CN108530997A - Interior wall coating of fungus-resistant and preparation method thereof - Google Patents
Interior wall coating of fungus-resistant and preparation method thereof Download PDFInfo
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- CN108530997A CN108530997A CN201810233095.XA CN201810233095A CN108530997A CN 108530997 A CN108530997 A CN 108530997A CN 201810233095 A CN201810233095 A CN 201810233095A CN 108530997 A CN108530997 A CN 108530997A
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- fungus
- resistant
- interior wall
- mass parts
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D101/00—Coating compositions based on cellulose, modified cellulose, or cellulose derivatives
- C09D101/08—Cellulose derivatives
- C09D101/26—Cellulose ethers
- C09D101/28—Alkyl ethers
- C09D101/284—Alkyl ethers with hydroxylated hydrocarbon radicals
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/14—Paints containing biocides, e.g. fungicides, insecticides or pesticides
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/61—Additives non-macromolecular inorganic
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/65—Additives macromolecular
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K5/00—Use of organic ingredients
- C08K5/0008—Organic ingredients according to more than one of the "one dot" groups of C08K5/01 - C08K5/59
- C08K5/0058—Biocides
Abstract
A kind of interior wall coating of fungus-resistant is provided, which includes the fungus-resistant lotion of 30 60 mass parts；Wherein, fungus-resistant lotion is extracts of Chinese herbal medicine.Interior wall sealing wax of the present invention not only has good workability, and fungus-resistant performance protrudes.
Description
Technical field
The present invention relates generally to paint fields, and particularly, are related to interior wall coating of fungus-resistant and preparation method thereof.
Background technology
Interior wall coating is relatively stable and ripe in terms of traditional performance and environmental protection at present, with people's living standard
The technology requirement improved to the industry is also higher and higher, and conventional interior wall paint cannot reach the requirement of people, it is therefore desirable to
The new function of invention coating.
Although currently, more to mould proof, antibacterial research, also about the research in fungus-resistant emulsion applications to coating
Less, the dosage and technology of preparing of fungus-resistant lotion have certain difference, therefore, how to provide a kind of fungus-resistant
Interior wall coating is those skilled in the art's technical problem urgently to be resolved hurrily.
Invention content
The present invention provides a kind of interior wall coating of fungus-resistant, has and effectively adjusts indoor air humidity, is allowed to control and exists
It is beneficial in the range of health, pollution-free, zero release is provided simultaneously with excellent anti-pollution characteristic, effectively to extend metope
The decoration time limit, the effect for making the living environment of people be optimal.
The present invention provides a kind of interior wall coating of fungus-resistant, which includes the fungus-resistant of 30-60 mass parts
Lotion；Wherein, the fungus-resistant lotion is extracts of Chinese herbal medicine.
In some embodiments, in the interior wall coating of the fungus-resistant, the fungus-resistant lotion is cloves, greatly
Yellow and galangal extracting solution.
In some embodiments, in the interior wall coating of the fungus-resistant, the preparation side of the fungus-resistant lotion
Method is：Each 20g of cloves, rheum officinale, galangal is weighed, 1000ml is added water to, is put into after being impregnated l days in 50 DEG C of waters bath with thermostatic control and filters,
Obtain the fungus-resistant lotion.
In some embodiments, include fourth in the interior wall coating of the fungus-resistant, in the fungus-resistant lotion
Fragrant phenol, aceteugenol, β-carypohyllene, methyl-n-amyl ketone and gaultherolin.
In some embodiments, in the interior wall coating of the fungus-resistant, also include in the fungus-resistant lotion
N- phenyl-salicyl imines and n-Hydroxyphthalimide.
In some embodiments, in the interior wall coating of the fungus-resistant, which further includes 2-6 parts of quality
The mass concentration of the Whey Protein Concentrate solution of part, the Whey Protein Concentrate solution is 10-20%.
In some embodiments, in the interior wall coating of the fungus-resistant, which further includes 0.1-0.2 matter
Point of the amount cellulose of part, the pH adjusting agent of 0.1-0.3 mass parts, the wetting agent of 0.1-0.5 mass parts, 0.2-0.4 mass parts
Powder, the antifoaming agent of 0.2-0.6 mass parts, the titanium dioxide of 100-250 mass parts, the filler of 15.3-25 mass parts, 0.1-0.15
The levelling agent of the coalescents of mass parts, the thickener of 0.1-0.8 mass parts, 0.3-0.8 mass parts.
In some embodiments, in the interior wall coating of the fungus-resistant, the wetting agent is polyxyethylated
Phenolic ether, polyoxyethylene aliphatic alcohol ether or polyoxyethylene polyoxypropylene block copolymer；The thickener be alkali soluble rise thickener or
Polyacrylate；The cellulose is hydroxyethyl cellulose；The dispersant is ammonium polyacrylate salt；The antifoaming agent is mineral
Oil；The titanium dioxide is rutile titanium white powder；The levelling agent is polyurethanes levelling agent；The filler be calcined kaolin,
One or more combinations in diatomite and powdered whiting.
Another aspect of the present invention provides a kind of preparation method of the interior wall coating of fungus-resistant comprising following steps：Step
Rapid one, deionized water is added in reaction kettle, cellulose, pH adjusting agent, profit is sequentially added with the speed stirring of 100-200rpm
Humectant, dispersant, antifoaming agent, antifreezing agent stir 2-5min to uniform with the speed of 500-800rpm；Step 2: to reaction kettle
In sequentially add titanium dioxide and filler, 30-40min is stirred under 1000-1200rpm rotating speeds, until fineness≤55um；Step 3: to
Fungus-resistant lotion and levelling agent are added in reaction kettle, 800-1200rpm rotary speeds stir 5-10min, be added thickener into
Row is thickened to 80-100KU/25 DEG C/stormer viscosity meter, and the interior wall coating of fungus-resistant is made.
In some embodiments, in the preparation method of the interior wall coating of the fungus-resistant, in the step 2
Further include the steps that the addition Whey Protein Concentrate solution into the fungus-resistant lotion between the step 3, according to volume
Glycerine is added in the fungus-resistant lotion than the ratio of 0.1-0.2/1,2-5min is stirred extremely in the speed of 500-600rpm
Uniformly obtain glycerine/fungus-resistant lotion mixed liquor；According to the ratio of volume ratio 2-3/1, glycerine/fungus-resistant lotion described in phase
Whey Protein Concentrate solution is added in mixed liquor, 1-5min is stirred under 10000-12000rpm rotating speeds.
Advantageous effect：
In the interior wall coating of fungus-resistant of the present invention, being added in interior wall coating has Chinese herbal medicine extract to be configured to
Fungus-resistant lotion, the fungus-resistant lotion that natural plants are configured to can increase interior wall coating mould proof, antibacterial function and
The environmental requirement of interior wall coating can be met.
Specific implementation mode
The existing various exemplary embodiment that the present invention will be described in detail, the detailed description are not considered as the limit to the present invention
System, and it is understood as the more detailed description to certain aspects of the invention, characteristic and embodiment.
It should be understood that heretofore described term is only to describe special embodiment, being not intended to limit this hair
It is bright.In addition, for the numberical range in the present invention, it is thus understood that it is also specifically disclosed that every between the upper and lower bound of the range
A median.Median and any other statement value in any statement value or stated ranges or in the range in
Between each of between value smaller range be also included in the present invention.These small range of upper and lower bounds can include independently
Or it excludes in range.
Unless otherwise stated, all technical and scientific terms used herein has the routine in field of the present invention
The normally understood identical meanings of technical staff.Although the present invention only describes preferred method and material, the present invention's
Implement or can also be used and similar or equivalent any method and material described herein in testing.The institute mentioned in this specification
There is document to be incorporated by reference into, to disclosure and description and the relevant method of the document and/or material.It is incorporated to any
When document conflicts, it is subject to the content of this specification.
Without departing substantially from the scope or spirit of the invention, the specific implementation mode of description of the invention can be done more
Kind is improved and variation, this will be apparent to those skilled in the art.Other realities obtained by the specification of the present invention
It is apparent obtain to apply mode for technical personnel.Present specification and embodiment are merely exemplary.
It is the term of opening, i.e., about "comprising" used herein, " comprising ", " having ", " containing " etc.
Mean including but not limited to.
Heretofore described " mass parts " or " % " unless otherwise instructed, by mass.
A kind of interior wall coating of fungus-resistant of the present invention, the interior wall sealing wax include the mould proof suppression of 30-60 mass parts
Bacterium lotion；Wherein, the fungus-resistant lotion is extracts of Chinese herbal medicine.
It using extracts of Chinese herbal medicine as fungus-resistant lotion, is added in interior wall coating, improves the mould proof of interior wall coating
Bacteriostasis property, while other chemical reagent are added not into interior wall coating, the VOC values of interior wall coating will not be increased, ensured
The feature of environmental protection of interior wall coating.
In some embodiments, the fungus-resistant lotion be cloves, rheum officinale and galangal extracting solution.Wherein, institute
The dry flower (flos caryophylli) that cloves is plant clove of myrtaceae is stated, the rheum officinale is polygonaceae (Polygonaceae) Rheum
(Rheum) perennial herb；The galangal is the dry root of zingiberaceous plant galangal Alpinia officinarum Hance
Stem.Cloves, rheum officinale and galangal all have antibacterial to 27 plants of moulds such as various article moulding fungis such as mould, aspergillus, trichoderma, head mold
Effect, wherein the minimum inhibitory concentration (MIC) of cloves extracting solution is 500~1250 mcg/mls, minimum bactericidal concentration (MFC)
For 2500~5000 mcg/mls.Microscopically observation arrives, and volatile clove oil can destroy rapidly mold structures, make mycotic spore
It falls off, decompose, to play the role of killing bacterium.
In some embodiments, eugenol, aceteugenol, β-carypohyllene, first are included in the fungus-resistant lotion
Base n-pentyl ketone and gaultherolin.Wherein, the eugenol comprising 40-60 mass parts, 20-30 matter in the fungus-resistant lotion
Measure the aceteugenol of part, β-carypohyllene of 20-30 mass parts, the methyl-n-amyl ketone of 10-20 mass parts and 30-40 mass parts
Gaultherolin.
In some embodiments, also include N- phenyl-salicyl imines and N- hydroxyls in the fungus-resistant lotion
Phthalimide.
Wherein, the N- phenyl-salicyl imines is salicylide to be extracted from plant as raw material, is repaiied by bromo
Decorations, are made 5- bromos and 3, and bis- bromo salicylides of 5- are condensed to yield N- phenyl-salicyl imines chemical combination with substituted aromatic amines
Object.N- phenyl-salicyl imines and n-Hydroxyphthalimide read staphylococcus aureus, Escherichia coli, white
Pearl bacterium all has stronger bacteriostatic activity.N- phenyl-salicyl the imines and n-Hydroxyphthalimide and cloves,
The extracting solution of rheum officinale and galangal has good intermiscibility, and N- phenyl-salicyl imines does not influence cloves, rheum officinale
With fungus-resistant effect of the extracting solution of galangal, and its bacteriostasis can be made to be enhanced.
In some embodiments, which further includes the Whey Protein Concentrate solution of 2-6 parts of mass parts, the breast
The mass concentration of clear protein concentrate solution is 10-20%.
In said program, the Whey Protein Concentrate of the Whey Protein Concentrate solution is WPC-80, and Whey Protein Concentrate is molten
Liquid energy is made into Whey Protein Concentrate/Chinese medical extract mixed solution with the Chinese medicine extract, and concrete configuration process is：Configuration
The WPC-80 solution of a concentration of 10-20%, stirring 15min make it fully dissolve, and solution ph is adjusted with 1mol/LNAOH solution,
It is put into water-bath and heats a period of time, while being mixed with Chinese medicine extract with glycerine, 5% is added after the cooling of WPC-80 solution
Glycerine/fourth Chinese medicine extract, and 1-5min is stirred under high speed dispersion homogenizer 10000rpm, ultrasonic wave removes bubble.Whey
Protein concentrate has preferable mechanical property and appearance transparent, energy after Whey Protein Concentrate/Chinese medical extract mixed solution drying
Enough rapid draing, shortens the surface drying time of interior wall coating of the present invention.
In some embodiments, which further includes the cellulose of 0.1-0.2 mass parts, 0.1-0.3 mass parts
PH adjusting agent, the wetting agent of 0.1-0.5 mass parts, the dispersant of 0.2-0.4 mass parts, 0.2-0.6 mass parts antifoaming agent,
The titanium dioxide of 100-250 mass parts, the filler of 15.3-25 mass parts, the coalescents of 0.1-0.15 mass parts, 0.1-0.8 matter
Measure the levelling agent of the thickener and 0.3-0.8 mass parts of part.
Wherein, the wetting agent is polyoxyethylated alkyl phenol, polyoxyethylene aliphatic alcohol ether or polyoxyethylene polyoxypropylene
Block copolymer；The thickener is that alkali soluble rises thickener or polyacrylate；The cellulose is hydroxyethyl cellulose；It is described
Dispersant is ammonium polyacrylate salt；The antifoaming agent is mineral oil；The titanium dioxide is rutile titanium white powder；The levelling agent is
Polyurethanes levelling agent；The filler is one or more combinations in calcined kaolin, diatomite and powdered whiting.
The present invention also provides a kind of preparation methods of the interior wall coating of fungus-resistant comprising following steps：
Step 1: deionized water is added in reaction kettle, cellulose, pH are sequentially added with the speed stirring of 100-200rpm
Conditioning agent, wetting agent, dispersant, antifoaming agent, antifreezing agent stir 2-5min to uniform with the speed of 500-800rpm；
Step 2: sequentially adding titanium dioxide and filler into reaction kettle, 30-40min is stirred under 1000-1200rpm rotating speeds,
To fineness≤55um；
Step 3: fungus-resistant lotion and levelling agent are added into reaction kettle, 800-1200rpm rotary speeds stir 5-
10min is added thickener and carries out being thickened to 80-100KU/25 DEG C/stormer viscosity meter, the interior wall coating of fungus-resistant is made.
In some embodiments, in the preparation method of the interior wall coating of the fungus-resistant, in the step 2 and
Further include the steps that the addition Whey Protein Concentrate solution into the fungus-resistant lotion between the step 3, according to volume ratio
Glycerine is added in the fungus-resistant lotion ratio of 0.1-0.2/1, and 2-5min is stirred to equal in the speed of 500-600rpm
It is even to obtain glycerine/fungus-resistant lotion mixed liquor；According to the ratio of volume ratio 2-3/1, glycerine/fungus-resistant lotion is mixed described in phase
It closes and Whey Protein Concentrate solution is added in liquid, 1-5min is stirred under 10000-12000rpm rotating speeds.
Fungus-resistant of the present invention is by the way that coating to be coated on the wall in room, and coated area is identical, room
Between door, window the case where opening, Escherichia coli on test metope, staphylococcus aureus and moulding fungi are carried out after 2 months
And measure mouldy area (mouldy region accounts for the range of coating coated area).
Surface drying time of the present invention is by referring to national standard《GB/T 6753.2-1986 coating surface drying experiments
Ballotini method》To test.
Contrast ratio of the present invention is by referring to national standard《GB/T23981-2009 whites and light colour paint contrast ratio
It measures》To test.
Acid resistance and alkali resistance of the present invention pass through national standard《GB/T 1763-1979 paint film chemical reagent resistances
Measuring method》To test.
Low temperature resistant storage property of the present invention is tested by the following method, product is coated on the coating with paint, -40
It is stored in DEG C temperature environment for 24 hours, observes coating conditions.
Embodiment
Embodiment 1
A kind of interior wall coating of fungus-resistant, wherein the interior wall sealing wax includes the fungus-resistant lotion of 30-60 mass parts；
Wherein, the fungus-resistant lotion is extracts of Chinese herbal medicine, wherein the fungus-resistant lotion is cloves, rheum officinale and galangal
Extracting solution.
In said program, the preparation method of the fungus-resistant lotion is：Each 20g of cloves, rheum officinale, galangal is weighed, is added
Water is put into after being impregnated l days in 50 DEG C of waters bath with thermostatic control and filters, obtain the fungus-resistant lotion to 1000ml.Wherein, described mould proof
Include eugenol, aceteugenol, β-carypohyllene, methyl-n-amyl ketone and gaultherolin in Bacteriostasis Emulsion.
In said program, the interior wall coating further include the cellulose of 0.1-0.2 mass parts, 0.1-0.3 mass parts pH tune
Save agent, the wetting agent of 0.1-0.5 mass parts, the dispersant of 0.2-0.4 mass parts, the antifoaming agent of 0.2-0.6 mass parts, 100-
The titanium dioxide of 250 mass parts, the filler of 15.3-25 mass parts, the coalescents of 0.1-0.15 mass parts, 0.1-0.8 mass parts
Thickener, 0.3-0.8 mass parts levelling agent.
Wherein, the wetting agent is polyoxyethylated alkyl phenol, polyoxyethylene aliphatic alcohol ether or polyoxyethylene polyoxypropylene
Block copolymer；The thickener is that alkali soluble rises thickener or polyacrylate；The cellulose is hydroxyethyl cellulose；It is described
Dispersant is ammonium polyacrylate salt；The antifoaming agent is mineral oil；The titanium dioxide is rutile titanium white powder；The levelling agent is
Polyurethanes levelling agent；The filler is one or more combinations in calcined kaolin, diatomite and powdered whiting.
Preparation method：
Step 1: deionized water is added in reaction kettle, cellulose, pH are sequentially added with the speed stirring of 100-200rpm
Conditioning agent, wetting agent, dispersant, antifoaming agent, antifreezing agent stir 2-5min to uniform with the speed of 500-800rpm；
Step 2: sequentially adding titanium dioxide and filler into reaction kettle, 30-40min is stirred under 1000-1200rpm rotating speeds,
To fineness≤55um；
Step 3: fungus-resistant lotion and levelling agent are added into reaction kettle, 800-1200rpm rotary speeds stir 5-
10min is added thickener and carries out being thickened to 80-100KU/25 DEG C/stormer viscosity meter, the interior wall coating of fungus-resistant is made.
Embodiment 2
A kind of interior wall coating of fungus-resistant, wherein the interior wall sealing wax includes the fungus-resistant lotion of 30-60 mass parts；
Wherein, the fungus-resistant lotion is extracts of Chinese herbal medicine, wherein the fungus-resistant lotion is cloves, rheum officinale and galangal
Extracting solution.
In said program, the preparation method of the fungus-resistant lotion is：Each 20g of cloves, rheum officinale, galangal is weighed, is added
Water is put into after being impregnated l days in 50 DEG C of waters bath with thermostatic control and filters, obtain the fungus-resistant lotion to 1000ml.Wherein, described mould proof
Include eugenol, aceteugenol, β-carypohyllene, methyl-n-amyl ketone and gaultherolin in Bacteriostasis Emulsion.
In said program, the interior wall coating further include the cellulose of 0.1-0.2 mass parts, 0.1-0.3 mass parts pH tune
Save agent, the wetting agent of 0.1-0.5 mass parts, the dispersant of 0.2-0.4 mass parts, the antifoaming agent of 0.2-0.6 mass parts, 100-
The titanium dioxide of 250 mass parts, the filler of 15.3-25 mass parts, the coalescents of 0.1-0.15 mass parts, 0.1-0.8 mass parts
Thickener, 0.3-0.8 mass parts levelling agent.
Wherein, the wetting agent is polyoxyethylated alkyl phenol, polyoxyethylene aliphatic alcohol ether or polyoxyethylene polyoxypropylene
Block copolymer；The thickener is that alkali soluble rises thickener or polyacrylate；The cellulose is hydroxyethyl cellulose；It is described
Dispersant is ammonium polyacrylate salt；The antifoaming agent is mineral oil；The titanium dioxide is rutile titanium white powder；The levelling agent is
Polyurethanes levelling agent；The filler is one or more combinations in calcined kaolin, diatomite and powdered whiting.
Preparation method：
Step 1: deionized water is added in reaction kettle, cellulose, pH are sequentially added with the speed stirring of 100-200rpm
Conditioning agent, wetting agent, dispersant, antifoaming agent, antifreezing agent stir 2-5min to uniform with the speed of 500-800rpm；
Step 2: sequentially adding titanium dioxide and filler into reaction kettle, 30-40min is stirred under 1000-1200rpm rotating speeds,
To fineness≤55um；
Step 3: fungus-resistant lotion and levelling agent are added into reaction kettle, 800-1200rpm rotary speeds stir 5-
10min is added thickener and carries out being thickened to 80-100KU/25 DEG C/stormer viscosity meter, the interior wall coating of fungus-resistant is made.
Embodiment 3
A kind of interior wall coating of fungus-resistant, wherein the interior wall sealing wax includes the fungus-resistant lotion of 30-60 mass parts；
Wherein, the fungus-resistant lotion is extracts of Chinese herbal medicine, wherein the fungus-resistant lotion is cloves, rheum officinale and galangal
Extracting solution.
In said program, the preparation method of the fungus-resistant lotion is：Each 20g of cloves, rheum officinale, galangal is weighed, is added
Water is put into after being impregnated l days in 50 DEG C of waters bath with thermostatic control and filters, obtain the fungus-resistant lotion to 1000ml.Wherein, described mould proof
Include eugenol, aceteugenol, β-carypohyllene, methyl-n-amyl ketone and gaultherolin in Bacteriostasis Emulsion.
In said program, the interior wall coating further include the cellulose of 0.1-0.2 mass parts, 0.1-0.3 mass parts pH tune
Save agent, the wetting agent of 0.1-0.5 mass parts, the dispersant of 0.2-0.4 mass parts, the antifoaming agent of 0.2-0.6 mass parts, 100-
The titanium dioxide of 250 mass parts, the filler of 15.3-25 mass parts, the coalescents of 0.1-0.15 mass parts, 0.1-0.8 mass parts
Thickener, 0.3-0.8 mass parts levelling agent.
Wherein, the wetting agent is polyoxyethylated alkyl phenol, polyoxyethylene aliphatic alcohol ether or polyoxyethylene polyoxypropylene
Block copolymer；The thickener is that alkali soluble rises thickener or polyacrylate；The cellulose is hydroxyethyl cellulose；It is described
Dispersant is ammonium polyacrylate salt；The antifoaming agent is mineral oil；The titanium dioxide is rutile titanium white powder；The levelling agent is
Polyurethanes levelling agent；The filler is one or more combinations in calcined kaolin, diatomite and powdered whiting.
Preparation method：
Step 1: deionized water is added in reaction kettle, cellulose, pH are sequentially added with the speed stirring of 100-200rpm
Conditioning agent, wetting agent, dispersant, antifoaming agent, antifreezing agent stir 2-5min to uniform with the speed of 500-800rpm；
Step 2: sequentially adding titanium dioxide and filler into reaction kettle, 30-40min is stirred under 1000-1200rpm rotating speeds,
To fineness≤55um；
Step 3: fungus-resistant lotion and levelling agent are added into reaction kettle, 800-1200rpm rotary speeds stir 5-
10min is added thickener and carries out being thickened to 80-100KU/25 DEG C/stormer viscosity meter, the interior wall coating of fungus-resistant is made.
Embodiment 4
A kind of interior wall coating of fungus-resistant, wherein the interior wall sealing wax includes the fungus-resistant lotion of 30-60 mass parts；
Wherein, the fungus-resistant lotion includes that extracts of Chinese herbal medicine, N- phenyl-salicyl imines and N- hydroxyls phthalyl are sub-
Amine, wherein the fungus-resistant lotion be cloves, rheum officinale and galangal extracting solution.
In said program, the preparation method of the fungus-resistant lotion is：Each 20g of cloves, rheum officinale, galangal is weighed, is added
Water is put into after being impregnated l days in 50 DEG C of waters bath with thermostatic control and filters, obtain the fungus-resistant lotion to 1000ml.Wherein, described mould proof
Include eugenol, aceteugenol, β-carypohyllene, methyl-n-amyl ketone and gaultherolin in Bacteriostasis Emulsion.
In said program, the interior wall coating further include the cellulose of 0.1-0.2 mass parts, 0.1-0.3 mass parts pH tune
Save agent, the wetting agent of 0.1-0.5 mass parts, the dispersant of 0.2-0.4 mass parts, the antifoaming agent of 0.2-0.6 mass parts, 100-
The titanium dioxide of 250 mass parts, the filler of 15.3-25 mass parts, the coalescents of 0.1-0.15 mass parts, 0.1-0.8 mass parts
Thickener, 0.3-0.8 mass parts levelling agent.
Wherein, the wetting agent is polyoxyethylated alkyl phenol, polyoxyethylene aliphatic alcohol ether or polyoxyethylene polyoxypropylene
Block copolymer；The thickener is that alkali soluble rises thickener or polyacrylate；The cellulose is hydroxyethyl cellulose；It is described
Dispersant is ammonium polyacrylate salt；The antifoaming agent is mineral oil；The titanium dioxide is rutile titanium white powder；The levelling agent is
Polyurethanes levelling agent；The filler is one or more combinations in calcined kaolin, diatomite and powdered whiting.
Preparation method：
Step 1: deionized water is added in reaction kettle, cellulose, pH are sequentially added with the speed stirring of 100-200rpm
Conditioning agent, wetting agent, dispersant, antifoaming agent, antifreezing agent stir 2-5min to uniform with the speed of 500-800rpm；
Step 2: sequentially adding titanium dioxide and filler into reaction kettle, 30-40min is stirred under 1000-1200rpm rotating speeds,
To fineness≤55um；
Step 3: glycerine is added in the fungus-resistant lotion ratio according to volume ratio 0.1-0.2/1, in 500-
The speed of 600rpm stirs 2-5min to uniformly obtaining glycerine/fungus-resistant lotion mixed liquor；According to the ratio of volume ratio 2-3/1
, Whey Protein Concentrate solution is added in glycerine/fungus-resistant lotion mixed liquor described in phase, is stirred under 10000-12000rpm rotating speeds
Mix 1-5min.
Step 4: fungus-resistant lotion and levelling agent are added into reaction kettle, 800-1200rpm rotary speeds stir 5-
10min is added thickener and carries out being thickened to 80-100KU/25 DEG C/stormer viscosity meter, the interior wall coating of fungus-resistant is made.
Embodiment 5
A kind of interior wall coating of fungus-resistant, wherein the interior wall sealing wax include 30-60 mass parts fungus-resistant lotion and
The mass concentration of the Whey Protein Concentrate solution of 2-6 parts of mass parts, the Whey Protein Concentrate solution is 10-20%；Wherein, institute
It states fungus-resistant lotion and includes extracts of Chinese herbal medicine, N- phenyl-salicyl imines and n-Hydroxyphthalimide,
In, the fungus-resistant lotion be cloves, rheum officinale and galangal extracting solution.
In said program, the preparation method of the fungus-resistant lotion is：Each 20g of cloves, rheum officinale, galangal is weighed, is added
Water is put into after being impregnated l days in 50 DEG C of waters bath with thermostatic control and filters, obtain the fungus-resistant lotion to 1000ml.Wherein, described mould proof
Include eugenol, aceteugenol, β-carypohyllene, methyl-n-amyl ketone and gaultherolin in Bacteriostasis Emulsion.
In said program, the interior wall coating further include the cellulose of 0.1-0.2 mass parts, 0.1-0.3 mass parts pH tune
Save agent, the wetting agent of 0.1-0.5 mass parts, the dispersant of 0.2-0.4 mass parts, the antifoaming agent of 0.2-0.6 mass parts, 100-
The titanium dioxide of 250 mass parts, the filler of 15.3-25 mass parts, the coalescents of 0.1-0.15 mass parts, 0.1-0.8 mass parts
Thickener, 0.3-0.8 mass parts levelling agent.
Wherein, the wetting agent is polyoxyethylated alkyl phenol, polyoxyethylene aliphatic alcohol ether or polyoxyethylene polyoxypropylene
Block copolymer；The thickener is that alkali soluble rises thickener or polyacrylate；The cellulose is hydroxyethyl cellulose；It is described
Dispersant is ammonium polyacrylate salt；The antifoaming agent is mineral oil；The titanium dioxide is rutile titanium white powder；The levelling agent is
Polyurethanes levelling agent；The filler is one or more combinations in calcined kaolin, diatomite and powdered whiting.
Preparation method：
Step 1: deionized water is added in reaction kettle, cellulose, pH are sequentially added with the speed stirring of 100-200rpm
Conditioning agent, wetting agent, dispersant, antifoaming agent, antifreezing agent stir 2-5min to uniform with the speed of 500-800rpm；
Step 2: sequentially adding titanium dioxide and filler into reaction kettle, 30-40min is stirred under 1000-1200rpm rotating speeds,
To fineness≤55um；
Step 3: glycerine is added in the fungus-resistant lotion ratio according to volume ratio 0.1-0.2/1, in 500-
The speed of 600rpm stirs 2-5min to uniformly obtaining glycerine/fungus-resistant lotion mixed liquor；According to the ratio of volume ratio 2-3/1
, Whey Protein Concentrate solution is added in glycerine/fungus-resistant lotion mixed liquor described in phase, is stirred under 10000-12000rpm rotating speeds
Mix 1-5min.
Step 4: fungus-resistant lotion and levelling agent are added into reaction kettle, 800-1200rpm rotary speeds stir 5-
10min is added thickener and carries out being thickened to 80-100KU/25 DEG C/stormer viscosity meter, the interior wall coating of fungus-resistant is made.
Comparative example 1
A kind of interior wall coating, wherein the interior wall sealing wax include the styrene-acrylic emulsion of 35 mass parts, 0.1-0.2 mass parts fibre
Tie up element, the pH adjusting agent of 0.1-0.3 mass parts, the wetting agent of 0.1-0.5 mass parts, the dispersant of 0.2-0.4 mass parts, 0.2-
The antifoaming agent of 0.6 mass parts, the titanium dioxide of 100-250 mass parts, the fillers of 15.3-25 mass parts, 0.1-0.15 mass parts
The levelling agent of coalescents, the thickener of 0.1-0.8 mass parts, 0.3-0.8 mass parts.
The characterization test result of the interior wall coating for the fungus-resistant being prepared in above-described embodiment 1-5 and comparative example 1 is such as
Shown in table 1, it can be seen that using the interior wall coating of fungus-resistant of the present invention, fungus-resistant is with obvious effects, and has
Good workability.
Table 1
Without departing substantially from the scope or spirit of the invention, the specific implementation mode of description of the invention can be done more
Kind is improved and variation, this will be apparent to those skilled in the art.Other realities obtained by the specification of the present invention
It is apparent obtain to apply mode for technical personnel.Present specification and embodiment are merely exemplary.
Claims (10)
1. a kind of interior wall coating of fungus-resistant, wherein the interior wall sealing wax includes the fungus-resistant lotion of 30-60 mass parts；
Wherein, the fungus-resistant lotion is extracts of Chinese herbal medicine.
2. the interior wall coating of fungus-resistant according to claim 1, wherein the fungus-resistant lotion is cloves, rheum officinale
With the extracting solution of galangal.
3. the interior wall coating of fungus-resistant according to claim 2, wherein the preparation method of the fungus-resistant lotion
For：Cloves, rheum officinale and each 20g of galangal are weighed, 1000ml is added water to, is put into after being impregnated l days in 50 DEG C of waters bath with thermostatic control and filters, obtain
To the fungus-resistant lotion.
4. the interior wall coating of fungus-resistant according to claim 3, wherein include cloves in the fungus-resistant lotion
Phenol, aceteugenol, β-carypohyllene, methyl-n-amyl ketone and gaultherolin.
5. the interior wall coating of fungus-resistant according to claim 4, wherein also include N- benzene in the fungus-resistant lotion
Base-salicyl imines and n-Hydroxyphthalimide.
6. the interior wall coating of fungus-resistant according to claim 5, wherein the interior wall coating further includes 2-6 parts of mass parts
Whey Protein Concentrate solution, the mass concentration of the Whey Protein Concentrate solution is 10-20%.
7. the interior wall coating of fungus-resistant according to claim 1, wherein the interior wall coating further includes 0.1-0.2 mass
The dispersion of the cellulose, the pH adjusting agent of 0.1-0.3 mass parts, the wetting agent of 0.1-0.5 mass parts, 0.2-0.4 mass parts of part
Agent, the antifoaming agent of 0.2-0.6 mass parts, the titanium dioxide of 100-250 mass parts, the filler of 15.3-25 mass parts, 0.1-0.15 matter
Measure the levelling agent of the coalescents of part, the thickener and 0.3-0.8 mass parts of 0.1-0.8 mass parts.
8. the interior wall coating of fungus-resistant according to claim 7, wherein
The wetting agent is polyoxyethylated alkyl phenol, polyoxyethylene aliphatic alcohol ether or polyoxyethylene polyoxypropylene block copolymerization
Object；
The thickener is that alkali soluble rises thickener or polyacrylate；
The cellulose is hydroxyethyl cellulose；
The dispersant is ammonium polyacrylate salt；
The antifoaming agent is mineral oil；
The titanium dioxide is rutile titanium white powder；
The levelling agent is polyurethanes levelling agent；
The filler is one or more combinations in calcined kaolin, diatomite and powdered whiting.
9. a kind of preparation method of interior wall coating according to claim 1 to 8 any one of them fungus-resistant comprising as follows
Step：
Step 1: deionized water is added in reaction kettle, with the speed stirring of 100-200rpm sequentially adds cellulose, pH is adjusted
Agent, wetting agent, dispersant, antifoaming agent and antifreezing agent stir 2-5min to uniform with the speed of 500-800rpm；
Step 2: sequentially adding titanium dioxide and filler into reaction kettle, 30-40min is stirred under 1000-1200rpm rotating speeds, until thin
Degree≤55um；
Step 3: fungus-resistant lotion and levelling agent are added into reaction kettle, 800-1200rpm rotary speeds stir 5-10min,
Thickener is added to carry out being thickened to 80-100KU/25 DEG C/stormer viscosity meter, the interior wall coating of fungus-resistant is made.
10. the preparation method of the interior wall coating according to the fungus-resistant described in claim 9, in the step 2 and the step
Further include the steps that the addition Whey Protein Concentrate solution into the fungus-resistant lotion between three, according to volume ratio 0.1-0.2/
Glycerine is added in the fungus-resistant lotion 1 ratio, sweet to uniformly obtaining in the speed stirring 2-5min of 500-600rpm
Oil/fungus-resistant lotion mixed liquor；According to the ratio of volume ratio 2-3/1, add in glycerine/fungus-resistant lotion mixed liquor described in phase
Enter Whey Protein Concentrate solution, 1-5min is stirred under 10000-12000rpm rotating speeds.
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