CN108636317A - A kind of heating of collection be mixed in integrated reaction kettle device - Google Patents

A kind of heating of collection be mixed in integrated reaction kettle device Download PDF

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Publication number
CN108636317A
CN108636317A CN201810493440.3A CN201810493440A CN108636317A CN 108636317 A CN108636317 A CN 108636317A CN 201810493440 A CN201810493440 A CN 201810493440A CN 108636317 A CN108636317 A CN 108636317A
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CN
China
Prior art keywords
tank body
heating
rotary shaft
mixed
brush
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Pending
Application number
CN201810493440.3A
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Chinese (zh)
Inventor
何磊
张冠龙
邵胜健
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Individual
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Individual
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Priority to CN201810493440.3A priority Critical patent/CN108636317A/en
Publication of CN108636317A publication Critical patent/CN108636317A/en
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18Stationary reactors having moving elements inside
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0006Controlling or regulating processes
    • B01J19/0013Controlling the temperature of the process
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049Controlling or regulating processes
    • B01J2219/00051Controlling the temperature
    • B01J2219/00132Controlling the temperature using electric heating or cooling elements
    • B01J2219/00135Electric resistance heaters

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)

Abstract

The invention discloses a kind of heating of collection and it is mixed in integrated reaction kettle device, heating stirrer including mixing tank body and mounted on mixing tank interior, mix tank body top connection charging manifold, it mixes tank body bottom side and connects drainage conduit, in mixing tank body top middle portion through connection rotary shaft, rotary shaft bottom is connected with heating stirrer, heating stirrer is by stirring frame, stull, thermal conductive silicon gum cover, binding post and heating plate composition, the positive and negative terminals of electrode circuit plate are connect one by one with two connecting lines, connecting line is threaded through in the rotary shaft of hollow structure, connecting line is connected with the conductive mechanism mounted on rotary shaft top;The heat that heating plate electrified regulation generates is conducted by thermal conductive silicon gum cover, the feed liquid in deflector hole that convection current is formed via several thermal conductive silicon gum covers and several stulls is heated, and heating stirrer keeps good electrical contact, improves overall stability and heating efficiency, feed liquid circulation is reinforced, and mixing efficiency is high.

Description

A kind of heating of collection be mixed in integrated reaction kettle device
Technical field
The present invention relates to chemical fields, more specifically, it relates to which a kind of collection heating is filled with integrated reaction kettle is mixed in It sets.
Background technology
With the development of Chinese industrial, industrial chemicals demand is increasing, needs to mix raw material in chemical process Stirring is closed, and needs, by providing suitable temperature and stirring, to improve production efficiency, mixing is needed to use blender, be stirred It mixes device and is also known as reaction kettle, reaction kettle is widely used in oil, chemical industry, rubber, pesticide, dyestuff, medicine and food engineering, has been used for At the pressure vessel of the technical process such as vulcanization, nitrification, hydrogenation, hydrocarbonylation, polymerization and condensation.
Reaction kettle refers to being held according to different process conditions demands with the rustless steel container physically or chemically reacted The structure design and parameter configuration of device, design condition, process, inspection and manufacture, examination are needed according to Its Relevant Technology Standards, to realize The heating of technological requirement, evaporation, cooling and low high speed mixture response function.Many reaction kettles are all single-blade stirrings at present, this The reaction kettle of sample frequently can lead to the uneven thorough of stirring, and only have the function of stirring, be needed in the control to temperature Heating device is added in inner wall of kettle or outer wall, thermal losses is serious and heating effect is poor, and stirring efficiency is relatively low, when needing longer Between can stir evenly, temperature heating is uneven, and temperature control is inaccurate, while energy consumption is big, and heat utilization ratio is low, city Field needs one kind that can be evenly heated, while can improve the industrial chemicals hybrid reaction blender of temperature utilization rate.
Invention content
In view of the deficiencies of the prior art, the present invention intends to provide a kind of collection heating be mixed in it is integrated anti- Kettle device is answered, the problems mentioned above in the background art have been solved.
To achieve the above object, the present invention provides the following technical solutions:
A kind of heating of collection be mixed in integrated reaction kettle device, including mixing tank body and mounted on mixing tank interior plus Thermal agitation device, mixing tank body top connection charging manifold, mixing tank body bottom side connect drainage conduit, are passed through in mixing tank body top middle portion Connection rotary shaft is worn, the rotary shaft is connected by mechanical seal with mixing tank body, is fixed in the rotary shaft outside blending tank body Sprocket wheel one, sprocket wheel one connect sprocket wheel two by driving chain, and sprocket wheel two is fixed in the drive shaft of servo motor, servo motor peace On the motor rack of mixing tank wall, started by servo motor, rotary shaft bottom is driven to be rotated with heating stirrer, heating Blender stirs the feed liquid in blending tank body, and rotary shaft bottom is connected with heating stirrer, heating stirrer by stirring frame, Stull, thermal conductive silicon gum cover, binding post and heating plate composition, stirring frame top middle portion are connected to a fixed with rotary shaft bottom end, stir It mixes and is laterally equidistantly equipped with several stulls in frame, it is longitudinal in stirring frame to be equidistantly equipped with several thermal conductive silicon gum covers, thermal conductive silicon gum cover It is embedded in heating plate, heating plate upper end connects binding post, and binding post is connected with the end row on electrode circuit plate, electrode circuit plate Positive and negative terminals connect one by one with two connecting lines, connecting line is threaded through in the rotary shaft of hollow structure, connecting line with installation Conductive mechanism on rotary shaft top is connected, and conductive mechanism is by positive pole current collections ring, cathode collector ring, brush one, brush two, just Pole electric wire and negative electrical wire composition, positive pole current collections ring and cathode collector ring are fixed on rotary shaft tip exterior, positive pole current collections ring by The positive terminals of a piece connecting line connection electrode wiring board, cathode collector ring is by the negative of another connecting line connection electrode wiring board Terminals.
Further, muff, charging manifold connection feed liquids pipe one and feed liquid pipe two, feed liquid are equipped with outside the blending tank body It is mounted on non-return valve on pipe one and feed liquid pipe two, facilitates and inputs two kinds of feed liquids in blending tank body by charging manifold, and thereon The non-return valve of installation prevents feed liquid from flowing backwards.
Further, the thermal conductive silicon gum cover is wrapped in outside heating plate, and connection connection copper sheet in heating plate lower end connects copper sheet It is connected on heating plate internal circuit.
Further, insulation filling is equipped in the rotary shaft, insulation filling is polyethylene foam insulation, and guarantee is filled out in insulation The insulation performance of the two strands of connecting lines worn in rotary shaft is also fixed this two strands of connecting lines, makes it together with rotary shaft Stablize rotation, avoid hitting with rotary shaft inner wall or winds each other.
Further, the conductive mechanism is set in insulating shield, and insulating shield connects mixing tank body by fixed frame.
Further, it is equipped with brush one on the outside of the positive pole current collections ring and is in contact with brush one, brush one connects positive electricity Line;It is equipped with brush two on the outside of cathode collector ring and is in contact with brush two, brush two connects negative electrical wire.
Further, the deflector hole of several thermal conductive silicon gum covers in the stirring frame and several stull square crossings composition.
In conclusion the present invention has the advantages that compared with prior art:
The present invention connects alternating current by positive electrical wire with negative electrical wire, to make electrode circuit plate power on, with electrode circuit plate The heat that connected heating plate electrified regulation generates is conducted by thermal conductive silicon gum cover, and convection current is via several thermal conductive silicon gum covers and several cross The feed liquid supportted in the deflector hole of composition is heated, and heating while is sufficiently mixed, and heating stirrer keeps good electricity Contact improves overall stability and heating efficiency, and feed liquid circulation is reinforced, and mixing efficiency is high.
More clearly to illustrate the structure feature and effect of the present invention, come below in conjunction with the accompanying drawings to this hair with specific embodiment It is bright to be described in detail.
Description of the drawings
Fig. 1 is the structural diagram of the present invention.
Fig. 2 is the structural schematic diagram of heating stirrer in the present invention.
Fig. 3 is the structural schematic diagram of conductive mechanism in the present invention.
Fig. 4 is the structural schematic diagram of heating plate in the present invention.
Reference numeral:1- feed liquids pipe one, 2- feed liquids pipe two, 3- charging manifold, 4- insulating shield, 5- conductive mechanisms, 6- are solid It is close to determine frame, 7- sprocket wheels one, 8- driving chains, 9- sprocket wheels two, 10- drive shafts, 11- servo motors, 12- rotary shafts, 13- machineries Envelope, 14- mixing tank body, 15- muffs, 16- heating stirrers, 17- drainage conduits, 18- stirring frames, 19- stulls, 20- thermal conductive silicons Gum cover, 21- binding posts, 22- connecting lines, 23- electrode circuits plate, the ends 24- row, 25- deflector holes, 26- connections copper sheet, 27- anodes Collector ring, 28- cathode collector ring, 29- brushes one, 30- brushes two, 31- positive electrical wires, 32- negative electrical wires, 33- heating plates.
Specific implementation mode
The following further describes the technical solution of the present invention in the following with reference to the drawings and specific embodiments.
Referring to Fig. 1-4, a kind of heating of collection be mixed in integrated reaction kettle device, including mixing tank body 14 and be mounted on The heating stirrer 16 inside tank body 14 is mixed, 14 outside of the mixing tank body is equipped with muff 15, and 14 top of mixing tank body connects Material manifold 3 is tapped into, charging manifold 3 is connected to feed liquid pipe 1 and feed liquid pipe 22, is mounted on feed liquid pipe 1 and feed liquid pipe 22 Non-return valve facilitates and is input in charging manifold 3 two kinds of feed liquids by feed liquid pipe 1 and feed liquid pipe 22 respectively and enters blending tank In body 14,14 bottom side of mixing tank body connects drainage conduit 17, and drainage conduit 17 is connected to 14 inside of mixing tank body, for that will heat mixing Feed liquid discharge after fully.
Mixing 14 top middle portion of tank body through connection rotary shaft 12, rotary shaft 12 with mix tank body 14 by mechanical seal 13 It is connected, 12 bottom of rotary shaft is connected with heating stirrer 16, mixes and is fixed with sprocket wheel one in the rotary shaft 12 outside tank body 14 7, sprocket wheel 1 connects sprocket wheel 29 by driving chain 8, and sprocket wheel 29 is fixed in the drive shaft 10 of servo motor 11, servo electricity Machine 11 is mounted on the motor rack of mixing 14 outer wall of tank body, drives drive shaft 10 to rotate after servo motor 11 powers on, and is driven Sprocket wheel 29 on moving axis 10 drives the sprocket wheel 1 being attached thereto to rotate by driving chain 8, to drive 12 bottom of rotary shaft It is rotated with heating stirrer 16, heating stirrer 16 stirs the feed liquid in mixing tank body 14.
The heating stirrer 16 is by 33 groups of stirring frame 18, stull 19, thermal conductive silicon gum cover 20, binding post 21 and heating plate At 18 top middle portion of stirring frame is connected to a fixed with 12 bottom end of rotary shaft, and several stulls are laterally equidistantly equipped in stirring frame 18 19, longitudinal in stirring frame 18 to be equidistantly equipped with several thermal conductive silicon gum covers 20, thermal conductive silicon gum cover 20 has been embedded in heating plate 33, heat conduction Silica gel sheath 20 is wrapped in outside heating plate 33, and for insulation and heat conduction, connection connection copper sheet 26 in 33 lower end of heating plate connects copper sheet 26 are connected on 3 internal circuit of heating plate, conducting when for being powered;33 upper end of heating plate connects binding post 21, binding post 21 It being connect with the end row 24 on electrode circuit plate 23, the positive and negative terminals of electrode circuit plate 23 are connect one by one with two connecting lines 22, Connecting line 22 is threaded through in the rotary shaft 12 of hollow structure, and insulation filling is equipped in rotary shaft 12, and preferably polyethylene foam insulate Layer.
Conductive mechanism 5 is installed on 12 top of rotary shaft, conductive mechanism 5 is set in insulating shield 4, and insulating shield 4 is logical The connection mixing tank body 14 of fixed frame 6 is crossed, conductive mechanism 5 is by positive pole current collections ring 27, cathode collector ring 28, brush 1, brush two 30, positive electrical wire 31 and negative electrical wire 32 form, and positive pole current collections ring 27 and cathode collector ring 28 are fixed on outside 12 top of rotary shaft Portion, positive pole current collections ring 27 is by the positive terminals of a 22 connection electrode wiring board 23 of connecting line, and cathode collector ring 28 is by another The negative terminals of 22 connection electrode wiring board 23 of connecting line;The outside of positive pole current collections ring 27 be equipped with brush 1 and with one 29 phase of brush Contact, brush 1 connect positive electrical wire 31;28 outside of cathode collector ring is equipped with brush 2 30 and is in contact with brush 2 30, electricity Brush 2 30 connection negative electrical wires 32.
Alternating current is connected with negative electrical wire 32 by positive electrical wire 31, to make electrode circuit plate 23 power on, with electrode wires The heat that connected 33 electrified regulation of heating plate of road plate 23 generates is conducted by thermal conductive silicon gum cover 20, and convection current is via several heat conductive silica gels The feed liquid in deflector hole 25 that set 20 and several stulls 19 form is heated, and heating while is sufficiently mixed, and heating is stirred It mixes device 16 and keeps good electrical contact, improve overall stability and heating efficiency, feed liquid circulation is reinforced, and mixing efficiency is high.
The technical principle that the present invention is described above in association with specific embodiment, is only the preferred embodiment of the present invention.This The protection domain of invention is not limited merely to above-described embodiment, and all technical solutions belonged under thinking of the present invention belong to the present invention Protection domain.Those skilled in the art would not require any inventive effort the other specific realities that can associate the present invention Mode is applied, these modes are fallen within protection scope of the present invention.

Claims (7)

1. a kind of collection heats and is mixed in integrated reaction kettle device, including mixes tank body (14) and be mounted on mixing tank body (14) internal heating stirrer (16), which is characterized in that mixing tank body (14) top connection charging manifold (3) mixes tank body (14) bottom side connection drainage conduit (17), mixing tank body (14) top middle portion through connection rotary shaft (12), rotary shaft (12) with It mixes tank body (14) by mechanical seal (13) to be connected, sprocket wheel one (7) is fixed in the external rotary shaft (12) of mixing tank body (14), Sprocket wheel one (7) connects sprocket wheel two (9) by driving chain (8), and sprocket wheel two (9) is fixed on the drive shaft (10) of servo motor (11) On, servo motor (11) is mounted on the motor rack of mixing tank body (14) outer wall, rotary shaft (12) bottom and heating stirrer (16) be connected, heating stirrer (16) by stirring frame (18), stull (19), thermal conductive silicon gum cover (20), binding post (21) and Heating plate (33) forms, and stirring frame (18) top middle portion is connected to a fixed with rotary shaft (12) bottom end, in stirring frame (18) laterally Several stulls (19) are equidistantly equipped with, longitudinal direction is equidistantly equipped with several thermal conductive silicon gum covers (20), heat conductive silica gel in stirring frame (18) Set (20) has been embedded in heating plate (33), and heating plate (33) upper end connects binding post (21), binding post (21) and electrode circuit plate (23) end row (24) connection on, the positive and negative terminals of electrode circuit plate (23) connect with two connecting lines (22), connect one by one Line (22) is threaded through in the rotary shaft (12) of hollow structure, connecting line (22) and the conductive mechanism for being mounted on rotary shaft (12) top (5) it is connected, the conductive mechanism (5) is by positive pole current collections ring (27), cathode collector ring (28), brush one (29), brush two (30), positive electrical wire (31) and negative electrical wire (32) composition, positive pole current collections ring (27) and cathode collector ring (28) are fixed on rotation Axis (12) tip exterior, positive pole current collections ring (27) are born by the positive terminals of connecting line (22) connection electrode wiring board (23) Pole collector ring (28) by another connecting line (22) connection electrode wiring board (23) negative terminals.
2. a kind of collection according to claim 1 heats and is mixed in integrated reaction kettle device, which is characterized in that described mixed It closes and is equipped with muff (15) outside tank body (14), charging manifold (3) is connected to feed liquid pipe one (1) and feed liquid pipe two (2), feed liquid pipe one (1) and on feed liquid pipe two (2) it is mounted on non-return valve.
3. a kind of collection according to claim 1 heats and is mixed in integrated reaction kettle device, which is characterized in that described to lead Hot silica gel sheath (20) is wrapped in heating plate (33) outside, heating plate (33) lower end connection connection copper sheet (26), connection copper sheet (26) It is connected on heating plate (3) internal circuit.
4. a kind of collection according to claim 1 heats and is mixed in integrated reaction kettle device, which is characterized in that the rotation Insulation filling is equipped in shaft (12), insulation filling is polyethylene foam insulation.
5. a kind of collection according to claim 1 heats and is mixed in integrated reaction kettle device, which is characterized in that described to lead Motor structure (5) is set in insulating shield (4), and insulating shield (4) connects mixing tank body (14) by fixed frame (6).
6. a kind of collection heating according to claim 1 be mixed in integrated reaction kettle device, which is characterized in that it is described just It is equipped with brush one (29) on the outside of pole collector ring (27) and is in contact with brush one (29), brush one (29) connects positive electrical wire (31);It is equipped with brush two (30) on the outside of cathode collector ring (28) and is in contact with brush two (30), brush two (30) connects cathode Electric wire (32).
7. a kind of collection according to claim 1 heats and is mixed in integrated reaction kettle device, which is characterized in that described to stir Mix the deflector hole (25) of several thermal conductive silicon gum covers (20) and several stulls (19) square crossing composition in frame (18).
CN201810493440.3A 2018-05-22 2018-05-22 A kind of heating of collection be mixed in integrated reaction kettle device Pending CN108636317A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201810493440.3A CN108636317A (en) 2018-05-22 2018-05-22 A kind of heating of collection be mixed in integrated reaction kettle device

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201810493440.3A CN108636317A (en) 2018-05-22 2018-05-22 A kind of heating of collection be mixed in integrated reaction kettle device

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Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2003181279A (en) * 2001-12-19 2003-07-02 Akira Suzuki Reactor for liquid
CN201454460U (en) * 2009-07-30 2010-05-12 裴丹平 Material stirrer
CN105268389A (en) * 2014-06-26 2016-01-27 东至天孚化工有限公司 Shock-absorbing rotary heating reaction kettle
CN206139169U (en) * 2016-08-31 2017-05-03 大田县伊鑫新型材料有限公司 Anti chamotte mould polycarboxylate water reducing agent synthesis system
CN206996385U (en) * 2017-06-01 2018-02-13 新乡市康健化工有限公司 A kind of paddle with high-temperature heating function

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2003181279A (en) * 2001-12-19 2003-07-02 Akira Suzuki Reactor for liquid
CN201454460U (en) * 2009-07-30 2010-05-12 裴丹平 Material stirrer
CN105268389A (en) * 2014-06-26 2016-01-27 东至天孚化工有限公司 Shock-absorbing rotary heating reaction kettle
CN206139169U (en) * 2016-08-31 2017-05-03 大田县伊鑫新型材料有限公司 Anti chamotte mould polycarboxylate water reducing agent synthesis system
CN206996385U (en) * 2017-06-01 2018-02-13 新乡市康健化工有限公司 A kind of paddle with high-temperature heating function

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
南京药学院: "《药剂学》", 31 March 1978 *

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Application publication date: 20181012