CN108610654A - A kind of finishing environmental-protection type sound-absorbing material and preparation method thereof - Google Patents

A kind of finishing environmental-protection type sound-absorbing material and preparation method thereof Download PDF

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Publication number
CN108610654A
CN108610654A CN201810466818.0A CN201810466818A CN108610654A CN 108610654 A CN108610654 A CN 108610654A CN 201810466818 A CN201810466818 A CN 201810466818A CN 108610654 A CN108610654 A CN 108610654A
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parts
anthocyanidin
protection type
intermediate product
absorbing material
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黄欣
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    • EFIXED CONSTRUCTIONS
    • E04BUILDING
    • E04BGENERAL BUILDING CONSTRUCTIONS; WALLS, e.g. PARTITIONS; ROOFS; FLOORS; CEILINGS; INSULATION OR OTHER PROTECTION OF BUILDINGS
    • E04B1/00Constructions in general; Structures which are not restricted either to walls, e.g. partitions, or floors or ceilings or roofs
    • E04B1/62Insulation or other protection; Elements or use of specified material therefor
    • E04B1/74Heat, sound or noise insulation, absorption, or reflection; Other building methods affording favourable thermal or acoustical conditions, e.g. accumulating of heat within walls
    • E04B1/82Heat, sound or noise insulation, absorption, or reflection; Other building methods affording favourable thermal or acoustical conditions, e.g. accumulating of heat within walls specifically with respect to sound only
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08LCOMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L99/00Compositions of natural macromolecular compounds or of derivatives thereof not provided for in groups C08L89/00 - C08L97/00
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08KUse of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K3/00Use of inorganic substances as compounding ingredients
    • C08K3/18Oxygen-containing compounds, e.g. metal carbonyls
    • C08K3/24Acids; Salts thereof
    • C08K3/26Carbonates; Bicarbonates
    • C08K2003/265Calcium, strontium or barium carbonate
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08KUse of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K2201/00Specific properties of additives
    • C08K2201/011Nanostructured additives
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08LCOMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2205/00Polymer mixtures characterised by other features
    • C08L2205/02Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group
    • C08L2205/025Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group containing two or more polymers of the same hierarchy C08L, and differing only in parameters such as density, comonomer content, molecular weight, structure
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08LCOMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2205/00Polymer mixtures characterised by other features
    • C08L2205/03Polymer mixtures characterised by other features containing three or more polymers in a blend

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  • Physics & Mathematics (AREA)
  • Architecture (AREA)
  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Acoustics & Sound (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Polymers & Plastics (AREA)
  • Medicinal Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Electromagnetism (AREA)
  • Civil Engineering (AREA)
  • Structural Engineering (AREA)
  • Building Environments (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)

Abstract

The invention discloses a kind of finishing environmental-protection type sound-absorbing materials and preparation method thereof.The finishing environmental-protection type sound-absorbing material includes the raw material of following parts by weight:20 34 parts of paper white sludge, 8 15 parts of nano medical stone, 10 15 parts of coffee grounds, 12 18 parts of flake powder, 6 15 parts of hair slag, 5 10 parts of lateritic nickel ore, 10 15 parts of anthocyanidin, 100 200 parts of water.The finishing of the present invention is prepared as a raw material with environmental-protection type sound-absorbing material by paper white sludge, nano medical stone, coffee grounds, flake powder, hair slag, lateritic nickel ore, anthocyanidin and water, has the advantages that sound-absorbing effect is excellent, adsorbable indoor formaldehyde;Raw material is easy to get, is nontoxic simultaneously, more environmentally-friendly, can protect the health of people, meet Green Development needs, has preferable promotional value.

Description

A kind of finishing environmental-protection type sound-absorbing material and preparation method thereof
Technical field
The present invention relates to a kind of sound-absorbing material, specifically a kind of finishing environmental-protection type sound-absorbing material and preparation method thereof.
Background technology
With industrial production, communications and transportation, the development of urban architecture and the increase of the density of population, home amenity (sound Sound, air-conditioning, television set etc.) increase, ambient noise getting worse, it have become pollution human society environment a big public hazards. Noise can not only influence hearing, but also the cardiovascular system to people, nervous system, internal system have an adverse effect.
Existing sound-absorbing material also have it is compound, but inorganic material and the compound performance indicator of organic materials it is excellent compared with It is few.See on the whole, China's sound-absorbing material industry product working ability is insufficient, the research and development and production of high-end sound-absorbing material it is upper with Developed country is compared to there is larger gaps.Current research and development one kind of being badly in need of has good mechanical property, service life length, inhales The good and environmentally friendly sound-absorbing material of audio fruit.
Invention content
The purpose of the present invention is to provide a kind of finishing environmental-protection type sound-absorbing materials and preparation method thereof, to solve the above-mentioned back of the body The problem of being proposed in scape technology.
To achieve the above object, the present invention provides the following technical solutions:
A kind of finishing environmental-protection type sound-absorbing material, the finishing environmental-protection type sound-absorbing material includes the original of following parts by weight Material:20-34 parts of paper white sludge, 8-15 parts of nano medical stone, 10-15 parts of coffee grounds, 12-18 parts of flake powder, 6-15 parts of hair slag, 5-10 parts of lateritic nickel ore, 10-15 parts of anthocyanidin, 100-200 parts of water.
As a further solution of the present invention:The finishing environmental-protection type sound-absorbing material includes the original of following parts by weight Material:24-31 parts of paper white sludge, 9-13 parts of nano medical stone, 11-13 parts of coffee grounds, 14-16 parts of flake powder, 8-12 parts of hair slag, 6-8 parts of lateritic nickel ore, 11-13 parts of anthocyanidin, 120-180 parts of water.
As a further solution of the present invention:The finishing environmental-protection type sound-absorbing material includes the original of following parts by weight Material:28 parts of paper white sludge, 11 parts of nano medical stone, 12 parts of coffee grounds, 15 parts of flake powder, 10 parts of hair slag, 7 parts of lateritic nickel ore, 12 parts of anthocyanidin, 165 parts of water.
A kind of preparation method of finishing environmental-protection type sound-absorbing material, includes the following steps:Anthocyanidin is uniformly mixed with water, Paper white sludge and nano medical stone are uniformly mixed, and then take out impregnation mixture after a certain period of time in the aqueous solution of anthocyanidin It is dried to obtain the first intermediate product, remaining anthocyanidin aqueous solution is spare;Then coffee grounds, flake powder and hair slag are immersed in It is taken out after a certain period of time in remaining anthocyanidin aqueous solution and is dried to obtain the second intermediate product, remaining anthocyanidin aqueous solution is standby With;First intermediate product is crushed to 100-200 mesh and obtains third intermediate product;By third intermediate product in inert atmosphere 1-2h is calcined at middle 500-700 DEG C, obtains the 4th intermediate product;Be sieved 50-100 mesh after 4th intermediate product is cooled down, Then it is mixed with lateritic nickel ore, obtains the 5th intermediate product;5th intermediate product is uniformly mixed with the second intermediate product, is added Remaining anthocyanidin aqueous solution, after stirring evenly, it is dry to get.
As a further solution of the present invention:Impregnation mixture is taken out in the aqueous solution of anthocyanidin after 20-40min and is done It is dry.
As a further solution of the present invention:It is water-soluble that coffee grounds, flake powder and hair slag are immersed in remaining anthocyanidin Drying is taken out in liquid after 30-45min.
Compared with prior art, the beneficial effects of the invention are as follows:
The finishing of the present invention passes through paper white sludge, nano medical stone, coffee grounds, flake powder, hair with environmental-protection type sound-absorbing material Hair wastes, lateritic nickel ore, anthocyanidin and water are prepared as a raw material, and have the advantages that sound-absorbing effect is excellent, adsorbable indoor formaldehyde; Raw material is easy to get, is nontoxic simultaneously, more environmentally-friendly, can protect the health of people, meet Green Development needs, has and preferably pushes away Wide value.
Specific implementation mode
The technical solution of this patent is described in more detail With reference to embodiment.
Embodiment 1
A kind of finishing environmental-protection type sound-absorbing material, the finishing environmental-protection type sound-absorbing material includes the original of following parts by weight Material:20 parts of paper white sludge, 8 parts of nano medical stone, 10 parts of coffee grounds, 12 parts of flake powder, 6 parts of hair slag, 5 parts of lateritic nickel ore, flower Green element 10 parts, 100 parts of water.
A kind of preparation method of finishing environmental-protection type sound-absorbing material, includes the following steps:Anthocyanidin is uniformly mixed with water, Paper white sludge and nano medical stone are uniformly mixed, and are then taken out impregnation mixture after 20min in the aqueous solution of anthocyanidin dry Dry to obtain the first intermediate product, remaining anthocyanidin aqueous solution is spare;Then coffee grounds, flake powder and hair slag are immersed in surplus It is taken out after 30min in remaining anthocyanidin aqueous solution and is dried to obtain the second intermediate product, remaining anthocyanidin aqueous solution is spare;By institute It states the first intermediate product and is crushed to 100 mesh and obtain third intermediate product;It will be forged at third intermediate product in an inert atmosphere 500 DEG C 1h is burnt, the 4th intermediate product is obtained;Be sieved 50 mesh after 4th intermediate product is cooled down, and then mixes, obtains with lateritic nickel ore To the 5th intermediate product;5th intermediate product is uniformly mixed with the second intermediate product, remaining anthocyanidin aqueous solution is added, stirs After mixing uniformly, it is dry to get.
Embodiment 2
A kind of finishing environmental-protection type sound-absorbing material, the finishing environmental-protection type sound-absorbing material includes the original of following parts by weight Material:34 parts of paper white sludge, 15 parts of nano medical stone, 15 parts of coffee grounds, 18 parts of flake powder, 15 parts of hair slag, 10 parts of lateritic nickel ore, 15 parts of anthocyanidin, 200 parts of water.
A kind of preparation method of finishing environmental-protection type sound-absorbing material, includes the following steps:Anthocyanidin is uniformly mixed with water, Paper white sludge and nano medical stone are uniformly mixed, and are then taken out impregnation mixture after 40min in the aqueous solution of anthocyanidin dry Dry to obtain the first intermediate product, remaining anthocyanidin aqueous solution is spare;Then coffee grounds, flake powder and hair slag are immersed in surplus It is taken out after 45min in remaining anthocyanidin aqueous solution and is dried to obtain the second intermediate product, remaining anthocyanidin aqueous solution is spare;By institute It states the first intermediate product and is crushed to 200 mesh and obtain third intermediate product;It will be forged at third intermediate product in an inert atmosphere 700 DEG C 2h is burnt, the 4th intermediate product is obtained;Be sieved 100 mesh after 4th intermediate product is cooled down, and then mixes, obtains with lateritic nickel ore To the 5th intermediate product;5th intermediate product is uniformly mixed with the second intermediate product, remaining anthocyanidin aqueous solution is added, stirs After mixing uniformly, it is dry to get.
Embodiment 3
A kind of finishing environmental-protection type sound-absorbing material, the finishing environmental-protection type sound-absorbing material includes the original of following parts by weight Material:28 parts of paper white sludge, 11 parts of nano medical stone, 12 parts of coffee grounds, 15 parts of flake powder, 10 parts of hair slag, 7 parts of lateritic nickel ore, 12 parts of anthocyanidin, 165 parts of water.
A kind of preparation method of finishing environmental-protection type sound-absorbing material, includes the following steps:Anthocyanidin is uniformly mixed with water, Paper white sludge and nano medical stone are uniformly mixed, and are then taken out impregnation mixture after 30min in the aqueous solution of anthocyanidin dry Dry to obtain the first intermediate product, remaining anthocyanidin aqueous solution is spare;Then coffee grounds, flake powder and hair slag are immersed in surplus It is taken out after 35min in remaining anthocyanidin aqueous solution and is dried to obtain the second intermediate product, remaining anthocyanidin aqueous solution is spare;By institute It states the first intermediate product and is crushed to 160 mesh and obtain third intermediate product;It will be forged at third intermediate product in an inert atmosphere 600 DEG C 1.3h is burnt, the 4th intermediate product is obtained;Be sieved 70 mesh after 4th intermediate product is cooled down, and is then mixed with lateritic nickel ore, Obtain the 5th intermediate product;5th intermediate product is uniformly mixed with the second intermediate product, remaining anthocyanidin aqueous solution is added, After stirring evenly, it is dry to get.
Embodiment 4
A kind of finishing environmental-protection type sound-absorbing material, the finishing environmental-protection type sound-absorbing material includes the original of following parts by weight Material:24 parts of paper white sludge, 9 parts of nano medical stone, 11 parts of coffee grounds, 14 parts of flake powder, 8 parts of hair slag, 6 parts of lateritic nickel ore, flower Green element 11 parts, 120 parts of water.
A kind of preparation method of finishing environmental-protection type sound-absorbing material, includes the following steps:Anthocyanidin is uniformly mixed with water, Paper white sludge and nano medical stone are uniformly mixed, and are then taken out impregnation mixture after 24min in the aqueous solution of anthocyanidin dry Dry to obtain the first intermediate product, remaining anthocyanidin aqueous solution is spare;Then coffee grounds, flake powder and hair slag are immersed in surplus It is taken out after 32min in remaining anthocyanidin aqueous solution and is dried to obtain the second intermediate product, remaining anthocyanidin aqueous solution is spare;By institute It states the first intermediate product and is crushed to 120 mesh and obtain third intermediate product;It will be forged at third intermediate product in an inert atmosphere 550 DEG C 1.2h is burnt, the 4th intermediate product is obtained;Be sieved 60 mesh after 4th intermediate product is cooled down, and is then mixed with lateritic nickel ore, Obtain the 5th intermediate product;5th intermediate product is uniformly mixed with the second intermediate product, remaining anthocyanidin aqueous solution is added, After stirring evenly, it is dry to get.
Embodiment 5
A kind of finishing environmental-protection type sound-absorbing material, the finishing environmental-protection type sound-absorbing material includes the original of following parts by weight Material:31 parts of paper white sludge, 13 parts of nano medical stone, 13 parts of coffee grounds, 16 parts of flake powder, 12 parts of hair slag, 8 parts of lateritic nickel ore, 13 parts of anthocyanidin, 180 parts of water.
A kind of preparation method of finishing environmental-protection type sound-absorbing material, includes the following steps:Anthocyanidin is uniformly mixed with water, Paper white sludge and nano medical stone are uniformly mixed, and are then taken out impregnation mixture after 35min in the aqueous solution of anthocyanidin dry Dry to obtain the first intermediate product, remaining anthocyanidin aqueous solution is spare;Then coffee grounds, flake powder and hair slag are immersed in surplus It is taken out after 40min in remaining anthocyanidin aqueous solution and is dried to obtain the second intermediate product, remaining anthocyanidin aqueous solution is spare;By institute It states the first intermediate product and is crushed to 180 mesh and obtain third intermediate product;It will be forged at third intermediate product in an inert atmosphere 660 DEG C 1.7h is burnt, the 4th intermediate product is obtained;Be sieved 90 mesh after 4th intermediate product is cooled down, and is then mixed with lateritic nickel ore, Obtain the 5th intermediate product;5th intermediate product is uniformly mixed with the second intermediate product, remaining anthocyanidin aqueous solution is added, After stirring evenly, it is dry to get.
Comparative example 1
Compared with Example 3, in addition to without coffee grounds, other preparation methods are consistent.
Comparative example 2
Compared with Example 3, in addition to without anthocyanidin, other preparation methods are consistent.
Comparative example 3
Compared with Example 3, in addition to without coffee grounds and anthocyanidin, other preparation methods are consistent.
Comparative example 4
Compared with Example 3, raw material is identical, preparation method be all raw materials be uniformly mixed to get.
Experimental example
One, the material of embodiment 1-3 and comparative example 1-4 are tested for the property, the results are shown in Table 1.Acoustic absorptivity shines GBT23451-2009 is detected;Oise insulation factor test condition is sample thickness 3.5cm, frequency of source 300Hz.
1 the performance test results of table
Two, each 100g of material for weighing embodiment 1-3, comparative example 1-4 is respectively put into the chamber that volume is 40L, The exemplar in equivalent formaldehyde pollution source made of sheet glass is respectively put into case, to make to keep certain concentration of formaldehyde in case, Middle glass chip size is 20cm × 32cm.Then closed joint sealing, formaldehyde original concentration in test box.Testing experiment case after 24 hours Interior concentration of formaldehyde is tested again after 48h, and test result is shown in Table 2.
2 formaldehyde absorbing effect of table
Project Initial concentration mg/m3 Concentration mg/m after for 24 hours3 Concentration mg/m after 48h3
Embodiment 1 0.5 0.12 0.03
Embodiment 2 0.5 0.10 0.02
Embodiment 3 0.5 0.09 0.02
Comparative example 1 0.5 0.19 0.11
Comparative example 2 0.5 0.20 0.08
Comparative example 3 0.5 0.25 0.14
Comparative example 4 0.5 0.15 0.05
The better embodiment of this patent is explained in detail above, but this patent is not limited to above-mentioned embodiment party Formula, one skilled in the relevant art within the scope of knowledge, can also be under the premise of not departing from this patent objective It makes a variety of changes.

Claims (6)

1. a kind of finishing environmental-protection type sound-absorbing material, which is characterized in that the finishing environmental-protection type sound-absorbing material includes following heavy Measure the raw material of number:20-34 parts of paper white sludge, 8-15 parts of nano medical stone, 10-15 parts of coffee grounds, 12-18 parts of flake powder, hair 6-15 parts of hair wastes, 5-10 parts of lateritic nickel ore, 10-15 parts of anthocyanidin, 100-200 parts of water.
2. finishing environmental-protection type sound-absorbing material according to claim 1, which is characterized in that the finishing environmental-protection type sound-absorbing Material includes the raw material of following parts by weight:24-31 parts of paper white sludge, 9-13 parts of nano medical stone, 11-13 parts of coffee grounds, fish 14-16 parts of powder of eye, 8-12 parts of hair slag, 6-8 parts of lateritic nickel ore, 11-13 parts of anthocyanidin, 120-180 parts of water.
3. finishing environmental-protection type sound-absorbing material according to claim 1, which is characterized in that the finishing environmental-protection type sound-absorbing Material includes the raw material of following parts by weight:28 parts of paper white sludge, 11 parts of nano medical stone, 12 parts of coffee grounds, 15 parts of flake powder, 10 parts of hair slag, 7 parts of lateritic nickel ore, 12 parts of anthocyanidin, 165 parts of water.
4. a kind of preparation method of finishing environmental-protection type sound-absorbing material as described in any one of claims 1-3, which is characterized in that packet Include following steps:Anthocyanidin is uniformly mixed with water, paper white sludge and nano medical stone are uniformly mixed, then by impregnation mixture It is taken out after a certain period of time in the aqueous solution of anthocyanidin and is dried to obtain the first intermediate product, remaining anthocyanidin aqueous solution is spare; Then coffee grounds, flake powder and hair slag are immersed in remaining anthocyanidin aqueous solution to take out after a certain period of time and are dried to obtain the Two intermediate products, remaining anthocyanidin aqueous solution are spare;First intermediate product is crushed to 100-200 mesh to obtain in third Between product;1-2h will be calcined at third intermediate product in an inert atmosphere 500-700 DEG C, obtains the 4th intermediate product;It will be described Be sieved 50-100 mesh after the cooling of 4th intermediate product, is then mixed with lateritic nickel ore, obtains the 5th intermediate product;Among the 5th Product is uniformly mixed with the second intermediate product, and remaining anthocyanidin aqueous solution is added, after stirring evenly, it is dry to get.
5. the preparation method of finishing environmental-protection type sound-absorbing material as claimed in claim 4, which is characterized in that by impregnation mixture In the aqueous solution of anthocyanidin drying is taken out after 20-40min.
6. the preparation method of finishing environmental-protection type sound-absorbing material as claimed in claim 4, which is characterized in that by coffee grounds, fish Eye powder and hair slag are immersed in remaining anthocyanidin aqueous solution and take out drying after 30-45min.
CN201810466818.0A 2018-05-16 2018-05-16 A kind of finishing environmental-protection type sound-absorbing material and preparation method thereof Pending CN108610654A (en)

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CN102943545A (en) * 2012-12-12 2013-02-27 耿文杰 Wallboard with function of improving tone quality
CN104529389A (en) * 2014-12-31 2015-04-22 广西科技大学 Papermaking white mud light shale brick and producing method thereof
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CN102424550A (en) * 2011-09-06 2012-04-25 池州西恩新材料科技有限公司 Laterite slag baking-free brick and preparation method thereof
CN102943545A (en) * 2012-12-12 2013-02-27 耿文杰 Wallboard with function of improving tone quality
CN104529389A (en) * 2014-12-31 2015-04-22 广西科技大学 Papermaking white mud light shale brick and producing method thereof
CN106186933A (en) * 2016-07-07 2016-12-07 长兴贝斯德邦建材科技有限公司 A kind of environment-friendly exterior wall heat preservation putty and preparation method thereof

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Title
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Application publication date: 20181002