the anti-corrosion repairing plate Determine turnbuckle, teflon gasket, the reaction kettle body internal jacket outer wall and reaction kettle body are cased on the turnbuckle Chuck distance sleeve is welded between external jacket, the turnbuckle is located at across reaction kettle internal jacket inside chuck distance sleeve, Tightening retaining nuts on the turnbuckle are equipped with butterfly spring between the turnbuckle and tightening retaining nuts.
In the present embodiment, the anti-corrosion repairing plate and teflon gasket are located at reaction kettle internal jacket inner wall.
Embodiment 2
On the one hand the present embodiment provides a kind of haloflex reaction kettle enamel method for repairing and mending, include the following steps:
1. selecting the specification of anti-corrosion repairing plate 1, teflon gasket 2, turnbuckle 3, butterfly spring 5;
The format diameter of corrosion-resistant plate 1 is bigger than failure area by 90;The outer diameter of teflon gasket 2 is more straight than anti-corrosion repairing plate 1 The size of the small 8mm of diameter, 2 internal diameter of teflon gasket are consistent with the diameter of failure area, 2 thickness of teflon gasket Take 5mm;The specification of turnbuckle 3 takes M12;
2. the central punch of the failure area in reaction kettle body internal jacket 6 is 1., reaction kettle body external jacket 8 is penetrated;
3. on reaction kettle body external jacket 8, by the centre bore of brill 1. centered on, 2., hole is 2. than the butterfly spring of selection 5 for trepanning The long 30mm of diameter;
4. will be with the hole 2. matched chuck distance sleeve of size 7 and 6 outer wall of reaction kettle body internal jacket and reaction kettle body external jacket 8 Welding keeps pressing container pressure grade, suppresses and do not leak;
5. by anti-corrosion repairing plate 1, teflon gasket 2 is packaged, is pierced by from reaction kettle body inner wall, disk spring 5 is set to drawing On tight bolt 3, locking nut 4 is screwed in turnbuckle 3, is tightened with torque wrench, locking nut 4 is turned round according to bolt required standard Square, which is tightened, to come into operation.
It is internal pressure vessel that method provided in this embodiment, which is suitable for glassed steel reaction vessels, is suitable for inside glassed steel reaction vessels In the production technology of pressure 0.6MPa.
On the other hand, the present embodiment also provides a kind of haloflex reaction kettle enamel repairing component, including:It is anti-corrosion to repair Mend plate, teflon gasket, reaction kettle inner body chuck, reaction kettle external jacket, it is characterised in that:It is solid on the anti-corrosion repairing plate Determine turnbuckle, teflon gasket, the reaction kettle body internal jacket outer wall and reaction kettle body are cased on the turnbuckle Chuck distance sleeve is welded between external jacket, the turnbuckle is located at across reaction kettle internal jacket inside chuck distance sleeve, Tightening retaining nuts on the turnbuckle are equipped with butterfly spring between the turnbuckle and tightening retaining nuts.
In the present embodiment, the anti-corrosion repairing plate and teflon gasket are located at reaction kettle internal jacket inner wall.
Embodiment 3
On the one hand the present embodiment provides a kind of haloflex reaction kettle enamel method for repairing and mending, include the following steps:
1. selecting the specification of anti-corrosion repairing plate 1, teflon gasket 2, turnbuckle 3, butterfly spring 5;
The specification of anti-corrosion repairing plate 1, determines according to the size of damaged condition, the format diameter of the corrosion-resistant plate 1 than Failure area is big by 110;The outer diameter of teflon gasket 2 is smaller 12mm than anti-corrosion 1 diameter of repairing plate, in teflon gasket 2 The size of diameter is consistent with the diameter of failure area, and 2 thickness of teflon gasket takes 8mm;The specification of turnbuckle 3 takes M12;
2. the central punch of the failure area in reaction kettle body internal jacket 6 is 1., reaction kettle body external jacket 8 is penetrated;
3. on reaction kettle body external jacket 8, by the centre bore of brill 1. centered on, 2., hole is 2. than the butterfly spring of selection 5 for trepanning The long 30mm of diameter;
4. will be with the hole 2. matched chuck distance sleeve of size 7 and 6 outer wall of reaction kettle body internal jacket and reaction kettle body external jacket 8 Welding keeps pressing container pressure grade, suppresses and do not leak;
5. by anti-corrosion repairing plate 1, teflon gasket 2 is packaged, is pierced by from reaction kettle body inner wall, disk spring 5 is set to drawing On tight bolt 3, locking nut 4 is screwed in turnbuckle 3, is tightened with torque wrench, locking nut 4 is turned round according to bolt required standard Square, which is tightened, to come into operation.
It is internal pressure vessel that method provided in this embodiment, which is suitable for glassed steel reaction vessels, is suitable for inside glassed steel reaction vessels In the production technology of pressure 0.65MPa.
On the other hand, the present embodiment also provides a kind of haloflex reaction kettle enamel repairing component, including:It is anti-corrosion to repair Mend plate, teflon gasket, reaction kettle inner body chuck, reaction kettle external jacket, it is characterised in that:It is solid on the anti-corrosion repairing plate Determine turnbuckle, teflon gasket, the reaction kettle body internal jacket outer wall and reaction kettle body are cased on the turnbuckle Chuck distance sleeve is welded between external jacket, the turnbuckle is located at across reaction kettle internal jacket inside chuck distance sleeve, Tightening retaining nuts on the turnbuckle are equipped with butterfly spring between the turnbuckle and tightening retaining nuts.
In the present embodiment, the anti-corrosion repairing plate and teflon gasket are located at reaction kettle internal jacket inner wall.
In addition to the technical characteristic described in specification, remaining technical characteristic is the known technology of those skilled in the art, is prominent Go out the innovative characteristics of the present invention, details are not described herein for remaining technical characteristic.To sum up, the foregoing is merely a prefered embodiment of the invention and , it should not be limited the scope of the invention with this, i.e., every claims under this invention and present specification are made Simple equivalent changes and modifications, should all still belong to the range that patent of the present invention covers.

Claims (10)

1. a kind of haloflex reaction kettle enamel method for repairing and mending, it is characterised in that:The specific steps are:
(1)Select the specification of anti-corrosion repairing plate, teflon gasket, turnbuckle, butterfly spring;
(2)1. the central punch of failure area in reaction kettle body internal jacket, penetrates reaction kettle body external jacket;
(3)On reaction kettle body external jacket, by centre bore 1. centered on, trepanning is 2.;
(4)It will be with the hole 2. matched chuck distance sleeve of size and the weldering of reaction kettle body internal jacket outer wall and reaction kettle body external jacket It connects, keeps pressing container pressure grade, suppress and do not leak;
(5)Turnbuckle is threadedly secured on anti-corrosion repairing plate and covers upper polytetrafluoroethylene (PTFE) pad in the turnbuckle other end Piece, and be pierced by from reaction kettle body inner wall, disk spring is set on turnbuckle, screws on locking nut in turnbuckle, you can It comes into operation.
2. seeking a kind of haloflex reaction kettle enamel method for repairing and mending described in 1 according to claim, it is characterised in that:Institute The diameter for stating corrosion-resistant plate is bigger 90~110mm than failure area diameter.
3. seeking a kind of haloflex reaction kettle enamel method for repairing and mending described in 1 according to claim, it is characterised in that:Institute The outer diameter for stating teflon gasket is smaller 8~12mm than anti-corrosion repairing board diameter, and the size of teflon gasket internal diameter is at least Consistent with the diameter of failure area, teflon gasket thickness takes 5~8mm.
4. seeking a kind of haloflex reaction kettle enamel method for repairing and mending described in 1 according to claim, it is characterised in that:Institute The specification for stating turnbuckle takes M12~M30.
5. seeking a kind of haloflex reaction kettle enamel method for repairing and mending described in 1 according to claim, it is characterised in that:Institute Butterfly spring is stated with turnbuckle to match.
6. seeking a kind of haloflex reaction kettle enamel method for repairing and mending described in 1 according to claim, it is characterised in that:Institute It is longer 30mm than the diameter of the butterfly spring of selection to state the diameter of hole 2..
7. a kind of haloflex reaction kettle enamel method for repairing and mending, it is characterised in that:Any means described in claim 1-6 are suitable It is internal pressure vessel for glassed steel reaction vessels.
8. a kind of haloflex reaction kettle enamel method for repairing and mending according to claim 7, it is characterised in that:It is described to ward off Glass reaction kettle is that internal pressure needed for production technology is less than 0.8MPa.
9. a kind of haloflex reaction kettle enamel repairs component, including:Anti-corrosion repairing plate, teflon gasket, reaction Kettle inner body chuck, reaction kettle external jacket, it is characterised in that:Fixed strain bolt on the anti-corrosion repairing plate, the turnbuckle On be cased with teflon gasket, between the reaction kettle body internal jacket outer wall and reaction kettle body external jacket weld chuck separation sleeve Cylinder, the turnbuckle are located at across reaction kettle internal jacket inside chuck distance sleeve, and the turnbuckle tightens solid locking screw Mother is equipped with butterfly spring between the turnbuckle and tightening retaining nuts.
10. a kind of haloflex reaction kettle enamel according to claim 9 repairs component, it is characterised in that:It is described Anti-corrosion repairing plate and teflon gasket are located at reaction kettle internal jacket inner wall.
CN201810526840.XA 2018-05-29 2018-05-29 Chlorinated polyethylene reaction kettle glass lining repairing method and component Active CN108686595B (en)

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CN201810526840.XA CN108686595B (en) 2018-05-29 2018-05-29 Chlorinated polyethylene reaction kettle glass lining repairing method and component

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Application Number Priority Date Filing Date Title
CN201810526840.XA CN108686595B (en) 2018-05-29 2018-05-29 Chlorinated polyethylene reaction kettle glass lining repairing method and component

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Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3986243A (en) * 1975-09-22 1976-10-19 Fansteel Inc. Method of repairing chemical process equipment
US4078697A (en) * 1976-03-02 1978-03-14 R. Gelb & Sons, Inc. Method and apparatus for repairing protectively lined reactor vessels
CN201921681U (en) * 2011-01-17 2011-08-10 广东红墙新材料股份有限公司 Reparation device of glass lined reactor
CN203043983U (en) * 2012-12-14 2013-07-10 内江市运通塑料助剂有限公司 Device for repairing inner wall of chlorination reaction kettle
CN103230768A (en) * 2013-04-24 2013-08-07 青岛元基再生资源科技有限公司 Manufacturing technology of stainless steel corrosion-resistant layer of bearing reaction kettle

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3986243A (en) * 1975-09-22 1976-10-19 Fansteel Inc. Method of repairing chemical process equipment
US4078697A (en) * 1976-03-02 1978-03-14 R. Gelb & Sons, Inc. Method and apparatus for repairing protectively lined reactor vessels
CN201921681U (en) * 2011-01-17 2011-08-10 广东红墙新材料股份有限公司 Reparation device of glass lined reactor
CN203043983U (en) * 2012-12-14 2013-07-10 内江市运通塑料助剂有限公司 Device for repairing inner wall of chlorination reaction kettle
CN103230768A (en) * 2013-04-24 2013-08-07 青岛元基再生资源科技有限公司 Manufacturing technology of stainless steel corrosion-resistant layer of bearing reaction kettle

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