CN1086087A - Preparation of lime sulphur mixture by substituting sulphur - Google Patents
Preparation of lime sulphur mixture by substituting sulphur Download PDFInfo
- Publication number
- CN1086087A CN1086087A CN 93114983 CN93114983A CN1086087A CN 1086087 A CN1086087 A CN 1086087A CN 93114983 CN93114983 CN 93114983 CN 93114983 A CN93114983 A CN 93114983A CN 1086087 A CN1086087 A CN 1086087A
- Authority
- CN
- China
- Prior art keywords
- lime
- sulphur
- sulfur
- preparation
- substituting
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical group [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 title claims abstract description 16
- JNVCSEDACVAATK-UHFFFAOYSA-L [Ca+2].[S-]SSS[S-] Chemical compound [Ca+2].[S-]SSS[S-] JNVCSEDACVAATK-UHFFFAOYSA-L 0.000 title claims abstract description 14
- 239000005864 Sulphur Substances 0.000 title claims description 14
- 239000000203 mixture Substances 0.000 title claims description 7
- 238000002360 preparation method Methods 0.000 title claims description 7
- 239000005866 Lime sulphur Substances 0.000 title claims description 4
- 238000000034 method Methods 0.000 claims abstract description 17
- 235000008733 Citrus aurantifolia Nutrition 0.000 claims abstract description 6
- 235000011941 Tilia x europaea Nutrition 0.000 claims abstract description 6
- 239000004571 lime Substances 0.000 claims abstract description 6
- 239000002994 raw material Substances 0.000 claims abstract description 5
- 230000003009 desulfurizing effect Effects 0.000 claims abstract description 4
- 239000000375 suspending agent Substances 0.000 claims abstract description 4
- 239000006260 foam Substances 0.000 claims description 6
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 claims description 4
- AXCZMVOFGPJBDE-UHFFFAOYSA-L calcium dihydroxide Chemical compound [OH-].[OH-].[Ca+2] AXCZMVOFGPJBDE-UHFFFAOYSA-L 0.000 claims description 4
- 239000012752 auxiliary agent Substances 0.000 claims description 3
- 238000009835 boiling Methods 0.000 claims description 3
- 239000002270 dispersing agent Substances 0.000 claims description 3
- 238000010438 heat treatment Methods 0.000 claims description 3
- 229910021529 ammonia Inorganic materials 0.000 claims description 2
- 239000007864 aqueous solution Substances 0.000 claims 1
- 238000005202 decontamination Methods 0.000 claims 1
- 230000003588 decontaminative effect Effects 0.000 claims 1
- 150000001875 compounds Chemical class 0.000 abstract description 4
- 239000003814 drug Substances 0.000 abstract description 4
- 238000003912 environmental pollution Methods 0.000 abstract description 2
- 229910052717 sulfur Inorganic materials 0.000 abstract description 2
- 239000011593 sulfur Substances 0.000 abstract description 2
- XAQHXGSHRMHVMU-UHFFFAOYSA-N [S].[S] Chemical compound [S].[S] XAQHXGSHRMHVMU-UHFFFAOYSA-N 0.000 abstract 1
- 238000004519 manufacturing process Methods 0.000 abstract 1
- 239000000575 pesticide Substances 0.000 abstract 1
- 230000001681 protective effect Effects 0.000 abstract 1
- 230000001954 sterilising effect Effects 0.000 abstract 1
- 238000004659 sterilization and disinfection Methods 0.000 abstract 1
- 231100000331 toxic Toxicity 0.000 abstract 1
- 230000002588 toxic effect Effects 0.000 abstract 1
- 239000002699 waste material Substances 0.000 description 4
- 239000000243 solution Substances 0.000 description 3
- ODINCKMPIJJUCX-UHFFFAOYSA-N Calcium oxide Chemical compound [Ca]=O ODINCKMPIJJUCX-UHFFFAOYSA-N 0.000 description 2
- 235000013399 edible fruits Nutrition 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 229910052573 porcelain Inorganic materials 0.000 description 2
- 239000002244 precipitate Substances 0.000 description 2
- 238000007670 refining Methods 0.000 description 2
- 238000000926 separation method Methods 0.000 description 2
- 102000002322 Egg Proteins Human genes 0.000 description 1
- 108010000912 Egg Proteins Proteins 0.000 description 1
- 230000001680 brushing effect Effects 0.000 description 1
- 235000012255 calcium oxide Nutrition 0.000 description 1
- 239000000292 calcium oxide Substances 0.000 description 1
- 239000003245 coal Substances 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 238000010790 dilution Methods 0.000 description 1
- 239000012895 dilution Substances 0.000 description 1
- 201000010099 disease Diseases 0.000 description 1
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 239000003337 fertilizer Substances 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 239000004519 grease Substances 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 210000004681 ovum Anatomy 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 239000003223 protective agent Substances 0.000 description 1
- 238000007789 sealing Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Landscapes
- Glass Compositions (AREA)
Abstract
The present invention has improved traditional compound method of a planting fruit-trees with medicament, the new method of producing " lime sulfur " for sulfur method particularly is provided, it is characterized in that the lime toner end of taking off with desulfurizing tower replaces bright sulfur sulphur, mix after technical process with other raw materials, can obtain " lime sulfur " stoste and the suspending agent thereof of Baume 20-30 degree.
" lime sulfur " is a kind of higher effective and lower toxic pesticide that integrates the sterilization and disinsection protective effect.With the method production cost is low, simple to operate, raw material is easy to get, free from environmental pollution.
Description
The present invention relates to the compound method of a planting fruit-trees, particularly change traditional compound method, and use preparation of lime sulphur mixture by substituting sulphur with the inorganic sulfur medicament.
To ending at present, be to be that primary raw material is produced " lime sulfur " with sulphur, this traditional preparation method needs a large amount of sulphur.And refining sulphur is wanted the cost of equipment investment, not only consumes a large amount of energy pollution environment and (produces SO
2), and it is also dangerous to store transportation sulphur.So improved the cost of producing this medicine.
The purpose of invention is the new method that a kind of replacement sulphur preparation " lime sulfur " will be provided.This method raw material is easy to get, and cost is low, not only can save a large amount of sulphur, and simple to operate, free from environmental pollution.
Invention is to implement like this: use chemical fertilizer factory in synthetic ammonia process, the lime toner foam that desulfurizing tower is taken off, contain a large amount of sulphur and compound thereof, replace sulphur, after dispersing and filtering, heat, mix, make mixed liquor in heater, become the transparent liquid of rufous with lime water, can produce " lime sulfur " stoste of Baume 20-30 degree after the separation, and part " suspending agent ".Its cost is 1/5th of tradition preparation.
This lime toner foam is by separated products in the coal, part is used for refining sulphur at present, but its overwhelming majority is regarded as waste material to discard, directly in the fruit tree medicament, do not use, particularly do not produce " lime sulfur " as replacing sulphur, therefore, method of the present invention is to turn waste into wealth, and directly utilizes one of the approach of " three wastes ".
The method of invention is finished by following embodiment:
Formula rate (to account for the total amount percentage):
1, lime toner foam 30% under the desulfurizing tower;
2, lime water solution (quicklime powder 1 part 3 part mix with water) 15%;
3, centesimal aqueous dispersant 50%;
4, auxiliary agent 5%.
Technological process:
Filtration-heating-mixing-refrigerated separation.
Method of operating:
1 and 3 mix in will filling a prescription, and cross with the gauze of 150-200 sieve mesh and filter to remove foreign material, are heated in heater and boil, and put into a small amount of defrother (grease) foam removal simultaneously.Mixes the back with 2 with the solution of boiling and add 4, and keep boiling to be rufous to solution in 60 minutes stopping to heat; Stoste after the heating is contained in the porcelain container made, treat nature cooling after, precipitate and isolate the transparent liquid of rufous, be " lime sulfur " stoste, detect with B, and be divided in small-sized porcelain or the glass container made, after dripping several waste diesels sealings, put shady and cool dry ventilate outer store standby.
The thickness of precipitate and separate partly is suspending agent, has and " lime sulfur " same usefulness, and excellent its is good fruit tree Wound protective agent.Available its sprayed or the brushing trunk in spring and autumn dilution back, can prevent and treat the worm that survives the winter, ovum and disease effectively.
Balanced and the timely moisture content that replenishes evaporation will keep seething with excitement when heating.
Claims (3)
1, the method for preparation of lime sulphur mixture by substituting sulphur, particularly changed the prescription of traditional raw material, it is characterized in that the lime toner foam taken off with the ammonia enterprise desulfurizing tower, with lime water, the aqueous solution that contains dispersant and auxiliary agent, through the Hybrid Heating separating technology, produce " lime sulfur " stoste and suspending agent thereof.
2, method according to claim 1 is characterized in that the lime toner foam with 30% dissolves with containing 0.5% aqueous dispersant 50%, after 150-200 sieve mesh decontamination is heated to and boils excessively, mixes with 15% lime water, 5% auxiliary agent.
3, according to claim 1,2 described methods, it is characterized in that mixed liquor in heater, keep in balance the boiling 60 minutes, to becoming rufous.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 93114983 CN1086087A (en) | 1993-11-30 | 1993-11-30 | Preparation of lime sulphur mixture by substituting sulphur |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 93114983 CN1086087A (en) | 1993-11-30 | 1993-11-30 | Preparation of lime sulphur mixture by substituting sulphur |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN1086087A true CN1086087A (en) | 1994-05-04 |
Family
ID=4990727
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 93114983 Pending CN1086087A (en) | 1993-11-30 | 1993-11-30 | Preparation of lime sulphur mixture by substituting sulphur |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN1086087A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103371194A (en) * | 2012-04-17 | 2013-10-30 | 江苏启和化工有限公司 | Insect-repelling liquid for trees |
| CN106900742A (en) * | 2017-03-06 | 2017-06-30 | 宜宾北方川安化工有限公司 | A kind of lime sulfur accessory substance liniment and its preparation technology |
-
1993
- 1993-11-30 CN CN 93114983 patent/CN1086087A/en active Pending
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103371194A (en) * | 2012-04-17 | 2013-10-30 | 江苏启和化工有限公司 | Insect-repelling liquid for trees |
| CN106900742A (en) * | 2017-03-06 | 2017-06-30 | 宜宾北方川安化工有限公司 | A kind of lime sulfur accessory substance liniment and its preparation technology |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C06 | Publication | ||
| PB01 | Publication | ||
| C01 | Deemed withdrawal of patent application (patent law 1993) | ||
| WD01 | Invention patent application deemed withdrawn after publication |