CN108675440A - A method of it is prepared by sludge accumulation body and aerobic particle mud is promoted quickly to be formed - Google Patents

A method of it is prepared by sludge accumulation body and aerobic particle mud is promoted quickly to be formed Download PDF

Info

Publication number
CN108675440A
CN108675440A CN201810616900.7A CN201810616900A CN108675440A CN 108675440 A CN108675440 A CN 108675440A CN 201810616900 A CN201810616900 A CN 201810616900A CN 108675440 A CN108675440 A CN 108675440A
Authority
CN
China
Prior art keywords
sludge
particle mud
accumulation body
aerobic particle
sludge accumulation
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
CN201810616900.7A
Other languages
Chinese (zh)
Other versions
CN108675440B (en
Inventor
邹金特
潘继杨
何航天
李军
倪永炯
吴淑云
何东芹
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Zhejiang University of Technology ZJUT
Original Assignee
Zhejiang University of Technology ZJUT
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Zhejiang University of Technology ZJUT filed Critical Zhejiang University of Technology ZJUT
Priority to CN201810616900.7A priority Critical patent/CN108675440B/en
Publication of CN108675440A publication Critical patent/CN108675440A/en
Application granted granted Critical
Publication of CN108675440B publication Critical patent/CN108675440B/en
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F3/00Biological treatment of water, waste water, or sewage
    • C02F3/02Aerobic processes
    • C02F3/12Activated sludge processes
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F3/00Biological treatment of water, waste water, or sewage
    • C02F3/02Aerobic processes
    • C02F3/12Activated sludge processes
    • C02F3/1236Particular type of activated sludge installations
    • C02F3/1263Sequencing batch reactors [SBR]
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F9/00Multistage treatment of water, waste water or sewage
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00Treatment of water, waste water, or sewage
    • C02F1/52Treatment of water, waste water, or sewage by flocculation or precipitation of suspended impurities
    • C02F1/54Treatment of water, waste water, or sewage by flocculation or precipitation of suspended impurities using organic material
    • C02F1/56Macromolecular compounds
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00Treatment of water, waste water, or sewage
    • C02F1/66Treatment of water, waste water, or sewage by neutralisation; pH adjustment
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02WCLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
    • Y02W10/00Technologies for wastewater treatment
    • Y02W10/10Biological treatment of water, waste water, or sewage

Abstract

The invention belongs to biological wastewater treatment fields, are related to a kind of method for promoting aerobic particle mud quickly to be formed by the preparation of sludge accumulation body.This method comprises the following steps:(1) it takes ordinary activated sludge and concentrates;(2) cationic high molecular polymer not soluble in water is added;(3) it is stirring evenly and then adding into glacial acetic acid;(4) it adds lye and adjusts mixed liquor pH value to alkalinity;(5) it will collect and be seeded in sequencing batch reactor SBR after the sludge accumulation body cleaning and dipping of formation and run;(6) it realizes after SBR is run 3 10 days and granulates completely, aerobic particle mud remains to holding structure stabilization after longtime running.The present invention can promote the quick formation of aerobic particle mud, and easy to operate efficient, be easy to practical application.

Description

A method of it is prepared by sludge accumulation body and aerobic particle mud is promoted quickly to be formed
Technical field
The invention belongs to biological wastewater treatment fields, and in particular to a kind of prepared by sludge accumulation body promotes aerobic grain The method that sludge is quickly formed.
Background technology
Aerobic particle mud is a kind of Novel sewage biologic treating technique emerging in recent years and traditional activated sludge Method is compared, and has the function of that compact structure, settling property are good, biomass is high and has synchronous denitrification dephosphorizing, anti-shock loading, resistance to The advantages that poisonous and harmful substance and small floor space.But the problems such as aerobic particle mud system start-up time is long still restricts this The development of technology.The exploitation of TU Delft polytechnical universityTechnology needs 3-5 months in practical engineering application Domestication, which cultivates one's ability, realizes aerobic sludge granulation.Document (the Aerobic sludge granulation in that Li Jun etc. is delivered A full-scale sequencing batch reactor) report practical scale sequencing batch reactor (SBR) pass through Culture in 337 days realizes aerobic sludge granulation.Currently, it is special to promote the correlative study that aerobic particle mud is quickly formed to have Profit application, but disclosed patent be all by change reactor operating parameter and structure or reactor operation in add object The method of matter promotes the quick formation of aerobic particle mud, and the settling property of initial operating stage sludge is poor, realize complete particle Change basic need 2-4 weeks or so.He Jian etc. has applied for a kind of preparation method of aerobic particle mud, high using the cation of amidino groups Molecular chemistry medicament prepares aerobic particle mud, but the patent is without reference to the characteristic index for preparing aerobic particle mud, such as grain Diameter, sedimentation index etc., do not refer to yet and prepare the operating condition of particle in the reactor, while the cation high molecular chemistry of amidino groups Medicament prepares difficulty, and cost is higher.
Find a kind of method that can rapidly promote the formation of aerobic particle mud aggregation so that reactor start-up operation is just Phase can obtain good settling property, while aerobic particle mud system can be run steadily in the long term to good in the process of running The application and development of oxygen granule sludge technology are of great significance.Cation polymeric flocculant has pole to active floc sludge Strong flocculation, can promote the formation of sludge accumulation body, but its to sludge activity, there are certain inhibiting effect.Therefore, Finding a kind of more suitable cation polymeric flocculant, intensity is high, formation of the strong sludge accumulation body of stability promoting, So that aerobic particle mud system initial start stage just has good settling property and can run steadily in the long term to aerobic grain dirt Mud technology has very important realistic meaning and economic value in the application of field of waste water treatment.
Invention content
It is an object of the invention in order to solve in prior art, initial operating stage sludge settling property is poor, realize complete The granulating time is longer (2-8 weeks or so), and common cationic high polymer coagulant (such as polyacrylamide) has sludge activity It certain inhibiting effect and can be provided a kind of by cationic high molecular polymer system not soluble in water with the defect that water outlet is lost in Standby sludge accumulation body is come the method that promotes aerobic particle mud quickly to be formed.
To achieve the above object, the present invention uses following technical scheme:
A method of it is prepared by sludge accumulation body and aerobic particle mud is promoted quickly to be formed, the method includes following steps Suddenly:
(1) 1L ordinary activated sludge gravity concentrations are taken;
(2) cationic high molecular polymer not soluble in water is added in the ordinary activated sludge after step (1) concentration;
(3) after stirring evenly, glacial acetic acid is added, continues to stir, obtains mixed liquor;
(4) lye is added in the mixed liquor after step (3), adjusts mixed liquor pH value to alkalinity, precipitation obtains sludge accumulation body;
(5) it will collect and be seeded in SBR after the sludge accumulation body tap water cleaning and dipping of step (4) formation, then press in Water, reaction, precipitation, water outlet and idle mode are run;
(6) SBR is run 3-10 days, and for the sludge in reactor mainly based on aerobic particle mud, particulates' properties are good, long-term to transport Aerobic particle mud remains to holding structure stabilization after row.
In the step (1), ordinary activated sludge is derived from the flco activated sludge of laboratory routine culture, gravity concentration Sludge concentration is 2-20g/L afterwards;
In the step (2), the dosage for the chitosan preferentially selected is 2%-50% (in terms of dewatered sludge quality, w/w).
In the step (3), the glacial acetic acid amount using mechanical agitation, mixing speed 100-1000rpm, addition makes to mix Conjunction liquid acetic acid concentration is 0.2%-5%, continues to stir 1-2min.
In the step (4), the lye added is NaOH, and a concentration of 2-6mol/L, adjusting pH of mixed is 7.5-11.
In the step (5), sludge accumulation body is cleaned 2-3 times with tap water, and each soaking time is 0.5-2.5h;It receives The average grain diameter of the sludge accumulation body integrated is 0.5-2.5mm, the sludge volume index (SVI of 5min and 30min5And SVI30) be 60-90mL/g;The running stages of reaction of SBR carry out anaerobism stirring, aerobic aeration operation or only carry out aerobic aeration operation.
In the step (6), aerobic particle mud structure is closely knit after operation 3-10 days, and sludge average grain diameter is 0.5- 2.0mm, SVI5And SVI30For 40-70mL/g, aerobic particle mud accounts for 75% or more in reactor;Longtime running is 60-100 It.
The present invention technical concept be:Aerobic particle mud have compact structure, settling property is good, biomass is high and energy The advantages that synchronous denitrification dephosphorizing, anti-shock loading and resistance to poisonous and harmful substance, has in biological wastewater treatment field and widely answers Use foreground.But the problems such as aerobic particle mud system start-up time is long still restricts the development of the technology.
Chitosan is a kind of natural macromolecule amylose, does not have inhibiting effect to microbial activity.Meanwhile chitosan contains ammonia Base is natural cationic flocculant.
It adds chitosan and using acetic acid to carry out dissolving can make chitosan as adhesive and skeleton, promote active floc sludge Quickly form sludge accumulation body.After pH is adjusted as alkalinity, the chitosan of dissolving can be precipitated and be adhered to sludge accumulation body in water On so that the chitosan added will not be lost in normal operation with water outlet, to ensure the stability of sludge accumulation body and good Good settleability.
Since sludge accumulation body has good settling property, in SBR culture can quickly form that structure is closely knit, settleability It can better aerobic particle mud.
Beneficial effects of the present invention are mainly reflected in:
(1) chitosan rich content in nature is prepared simply, cheap, is a kind of natural cation high molecular wadding Solidifying agent, does not have inhibiting effect to microbial activity in sludge.
(2) by preparing sludge accumulation body, the time of aerobic particle mud formation is highly shortened, while in reactor The initial stage of startup stage can obtain good sludge settling property, be conducive to the stable operation of aerobic particle mud system.
(3) it when Fragmentation Phenomena occurs in aerobic particle mud system, can be carried with the present invention with the floc sludge of water outlet discharge The method of confession quickly forms sludge accumulation body, then puts into granular sludge reactor and run again, ensure that aerobic particle mud Long-term stable operation.
(4) what prepared by sludge accumulation body is easy to operate, is easy to practical application.
Description of the drawings
Fig. 1 is the shape appearance figure of the sludge accumulation body prepared.
Fig. 2 is the aerobic particle mud shape appearance figure after running 6 days.
Specific implementation mode
Present disclosure is illustrated in further detail by the following examples.
Embodiment 1
A method of it is prepared by sludge accumulation body and aerobic particle mud is promoted quickly to be formed, included the following steps:
(1) take the ordinary activated sludge of 1L laboratory cultures in beaker, sludge concentration 2g/L;
(2) the chitosan 0.04g of dewatered sludge quality 2% is added in the sludge of step (1);
(3) it uses machine mixer, rotating speed 100rpm to stir evenly sludge and chitosan, 2mL glacial acetic acids is then added (mixed liquid concentration 0.2%), 100rpm stir 2min;
(4) NaOH solution of 3mol/L is added dropwise afterwards in step (3), it is 7.5 to adjust pH;
(5) stop stirring afterwards in step (4), pour out supernatant after precipitating 10min, tap water cleaning and dipping sludge accumulation body is used in combination 3 times, each 0.5h, it is 0.55mm, SVI to obtain sludge average grain diameter5For 85mL/g, SVI30For 80mL/g;
(6) the sludge accumulation body that step (5) is collected is seeded to sbr reactor device, by water inlet, anaerobism stirring, aerobic aeration, sunk Shallow lake, water outlet and idle mode are run, and SBR water-filling ratios are 50%, cycle of operation 6h:Water inlet 10min, anaerobism stirring 90min, It is aerated 180min, precipitation 3-5min, water outlet 10min, idle 65-67min;
(7) closely knit aerobic particle mud is formed after running 3 days in SBR, sludge average grain diameter is 0.55mm, SVI5For 70mL/ G, SVI30For 65mL/g, SVI30/SVI5It is 0.93, aerobic particle mud accounts for 75% or more, after operation 60 days in SBR in reactor Aerobic particle mud remain to holding structure stabilization.
Embodiment 2
A method of it is prepared by sludge accumulation body and aerobic particle mud is promoted quickly to be formed, included the following steps:
(1) take the ordinary activated sludge of 1L laboratory cultures in beaker, sludge concentration 4g/L;
(2) the chitosan 0.4g of dewatered sludge quality 10% is added in the sludge of step (1);
(3) it uses machine mixer, rotating speed 200rpm to stir evenly sludge and chitosan, 5mL glacial acetic acids is then added (mixed liquid concentration 0.5%), 200rpm stir 2min;
(4) NaOH solution of 6mol/L is added dropwise afterwards in step (3), it is 9 to adjust pH;
(5) stop stirring afterwards in step (4), pour out supernatant after precipitating 10min, tap water cleaning and dipping sludge accumulation body is used in combination 3 times, each 0.5h, it is 0.93mm, SVI to obtain sludge average grain diameter5For 70mL/g, SVI30For 68mL/g;
(6) the sludge accumulation body that step (5) is collected is seeded to sbr reactor device, presses water inlet, aerobic aeration, precipitation, water outlet and spare time The mode set is run, and SBR water-filling ratios are 50%, cycle of operation 4h:Water inlet 10min, aerobic aeration 180min, precipitation 3- 5min, water outlet 10min, idle 35-37min;
(7) closely knit aerobic particle mud is formed after running 5 days in SBR, sludge average grain diameter is 0.85mm, SVI5For 60mL/ G, SVI30For 55mL/g, SVI30/SVI5It is 0.92, aerobic particle mud accounts for 85% or more, after operation 75 days in SBR in reactor Aerobic particle mud remain to holding structure stabilization.
Embodiment 3
A method of it is prepared by sludge accumulation body and aerobic particle mud is promoted quickly to be formed, included the following steps:
(1) take the ordinary activated sludge of 1L laboratory cultures in beaker, it is 7g/L to be concentrated into sludge concentration;
(2) the chitosan 1.4g of dewatered sludge quality 20% is added in the sludge of step (1);
(3) it uses machine mixer, rotating speed 300rpm to stir evenly sludge and chitosan, 5mL glacial acetic acids is then added (mixed liquid concentration 0.5%), 300rpm stir 1min;
(4) NaOH solution of 5mol/L is added dropwise afterwards in step (3), it is 10 to adjust pH;
(5) stop stirring afterwards in step (4), pour out supernatant after precipitating 10min, tap water cleaning and dipping sludge accumulation body is used in combination 2 times, each 2h, it is 1.3mm, SVI to obtain sludge average grain diameter5For 60mL/g, SVI30For 60mL/g;
(6) the sludge accumulation body that step (5) is collected is seeded to sbr reactor device, by water inlet, anaerobism stirring, aerobic aeration, sunk Shallow lake, water outlet and idle mode are run, and SBR water-filling ratios are 50%, cycle of operation 6h:Water inlet 10min, anaerobism stirring 90min, Aerobic aeration 180min, precipitation 3-5min, water outlet 10min, idle 65-67min;
(7) closely knit aerobic particle mud is formed after running 5 days in SBR, sludge average grain diameter is 1.2mm, SVI5For 55mL/g, SVI30For 50mL/g, SVI30/SVI5It is 0.91, aerobic particle mud accounts for 90% or more, after operation 60 days in SBR in reactor Aerobic particle mud remains to holding structure stabilization.
Embodiment 4
A method of it is prepared by sludge accumulation body and aerobic particle mud is promoted quickly to be formed, included the following steps:
(1) take the ordinary activated sludge of 1L laboratory cultures in beaker, it is 6g/L to be concentrated into sludge concentration;
(2) the chitosan 0.3g of dewatered sludge quality 5% is added in the sludge of step (1);
(3) it uses machine mixer, rotating speed 200rpm to stir evenly sludge and chitosan, 15mL glacial acetic acids is then added (mixed liquid concentration 1.5%), 200rpm stir 2min;
(4) NaOH solution of 4mol/L is added dropwise afterwards in step (3), it is 9 to adjust pH;
(5) stop stirring afterwards in step (4), pour out supernatant after precipitating 10min, tap water cleaning and dipping sludge accumulation body is used in combination 3 times, each 1.5h, it is 0.9mm, SVI to obtain sludge average grain diameter5For 70mL/g, SVI30For 68mL/g;
(6) the sludge accumulation body that step (5) is collected is seeded to sbr reactor device, presses water inlet, aerobic aeration, precipitation, water outlet and spare time The mode set is run, and SBR water-filling ratios are 50%, cycle of operation 4h:Water inlet 10min, aerobic aeration 180min, precipitation 3- 5min, water outlet 10min, idle 35-37min;
(7) closely knit aerobic particle mud is formed after running 7 days in SBR, sludge average grain diameter is 0.8mm, SVI5For 60mL/g, SVI30For 55mL/g, SVI30/SVI5It is 0.92, aerobic particle mud accounts for 75% or more, after operation 70 days in SBR in reactor Aerobic particle mud remains to holding structure stabilization.
Embodiment 5
A method of it is prepared by sludge accumulation body and aerobic particle mud is promoted quickly to be formed, included the following steps:
(1) take the ordinary activated sludge of 1L laboratory cultures in beaker, it is 8g/L to be concentrated into sludge concentration;
(2) the chitosan 2g of dewatered sludge quality 25% is added in the sludge of step (1);
(3) it uses machine mixer, rotating speed 600rpm to stir evenly sludge and chitosan, 10mL glacial acetic acids is then added (mixed liquid concentration 1%), 600rpm stir 1min;
(4) NaOH solution of 6mol/L is added dropwise afterwards in step (3), it is 11 to adjust pH;
(5) stop stirring afterwards in step (4), pour out supernatant after precipitating 10min, tap water cleaning and dipping sludge accumulation body is used in combination 3 times, each 2h, it is 1.2mm, SVI to obtain sludge average grain diameter5For 60mL/g, SVI30For 60mL/g;
(6) the sludge accumulation body that step (5) is collected is seeded to sbr reactor device, by water inlet, anaerobism stirring, aerobic aeration, sunk Shallow lake, water outlet and idle mode are run, and SBR water-filling ratios are 50%, cycle of operation 6h:Water inlet 10min, anaerobism stirring 120min, aerobic aeration 180min, precipitation 3-5min, water outlet 10min, idle 35-37min;
(7) closely knit aerobic particle mud is formed after running 10 days in SBR, sludge average grain diameter is 1.1mm, SVI5For 50mL/ G, SVI30For 48mL/g, SVI30/SVI5It is 0.96, aerobic particle mud accounts for 90% or more, after operation 90 days in SBR in reactor Aerobic particle mud remain to holding structure stabilization.
Embodiment 6
A method of it is prepared by sludge accumulation body and aerobic particle mud is promoted quickly to be formed, included the following steps:
(1) take the ordinary activated sludge of 1L laboratory cultures in beaker, it is 10g/L to be concentrated into sludge concentration;
(2) the chitosan 5g of dewatered sludge quality 50% is added in the sludge of step (1);
(3) it uses machine mixer, rotating speed 1000rpm to stir evenly sludge and chitosan, 40mL glacial acetic acids is then added (mixed liquid concentration 4%), 1000rpm stir 1min;
(4) NaOH solution of 5mol/L is added dropwise afterwards in step (3), it is 11 to adjust pH;
(5) stop stirring afterwards in step (4), pour out supernatant after precipitating 10min, tap water cleaning and dipping sludge accumulation body is used in combination 3 times, each 2.5h, it is 2.2mm, SVI to obtain sludge average grain diameter5For 65mL/g, SVI30For 65mL/g;
(6) the sludge accumulation body that step (5) is collected is seeded to sbr reactor device, presses water inlet, aerobic aeration, precipitation, water outlet and spare time The mode set is run, and SBR water-filling ratios are 50%, cycle of operation 4h:Water inlet 10min, aerobic aeration 180min, precipitation 3- 5min, water outlet 10min, idle 35-37min;
(7) closely knit aerobic particle mud is formed after running 8 days in SBR, sludge average grain diameter is 1.8mm, SVI5For 55mL/g, SVI30For 50mL/g, SVI30/SVI5It is 0.91, aerobic particle mud accounts for 80% or more, after operation 80 days in SBR in reactor Aerobic particle mud remains to holding structure stabilization.
Embodiment 7
A method of it is prepared by sludge accumulation body and aerobic particle mud is promoted quickly to be formed, included the following steps:
(1) take the ordinary activated sludge of 1L laboratory cultures in beaker, it is 20g/L to be concentrated into sludge concentration;
(2) the chitosan 5g of dewatered sludge quality 25% is added in the sludge of step (1);
(3) it uses machine mixer, rotating speed 800rpm to stir evenly sludge and chitosan, 50mL glacial acetic acids is then added (mixed liquid concentration 5%), 800rpm stir 1min;
(4) NaOH solution of 3mol/L is added dropwise afterwards in step (3), it is 8 to adjust pH;
(5) stop stirring afterwards in step (4), pour out supernatant after precipitating 10min, tap water cleaning and dipping sludge accumulation body is used in combination 3 times, each 1.5h, it is 2.5mm, SVI to obtain sludge average grain diameter5For 75mL/g, SVI30For 70mL/g;
(6) the sludge accumulation body that step (5) is collected is seeded to sbr reactor device, by water inlet, anaerobism stirring, aerobic aeration, sunk Shallow lake, water outlet and idle mode are run, and SBR water-filling ratios are 50%, cycle of operation 6h:Water inlet 10min, anaerobism stir 90min, Aerobic aeration 180min, precipitation 3-5min, water outlet 10min, idle 65-67min;
(7) closely knit aerobic particle mud is formed after running 7 days in SBR, sludge average grain diameter is 2.0mm, SVI5For 58mL/g, SVI30For 55mL/g, SVI30/SVI5It is 0.95, aerobic particle mud accounts for 85% or more, after operation 100 days in SBR in reactor Aerobic particle mud remain to holding structure stabilization.
This hair can be understood and applied the above description of the embodiments is intended to facilitate those skilled in the art It is bright.Person skilled in the art obviously can easily to these embodiments, various modification can be adapted, and described herein General Principle is applied in other embodiment without having to go through creative labor.Therefore, the present invention is not limited to implementations here Example, the scope of the present invention are limited by claim and its equivalent.

Claims (7)

1. a kind of preparing the method for promoting aerobic particle mud quickly to be formed by sludge accumulation body, it is characterised in that:The side Method includes the following steps:
(1) 1L ordinary activated sludge gravity concentrations are taken;
(2) cationic high molecular polymer not soluble in water is added in the ordinary activated sludge after step (1) concentration;
(3) after stirring evenly, glacial acetic acid is added, continues to stir, obtains mixed liquor;
(4) lye is added in the mixed liquor after step (3), adjusts mixed liquor pH value to alkalinity, precipitation obtains sludge accumulation body;
(5) it will collect and be seeded in SBR after the sludge accumulation body tap water cleaning and dipping of step (4) formation, then press in Water, reaction, precipitation, water outlet and idle mode are run;
(6) SBR is run 3-10 days.
2. a kind of side for promoting aerobic particle mud quickly to be formed by the preparation of sludge accumulation body according to claim 1 Method, it is characterised in that:In the step (1), a concentration of 2-20g/L of ordinary activated sludge after concentration.
3. a kind of side for promoting aerobic particle mud quickly to be formed by the preparation of sludge accumulation body according to claim 1 Method, it is characterised in that:In the step (2), the cationic high molecular polymer not soluble in water is chitosan, is added Amount is calculated as 2%-50% with dewatered sludge quality.
4. a kind of side for promoting aerobic particle mud quickly to be formed by the preparation of sludge accumulation body according to claim 1 Method, it is characterised in that:In the step (3), using mechanical agitation, mixing speed 100-1000rpm, the glacial acetic acid of addition Amount makes mixed liquor acetic acid concentration be 0.2%-5%, continues to stir 1-2min.
5. a kind of side for promoting aerobic particle mud quickly to be formed by the preparation of sludge accumulation body according to claim 1 Method, it is characterised in that:In the step (4), it is 7.5-11 to add lye and adjust pH of mixed.
6. a kind of side for promoting aerobic particle mud quickly to be formed by the preparation of sludge accumulation body according to claim 1 Method, it is characterised in that:In the step (5), sludge accumulation body is cleaned 2-3 times with tap water, and each soaking time is 0.5- 2.5h;The average grain diameter of the sludge accumulation body of collection is 0.5-2.5mm, the sludge volume index SVI of 5min5For 60-90mL/g, The sludge volume index SVI of 30min30For 60-90mL/g.
7. a kind of side for promoting aerobic particle mud quickly to be formed by the preparation of sludge accumulation body according to claim 1 Method, it is characterised in that:In the step (6), aerobic particle mud structure is closely knit after operation 3-10 days, and sludge average grain diameter is 0.5-2.0mm, SVI5For 40-70mL/g, SVI30For 40-70mL/g, aerobic particle mud accounts for 75% or more in reactor.
CN201810616900.7A 2018-06-14 2018-06-14 Method for promoting quick formation of aerobic granular sludge through sludge aggregate preparation Active CN108675440B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201810616900.7A CN108675440B (en) 2018-06-14 2018-06-14 Method for promoting quick formation of aerobic granular sludge through sludge aggregate preparation

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201810616900.7A CN108675440B (en) 2018-06-14 2018-06-14 Method for promoting quick formation of aerobic granular sludge through sludge aggregate preparation

Publications (2)

Publication Number Publication Date
CN108675440A true CN108675440A (en) 2018-10-19
CN108675440B CN108675440B (en) 2021-05-18

Family

ID=63811089

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201810616900.7A Active CN108675440B (en) 2018-06-14 2018-06-14 Method for promoting quick formation of aerobic granular sludge through sludge aggregate preparation

Country Status (1)

Country Link
CN (1) CN108675440B (en)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109095601A (en) * 2018-10-25 2018-12-28 江西理工大学 Aerobic granular sludge reactor operation stability based on size controlling maintains method
CN114853155A (en) * 2022-03-16 2022-08-05 西南科技大学 Method for rapidly culturing aerobic granular sludge
CN115215432A (en) * 2022-07-09 2022-10-21 同济大学 Granular sludge suitable for town sewage treatment and rapid generation method thereof

Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4729831A (en) * 1985-03-06 1988-03-08 Mitsubishi Monsanto Chemical Company Method for preventing the bulking of activated sludge
JP2001129310A (en) * 1999-11-08 2001-05-15 Kansai Kako Kk Flocculant and sludge treatment method
CN101367590A (en) * 2008-09-01 2009-02-18 浙江大学 Process for treating heavy-metal waste water containing high concentration suspended matter
WO2010074358A1 (en) * 2008-12-24 2010-07-01 Korea Institute Of Energy Research Chitosan-nipam thermosensitive polymer coagulant and method for the preparation therefor
CN102583722A (en) * 2012-03-12 2012-07-18 北京化工大学 Immobilized-cultivation method for aerobic granular sludge
CN105481070A (en) * 2015-11-26 2016-04-13 廊坊金诺生物科技开发有限公司 Inorganic-organic composite polymeric flocculant and preparation method thereof
CN105585112A (en) * 2015-12-09 2016-05-18 复旦大学 Preparation method for aerobic granular sludge
CN106348432A (en) * 2016-11-02 2017-01-25 西华大学 Rapid culturing method for aerobic granular sludge for treating printing and dying waste water

Patent Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4729831A (en) * 1985-03-06 1988-03-08 Mitsubishi Monsanto Chemical Company Method for preventing the bulking of activated sludge
JP2001129310A (en) * 1999-11-08 2001-05-15 Kansai Kako Kk Flocculant and sludge treatment method
CN101367590A (en) * 2008-09-01 2009-02-18 浙江大学 Process for treating heavy-metal waste water containing high concentration suspended matter
WO2010074358A1 (en) * 2008-12-24 2010-07-01 Korea Institute Of Energy Research Chitosan-nipam thermosensitive polymer coagulant and method for the preparation therefor
CN102583722A (en) * 2012-03-12 2012-07-18 北京化工大学 Immobilized-cultivation method for aerobic granular sludge
CN105481070A (en) * 2015-11-26 2016-04-13 廊坊金诺生物科技开发有限公司 Inorganic-organic composite polymeric flocculant and preparation method thereof
CN105585112A (en) * 2015-12-09 2016-05-18 复旦大学 Preparation method for aerobic granular sludge
CN106348432A (en) * 2016-11-02 2017-01-25 西华大学 Rapid culturing method for aerobic granular sludge for treating printing and dying waste water

Non-Patent Citations (6)

* Cited by examiner, † Cited by third party
Title
JINTE ZOU ET AL.: "Cultivating aerobic granular sludge in a developed continuous-flow reactor", 《BIORESOURCE TECHNOLOGY》 *
JINTE ZOU ET AL.: "Rapid control of activated sludge bulking and simultaneous acceleration", 《SCIENCE OF THE TOTAL ENVIRONMENT》 *
JINTE ZOU ET AL.: "Rapid start-up of an aerobic granular sludge system for nitrogen and", 《SCIENCE OF THE TOTAL ENVIRONMENT》 *
K. TORRES ET AL: "Granulation and microbial community dynamics in the", 《WATER RESEARCH》 *
YONGJUN LIU ET AL.: "Regulation of aerobic granular sludge reformulation after granular", 《BIORESOURCE TECHNOLOGY》 *
易诚: "混凝好氧颗粒污泥的絮凝剂选择", 《环境工程学报》 *

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109095601A (en) * 2018-10-25 2018-12-28 江西理工大学 Aerobic granular sludge reactor operation stability based on size controlling maintains method
CN114853155A (en) * 2022-03-16 2022-08-05 西南科技大学 Method for rapidly culturing aerobic granular sludge
CN115215432A (en) * 2022-07-09 2022-10-21 同济大学 Granular sludge suitable for town sewage treatment and rapid generation method thereof
CN115215432B (en) * 2022-07-09 2023-07-21 同济大学 Granular sludge suitable for town sewage treatment and rapid generation method thereof

Also Published As

Publication number Publication date
CN108675440B (en) 2021-05-18

Similar Documents

Publication Publication Date Title
CN105693029A (en) Landfill leachate treatment process
CN207047067U (en) A kind of livestock breeding wastewater processing system
CN104291443B (en) The apparatus and method of half nitrated/part denitrification/Anammox process low ratio of carbon to ammonium municipal effluent
CN102153232B (en) Side-flow circulation BAF (Biological Aerated Filter) intensified dephosphorization system and method for treating urban sewage with the dephosphorization system
CN109574218B (en) Device and method for treating late landfill leachate through shortcut nitrification-fermentation/denitrification-anaerobic ammonia oxidation process
CN102583741A (en) Slow-release carbon source material using sodium alginate as base material and preparation method thereof
CN108751625A (en) A kind of processing system and technique of ferment antibiotics waste water
CN108675440A (en) A method of it is prepared by sludge accumulation body and aerobic particle mud is promoted quickly to be formed
CN104649521B (en) The printing-dyeing waste water treatment process of circulation in a kind of muddy water strengthening
CN103819049A (en) Sewage treatment method and system
CN101708923A (en) Denitrifying phosphorus and nitrogen removal method for wastewater with low carbon-phosphorus ratio
CN101508485A (en) System and method for cultivation of aerobic particle sewage sludge and for treating organic waste water
CN104609557A (en) Method for treating slaughter wastewater by using sequencing batch reactor (SBR) activated sludge process
CN105110572A (en) Device and method for treating municipal wastewater with low C/N ratio through silicon source adsorption/nitrification/partial denitrification/anaerobic ammonia oxidation coupling process
CN102173506A (en) Bioactive compound filling material
CN208667436U (en) A kind of processing system of ferment antibiotics waste water
CN108947098A (en) The processing method of pig breeding wastewater
CN101186387A (en) Method for increasing organism synchronous dephosphorization denitrogenation effect of sewage under anaerobic-hypoxia condition
CN103435233A (en) Equipment and method for recycling chemical fiber continuous-spinning wastewater
CN103112948B (en) Method for rapidly culturing autotrophic nitrogen removal granule sludge under conditions of low substrate concentration and high ascending velocity
CN103739156B (en) Method for performing biological denitrification of wastewater by using residual sludge and biological denitrification system for implementing same
CN103073156B (en) Method for treating poly butylene succinate production waste water by biochemical method
CN112876024B (en) Modification method for in-situ sludge reduction of sewage treatment plant
CN106007171A (en) Integrated sludge reduction recycling and N2O emission reduction sewage treatment device and method for operating same
CN105129991B (en) A kind of method of nitrification/part denitrification/low C/N municipal sewages of Anammox coupling technique process

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
GR01 Patent grant
GR01 Patent grant