CN108623820A - A kind of orange oil pickering emulsion and preparation method thereof stablized using regenerated cellulose - Google Patents
A kind of orange oil pickering emulsion and preparation method thereof stablized using regenerated cellulose Download PDFInfo
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- CN108623820A CN108623820A CN201810371632.7A CN201810371632A CN108623820A CN 108623820 A CN108623820 A CN 108623820A CN 201810371632 A CN201810371632 A CN 201810371632A CN 108623820 A CN108623820 A CN 108623820A
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- regenerated cellulose
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J3/00—Processes of treating or compounding macromolecular substances
- C08J3/02—Making solutions, dispersions, lattices or gels by other methods than by solution, emulsion or suspension polymerisation techniques
- C08J3/03—Making solutions, dispersions, lattices or gels by other methods than by solution, emulsion or suspension polymerisation techniques in aqueous media
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08B—POLYSACCHARIDES; DERIVATIVES THEREOF
- C08B16/00—Regeneration of cellulose
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J2391/00—Characterised by the use of oils, fats or waxes; Derivatives thereof
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Abstract
The present invention provides a kind of orange oil pickering emulsions stablized using regenerated cellulose, and using regenerated cellulose as Solid particle emulsifying agents, orange oil is oil phase, and the embedding rate of orange oil is 76.03 ~ 89.35%.The present invention also provides the preparation methods of above-mentioned orange oil pickering emulsion, and using microcrystalline cellulose as raw material, after phosphoric acid dissolution process, regeneration is diluted with water, and regenerated cellulose suspension is obtained by washing；This suspension is freeze-dried, regenerated cellulose powder is obtained；Regenerated cellulose powder is scattered in deionized water, regenerated cellulose suspension is formed and, by high speed homogenization, obtains stable orange oil pickering emulsion then to orange oil is added in above-mentioned suspension.Orange oil pickering emulsion prepared by the present invention has the characteristics that regenerated cellulose dosage is few, preparation process is simple, environmental-friendly and application cost is low, can effectively reduce the volatilization of aroma substance in orange oil, increase its stability.
Description
Technical field
The invention belongs to field of food chemical industry, are related to a kind of orange oil pickering emulsion, specifically a kind of using again
The orange oil pickering emulsion and preparation method thereof that raw cellulose is stablized.
Background technology
Orange oil is typically to be extracted from the full fruit of sweet orange or pericarp with cold-press or steam distillation, and main component is
Alkene, bay firpene, octanal, capraldehyde, citral, terpinol etc., fragrant with adipocere aldehyde, flavor is mild, and fragrance is unique, has
Fresh sweet feeling.It is widely used in food, cosmetics, tobacco and field of medicaments.Orange oil can be used for allocating each
The different savory essence of orange of kind, while can also arrange in pairs or groups with other essence.In addition, also there is regulating qi-flowing for eliminating phlegm, relieving cough and asthma, antibacterial to disappear
The multiple efficacies such as scorching, relieving mood and the improvement state of mind.
Orange oil belongs to volatile essential oil, is insoluble in water, and fragrance matter majority is volatile, and fragrance remaining time is short, stores
Other bad smells are easily lost or be converted in journey, especially lose bigger under the processing environment of high temperature, to influence food
Quality.Therefore, it during food processing and production, needs to embed orange oil, itself and ambient environment, reduction is made to wave
Hair property avoids oxidation deterioration and aroma substance from losing, improves the comprehensive utilization ratio of orange oil.Mostly use microencapsulation skill at present
Art embeds orange oil.
In food processing technology, the carrier systems based on lotion are widely used, can effectively deliver, protect and
Release lipotropic component improves the quality of product, extends its shelf life to make it be not easy to be aoxidized during preservation.Using breast
Change technology, orange oil is emulsified, and can increase its dissolubility, protects aromatic substance from the influence of external environment, thus
Reduce the volatility of its aroma substance.Application range of the expansion orange oil in food industry.
Pickering emulsion is a kind of New Emulsion stablized using solid particle, and solid particle adsorbed close is in water-oil phase
Interface generates certain steric hindrance, electrostatic repulsion and rheology resistance so that certain distance is kept between oil droplet, to
Prevent the collision or fusion between drop so that lotion is stabilized.Compared with the lotion that conventional emulsifier is stablized, pik woods breast
Liquid has many advantages, such as that the dosage of required emulsifier is few, there are no pollution to the environment and stability of emulsion is high.In recent years, researcher
With a series of edible solid particles such as polysaccharide, protein, it is prepared for stable food-grade pickering emulsion, which has both work
Property object conveying, the improvement of low in calories and quality function, be hot spot and the challenge of food colloid research field.It is with regenerated cellulose
Solid particle emulsifying agents prepare orange oil pickering emulsion by high speed homogenization so that while orange oil water solubility improves very
Good improves its stability, and this method has many advantages, such as that preparation process is simply and at low cost, and gained lotion has very strong steady
It is qualitative, it is not easy to be influenced by factors such as system pH, salinity and temperature.It is emulsified at present by solid particle of regenerated cellulose
Agent, the correlative study for preparing orange oil pickering emulsion have not been reported.
Invention content
For above-mentioned technical problem in the prior art, the present invention provides a kind of orange oil pickering emulsion and its preparations
Method, described this orange oil pickering emulsion and preparation method thereof will solve in the prior art that orange oil aroma quality is not
It is good, oxidizable rotten technical problem.
The present invention provides a kind of orange oil pickering emulsions stablized using regenerated cellulose, and the lotion is to regenerate
Cellulose is Solid particle emulsifying agents, and orange oil is oil phase, and the embedding rate of orange oil is 76.03 ~ 89.35%.
The present invention also provides a kind of preparation sides of above-mentioned orange oil pickering emulsion stablized using regenerated cellulose
Method includes the following steps：
1）One the step of dissolving microcrystalline cellulose；
Microcrystalline cellulose is weighed in a container, after deionized water wetting is added, the phosphoric acid that mass fraction is 70% ~ 85% is added
In, after whirlpool concussion so that microcrystalline cellulose is substantially soluble in phosphoric acid, obtains microcrystalline cellulose solution, the microcrystalline cellulose
The material ratio for the phosphoric acid that element, deionized water and mass fraction are 70% ~ 85% is 2 ~ 4 grams：2~4mL：100mL；
2）One the step of preparing regenerated cellulose suspension；
By step 1）After obtained microcrystalline cellulose solution stands 20 ~ 32h at 5 ~ 20 DEG C, after deionized water diluting reaction is added
Microcrystalline cellulose solution, the addition of the deionized water is step 1）The 80 of obtained microcrystalline cellulose liquor capacity ~
150%, after mixing well, obtain regenerated cellulose suspension；
3）One the step of preparing regenerated cellulose powder；
By step 2）Obtained regenerated cellulose suspension is centrifuged at 10000rpm, removes remaining phosphoric acid, centrifugation at least two
It is secondary, until the pH of suspension is 7；Precooling 4h under the conditions of suspension after having centrifuged is placed in -70 DEG C, then in condenser temperature
It is freeze-dried for 24 hours under the conditions of being 5Pa for -70 DEG C, vacuum degree, obtains regenerated cellulose powder；
4）One the step of preparing orange oil pickering emulsion；
By step 3）Obtained regenerated cellulose powder is dissolved in deionized water, after being sufficiently stirred, obtains regenerated cellulose suspension
Liquid, in the regenerated cellulose suspension, a concentration of 4 ~ 16g/L of regenerated cellulose.In 10000 ~ 19000rpm high
Under fast homogeneous, the orange oil of 2 ~ 8% amounts, high speed homogenization time is added dropwise by percent by volume in regenerated cellulose suspension
For 2 ~ 5min, orange oil pickering emulsion is obtained.
A kind of orange oil pickering emulsion of the present invention is that regeneration is diluted with water and is formed again after phosphoric acid dissolution process
Raw cellulose is Solid particle emulsifying agents, and orange oil is then added and is formed by lotion.
The preparation method for the orange oil pickering emulsion of the present invention stablized using regenerated cellulose is with commercially available crystallite fibre
Dimension element is that regeneration is diluted with water after phosphoric acid dissolution process in raw material, and regenerated cellulose suspension is obtained by washing；By this
Suspension is freeze-dried, and obtains regenerated cellulose powder；Regenerated cellulose powder is scattered in deionized water, it is fine to form regeneration
The plain suspension of dimension, by high speed homogenization, obtains stable orange oil pik woods breast then to orange oil is added in above-mentioned suspension
Liquid.
Cellulose is renewable resource most abundant on one of most important natural organic matter and the earth, is widely present
In various biologies.A kind of important derivatives of the microcrystalline cellulose as cellulose are by native cellulose through acidolysis or machine
Tool handles to obtain, and has the characteristics such as large specific surface area, high-hydroscopicity and fabulous mobility, in view of its unique structure and property
Matter can be used as emulsifier and anti-agglomerating agent.But microcrystalline cellulose has a great amount of hydroxy group, the presence of these hydroxyls make it have compared with
Strong intermolecular and intramolecular active force greatly limits its emulsifiability to make it be insoluble in water.Through phosphoric acid dissolution process
Afterwards, the regenerated cellulose that regeneration obtains is diluted with water, hydrophobicity and dissolubility increase, and can preferably be adsorbed on oil-water interfaces,
And regenerated cellulose forms reticular structure in continuous phase so that emulsion intercalation method greatly improves.
The present invention is compared with prior art, and technological progress is significant.Orange oil pickering emulsion prepared by the present invention,
Grain size is small and particle diameter distribution is uniform, and regenerated cellulose is arranged closely in oil-water interfaces, and Irreversible Adsorption shape occurs in oil-water interfaces
At stable emulsion, and reticular structure is formed in continuous phase, effectively prevent emulsion polymerization and Ostwald ripening, and the embedding of orange oil
Rate is up to 76.03 ~ 89.35%.To effectively prevent orange oil fragrance to escape, increase its stability.Moreover, prepared by the present invention
Orange oil pickering emulsion has the characteristics that regenerated cellulose dosage is few, preparation process is simple, environmental-friendly and application cost is low.
Description of the drawings
Fig. 1 is the orange oil pickering emulsion outside drawing prepared by the embodiment of the present invention 3.
Specific implementation mode
The invention will now be described in further detail by way of examples and with reference to the accompanying drawings, but is not intended to limit the present invention.
Embodiment 1
（1）The dissolving of microcrystalline cellulose
4 grams of microcrystalline celluloses are weighed in beaker, after the wetting of 4mL deionized waters is added, it is 75% that 100mL mass fractions, which are added,
In phosphoric acid, after whirlpool shakes 2min so that microcrystalline cellulose is substantially soluble in phosphoric acid, obtains microcrystalline cellulose solution.
（2）The preparation of regenerated cellulose suspension
By step（1）After obtained microcrystalline cellulose solution is stood for 24 hours at 15 DEG C, 400mL deionized water diluting reactions are added
Cellulose suspension afterwards after mixing well, obtains regenerated cellulose suspension；
（3）The preparation of regenerated cellulose powder
By step（2）Obtained regenerated cellulose suspension is centrifuged at 10000rpm, removes remaining phosphoric acid, is centrifuged for several times,
Until the pH of suspension is 7；Precooling 4h under the conditions of suspension after having centrifuged is placed in -70 DEG C, then condenser temperature be -
70 DEG C, vacuum degree be 5Pa under the conditions of be freeze-dried for 24 hours, obtain regenerated cellulose powder；
(4）The preparation of orange oil pickering emulsion
By 0.8g steps (3）Obtained regenerated cellulose powder is dissolved in 100mL deionized waters, after being sufficiently stirred, is regenerated
Cellulose suspension.In the regenerated cellulose suspension, a concentration of 8g/L of regenerated cellulose.In 13000rpm high
Under fast homogeneous, 6mL orange oils are added dropwise in regenerated cellulose suspension, the high speed homogenization time is 2min, is formed stable
Orange oil pickering emulsion.
Through determined by ultraviolet spectrophotometry, orange oil embedding rate is 78.11% in the orange oil pickering emulsion of gained.
The assay method of embedding rate is as follows：It takes 2mL lotions to be added in 5mL absolute ethyl alcohols, after whirlpool shakes 3min, stands
3h takes upper layer alcohol layer, is diluted 40 times, its absorbance is surveyed in maximum absorption wave strong point, according to standard curve determination ethyl alcohol
The concentration of orange oil in layer calculates embedding rate according to following equation：
E（Embedding rate）=（m-m1）/m×100%
m：The addition of orange oil, g in emulsion preparation process；
m1：The amount for the orange oil not embedded, g.
Embodiment 2
(1）The dissolving of microcrystalline cellulose
3 grams of microcrystalline celluloses are weighed in beaker, after the wetting of 3mL deionized waters is added, it is 70% that 100mL mass fractions, which are added,
In phosphoric acid, after whirlpool shakes 2min so that microcrystalline cellulose is substantially soluble in phosphoric acid, obtains microcrystalline cellulose solution.
（2）The preparation of regenerated cellulose suspension
By step（1）After obtained microcrystalline cellulose solution stands 28h at 20 DEG C, 400mL deionized water diluting reactions are added
Microcrystalline cellulose solution afterwards after mixing well, obtains regenerated cellulose suspension；
（3）The preparation of regenerated cellulose powder
By step（2）Obtained regenerated cellulose suspension is centrifuged at 10000rpm, removes remaining phosphoric acid, is centrifuged for several times,
Until the pH of suspension is 7；Precooling 4h under the conditions of suspension after having centrifuged is placed in -70 DEG C, then condenser temperature be -
70 DEG C, vacuum degree be 5Pa under the conditions of be freeze-dried for 24 hours, obtain regenerated cellulose powder；
(4）The preparation of orange oil pickering emulsion
By 0.4g steps (3）Obtained regenerated cellulose powder is dissolved in 100mL deionized waters, after being sufficiently stirred, is regenerated
Cellulose suspension.In the regenerated cellulose suspension, a concentration of 4g/L of regenerated cellulose.In 10000rpm high
Under fast homogeneous, 8mL orange oils are added dropwise in regenerated cellulose suspension, the high speed homogenization time is 3min, is formed stable
Orange oil pickering emulsion.
Through determined by ultraviolet spectrophotometry, orange oil embedding rate is 76.03% in the orange oil pickering emulsion of gained.
Embodiment 3
(1）The dissolving of microcrystalline cellulose
2 grams of microcrystalline celluloses are weighed in beaker, after the wetting of 2mL deionized waters is added, it is 85% that 100mL mass fractions, which are added,
In phosphoric acid, after whirlpool shakes 2min so that microcrystalline cellulose is substantially soluble in phosphoric acid, obtains microcrystalline cellulose solution.
(2）The preparation of regenerated cellulose suspension
By step（1）After obtained microcrystalline cellulose solution stands 32h at 5 DEG C, after 400mL deionized water diluting reactions are added
Cellulose solution, after mixing well, obtain regenerated cellulose suspension；
（3）The preparation of regenerated cellulose powder
By step（2）Obtained regenerated cellulose suspension is centrifuged at 10000rpm, removes remaining phosphoric acid, is centrifuged for several times,
Until the pH of suspension is 7；Precooling 4h under the conditions of suspension after having centrifuged is placed in -70 DEG C, then condenser temperature be -
70 DEG C, vacuum degree be 5Pa under the conditions of be freeze-dried for 24 hours, obtain regenerated cellulose powder；
(4）The preparation of orange oil pickering emulsion
By 1.6g steps (3）Obtained regenerated cellulose powder is dissolved in 100mL deionized waters, after being sufficiently stirred, is regenerated
Cellulose suspension.In the regenerated cellulose suspension, a concentration of 16g/L of regenerated cellulose.In 19000rpm
Under high speed homogenization, 4mL orange oils are added dropwise in regenerated cellulose suspension, the high speed homogenization time is 5min, is formed and is stablized
Orange oil pickering emulsion.
Through determined by ultraviolet spectrophotometry, orange oil embedding rate is 89.35% in the orange oil pickering emulsion of gained.
Embodiment 4
(1）The dissolving of microcrystalline cellulose
2.5 grams of microcrystalline celluloses are weighed in beaker, after the wetting of 2.5mL deionized waters is added, 100mL mass fractions, which are added, is
In 80% phosphoric acid, after whirlpool shakes 2min so that microcrystalline cellulose is substantially soluble in phosphoric acid, obtains microcrystalline cellulose solution.
（2）The preparation of regenerated cellulose suspension
By step（1）After obtained microcrystalline cellulose solution stands 20h at 10 DEG C, after 4 times of deionized water diluting reactions are added
Cellulose suspension, after mixing well, obtain regenerated cellulose suspension；
3）The preparation of regenerated cellulose powder
By step（2）Obtained regenerated cellulose suspension is centrifuged at 10000rpm, removes remaining phosphoric acid, is centrifuged for several times,
Until the pH of suspension is 7；Precooling 4h under the conditions of suspension after having centrifuged is placed in -70 DEG C, then condenser temperature be -
70 DEG C, vacuum degree be 5Pa under the conditions of be freeze-dried for 24 hours, obtain regenerated cellulose powder；
(4）The preparation of orange oil pickering emulsion
By 1.2g steps (3）Obtained regenerated cellulose powder is dissolved in 100mL deionized waters, after being sufficiently stirred, is regenerated
Cellulose suspension.In the regenerated cellulose suspension, a concentration of 12g/L of regenerated cellulose.In 16000rpm
Under high speed homogenization, 2mL orange oils are added dropwise in regenerated cellulose suspension, the high speed homogenization time is 4min, is formed and is stablized
Orange oil pickering emulsion.
Through determined by ultraviolet spectrophotometry, orange oil embedding rate is 85.02% in the orange oil pickering emulsion of gained.
Claims (2)
1. a kind of orange oil pickering emulsion stablized using regenerated cellulose, it is characterised in that：The lotion is to regenerate fibre
Dimension element is Solid particle emulsifying agents, and orange oil is oil phase, and the embedding rate of orange oil is 76.03 ~ 89.35%.
2. a kind of preparation method of orange oil pickering emulsion stablized using regenerated cellulose described in claim 1, special
Sign is：Include the following steps：
1）One the step of dissolving microcrystalline cellulose；
Microcrystalline cellulose is weighed in a container, after deionized water wetting is added, the phosphoric acid that mass fraction is 70% ~ 85% is added
In, after whirlpool concussion so that microcrystalline cellulose is substantially soluble in phosphoric acid, obtains microcrystalline cellulose solution, the microcrystalline cellulose
The material ratio for the phosphoric acid that element, deionized water and mass fraction are 70% ~ 85% is 2 ~ 4 grams：2~4mL：100mL；
2）One the step of preparing regenerated cellulose suspension；
By step 1）After obtained microcrystalline cellulose solution stands 20 ~ 32h at 5 ~ 20 DEG C, after deionized water diluting reaction is added
Microcrystalline cellulose solution, the addition of the deionized water is step 1）The 80 of obtained microcrystalline cellulose liquor capacity ~
150%, after mixing well, obtain regenerated cellulose suspension；
3）One the step of preparing regenerated cellulose powder；
By step 2）Obtained regenerated cellulose suspension is centrifuged at 10000rpm, removes remaining phosphoric acid, centrifugation at least two
It is secondary, until the pH of suspension is 7；Precooling 4h under the conditions of suspension after having centrifuged is placed in -70 DEG C, then in condenser temperature
24 are freeze-dried under the conditions of being 5Pa for -70 DEG C, vacuum degree, obtains regenerated cellulose powder；
4）One the step of preparing orange oil pickering emulsion；
By step 3）Obtained regenerated cellulose powder is dissolved in deionized water, after being sufficiently stirred, obtains regenerated cellulose suspension
Liquid, in the regenerated cellulose suspension, a concentration of 4 ~ 16g/L of regenerated cellulose；
Under 10000 ~ 19000rpm high speed homogenizations, 2 ~ 8% amounts are added dropwise by percent by volume in regenerated cellulose suspension
Orange oil, the high speed homogenization time be 2 ~ 5min, obtain orange oil pickering emulsion.
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110563964A (en) * | 2019-10-24 | 2019-12-13 | 福州大学 | kelp cellulose nanofiber stabilized sunflower seed oil Pickering emulsion and preparation method thereof |
| CN112108122A (en) * | 2020-08-18 | 2020-12-22 | 江苏省农业科学院 | Burdock root residue porous adsorption material and preparation method and use method thereof |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101917959A (en) * | 2006-12-01 | 2010-12-15 | 安特里奥公司 | Peptide nanoparticles and uses therefor |
| CN107593934A (en) * | 2017-10-24 | 2018-01-19 | 东华大学 | A kind of edible oil gel based on regenerated cellulose and its preparation method and application |
| CN107875986A (en) * | 2016-09-30 | 2018-04-06 | 爱尔伯股份公司 | Particle and its preparation method at least containing volatile materials |
-
2018
- 2018-04-24 CN CN201810371632.7A patent/CN108623820A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101917959A (en) * | 2006-12-01 | 2010-12-15 | 安特里奥公司 | Peptide nanoparticles and uses therefor |
| CN107875986A (en) * | 2016-09-30 | 2018-04-06 | 爱尔伯股份公司 | Particle and its preparation method at least containing volatile materials |
| CN107593934A (en) * | 2017-10-24 | 2018-01-19 | 东华大学 | A kind of edible oil gel based on regenerated cellulose and its preparation method and application |
Non-Patent Citations (4)
| Title |
|---|
| CHUNXIA WEN等: ""Preparation and stabilization of d-limonene Pickering emulsions bycellulose nanocrystals"", 《CARBOHYDRATE POLYMERS》 * |
| 天津轻工业学院食品工业教学研究室编: "《食品添加剂》", 31 January 2008, 中国轻工业出版社 * |
| 徐然然: ""磷酸法再生纤维素稳定水包油乳状液的应用"", 《中国优秀硕士学位论文全文数据库工程科学Ⅰ辑》 * |
| 田怀香: ""食品级皮克林乳液制备及应用研究进展"", 《中国食品学报》 * |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110563964A (en) * | 2019-10-24 | 2019-12-13 | 福州大学 | kelp cellulose nanofiber stabilized sunflower seed oil Pickering emulsion and preparation method thereof |
| CN112108122A (en) * | 2020-08-18 | 2020-12-22 | 江苏省农业科学院 | Burdock root residue porous adsorption material and preparation method and use method thereof |
| CN112108122B (en) * | 2020-08-18 | 2023-03-10 | 江苏省农业科学院 | Preparation method of burdock root residue porous adsorptive food raw material |
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