CN108557847A - A kind of sour mine hybrid system in lithium carbonate preparation process - Google Patents

A kind of sour mine hybrid system in lithium carbonate preparation process Download PDF

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Publication number
CN108557847A
CN108557847A CN201810320208.XA CN201810320208A CN108557847A CN 108557847 A CN108557847 A CN 108557847A CN 201810320208 A CN201810320208 A CN 201810320208A CN 108557847 A CN108557847 A CN 108557847A
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CN
China
Prior art keywords
feed hopper
batch mixing
fixed case
lithium carbonate
preparation process
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201810320208.XA
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Chinese (zh)
Inventor
严晓晖
张婷
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Yichun Dingxin High Energy Science And Technology Co Ltd
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Yichun Dingxin High Energy Science And Technology Co Ltd
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Publication date
Application filed by Yichun Dingxin High Energy Science And Technology Co Ltd filed Critical Yichun Dingxin High Energy Science And Technology Co Ltd
Priority to CN201810320208.XA priority Critical patent/CN108557847A/en
Publication of CN108557847A publication Critical patent/CN108557847A/en
Pending legal-status Critical Current

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Classifications

    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01DCOMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
    • C01D15/00Lithium compounds
    • C01D15/08Carbonates; Bicarbonates
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F27/00Mixers with rotary stirring devices in fixed receptacles; Kneaders
    • B01F27/05Stirrers
    • B01F27/11Stirrers characterised by the configuration of the stirrers
    • B01F27/19Stirrers with two or more mixing elements mounted in sequence on the same axis
    • B01F27/191Stirrers with two or more mixing elements mounted in sequence on the same axis with similar elements
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F27/00Mixers with rotary stirring devices in fixed receptacles; Kneaders
    • B01F27/60Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a horizontal or inclined axis
    • B01F27/70Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a horizontal or inclined axis with paddles, blades or arms
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F35/00Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
    • B01F35/71Feed mechanisms

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Accessories For Mixers (AREA)

Abstract

The invention discloses a kind of sour mine hybrid systems in lithium carbonate preparation process,Including system base,Feed hopper fixed case is provided at the top of system base,The inner wall of feed hopper fixed case is provided with feed hopper filter plate,It is provided with feed hopper at the top of feed hopper fixed case,The side of feed hopper fixed case is provided with batch mixing favourable turn,The side of batch mixing favourable turn is provided with heat emission hole,The other side of feed hopper fixed case is connected with mixing machine,Steam jet is provided at the top of mixing machine,The top of mixing machine is connected with appendix by steam jet,One end of appendix is provided with steam chest,Mixing machine is internally provided with batch mixing bar shaft,The inside of mixing machine is connected with batch mixing bar by batch mixing bar shaft,One end of mixing machine is provided with discharge port,Therefore this kind realizes uniform stirring acid mine using its powerful batch mixing bar and steam chest for the sour mine hybrid system in lithium carbonate preparation process and improves the purpose of the quality of sour mine.

Description

A kind of sour mine hybrid system in lithium carbonate preparation process
Technical field
The present invention relates to mixing equipment and technology, specially a kind of sour mine mixed stockers in lithium carbonate preparation process System.
Background technology
Lithium carbonate, a kind of inorganic compound, chemical formula Li2CO3, be colourless monoclinic system crystal body or white powder, Be dissolved in diluted acid, be slightly soluble in water, solubility is big compared under hot water in cold water, does not dissolve in alcohol and acetone, can be used for potting porcelain, drug, Catalyst etc., common lithium ion battery raw material, since global salt lake overwhelming majority resource is all the low lithium type of high magnesium, and from high magnesium The technological difficulty of purification & isolation lithium carbonate is very big in the low old halogen of lithium, these technologies only rest in a small number of offshore company's hands before In, this makes lithium carbonate industry but also with technical barrier, therefore, creates the global oligopoly pattern of lithium carbonate industry.
But the sour mine that existing system processes is of low quality, and can not sour mine one be uniformly blended in mixed acid mine It rises, and because lithium carbonate is relatively dry, can not be fused in mine and go, the sour mineral amount processed in this way is not good enough, and in mine Part sundries can be mixed, if the mixing that these sundries also influence whether sour mine can not be handled.
So how to design a kind of sour mine hybrid system in lithium carbonate preparation process, becoming us will currently solve Certainly the problem of.
Invention content
It is above-mentioned to solve the purpose of the present invention is to provide a kind of sour mine hybrid system in lithium carbonate preparation process The problem of sour mine mixing unevenness and the sour mine poor quality processed are proposed in background technology.
To achieve the above object, the present invention provides the following technical solutions:A kind of sour mine in lithium carbonate preparation process The bottom of hybrid system, including system base, the system base is fixed with support leg, and the side of the system base is provided with The outer surface insertion of console, the operation console is provided with operation button and display screen, is provided at the top of the system base The inner wall of feed hopper fixed case, the feed hopper fixed case is provided with feed hopper filter plate, the top of the feed hopper fixed case It is provided with feed hopper, the side of the feed hopper fixed case is provided with batch mixing favourable turn, and the side that the batch mixing is made a connection is provided with scattered The other side of hot hole, the feed hopper fixed case is connected with mixing machine, and steam jet is provided at the top of the mixing machine, described The top of mixing machine is connected with appendix by steam jet, and one end of the appendix is provided with steam chest, the mixing machine Be internally provided with batch mixing bar shaft, the inside of the mixing machine is connected with batch mixing bar, the mixing machine by batch mixing bar shaft One end be provided with discharge port.
Further, there are four the support leg settings, and four support legs are closely welded with system base, and four A support leg is located at the quadrangle of system base.
Further, the batch mixing bar shape is in " field word " shape, and the batch mixing bar is dislocation and sets, and the batch mixing bar It is fixedly connected with batch mixing bar shaft.
Further, the feed hopper includes that the feed hopper fixed case of feeding funnel bottom part and feed hopper are fixed on chamber interior wall Feed hopper filter plate, and the feed hopper filter plate is connected on feed hopper fixed case.
Further, the appendix is metal hose, and the appendix is worked out by stone dead wire, and the gas transmission Pipe is flexibly connected with steam chest.
Further, the bottom of the steam jet is provided with multiple pin holes, and small needle diameter is consistent, and pin hole is embedding Enter to be arranged in steam jet.
Compared with prior art, the beneficial effects of the invention are as follows:This kind is used for the sour mine mixing in lithium carbonate preparation process System is equipped with batch mixing favourable turn, batch mixing bar shaft and batch mixing bar, batch mixing bar one is driven using batch mixing bar shaft when batch mixing favourable turn is run Rotation is played, is set because batch mixing bar is dislocation, when batch mixing bar rotates in mixing drum, the overturning sliding back and forth just as quant, Batch mixing bar shaft coordinates batch mixing bar, enables acid in mixing machine and mine is full and uniform mixes, prevent mixing unevenness Situation occurs, and is provided with steam chest and steam jet, and when batch mixing, the characteristic of water is dissolved in using lithium carbonate in mixing drum for material, Steam chest can be started, steam is sprayed by appendix out of steam jet bottom aperture when steam chest is run, is sprayed onto The outer surface of mine, steam are adequately dissolved into mine with acid, are improved the quality of sour mine, are provided with feeding mouth filter plate, work When personnel pour into mine in material mouth, feeding mouth filter plate can keep off the larger sundries of mine inner volume, wait for that system job is complete It can be taken off the cleaning of feeding mouth filter plate after finishing, not only can prevent sundries from mixing in mine in this way but also be convenient to clean.
Description of the drawings
Fig. 1 is the overall structure diagram of the present invention;
Fig. 2 is the batch mixing bar sectional view of the present invention;
Fig. 3 is the feed hopper filter plate sectional view of the present invention.
In figure:1, support leg, 2, console, 3, operation button, 4, display screen, 5, system base, 6, feed hopper fixed case, 7, batch mixing is made a connection, 701, batch mixing bar shaft, 702, batch mixing bar, 703, heat emission hole, 8, feed hopper, 801, feed hopper filter plate, 9, Appendix, 10, steam chest, 11, discharge port, 12, steam jet, 13, mixing machine.
Specific implementation mode
Following will be combined with the drawings in the embodiments of the present invention, and technical solution in the embodiment of the present invention carries out clear, complete Site preparation describes, it is clear that described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.It is based on Embodiment in the present invention, it is obtained by those of ordinary skill in the art without making creative efforts every other Embodiment shall fall within the protection scope of the present invention.
- 3 are please referred to Fig.1, the present invention provides a kind of technical solution:A kind of sour mine mixing in lithium carbonate preparation process System, including support leg 1, console 2, operation button 3, display screen 4, system base 5, feed hopper fixed case 6, batch mixing favourable turn 7, Batch mixing bar shaft 701, heat emission hole 703, feed hopper 8, feed hopper filter plate 801, appendix 9, steam chest 10, goes out batch mixing bar 702 The bottom of material mouth 11,12 steam jets, mixing machine 13, system base 4 is fixed with support leg 1, and there are four the settings of support leg 1, and Four support legs 1 are closely welded with system base 5, and four support legs 1 are located at the quadrangle of system base 5, and support leg 1 can Whole system is supported with document, the side of system base 4 is provided with console 2, and the outer surface insertion of operation console 2 is provided with behaviour Make button 3 and display screen 4, the top of system base 5 is provided with feed hopper fixed case 6, and the inner wall of feed hopper fixed case 6 is provided with The top of feed hopper filter plate 803, feed hopper fixed case 6 is provided with feed hopper 8, and feed hopper 8 includes the charging of 8 bottom of feed hopper The feed hopper filter plate 801 to struggle against on fixed case 6 and 6 inner wall of feed hopper fixed case, and feed hopper filter plate 801 is connected to charging It struggles against on fixed case 6, feed hopper filter plate 801 can filter the sundries in lower mine, and the side of feed hopper fixed case 6 is provided with batch mixing The side of favourable turn 7, batch mixing favourable turn 7 is provided with heat emission hole 703, and the other side of feed hopper fixed case 6 is connected with mixing machine 13, batch mixing The top of cylinder 13 is provided with steam jet 12, and the bottom of steam jet 12 is provided with multiple pin holes, and small needle diameter is consistent, And the aperture that pin hole insertion is arranged on steam jet 12, steam jet 12 is used for burst of steam, the top for going out mixing machine 13 is logical It crosses steam jet 12 and is connected with appendix 9, appendix 9 is metal hose, and appendix 9 is worked out by stone dead wire, and gas transmission Pipe 9 is flexibly connected with steam chest 10, and the steam that steam chest 10 generates can be sent into mixing drum 13 by appendix 9, and the one of appendix 9 End is provided with steam chest 10, and mixing machine 7 is internally provided with batch mixing bar shaft 701, and the inside of mixing machine 7 passes through batch mixing bar shaft 701 are connected with batch mixing bar 702, and 702 shape of batch mixing bar is in " field word " shape, and batch mixing bar 702 is dislocation and sets, and batch mixing bar 702 It is fixedly connected with batch mixing bar shaft 701, batch mixing bar shaft 701 coordinates batch mixing bar 702, keeps the sour and mine in mixing machine fully equal Even mixes, and the situation for preventing mixing uneven occurs, and one end of mixing machine 13 is provided with discharge port 11.
Operation principle:First, staff check system component can normal operation, pinpointing the problems can replacement portion at once Part first pours into material in feed hopper 8, and system starts to transport after the operation button 3 on pressing console 2 starts batch mixing favourable turn 7 It goes, it is mixed using the drive of batch mixing bar shaft 701 when batch mixing favourable turn 7 is run under the sundries in material can be kept off by feed hopper filter plate 801 Material bar 702 rotates together, and is set because batch mixing bar 702 is dislocation, when batch mixing bar 702 rotates in mixing drum 13, just as quant Equally overturning sliding back and forth, batch mixing bar shaft 701 coordinate batch mixing bar 702, keep the sour and mine in mixing machine 13 full and uniform It mixes, is dissolved in the characteristic of water using lithium carbonate in batch mixing, steam chest 10 can be started, steam chest 10 passes through when running Appendix 9 sprays steam out of 12 bottom of steam jet aperture, is sprayed onto the outer surface of mine, process acid it is mad finally from Outflow in discharge port 11.
It although an embodiment of the present invention has been shown and described, for the ordinary skill in the art, can be with Understanding without departing from the principles and spirit of the present invention can carry out these embodiments a variety of variations, modification, replace And modification, the scope of the present invention is defined by the appended.

Claims (6)

1. a kind of sour mine hybrid system in lithium carbonate preparation process, including system base(5), it is characterised in that:It is described System base(4)Bottom be fixed with support leg(1), the system base(4)Side be provided with console(2), the behaviour Make platform(2)Outer surface insertion be provided with operation button(3)And display screen(4), the system base(5)Top be provided with into Hopper fixed case(6), the feed hopper fixed case(6)Inner wall be provided with feed hopper filter plate(801), the feed hopper fixes Case(6)Top be provided with feed hopper(8), the feed hopper fixed case(6)Side be provided with batch mixing favourable turn(7), described mixed Material favourable turn(7)Side be provided with heat emission hole(703), the feed hopper fixed case(6)The other side be connected with mixing machine(13), The mixing machine(13)Top be provided with steam jet(12), the mixing machine(13)Top pass through steam jet(12)Even It is connected to appendix(9), the appendix(9)One end be provided with steam chest(10), the mixing machine(7)Be internally provided with it is mixed Expect bar shaft(701), the mixing machine(7)Inside pass through batch mixing bar shaft(701)It is connected with batch mixing bar(702), described mixed Barrel(13)One end be provided with discharge port(11).
2. a kind of sour mine hybrid system in lithium carbonate preparation process according to claim 1, it is characterised in that:Institute State support leg(1)There are four settings, and four support legs(1)With system base(5)Close welding, and four supports Leg(1)It is located at system base(5)Quadrangle.
3. a kind of sour mine hybrid system in lithium carbonate preparation process according to claim 1, it is characterised in that:Institute State batch mixing bar(702)Shape is in " field word " shape, and the batch mixing bar(702)It is dislocation and sets, and the batch mixing bar(702)With it is mixed Expect bar shaft(701)It is fixedly connected.
4. a kind of sour mine hybrid system in lithium carbonate preparation process according to claim 1, it is characterised in that:Institute State feed hopper(8)Including feed hopper(8)The feed hopper fixed case of bottom(6)And feed hopper fixed case(6)Charging on inner wall Struggle against filter plate(801), and the feed hopper filter plate(801)It is connected to feed hopper fixed case(6)On.
5. a kind of sour mine hybrid system in lithium carbonate preparation process according to claim 1, it is characterised in that:Institute State appendix(9)For metal hose, and the appendix(9)It is worked out by stone dead wire, and the appendix(9)With steam chest (10)Flexible connection.
6. a kind of sour mine hybrid system in lithium carbonate preparation process according to claim 1, it is characterised in that:Institute State steam jet(12)Bottom be provided with multiple pin holes, and small needle diameter is consistent, and pin hole insertion setting is sprayed in steam Head(12).
CN201810320208.XA 2018-04-11 2018-04-11 A kind of sour mine hybrid system in lithium carbonate preparation process Pending CN108557847A (en)

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Application Number Priority Date Filing Date Title
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* Cited by examiner, † Cited by third party
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CN206526765U (en) * 2017-02-24 2017-09-29 东莞市思卡阻燃材料有限公司 A kind of cooling combined batch mixer of granular material
CN107287457A (en) * 2017-07-17 2017-10-24 中国恩菲工程技术有限公司 Rare earth ore concentrate continuous decomposition equipment
CN206631507U (en) * 2017-04-08 2017-11-14 连云港市金囤农化有限公司 A kind of rotary mixing device of pesticide processing
CN208485608U (en) * 2018-04-11 2019-02-12 宜春市鼎鑫高能科技有限公司 A kind of sour mine mixing arrangement in lithium carbonate preparation process

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GB385071A (en) * 1931-11-07 1932-12-22 Phosphate Acidulating Corp Improvements in or relating to methods of and apparatus for producing soluble phosphate from phosphate rock
CN102874850A (en) * 2012-10-25 2013-01-16 西安三瑞实业有限公司 Roasting system and roasting method for lithium-ore acidification by using externally-heated type rotary furnace
CN104289133A (en) * 2014-09-03 2015-01-21 江阴市创裕机械有限公司 Novel horizontal mixer
CN204170671U (en) * 2014-10-21 2015-02-25 江西科诺生物科技有限公司 A kind of slurry by filtration and two-dimentional mixing arrangement
CN205368457U (en) * 2016-01-13 2016-07-06 晟通亿和(天津)企业管理咨询有限公司 Composition of mineral's portable compounding cloth system is drawed to concentrated sulfuric acid curing method
CN205288169U (en) * 2016-01-26 2016-06-08 山东瑞福锂业有限公司 A sour ore deposit mixing arrangement for lithium carbonate preparation in -process
CN205517762U (en) * 2016-04-20 2016-08-31 四川锦成化学催化剂有限公司 A in washing and cauldron for what thick liquid polyolefin catalyst liquid water disposal
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CN206526765U (en) * 2017-02-24 2017-09-29 东莞市思卡阻燃材料有限公司 A kind of cooling combined batch mixer of granular material
CN206631507U (en) * 2017-04-08 2017-11-14 连云港市金囤农化有限公司 A kind of rotary mixing device of pesticide processing
CN107287457A (en) * 2017-07-17 2017-10-24 中国恩菲工程技术有限公司 Rare earth ore concentrate continuous decomposition equipment
CN208485608U (en) * 2018-04-11 2019-02-12 宜春市鼎鑫高能科技有限公司 A kind of sour mine mixing arrangement in lithium carbonate preparation process

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上海金属软管厂编, 北京理工大学出版社 *

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Application publication date: 20180921

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