CN108660760A - A kind of warming moisture-resistant self-cleaning silk scarf and preparation method thereof - Google Patents
A kind of warming moisture-resistant self-cleaning silk scarf and preparation method thereof Download PDFInfo
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- CN108660760A CN108660760A CN201710213780.1A CN201710213780A CN108660760A CN 108660760 A CN108660760 A CN 108660760A CN 201710213780 A CN201710213780 A CN 201710213780A CN 108660760 A CN108660760 A CN 108660760A
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/21—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/263—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds of unsaturated carboxylic acids; Salts or esters thereof
- D06M15/277—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds of unsaturated carboxylic acids; Salts or esters thereof containing fluorine
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/77—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with silicon or compounds thereof
- D06M11/79—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with silicon or compounds thereof with silicon dioxide, silicic acids or their salts
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/144—Alcohols; Metal alcoholates
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/50—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with organometallic compounds; with organic compounds containing boron, silicon, selenium or tellurium atoms
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/02—Natural fibres, other than mineral fibres
- D06M2101/10—Animal fibres
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
- D06M2200/01—Stain or soil resistance
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
- D06M2200/10—Repellency against liquids
- D06M2200/11—Oleophobic properties
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
- D06M2200/10—Repellency against liquids
- D06M2200/12—Hydrophobic properties
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- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Inorganic Chemistry (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
- Chemical Or Physical Treatment Of Fibers (AREA)
Abstract
The invention belongs to textile technology fields, and in particular to a kind of warming moisture-resistant self-cleaning silk scarf and preparation method thereof.The silk scarf by hydrophobic oil transportation antifouling paint pass through to silk scarf surface treatment be prepared or the silk scarf be by hydrophobic oil transportation antifouling paint by raw material silk processing after be prepared again.Silk scarf of the present invention has very strong moisture-resistant antifouling property, moist, the weather such as rain, snow, warmth retention property will not be caused to reduce because of soaking for sleet, silk scarf itself has good permeability, anti-pollution and antibacterial functions so that silk scarf can be always maintained at warming effect and comfort dry, ventilative and in cold snap.
Description
Technical field
The invention belongs to textile applications fields, and in particular to a kind of warming silk scarf of hydrophobic oil transportation automatically cleaning and its preparation side
Method.
Background technology
As the improvement of people's living standards, requirement of the people to wearing comfort and various functions is higher and higher, not
It is limited only to the level that clothing covers body, but is developed to multi-functional, diversification direction.Silk scarf can not only be brought
Attractive, decorative effect, can be with keep warm.People are when wearing silk scarf, having a meal or have tea, it is easy to by the oil stain of food or
The liquid such as beverage are done on silk scarf, and most oil stains are difficult to wash off, and can thus influence the aesthetics that silk scarf is brought to human body, can only
It discards.In cold environment, the good silk scarf of warmth retention property receives favor, but ought encounter rainy day or the larger weather of humidity and be,
Silk scarf can become moist through because of adsorption moisture, not only reduce warming effect, and reduce the comfort worn.
Invention content
It is an object of the present invention to overcome the above mentioned deficiencies, a kind of warming moisture-resistant self-cleaning silk scarf of offer and its preparation side
Method.The present invention is surface-treated silk scarf using dip coating technique, and making that treated, silk scarf does not get wet, oily dirt free, generates
Self-cleaning function, while there is good thermal property and permeability.The warming silk scarf of automatically cleaning can not only alleviate washing band
The environmental problem come, moreover it is possible to which the effectively shielding various environmental contaminants of such as spot avoid these pollutants from passing through skin
Human body is damaged.
The technical scheme is that：
A kind of warming moisture-resistant self-cleaning silk scarf, which is characterized in that the silk scarf is by hydrophobic oil transportation antifouling paint process pair
Silk scarf surface treatment be prepared or the silk scarf be by hydrophobic oil transportation antifouling paint by raw material silk processing after again
It is prepared.
Further, the hydrophobic oil transportation antifouling paint is by nonpolar nano-powder, silane coupling agent and water base low surface
It can dispersant composition；
Its mass percentage composition is：Nonpolar nano-powder：Silane coupling agent：Water base low-surface-energy dispersant=2:
0.1~1:3~5；
The nonpolarity nano-powder is silica, and silane coupling agent is siloxanes or silicon fluoride, water base low-surface-energy
Dispersant is fluorinated polypropylene acid surfaces activating agent.
Further, a diameter of 150~200 nanometers of the silica.
A kind of warming moisture-resistant self-cleaning silk scarf of the present invention is passed through by hydrophobic oil transportation antifouling paint and is surface-treated to silk scarf
It is prepared or the silk scarf is prepared again after to the processing of raw material silk by hydrophobic oil transportation antifouling paint, apply
The thickness of layer is 0.1 μm~1 μm.
A kind of warming moisture-resistant self-cleaning silk scarf of the present invention is passed through by hydrophobic oil transportation antifouling paint and is surface-treated to silk scarf
It is prepared, specifically, silk scarf finished textile product is handled, it is using dipping or spraying technology that hydrophobic oil transportation antifouling paint is equal
Even is coated on integral fabric, or every with plasma, vapor deposition method by the coating uniform treatment in silk scarf
On fiber, treated, and silk scarf has good moisture-resistant effect.
A kind of warming moisture-resistant self-cleaning silk scarf of the present invention is passed through by hydrophobic oil transportation antifouling paint to raw material silk
Be prepared again after reason, specifically, silk fiber is cleaned up, after carrying out moisture-resistant processing after drying, then using dipping, etc. from
Son, vapor deposition are by the coating uniform treatment in the fiber of silk, and treated, and silk fiber has good moisture-resistant effect.
The present invention also provides a kind of preparation method of the warming moisture-resistant self-cleaning silk scarf,
To needing the silk scarf fabric surface for carrying out automatically cleaning processing to handle, it is immersed in ethanol-water solution (preferably
Water content<5%, room temperature) after, it is rinsed with water, then dry；Hydrophobic oil transportation antifouling paint is prepared with water：Specially press quality percentage
Than by nonpolar powder silica 0.5%~3.0%, silicon fluoride 0.2%~2% and aqueous dispersion agent Zonyl3211%~
10% mixing, is added water, and stable hydrophobic oil transportation antifouling paint is obtained after stirring；
Silk scarf is immersed in the hydrophobic oil transportation antifouling paint 0.5-1 minutes (room temperature), extra solution is removed after taking-up,
It is put into baking oven to dry 10 minutes at 100 DEG C and obtains warming moisture-resistant self-cleaning silk scarf.
The present invention also provides a kind of preparation method of the warming moisture-resistant self-cleaning silk scarf,
Silk is handled first, silk surface is handled, and is immersed in ethanol-water solution (preferably water content<5%,
Room temperature) after be rinsed with water, then dry；
Hydrophobic oil transportation antifouling paint is prepared with water：By silicon fluoride or siloxanes with aqueous dispersion agent according to 1:3 mass ratioes are mixed
It closes, water is added, stable hydrophobic oil transportation antifouling paint is obtained after stirring, the mass percent of solution is 1%~10%wt/v；It will
Silk is immersed in coating about 0.5-1 minutes (room temperature), is put into 60 DEG C of -100 DEG C of drying in baking oven, treated, and silk has very well
Hydrophobic oil transportation anti-fouling effect；Can warming moisture-resistant self-cleaning silk scarf finished product be made with different weaving methods as needed.
Detailed description of the invention：
A kind of moisture-resistant, antifouling warming silk scarf, water-based coating solution include nonpolar nano-powder, silane coupling agent and water
Base low-surface-energy dispersant, silk scarf pass through dip coating and drying and processing, hydrophobic oil transportation effect that silk scarf does well that treated
Fruit, by controlling the thickness of coating, silk scarf can keep original permeability.In addition, since silk scarf surface hydrophobicity oil transportation applies
The low heat conductivity energy of layer material can make silk scarf keep good warming effect.
The object of the present invention is achieved like this：A kind of moisture-resistant, antifouling warming silk scarf, by the silicon with hydrophobic oil transportation effect
Alkane couplant, such as siloxanes or silicon fluoride are handled to every fiber surface in silk scarf using plasma technology, by drying
Treated, and silk scarf has good moisture-resistant, anti-fouling effect.
The object of the present invention is achieved like this：A kind of moisture-resistant, antifouling warming silk scarf will be applied using the method for vapor deposition
Silk scarf surface is arrived in the uniform processing of material, and the silk scarf after drying and processing has good moisture-resistant, anti-fouling effect.And it can also protect
Hold the original performance of silk scarf.For example color is ventilative, feel etc..
The object of the present invention is achieved like this：A kind of moisture-resistant, antifouling warming silk scarf, the method by handling silk first
To realize.The silk cleaned up is obtained into the silk fiber with moisture-resistant, anti-fouling effect by processing.Processing method can be used
The methods of infusion process, plasma, vapor deposition.Treated, and silk can also keep original silk fiber performance.Treated
Silk is by post-processing at silk scarf finished product so that silk scarf has good moisture-resistant, antifouling thermal property.
Moisture-resistant of the present invention, the warming silk scarf of ventilative automatically cleaning have good moisture-resistant, antifouling property, under hygrometric state, by
In not absorbing moisture, the air layer between internal fiber can be firmly lockked so that silk scarf has good warming effect, especially
It is that during the cold season, aesthetic effect can not only be played by wearing this silk scarf, and the functional of silk scarf itself can play windproof guarantor again
Warm effect.Its good moisture resistance makes it have good antifouling capacity, can resist the contamination of milk, coffee, beverage etc.,
To reduce daily washing times, extend the service life of silk scarf.
Processing method used by moisture-resistant of the present invention, the warming silk scarf of ventilative automatically cleaning does not influence the appearance and original of silk scarf
Some performances, such as color, gas permeability, comfort and feel etc..
Moisture-resistant of the present invention, the ventilative warming silk scarf of automatically cleaning be prepared by surface treatment by hydrophobic oil transportation material and
At.A variety of preparation methods, such as water based paint, plasma, vapor deposition etc. may be used.
Moisture-resistant of the present invention, the ventilative warming silk scarf processing procedure of automatically cleaning include final finishing technology, i.e., to silk scarf finished product
Fabric is handled.Water-base hydrophobic, oil transportation coating may be used, coating is uniformly coated in entirety using dipping or spraying technology
On fabric, other treatment technologies such as plasma, vapor deposition method also can be by every piece fibre of the coating uniform treatment in silk scarf
In dimension, treated, and silk scarf has good moisture-resistant effect.
Moisture-resistant of the present invention, the ventilative warming silk scarf processing procedure of automatically cleaning include that processing procedure can also include locating first
Manage silk fiber.Silk fiber is cleaned up, moisture-resistant processing is carried out after drying.Dipping, plasma, gas can be used in processing method
Mutually deposition etc..Treated, and silk fiber has good moisture-resistant effect.The silk being processed into using this moisture-resistant silk fiber
Towel has good moisture-resistant effect.
Moisture-resistant of the present invention, the ventilative warming silk scarf processing procedure of automatically cleaning include entire stereochemical structure all by processing,
So that good water delivery performance of feeding oil is presented in entire silk scarf from inside to outside.
Moisture-resistant of the present invention, the ventilative warming silk scarf of automatically cleaning are due in stronger adherency between coating and base material so that
Treated, and silk scarf has good durability.Pass through 50-200 washing test, the silk scarf after washing according to AATCC standards
Hydrophobic, oil transportation and anti-pollution characteristic remain unchanged.Processed fabric passes through 1000 wear-resisting surveys according to DMTC standards
After examination, the silk scarf after abrasion still has good hydrophobic, oil transportation and antifouling property.
The entire stereochemical structure of moisture-resistant of the present invention, the warming silk scarf of ventilative automatically cleaning all by processing, knit by final silk scarf
Every fiber in object can all have one layer of uniform coating, and it is good anti-thus so that silk scarf is integrally presented from inside to outside
Wet, antifouling property.Under hygrometric state, fiber just can firmly lock the air layer between internal fiber due to not absorbing moisture so that
Silk scarf has good warming effect.
Warming moisture-resistant self-cleaning silk scarf of the present invention is prepared as nontoxic, environmental-friendly preparation process, because
Solvent only is made with water in entire processing procedure, and it is completely useless to organic solvent.This preparation method is not only without environment dirt
Dye, but also cost can be saved.
The beneficial effects of the invention are as follows：The processing method of the hydrophobic warming silk scarf of oil transportation automatically cleaning of the present invention is simple, place
Good water delivery performance of feeding oil is presented in silk scarf after reason from inside to outside, has good automatically cleaning and warming effect, has very
Good moisture-resistant effect, permeability is good, increases the functionality and service life of silk scarf.
Description of the drawings
Fig. 1 is the coating treatment flow chart of the hydrophobic warming silk scarf fabric of oil transportation automatically cleaning of the present invention, to silk scarf finished product
It is handled.
Fig. 2 is the coating treatment flow chart of the hydrophobic warming silk scarf fabric of oil transportation automatically cleaning of the present invention, handles silkworm first
Silk method.
Fig. 3 be before and after the processing after silk scarf fabric hydrophobic performance of feeding oil, wherein yellow be water, it is transparent be paraffin oil, it is red
Color is edible olive oil, and blue is hexadecane, each droplet size is 5~20 μ L.
Fig. 4 changes for silk scarf gas permeability before and after the processing, and treated, and silk scarf permeability has almost no change.
Fig. 5 is the curve of the contact angle to water and olive oil after 200 washings with the processed silk scarf of the present invention
Variation diagram.
Fig. 6 is the curve of the contact angle to water and olive oil after 2000 abrasions with the processed silk scarf of the present invention
Variation diagram.
Specific implementation mode
Below by specific implementation mode, the present invention is further elaborated, and most preferred embodiment is embodiment 2, but of the invention
It is not limited to these embodiments.The schematic illustration of each embodiment is see Fig. 1.
Embodiment 1
To needing the silk scarf fabric surface for carrying out automatically cleaning processing to handle, 10 points are immersed in ethanol solution
Then clock is rinsed with water, remove surface dirt, grease, impurity, then dry, and ensures the drying of silk scarf fabric clean surface.
The present invention keeps original automatically cleaning effect using water as solvent.
Hydrophobic oil transportation antifouling paint is prepared, preparation method is：Nonpolar seperated (silica, 150-200 nanometers of left sides of diameter
It is right) 2 grams, it mixes, adds with silicon fluoride (0.5-1 grams) and aqueous dispersion agent (Zonyl321 fluorinated polypropylene acid surfaces activating agent)
Enter 100 milliliters of water, stable hydrophobic oil transportation coating is obtained after stirring.
Silk scarf is immersed in coating about 30 seconds and removes extra solution by 1 minute, after taking-up, is put into baking oven under 100 ° of С
Drying 10 minutes.Treated, and silk scarf surface has good hydrophobic oil transportation anti-fouling effect, and the endurance quality of coating is very
It is good, repeated washing more than 100 times or 2000 repeated wears can be subjected to still
Embodiment 2
Silk is handled first, to needing the silk surface for carrying out moisture-resistant, automatically cleaning is handled to handle, is immersed in second
It half an hour in alcoholic solution, is then rinsed with water, removes surface dirt, grease, impurity, then dry, ensure every silk fiber
Clean dried.
Hydrophobic oil transportation antifouling paint is prepared as solvent using water, preparation method is：By silicon fluoride or siloxanes and water
Water is added in base dispersant, and stable hydrophobic oil transportation coating is obtained after stirring.The final mass percentage control of solution exists
1%~5% (wt/v).Silk is immersed in coating about 30 seconds and removes extra solution by 1 minute, after taking-up, is put into baking oven
60 DEG C of -100 DEG C of drying.Treated, and silk has good hydrophobic oil transportation anti-fouling effect.Next difference can be used as needed
Weaving method final silk scarf finished product is made.Due to stronger adhesion strength between coating and silk scarf fiber base material, process is woven
The treatment effect of silk is not interfered with.Manufactured silk scarf finished product has good endurance quality, can be subjected to the weight more than 100 times
After backwashing is washed or 2000 repeated wears still maintain original automatically cleaning effect.
Example the above is only the implementation of the present invention is not intended to limit the invention, all design philosophys in the present invention
Within principle, any modification, equivalent substitution, improvement and etc. done should all be included in the protection scope of the present invention.
Claims (10)
1. a kind of warming moisture-resistant self-cleaning silk scarf, which is characterized in that the silk scarf is passed through to silk by hydrophobic oil transportation antifouling paint
Towel surface treatment is prepared or the silk scarf is made again after to the processing of raw material silk by hydrophobic oil transportation antifouling paint
It is standby to form.
2. a kind of warming moisture-resistant self-cleaning silk scarf according to claim 1, which is characterized in that hydrophobic oil transportation antifouling paint is by non-
Polar nano powder, silane coupling agent and water base low-surface-energy dispersant composition；
Its mass percentage composition is：Nonpolar nano-powder：Silane coupling agent：Water base low-surface-energy dispersant=2:0.1~
1:3~5；
The nonpolarity nano-powder is silica, and silane coupling agent is siloxanes or silicon fluoride, water base low-surface-energy dispersion
Agent is fluorinated polypropylene acid surfaces activating agent.
3. a kind of warming moisture-resistant self-cleaning silk scarf according to claim 2, which is characterized in that the silica it is a diameter of
150~200 nanometers.
4. a kind of warming moisture-resistant self-cleaning silk scarf according to claim 1, which is characterized in that the silk scarf is by hydrophobic oil transportation
Antifouling paint pass through to silk scarf surface treatment be prepared or the silk scarf be by hydrophobic oil transportation antifouling paint pass through to former material
It is prepared again after material silk processing, the thickness of coating is 0.1 μm~1 μm.
5. a kind of warming moisture-resistant self-cleaning silk scarf according to claim 1, which is characterized in that the silk scarf is by hydrophobic oil transportation
Antifouling paint, which passes through, is prepared silk scarf surface treatment, specifically, handling silk scarf finished textile product, utilizes dipping or spray
Hydrophobic oil transportation antifouling paint is uniformly coated on integral fabric by painting technology, or will be described with plasma, vapor deposition method
Coating uniform treatment is on the every fiber in silk scarf, and treated, and silk scarf has good moisture-resistant effect.
6. a kind of warming moisture-resistant self-cleaning silk scarf according to claim 1, which is characterized in that the silk scarf is by hydrophobic oil transportation
Antifouling paint is prepared again after to the processing of raw material silk, specifically, silk fiber is cleaned up, is carried out after drying
After moisture-resistant processing, then using dipping, plasma, vapor deposition by the coating uniform treatment in the fiber of silk, treated
Silk fiber has good moisture-resistant effect.
7. the preparation method of warming moisture-resistant self-cleaning silk scarf described in a kind of claim 1, which is characterized in that
To needing the silk scarf fabric surface for carrying out automatically cleaning processing to handle, after being immersed in ethanol-water solution, rushed with water
It washes, then dries；Hydrophobic oil transportation antifouling paint is prepared with water：Specially by mass percentage by nonpolar powder silica
0.5%~3.0%, silicon fluoride 0.2%~2% and aqueous dispersion agent Zonyl3211%~10% are mixed, and water are added, after stirring
Obtain stable hydrophobic oil transportation antifouling paint；
Silk scarf is immersed in the hydrophobic oil transportation antifouling paint 0.5-1 minutes, extra solution is removed after taking-up, is put into baking oven
It is dried 10 minutes at 100 DEG C and obtains warming moisture-resistant self-cleaning silk scarf.
8. the preparation method of warming moisture-resistant self-cleaning silk scarf according to claim 7, which is characterized in that the alcohol-water is molten
Liquid is water content<5%.
9. the preparation method of warming moisture-resistant self-cleaning silk scarf described in a kind of claim 1, which is characterized in that
Silk is handled first, silk surface is handled, and is rinsed with water after being immersed in ethanol-water solution, then dry；
Hydrophobic oil transportation antifouling paint is prepared with water：By silicon fluoride or siloxanes with aqueous dispersion agent according to 1:3 mass ratioes mix, and add
Enter water, stable hydrophobic oil transportation antifouling paint is obtained after stirring, the mass percent of solution is 1%~10%wt/v；By silk
It is immersed in coating about 0.5-1 minutes, is put into 60 DEG C of -100 DEG C of drying in baking oven, treated, and silk has good hydrophobic oil transportation
Anti-fouling effect；Can warming moisture-resistant self-cleaning silk scarf finished product be made with different weaving methods as needed.
10. the preparation method of warming moisture-resistant self-cleaning silk scarf according to claim 9, which is characterized in that the alcohol-water is molten
Liquid is water content<5%.
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| AU2014203168A1 (en) * | 2007-05-18 | 2014-07-03 | Invista Technologies S.A R.L. | Method and composition for treating fibrous substrates |
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