CN108641437A - A kind of insulating glass coating and preparation method thereof - Google Patents
A kind of insulating glass coating and preparation method thereof Download PDFInfo
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- CN108641437A CN108641437A CN201810294242.4A CN201810294242A CN108641437A CN 108641437 A CN108641437 A CN 108641437A CN 201810294242 A CN201810294242 A CN 201810294242A CN 108641437 A CN108641437 A CN 108641437A
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- insulating glass
- glass coating
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- 239000011521 glass Substances 0.000 title claims abstract description 35
- 238000000576 coating method Methods 0.000 title claims abstract description 30
- 239000011248 coating agent Substances 0.000 title claims abstract description 28
- 238000002360 preparation method Methods 0.000 title claims abstract description 20
- 239000006185 dispersion Substances 0.000 claims abstract description 20
- 239000012530 fluid Substances 0.000 claims abstract description 20
- YCKRFDGAMUMZLT-UHFFFAOYSA-N Fluorine atom Chemical compound [F] YCKRFDGAMUMZLT-UHFFFAOYSA-N 0.000 claims abstract description 15
- 229910052731 fluorine Inorganic materials 0.000 claims abstract description 15
- 239000011737 fluorine Substances 0.000 claims abstract description 15
- 239000002562 thickening agent Substances 0.000 claims abstract description 12
- 239000008367 deionised water Substances 0.000 claims abstract description 11
- 229910021641 deionized water Inorganic materials 0.000 claims abstract description 11
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 10
- 239000002518 antifoaming agent Substances 0.000 claims abstract description 9
- 239000002270 dispersing agent Substances 0.000 claims description 11
- 239000004744 fabric Substances 0.000 claims description 10
- 229920001774 Perfluoroether Polymers 0.000 claims description 9
- 125000000118 dimethyl group Chemical group [H]C([H])([H])* 0.000 claims description 8
- 239000003002 pH adjusting agent Substances 0.000 claims description 8
- 229920005573 silicon-containing polymer Polymers 0.000 claims description 8
- ABBZJHFBQXYTLU-UHFFFAOYSA-N but-3-enamide Chemical compound NC(=O)CC=C ABBZJHFBQXYTLU-UHFFFAOYSA-N 0.000 claims description 7
- UJMWVICAENGCRF-UHFFFAOYSA-N oxygen difluoride Chemical compound FOF UJMWVICAENGCRF-UHFFFAOYSA-N 0.000 claims description 7
- QGLKJKCYBOYXKC-UHFFFAOYSA-N nonaoxidotritungsten Chemical compound O=[W]1(=O)O[W](=O)(=O)O[W](=O)(=O)O1 QGLKJKCYBOYXKC-UHFFFAOYSA-N 0.000 claims description 6
- 229910001930 tungsten oxide Inorganic materials 0.000 claims description 6
- 238000001914 filtration Methods 0.000 claims description 5
- 239000002994 raw material Substances 0.000 claims description 5
- 239000002002 slurry Substances 0.000 claims description 5
- 239000007787 solid Substances 0.000 claims description 5
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 claims description 4
- 239000007822 coupling agent Substances 0.000 claims description 4
- 239000010703 silicon Substances 0.000 claims description 4
- 229910052710 silicon Inorganic materials 0.000 claims description 4
- 239000003513 alkali Substances 0.000 claims description 3
- 239000000203 mixture Substances 0.000 claims description 3
- 229940058020 2-amino-2-methyl-1-propanol Drugs 0.000 claims description 2
- CBTVGIZVANVGBH-UHFFFAOYSA-N aminomethyl propanol Chemical group CC(C)(N)CO CBTVGIZVANVGBH-UHFFFAOYSA-N 0.000 claims description 2
- -1 perfluoroether alkene Chemical class 0.000 claims 3
- CWAFVXWRGIEBPL-UHFFFAOYSA-N ethoxysilane Chemical compound CCO[SiH3] CWAFVXWRGIEBPL-UHFFFAOYSA-N 0.000 claims 1
- 239000007788 liquid Substances 0.000 claims 1
- WGYKZJWCGVVSQN-UHFFFAOYSA-N propylamine Chemical class CCCN WGYKZJWCGVVSQN-UHFFFAOYSA-N 0.000 claims 1
- 238000002834 transmittance Methods 0.000 abstract description 5
- 238000002955 isolation Methods 0.000 abstract description 3
- 230000003287 optical effect Effects 0.000 abstract description 3
- 238000009413 insulation Methods 0.000 abstract description 2
- 229920002050 silicone resin Polymers 0.000 abstract 1
- 238000005265 energy consumption Methods 0.000 description 6
- 239000006087 Silane Coupling Agent Substances 0.000 description 4
- 239000003795 chemical substances by application Substances 0.000 description 3
- 238000000034 method Methods 0.000 description 3
- WYTZZXDRDKSJID-UHFFFAOYSA-N (3-aminopropyl)triethoxysilane Chemical group CCO[Si](OCC)(OCC)CCCN WYTZZXDRDKSJID-UHFFFAOYSA-N 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 230000005855 radiation Effects 0.000 description 2
- 239000000853 adhesive Substances 0.000 description 1
- 230000001070 adhesive effect Effects 0.000 description 1
- 230000032683 aging Effects 0.000 description 1
- 230000004888 barrier function Effects 0.000 description 1
- 230000005540 biological transmission Effects 0.000 description 1
- 239000003245 coal Substances 0.000 description 1
- 238000001514 detection method Methods 0.000 description 1
- 235000013870 dimethyl polysiloxane Nutrition 0.000 description 1
- 239000004205 dimethyl polysiloxane Substances 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 238000000465 moulding Methods 0.000 description 1
- BDERNNFJNOPAEC-UHFFFAOYSA-N n-propyl alcohol Natural products CCCO BDERNNFJNOPAEC-UHFFFAOYSA-N 0.000 description 1
- 239000003921 oil Substances 0.000 description 1
- 229920000435 poly(dimethylsiloxane) Polymers 0.000 description 1
- 230000011514 reflex Effects 0.000 description 1
- 239000011347 resin Substances 0.000 description 1
- 229920005989 resin Polymers 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D4/00—Coating compositions, e.g. paints, varnishes or lacquers, based on organic non-macromolecular compounds having at least one polymerisable carbon-to-carbon unsaturated bond ; Coating compositions, based on monomers of macromolecular compounds of groups C09D183/00 - C09D183/16
- C09D4/06—Organic non-macromolecular compounds having at least one polymerisable carbon-to-carbon unsaturated bond in combination with a macromolecular compound other than an unsaturated polymer of groups C09D159/00 - C09D187/00
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/004—Reflecting paints; Signal paints
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/24—Electrically-conducting paints
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/61—Additives non-macromolecular inorganic
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Paints Or Removers (AREA)
Abstract
The invention discloses a kind of insulating glass coating and preparation method thereof, a kind of insulating glass coating of the invention, including according to the mass fraction following group are grouped as：15 20 parts of deionized water, 0.3 0.6 parts of antifoaming agent, 30 60 parts of nano dispersion fluid, 0.6 1 parts of thickener, 35 55 parts of fluorine richness modified organic silicone resin.The present invention has high light transmittance, does not influence the optical property of glass；High thermal insulation, effectively obstructs solar energy；The advantages that high ultraviolet light isolation rate.
Description
Technical field
The present invention relates to technical field of coatings, and in particular to a kind of insulating glass coating and preparation method thereof.
Background technology
Currently, China's building energy consumption is higher by one times than western developed country, with oil, coal it is in short supply, price is not
Disconnected to go up, energy supply is more becoming tight, and country attaches great importance to energy-saving and emission-reduction, advocates and develop energy-conserving product energetically.According to statistics
China accounts for the 40% of total energy consumption by the energy consumption that building loses, and is about 46% by the energy that door and window loses, if passed through
Insulating moulding coating product is used to the glass of door and window, function of the glass to the selective transmission of light can be made, visible light can penetrated
Under the premise of not influencing daylighting, shielding infrared light, ultraviolet light, block heat radiation, reduce summer sunlight enter be can heat,
Air conditioner refrigerating energy consumption is reduced, while reducing energy consumption of the winter heat by radiation loss, improves heating efficiency, to reach building
Energy-efficient purpose.
Glass heat-proof currently on the market is mainly Low-E glass and adhering film to glass, the investment of Low-E glass production lines is big,
High energy consumption in product cost height and production, does not meet ideas of energy-saving；Adhering film to glass is made due to its adhesive meeting chronological aging
Phenomena such as film forming blisters, falls off.Therefore a glass coating with high heat-proof quality is developed to have a very big significance.
Currently, lacking a kind of insulating glass coating and preparation method thereof with high light transmittance.
Invention content
The purpose of the present invention is to provide one kindWith high light transmittanceInsulating glass coating and preparation method thereof.
In order to achieve the above objectives, present invention employs following technical proposals：A kind of insulating glass coating of the present invention, including
Following group according to the mass fraction is grouped as：
Further, the antifoaming agent is organic silicon antifoaming agent.
Further, the fluorine richness organic siliconresin is the mixed of perfluoroether allyl amide and dimethyl silicone polymer
The mass ratio of conjunction object, the perfluoroether allyl amide and dimethyl silicone polymer is 0.15:0.85, fluorine richness organosilicon tree
Fat solid content is 47 ± 3%.
Further, the thickener is that alkali soluble rises class thickener.
Further, the nano dispersion fluid includes that by mass percentage following group is grouped as：
Further, the dispersant is non-ionic dispersing agent；The pH adjusting agent is 2- amino-2-methyls-
1- propyl alcohol；The coupling agent is gamma-aminopropyl-triethoxy-silane.
The preparation method of insulating glass coating of the present invention, includes the following steps：
(1) deionized water is added, by raw material proportioning in parts by weight precise each component according to claim 1
Antifoaming agent, nano dispersion fluid and fluorine richness organic siliconresin, jitter time 10-15min is added；
(2) step (1) slurry thickener is adjusted into viscosity to 25-35s, with filter-cloth filtering, finished product.
Further, in step (1), the preparation method of nano dispersion fluid：Precise deionized water addition dispersant,
PH adjusting agent and silane coupling agent, jitter time 3-5min are added nano ATO, nanometer tungsten oxide using ultrasonic disperse, are made
Nano dispersion fluid.
Further, in step (2), the filter cloth is 200-300 mesh.
Advantageous effect：The present invention has high light transmittance, does not influence the optical property of glass；High thermal insulation, effectively barrier are too
Sunlight energy；The advantages that high ultraviolet light isolation rate.
Compared with prior art, coating of the invention is particularly advantageous in that：
(1) optical property for utilizing nano ATO special, there is very high resistance in infrared light district long wavelength part and ultraviolet region
Reinforce the reflex to near-infrared region energy using nanometer tungsten oxide simultaneously every rate；
(2) resin obtained by perfluoroether allyl amide modified dimethyl polysiloxane is utilized, in the heat that ensure that organosilicon
It is stability, flexible while obtaining excellent cryogenic property, solvent resistance and weather resistance, uvioresistant and anti-
Antistatic property is excellent.
Specific implementation mode
By following embodiment, present invention be described in more detail, but should be noted that the scope of the present invention is not implemented by these
Any restrictions of example.
Embodiment 1
A kind of insulating glass coating of invention, including according to the mass fraction following group are grouped as：
The antifoaming agent is organic silicon antifoaming agent.
The fluorine richness organic siliconresin is the mixture of perfluoroether allyl amide and dimethyl silicone polymer, described
Perfluoroether allyl amide and dimethyl silicone polymer mass ratio be 0.15:0.85, fluorine richness organic siliconresin solid content
It is 47%.The thickener is that alkali soluble rises class thickener.
The nano dispersion fluid includes that by mass percentage following group is grouped as：
The dispersant is non-ionic dispersing agent；The pH adjusting agent is 2-amino-2-methyl-1-propanol；Institute
The coupling agent stated is gamma-aminopropyl-triethoxy-silane.
The preparation method of insulating glass coating of the present invention, includes the following steps：
(1) according to the parts by weight precise each component, deionized water is added, is added and defoams by raw material proportioning
Agent, nano dispersion fluid and fluorine richness organic siliconresin, jitter time 10min；In step (1), the preparation of nano dispersion fluid
Method：Dispersant, pH adjusting agent and silane coupling agent is added in precise deionized water, and nanometer is added in jitter time 3min
ATO, nanometer tungsten oxide use ultrasonic disperse, and nano dispersion fluid is made.
(2) step (1) slurry thickener is adjusted into viscosity to 35s, with filter-cloth filtering, finished product.The filter cloth
For 200 mesh.
Embodiment 2
Embodiment 2 and embodiment 1 difference lies in：
A kind of insulating glass coating of the present invention, including according to the mass fraction following group are grouped as：
The fluorine richness organic siliconresin is the mixture of perfluoroether allyl amide and dimethyl silicone polymer, described
Perfluoroether allyl amide and dimethyl silicone polymer mass ratio be 0.15:0.85, fluorine richness organic siliconresin solid content
It is 44%.The nano dispersion fluid includes that by mass percentage following group is grouped as：
The preparation method of insulating glass coating of the present invention, includes the following steps：
(1) according to the parts by weight precise each component, deionized water is added, is added and defoams by raw material proportioning
Agent, nano dispersion fluid and fluorine richness organic siliconresin, jitter time 15min；In step (1), the preparation of nano dispersion fluid
Method：Dispersant, pH adjusting agent and silane coupling agent is added in precise deionized water, and nanometer is added in jitter time 4min
ATO, nanometer tungsten oxide use ultrasonic disperse, and nano dispersion fluid is made.
(2) step (1) slurry thickener is adjusted into viscosity to 28s, with filter-cloth filtering, finished product.The filter cloth
For 250 mesh.
Embodiment 3
Embodiment 3 and embodiment 1 difference lies in：
A kind of insulating glass coating of the present invention, including according to the mass fraction following group are grouped as：
Fluorine richness organic siliconresin solid content is 50%.
The nano dispersion fluid includes that by mass percentage following group is grouped as：
The preparation method of insulating glass coating of the present invention, includes the following steps：
(1) according to the parts by weight precise each component, deionized water is added, is added and defoams by raw material proportioning
Agent, nano dispersion fluid and fluorine richness organic siliconresin, jitter time 12min；In step (1), the preparation of nano dispersion fluid
Method：Dispersant, pH adjusting agent and silane coupling agent is added in precise deionized water, and nanometer is added in jitter time 5min
ATO, nanometer tungsten oxide use ultrasonic disperse, and nano dispersion fluid is made.
(2) step (1) slurry thickener is adjusted into viscosity to 25s, with filter-cloth filtering, finished product.The filter cloth
For 300 mesh.
Experiment 1
The insulating glass coating progress performance detection of the present invention, all technical measured, as shown in table 1：
Table 1
As can be seen from Table 1, the coating prepared by the embodiment of the present invention 1~3 has excellent high light transmittance, height heat-insulated
The advantages that property, high ultraviolet light isolation rate.
The basic principles, main features and advantages of the present invention have been shown and described above.The technology of the industry
Personnel are it should be appreciated that the present invention is not limited to the above embodiments, and the above embodiments and description only describe this
The principle of invention, without departing from the spirit and scope of the present invention, various changes and improvements may be made to the invention, the present invention
Claimed range is delineated by the appended claims, the specification and equivalents thereof from the appended claims.
Claims (9)
1. a kind of insulating glass coating, it is characterised in that be grouped as including following group according to the mass fraction：
2. the insulating glass coating described in parts by weight according to claim 1, it is characterised in that：The antifoaming agent is
Organic silicon antifoaming agent.
3. the insulating glass coating and preparation method thereof described in parts by weight according to claim 1, it is characterised in that：Institute
The fluorine richness organic siliconresin stated is the mixture of perfluoroether allyl amide and dimethyl silicone polymer, the perfluoroether alkene
The mass ratio of propyl amides and dimethyl silicone polymer is 0.15:0.85, fluorine richness organic siliconresin solid content is 47 ± 3%.
4. the insulating glass coating and preparation method thereof described in parts by weight according to claim 1, it is characterised in that：Institute
The thickener stated is that alkali soluble rises class thickener.
5. the insulating glass coating described in parts by weight according to claim 1, it is characterised in that：The nano-dispersed
Liquid includes that by mass percentage following group is grouped as：
6. the insulating glass coating described in parts by weight according to claim 1, it is characterised in that：The dispersant is
Non-ionic dispersing agent；The pH adjusting agent is 2-amino-2-methyl-1-propanol；The coupling agent is γ-aminopropyl three
Ethoxysilane.
7. the preparation method of claim 1-6 any one of them insulating glass coatings, it is characterised in that include the following steps：
(1) deionized water is added in parts by weight precise each component according to claim 1, is added by raw material proportioning
Antifoaming agent, nano dispersion fluid and fluorine richness organic siliconresin, jitter time 10-15min；
(2) step (1) slurry thickener is adjusted into viscosity to 25-35s, with filter-cloth filtering, finished product.
8. the preparation method of insulating glass coating according to claim 7, it is characterised in that：
In step (1), the preparation method of nano dispersion fluid：Dispersant, pH adjusting agent and silicon is added in precise deionized water
Alkane coupling agent, nano ATO is added in jitter time 3-5min, nanometer tungsten oxide uses ultrasonic disperse, obtained nano dispersion fluid.
9. the preparation method of insulating glass coating according to claim 7, it is characterised in that：It is described in step (2)
Filter cloth is 200-300 mesh.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810294242.4A CN108641437A (en) | 2018-04-03 | 2018-04-03 | A kind of insulating glass coating and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810294242.4A CN108641437A (en) | 2018-04-03 | 2018-04-03 | A kind of insulating glass coating and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN108641437A true CN108641437A (en) | 2018-10-12 |
Family
ID=63745276
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201810294242.4A Pending CN108641437A (en) | 2018-04-03 | 2018-04-03 | A kind of insulating glass coating and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN108641437A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115260821A (en) * | 2022-07-19 | 2022-11-01 | 广州大学 | Transparent heat-insulating coating with microstructure and preparation method and application thereof |
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-
2018
- 2018-04-03 CN CN201810294242.4A patent/CN108641437A/en active Pending
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| CN102643434A (en) * | 2012-04-23 | 2012-08-22 | 上海大学 | Preparation method and application of epoxy fluoro-silicone resin |
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| Title |
|---|
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