CN108554344A - A kind of reaction kettle - Google Patents
A kind of reaction kettle Download PDFInfo
- Publication number
- CN108554344A CN108554344A CN201810377279.3A CN201810377279A CN108554344A CN 108554344 A CN108554344 A CN 108554344A CN 201810377279 A CN201810377279 A CN 201810377279A CN 108554344 A CN108554344 A CN 108554344A
- Authority
- CN
- China
- Prior art keywords
- stirring
- block
- autoclave body
- agitating
- grinding block
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
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Classifications
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/18—Stationary reactors having moving elements inside
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00051—Controlling the temperature
- B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
- B01J2219/00087—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor
- B01J2219/00094—Jackets
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Mixers Of The Rotary Stirring Type (AREA)
- Processing Of Solid Wastes (AREA)
Abstract
The invention discloses a kind of reaction kettles, agitating plate is fixed in autoclave body, and the inner cavity of autoclave body is separated into upper stir chamber and lower stir chamber by agitating plate, stirring block is coaxially fixed on agitating shaft, and stirring block is placed in the top of agitating plate, stirring gap is formed between stirring block and agitating plate, supporting rack is fixed in autoclave body, and supporting rack is located at the lower section of agitating plate, agitating shaft is by bearing support on supporting rack, and the bottom end of agitating shaft stretches in the lower section of supporting rack, autoclave body is set in heating tank, and closed heating chamber is formed between the outer wall of autoclave body and the inner wall of heating tank, the inlet to connect with heating chamber is equipped on the outer wall of heating tank, liquid outlet and exhaust outlet.The configuration of the present invention is simple, mixing effect is good, and bulk solid reactant is smashed in reaction kettle, reduces pollution and waste, and agitating shaft is sufficiently stirred convenient for material in reaction, and using effect is good.
Description
Technical field：
The present invention relates to a kind of reaction kettles.
Background technology：
Bulk solid reactant and reaction solution by reaction kettle when being reacted, to accelerate the reaction time, usually by bulk
Reaction kettle is broken up or poured into after crushing to solid reactant, and the comminution process of existing solid reactant is often completed outside kettle.One
Aspect needs special grinding device to complete the process, on the other hand during comminuted solids reactant, can cause to raise
The phenomenon that dirt, if control is bad, it will cause the wastes of environmental pollution and material.In addition, the agitating paddle of reaction kettle is anti-in stirring
It answers and will appear vortex phenomenon in solution processes, the solid reactant for not being in time for reaction is concentrated in reactor bottom, in vortex
The reaction solution of the heart is less, therefore can extend the reaction time, reduces efficiency.
Therefore, it is necessory to be improved to the prior art to solve the deficiency of the prior art.
Invention content：
The present invention is to provide a kind of reaction kettle to solve the above-mentioned problems of the prior art.
The technical solution adopted in the present invention has：A kind of reaction kettle, including autoclave body, motor and agitating shaft, the motor are solid
Due on autoclave body, agitating shaft is rotatably connected on autoclave body, and the top of agitating shaft is fixedly connected with the shaft of motor, on autoclave body
Further include stirring block, agitating plate, supporting rack and heating tank, the agitating plate is fixed in autoclave body, and is stirred equipped with into and out of material mouth
It mixes plate and the inner cavity of autoclave body is separated into upper stir chamber and lower stir chamber, stirring block is coaxially fixed on agitating shaft, and stirring block is set
Stirring gap is formed in the top of agitating plate, between stirring block and agitating plate, supporting rack is fixed in autoclave body, and supporting rack position
In the lower section of agitating plate, agitating shaft is by bearing support on supporting rack, and the bottom end of agitating shaft stretches in the lower section of supporting rack, kettle
Body is set in heating tank, and closed heating chamber is formed between the outer wall of autoclave body and the inner wall of heating tank, in the outer of heating tank
Wall is equipped with inlet, liquid outlet and the exhaust outlet to connect with heating chamber；
The stirring block is that bottom surface is plane, and upper surface is the fast structure of taper of the conical surface, is equipped on the bottom surface of stirring block
First grinding block and the second grinding block, the first grinding block and the second grinding block are circular configuration, and the first grinding block is located at the
The outside of two grinding blocks；
The agitating plate is inverted cone-shaped structure, the bottom surface correspondence and stirring of the bottom surface of the first grinding block and the second grinding block
Stirring gap is formed between the inner conical surface of plate；Discharge groove is equipped on agitating plate, which is located at the inside of the second grinding block；
The agitating shaft includes axis body, paddle, stirring rod, outer stirrer gear and interior stirrer gear, and the paddle is fixed on
On axis body, and paddle is horizontally disposed, several stirring rods are fixed on the lower face of paddle vertically, and stirring rod is along stirring
The circumferencial direction for mixing leaf is uniformly distributed, the fixed several outer stirrer gears of layering in the outside of every stirring rod, the inside point of every stirring rod
The fixed several interior stirrer gears of layer.
Further, adjacent outer stirrer gear and interior stirrer gear are staggered on every stirring rod.
Further, the outer stirrer gear and interior stirrer gear tilt down setting.
Further, the bottom surface of first grinding block and the bottom surface of the second grinding block are ramp structure, and two grind
Block bottom surface is parallel with the conical surface of agitating plate.
Further, the height of first grinding block is less than the height of the second grinding block.
Further, support frame as described above includes supporter and the body of rod, and three bodies of rod are uniformly fixed on the outer wall of supporter,
Agitating shaft is by bearing support on supporter.
Further, the inner wall of the autoclave body is equipped with mounting blocks, and the body of rod is fixed on mounting blocks.
The present invention has the advantages that：The configuration of the present invention is simple, mixing effect is good, and bulk solid reactant is reacting
It is smashed in kettle, reduces pollution and waste, agitating shaft is sufficiently stirred convenient for material in reaction, and using effect is good.
Description of the drawings：
Fig. 1 is structure of the invention figure.
Fig. 2 is the structure chart of agitating shaft in the present invention.
Fig. 3 is the structure chart of supporting rack in the present invention.
Specific implementation mode：
The present invention will be further described below with reference to the drawings.
Such as Fig. 1 to Fig. 3, a kind of reaction kettle of the present invention, including autoclave body 11, motor 12, agitating shaft 13, stirring block 21, stirring
Plate 22, supporting rack 31 and heating tank 61, motor 12 are fixed on autoclave body 11, and agitating shaft 13 is rotatably connected on autoclave body 11, and is stirred
The top for mixing axis 13 is fixedly connected with the shaft of motor 12, is equipped with feed inlet on 11 top of autoclave body, bottom end is equipped with discharge port.Stirring
Plate 22 is fixed in autoclave body 11, and the inner cavity of autoclave body 11 is separated into upper stir chamber 100 and lower stir chamber 200 by agitating plate 22.It stirs
Mix block 21 to be coaxially fixed on agitating shaft 13, and stirring block 21 is placed in the top of agitating plate 22, stirring block 21 and agitating plate 22 it
Between be formed with stirring gap 20.Supporting rack 31 is fixed in autoclave body 11, and supporting rack 31 is located at the lower section of agitating plate 22, agitating shaft
13 by bearing support on supporting rack 31, and the bottom end of agitating shaft 13 stretches in the lower section of supporting rack 31.Autoclave body 11 is set to heating
In tank 61, and closed heating chamber 60 is formed between the outer wall of autoclave body 11 and the inner wall of heating tank 61, in the outer of heating tank 61
Wall is equipped with inlet, liquid outlet and the exhaust outlet to connect with heating chamber 60.
Stirring block 21 in the present invention is that bottom surface is plane, and upper surface is the fast structure of taper of the conical surface, in stirring block 21
Bottom surface is equipped with the first grinding block 211 and the second grinding block 212, and the first grinding block 211 and the second grinding block 212 are round knot
Structure, the first grinding block 211 and the second grinding block 212 are coaxially disposed, and the first grinding block 211 is located at the outer of the second grinding block 212
Side.
Agitating plate 22 is inverted cone-shaped structure, the bottom surface of the bottom surface of the first grinding block 211 and the second grinding block 212 correspond to
Stirring gap 20 is formed between the upper conical surface of agitating plate 22.The lower section for entering agitating plate 22 for ease of material, on agitating plate 22
Equipped with discharge groove 220, which is located at the inside of the second grinding block 212.
The bottom surface of first grinding block 211 and the bottom surface of the second grinding block 212 are ramp structure, and the bottom surface of two grinding blocks
It is parallel with the conical surface of agitating plate 22.
The height of first grinding block 211 is less than the height of the second grinding block 121, that is, the first grinding block 211 and agitating plate 22
Between stirring gap be more than stirring gap between the second grinding block 212 and agitating plate 22.It is gradual from outside to inside to stir gap
Become smaller, realizes the gradual grinding of material.
Bulk solid reactant and reaction solution are poured into together in autoclave body 11, bulk solid reactant is located at autoclave body 11
In upper stir chamber 100, agitating shaft 13 is rotated and is stirred, and in agitation, bulk solid reactant and reaction solution carry out
Reaction.When stirring, bulk solid reactant enters in stirring gap 20, is ground by the first grinding block 211 and the second grinding block 212
Milling is broken into bit solid reactant, enters lower stir chamber 200 eventually by the discharge groove 220 on agitating plate 22, continues
Reaction.
The conical surface in stirring block 21 enters convenient for solid reactant on agitating plate 22, and agitating plate 22 is cone structure, is convenient for
Solid reactant enters in stirring gap 20.
Agitating shaft 13 in the present invention includes axis body 131, paddle 132, stirring rod 133, outer stirrer gear 134 and interior stirring
Tooth 135, paddle 132 are fixed on axis body 131, and paddle 132 is horizontally disposed, several stirring rods 133 are fixed on vertically
On the lower face of paddle 132, and stirring rod 133 is uniformly distributed along the circumferencial direction of paddle 132, in every stirring rod 133
Several interior stirrer gears 135 are fixed in the inside layering of the fixed several outer stirrer gears 134 of outside layering, every stirring rod 133.
Adjacent outer stirrer gear 134 and interior stirrer gear 135 are staggered on every stirring rod 133.Outer stirrer gear 134 and interior
Stirrer gear 135 tilts down setting.
Outer stirrer gear 134 and interior stirrer gear 135 can stir while increasing mixing effect and concentrate on reaction kettle bottom
The solid reactant in portion, outer stirrer gear 134 and interior stirrer gear 135 interlock and are obliquely installed, and in whipping process, can also smash solid
Precursor reactant object, mixing effect are good.
Supporting rack 31 includes supporter 311 and the body of rod 312, and three bodies of rod 312 are uniformly fixed on the outer wall of supporter 311
On, agitating shaft 13 is by bearing support on supporter 311.The inner wall of autoclave body 11 is equipped with mounting blocks, and the body of rod 312 is fixed on peace
It fills on block.
Extension supporting frame 31, agitating shaft 13 is by bearing support on supporting rack 31, it is ensured that agitating shaft rotation is put down
Stability.
The above is only a preferred embodiment of the present invention, it is noted that for the ordinary skill people of the art
It for member, can also make several improvements without departing from the principle of the present invention, these improvement also should be regarded as the present invention's
Protection domain.
Claims (7)
1. a kind of reaction kettle, including autoclave body (11), motor (12) and agitating shaft (13), the motor (12) are fixed on autoclave body (11)
On, agitating shaft (13) is rotatably connected on autoclave body (11), and the top of agitating shaft (13) is fixedly connected with the shaft of motor (12),
It is equipped on autoclave body (11) into and out of material mouth, it is characterised in that:Further include stirring block (21), agitating plate (22), supporting rack (31) and
Heating tank (61), the agitating plate (22) is fixed in autoclave body (11), and the inner cavity of autoclave body (11) is separated by agitating plate (22)
Upper stir chamber (100) and lower stir chamber (200), stirring block (21) are coaxially fixed on agitating shaft (13), and stirring block (21) is set
Top in agitating plate (22), is formed with stirring gap (20) between stirring block (21) and agitating plate (22), supporting rack (31) is solid
It is interior due to autoclave body (11), and supporting rack (31) is located at the lower section of agitating plate (22), agitating shaft (13) is by bearing support in support
On frame (31), and the bottom end of agitating shaft (13) stretches in the lower section of supporting rack (31), and autoclave body (11) is set in heating tank (61), and kettle
It is formed with closed heating chamber (60) between the outer wall and the inner wall of heating tank (61) of body (11), on the outer wall of heating tank (61)
Equipped with inlet, liquid outlet and the exhaust outlet to connect with heating chamber (60)；
The stirring block (21) is that bottom surface is plane, and upper surface is the fast structure of taper of the conical surface, on the bottom surface of stirring block (21)
Equipped with the first grinding block (211) and the second grinding block (212), the first grinding block (211) and the second grinding block (212) are circle
Structure, and the first grinding block (211) is located at the outside of the second grinding block (212)；
The agitating plate (22) is inverted cone-shaped structure, the bottom surface of the first grinding block (211) and the bottom surface of the second grinding block (212)
Stirring gap (20) is formed between the corresponding and inner conical surface of agitating plate (22)；Discharge groove (220) is equipped on agitating plate (22), it should
Discharge groove (220) is located at the inside of the second grinding block (212)；
The agitating shaft (13) includes axis body (131), paddle (132), stirring rod (133), outer stirrer gear (134) and interior stirring
Tooth (135), the paddle (132) are fixed on axis body (131), and paddle (132) is horizontally disposed, several stirring rods
(133) it is fixed on vertically on the lower face of paddle (132), and stirring rod (133) is equal along the circumferencial direction of paddle (132)
Cloth, the fixed several outer stirrer gears (134) of layering in the outside of every stirring rod (133), the inside layering of every stirring rod (133)
Fixed several interior stirrer gears (135).
2. reaction kettle as described in claim 1, it is characterised in that:Adjacent outer stirrer gear (134) on every stirring rod (133)
It is staggered with interior stirrer gear (135).
3. reaction kettle as described in claim 1, it is characterised in that:The outer stirrer gear (134) and interior stirrer gear (135) to
Under be obliquely installed.
4. reaction kettle as described in claim 1, it is characterised in that:The bottom surface of first grinding block (211) and the second grinding
The bottom surface of block (212) is ramp structure, and two grinding block bottom surfaces are parallel with the conical surface of agitating plate (22).
5. reaction kettle as described in claim 1, it is characterised in that:The height of first grinding block (211) is ground less than second
The height of abrading block (212).
6. reaction kettle as described in claim 1, it is characterised in that:Support frame as described above (31) includes supporter (311) and the body of rod
(312), three bodies of rod (312) are uniformly fixed on the outer wall of supporter (311), and agitating shaft (13) is by bearing support in support
On body (311).
7. reaction kettle as claimed in claim 6, it is characterised in that:The inner wall of the autoclave body (11) is equipped with mounting blocks, the body of rod
(312) it is fixed on mounting blocks.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810377279.3A CN108554344A (en) | 2018-04-25 | 2018-04-25 | A kind of reaction kettle |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810377279.3A CN108554344A (en) | 2018-04-25 | 2018-04-25 | A kind of reaction kettle |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN108554344A true CN108554344A (en) | 2018-09-21 |
Family
ID=63536417
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201810377279.3A Pending CN108554344A (en) | 2018-04-25 | 2018-04-25 | A kind of reaction kettle |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN108554344A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110711538A (en) * | 2019-11-20 | 2020-01-21 | 江苏文理新材料科技有限公司 | Moisture absorption and sweat releasing finishing agent blanking system |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106390888A (en) * | 2015-07-31 | 2017-02-15 | 天津市亿腾顺泰建筑材料有限公司 | Reaction vessel |
| CN206980859U (en) * | 2017-05-17 | 2018-02-09 | 浙江工业职业技术学院 | Industrial chemicals grind and drying equipment |
| CN107694450A (en) * | 2017-11-10 | 2018-02-16 | 余姚市婉珍五金厂 | A kind of Feed Manufacturing chelates device with two-way stirring |
-
2018
- 2018-04-25 CN CN201810377279.3A patent/CN108554344A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106390888A (en) * | 2015-07-31 | 2017-02-15 | 天津市亿腾顺泰建筑材料有限公司 | Reaction vessel |
| CN206980859U (en) * | 2017-05-17 | 2018-02-09 | 浙江工业职业技术学院 | Industrial chemicals grind and drying equipment |
| CN107694450A (en) * | 2017-11-10 | 2018-02-16 | 余姚市婉珍五金厂 | A kind of Feed Manufacturing chelates device with two-way stirring |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110711538A (en) * | 2019-11-20 | 2020-01-21 | 江苏文理新材料科技有限公司 | Moisture absorption and sweat releasing finishing agent blanking system |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20180921 |
|
| RJ01 | Rejection of invention patent application after publication |