CN108543325A - High-efficiency environment friendly distillation still - Google Patents
High-efficiency environment friendly distillation still Download PDFInfo
- Publication number
- CN108543325A CN108543325A CN201810675347.4A CN201810675347A CN108543325A CN 108543325 A CN108543325 A CN 108543325A CN 201810675347 A CN201810675347 A CN 201810675347A CN 108543325 A CN108543325 A CN 108543325A
- Authority
- CN
- China
- Prior art keywords
- autoclave body
- inner cylinder
- slag notch
- discharge port
- tube bundle
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
- B01D3/02—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping in boilers or stills
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J11/00—Recovery or working-up of waste materials
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J11/00—Recovery or working-up of waste materials
- C08J11/04—Recovery or working-up of waste materials of polymers
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J2377/00—Characterised by the use of polyamides obtained by reactions forming a carboxylic amide link in the main chain; Derivatives of such polymers
- C08J2377/02—Polyamides derived from omega-amino carboxylic acids or from lactams thereof
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/141—Feedstock
- Y02P20/143—Feedstock the feedstock being recycled material, e.g. plastics
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02W—CLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
- Y02W30/00—Technologies for solid waste management
- Y02W30/50—Reuse, recycling or recovery technologies
- Y02W30/62—Plastics recycling; Rubber recycling
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Life Sciences & Earth Sciences (AREA)
- Sustainable Development (AREA)
- Health & Medical Sciences (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Abstract
The present invention relates to a kind of high-efficiency environment friendly distillation stills, including autoclave body, feed inlet, upper part discharge port, slag notch and each nozzle component；Autoclave body includes inner cylinder and chuck, and chuck is set to the outside of inner cylinder, forms cavity between inner cylinder；Feed inlet and upper part discharge port are set to the top of autoclave body, and slag notch is set to the bottom of autoclave body；U-tube bundle heater is equipped on autoclave body, the U-tube bundle heat exchanger tube of U-tube bundle heater is from the inner cylinder that one end side wall of autoclave body lower half is extend into；Filter device is equipped in upper part discharge port；Each nozzle component includes the steam blowing mouth and hydraulic control mouth being arranged at the top of autoclave body, and steam blowing mouth and hydraulic control mouth are connected to the inner cylinder of autoclave body；Bottom temp meter interface is equipped on side wall of the autoclave body close to bottom；Slag notch is trumpet type.The present invention has the advantages of decomposition rate for accelerating material, the technique productions period of high-purity caprolactam low polymer-monomer is refined in shortening.
Description
Technical field
The present invention relates to core equipment-steamings in a kind of distillation still more particularly to a kind of Pa-6 Polymerization MONOMER RECOVERY device
Evaporate kettle.
Background technology
Currently, the enterprise of domestic chemical fibre industry production polyamide fibre 6, environmental protection consciousness enhancing, the extraction after being extracted to slice
Caprolactam low polymer-monomer is carried out recycling after polymerization again by water intaking no longer arbitrarily discharge by MONOMER RECOVERY device
It utilizes, had not only protected environment and carried out " zero " disposal of pollutants, but also can be enterprise to reduce cost of material, while the waste residue being discharged is through phase
After the processing of pass, low intensive engineering plastics can be manufactured.But the core equipment-of MONOMER RECOVERY high-purity monomer material system at present
Distillation still, distillation efficiency is not high, and general design structure is：Inner cylinder, chuck, feed inlet, upper part discharge port, slag notch and each
Nozzle component.
Invention content
Against the above deficiency, the present invention provides a kind of high-efficiency environment friendly steaming for caprolactam low polymer-MONOMER RECOVERY
Evaporate kettle.
In order to solve the above-mentioned technical problem, the present invention adopts the following technical scheme that.
A kind of high-efficiency environment friendly distillation still, including autoclave body, feed inlet, upper part discharge port, slag notch and each nozzle component；Autoclave body
Including inner cylinder and chuck, chuck is set to the outside of inner cylinder, forms cavity between inner cylinder；Feed inlet and upper part discharge port are set to kettle
The top of body, slag notch are set to the bottom of autoclave body；U-tube bundle heater, the U-tube of U-tube bundle heater are equipped on autoclave body
Beam heat exchanger tube is from the inner cylinder that one end side wall of autoclave body lower half is extend into；Filter device is equipped in upper part discharge port；Each pipe
Mouth component includes the steam blowing mouth and hydraulic control mouth being arranged at the top of autoclave body, the inner cylinder of steam blowing mouth and hydraulic control mouth and autoclave body
Connection；Bottom temp meter interface is equipped on side wall of the autoclave body close to bottom；Slag notch is trumpet type.
Further, slag notch（5）Loudspeaker angle be 30o.
A kind of high-efficiency environment friendly distillation still disclosed by the invention, operation principle are changed by chuck, U-tube bundle heater
Medium-steam in heat pipe heats the inside and outside of autoclave body inner cylinder simultaneously, by the caprolactam low polymer-in material
Monomer becomes gaseous state from mushy stage, and the gaseous monomer material distilled out is sent into monomer receiver by upper part discharge port；Waste residue is through loudspeaker
Type slag notch enters tapping equipment cooling, send to professional dirt recycling company processing.In this way, by Extraction For Pa 6 Chips
Later it is rationally recycled after effective ingredient caprolactam low polymer-monomer distillation, refinement in extract liquor, to reduce brocade
The production cost that synthetic fibre 6 is sliced.
The present invention increases U-tube bundle heater in autoclave body, and the material in inner cylinder is made to pass through chuck and U-tube bundle heater
Heat exchanger tube in medium dual-heated, can be rapidly heated, accelerate material decomposition rate；The steam blowing mouth added, is being opened
In docking process, steam is passed through by the nozzle, purges, remove the inner wall attachment of clean inner cylinder；The present invention is in upper outlet
Mouth is also additionally arranged filter device, and the monomer gas recycling of high-purity is effectively ensured；The hydraulic control mouth and bottom temp at the top added
Meter interface is matched with sensor electricity conference system, monitors the temperature of material liquid surface adjustable height and bottoms material in inner cylinder in time,
Feedback process data controls in inner cylinder the capacity of material and temperature within the scope of process stipulation；Bottom slag notch uses loudspeaker
Type structure, it can be ensured that waste residue thoroughly discharges.
Compared with the prior art, the advantages of the present invention are as follows：Both ensured that distillation still was quick, be evenly heated, and accelerated material point
Speed is solved, and medium liquid level, temperature in kettle are monitored in real time, convenient for periodic cleaning in kettle and detection convenient for user；Shortening carries
Refine the technique productions period of high-purity caprolactam low polymer-monomer.
Description of the drawings
Fig. 1 is schematic structural view of the invention.
Specific implementation mode
Present invention is further described in detail below in conjunction with the accompanying drawings.
As shown in Figure 1, a kind of high-efficiency environment friendly distillation still, including autoclave body, feed inlet 3, upper part discharge port 4, slag notch 5 and each
Nozzle component；Autoclave body includes inner cylinder 1 and chuck 2, and chuck 2 is set to the outside of inner cylinder 1, cavity is formed between inner cylinder 1；Feed inlet
3 and upper part discharge port 4 be set to autoclave body top, slag notch 5 be set to autoclave body bottom；U-tube bundle heater is equipped on autoclave body
6, the U-tube bundle heat exchanger tube of U-tube bundle heater 6 is from the inner cylinder 1 that one end side wall of autoclave body lower half is extend into；Go out on top
Material mouth 4 is equipped with filter device 8；Each nozzle component includes the steam blowing mouth 7 and hydraulic control mouth 9 being arranged at the top of autoclave body, is steamed
Vapour blow valve port 7 and hydraulic control mouth 9 are connected to the inner cylinder 1 of autoclave body；Bottom temp meter interface is equipped on side wall of the autoclave body close to bottom
10；Slag notch 5 is trumpet type, and loudspeaker angle uses 30o.
The equipment performance is good, homogeneous heating, quickly, the finished product caprolactam low polymer-monomer qualification rate distilled out
Up to 100%, meanwhile, sludge discharge is thorough, clean in kettle.
Claims (2)
1. a kind of high-efficiency environment friendly distillation still, including autoclave body, feed inlet（3）, upper part discharge port（4）, slag notch（5）And each nozzle group
Part；The autoclave body includes inner cylinder（1）And chuck（2）, the chuck（2）Set on the inner cylinder（1）Outside, with the inner cylinder
（1）Between form cavity；The feed inlet（3）With the upper part discharge port（4）Set on the top of the autoclave body, the slag notch
（5）Set on the bottom of the autoclave body；It is characterized in that, being equipped with U-tube bundle heater on the autoclave body（6）, the U-tube bundle
Heater（6）U-tube bundle heat exchanger tube the inner cylinder is extend into from one end side wall of the autoclave body lower half（1）In；Institute
State upper part discharge port（4）It is equipped with filter device（8）；Each nozzle component includes the steam being arranged at the top of the autoclave body
Blow valve port（7）With hydraulic control mouth（9）, the steam blowing mouth（7）With the hydraulic control mouth（9）With the inner cylinder of the autoclave body（1）
Connection；Bottom temp meter interface is equipped on side wall of the autoclave body close to bottom（10）；The slag notch（5）For trumpet type.
2. a kind of high-efficiency environment friendly distillation still according to claim 1, which is characterized in that the slag notch（5）Loudspeaker angle
For 30o.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810675347.4A CN108543325A (en) | 2018-06-27 | 2018-06-27 | High-efficiency environment friendly distillation still |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810675347.4A CN108543325A (en) | 2018-06-27 | 2018-06-27 | High-efficiency environment friendly distillation still |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN108543325A true CN108543325A (en) | 2018-09-18 |
Family
ID=63494028
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201810675347.4A Pending CN108543325A (en) | 2018-06-27 | 2018-06-27 | High-efficiency environment friendly distillation still |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN108543325A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112138418A (en) * | 2020-10-28 | 2020-12-29 | 贵州航天乌江机电设备有限责任公司 | Kettle type heat exchange separator |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN204233800U (en) * | 2014-08-29 | 2015-04-01 | 江苏弘盛新材料股份有限公司 | A kind of horizontal distillation still |
| CN204973114U (en) * | 2015-09-22 | 2016-01-20 | 成都艾比科生物科技有限公司 | Flash tank for preparing dimethyl ether |
| CN205461096U (en) * | 2016-01-29 | 2016-08-17 | 石家庄开泰科技有限公司 | Purified petroleum benzin distillation system |
| CN208406130U (en) * | 2018-06-27 | 2019-01-22 | 江阴中南重工有限公司 | High-efficiency environment friendly distillation still |
-
2018
- 2018-06-27 CN CN201810675347.4A patent/CN108543325A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN204233800U (en) * | 2014-08-29 | 2015-04-01 | 江苏弘盛新材料股份有限公司 | A kind of horizontal distillation still |
| CN204973114U (en) * | 2015-09-22 | 2016-01-20 | 成都艾比科生物科技有限公司 | Flash tank for preparing dimethyl ether |
| CN205461096U (en) * | 2016-01-29 | 2016-08-17 | 石家庄开泰科技有限公司 | Purified petroleum benzin distillation system |
| CN208406130U (en) * | 2018-06-27 | 2019-01-22 | 江阴中南重工有限公司 | High-efficiency environment friendly distillation still |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112138418A (en) * | 2020-10-28 | 2020-12-29 | 贵州航天乌江机电设备有限责任公司 | Kettle type heat exchange separator |
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| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20180918 |
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| WD01 | Invention patent application deemed withdrawn after publication |