CN108504282A - A kind of nanometer of moisture retardant blocks agent prescription and preparation method - Google Patents
A kind of nanometer of moisture retardant blocks agent prescription and preparation method Download PDFInfo
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- CN108504282A CN108504282A CN201810433917.9A CN201810433917A CN108504282A CN 108504282 A CN108504282 A CN 108504282A CN 201810433917 A CN201810433917 A CN 201810433917A CN 108504282 A CN108504282 A CN 108504282A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D183/00—Coating compositions based on macromolecular compounds obtained by reactions forming in the main chain of the macromolecule a linkage containing silicon, with or without sulfur, nitrogen, oxygen, or carbon only; Coating compositions based on derivatives of such polymers
- C09D183/04—Polysiloxanes
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/18—Fireproof paints including high temperature resistant paints
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/61—Additives non-macromolecular inorganic
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
- C08K3/20—Oxides; Hydroxides
- C08K3/22—Oxides; Hydroxides of metals
- C08K2003/2227—Oxides; Hydroxides of metals of aluminium
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
- C08K3/24—Acids; Salts thereof
- C08K3/26—Carbonates; Bicarbonates
- C08K2003/265—Calcium, strontium or barium carbonate
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K2201/00—Specific properties of additives
- C08K2201/011—Nanostructured additives
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- Chemical Kinetics & Catalysis (AREA)
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Abstract
A kind of nanometer of moisture retardant of the present invention blocks agent prescription and preparation method, calculates by following weight and is formulated by following components：50 60Kg of viscosity agent of 107 5000CPS,380 390Kg of 10000CPS viscosity agents,120 180Kg of silicone oil,45 55Kg of active coarse whiting,90 110Kg of nano-calcium carbonate,140 160Kg of aluminium hydroxide,230 250Kg of antimony oxide,10 20Kg of Nano carbon white,160 180Kg of JT 316A curing agent,550 coupling agent, 15 16Kg,560 coupling agent, 4 5Kg,801 toughener, 2 4Kg,5 6Kg of dibutyl tin laurate,1 2Kg of catalyst,Present invention aims at the problems for prior art deficiency,And it is not numerous to provide a kind of formula,It prepares simple,It can be moisture-proof,The nanometer moisture retardant of insulation blocks agent prescription and preparation method.
Description
【Technical field】
The invention belongs to equipment moisture retardant object technical fields, and in particular to a kind of nanometer of moisture retardant block agent prescription and
Preparation method.
【Background technology】
Electrical equipment makes moist, and shows that the decreasing insulating of equipment, insulation ag(e)ing accelerate first.According to current medium
Theory, ambient humidity, which increases, makes dielectric conductivity, relative dielectric coefficient, medium consumpting angle tgδ accordingly increase, and hits
Wear field strength reduction.It is worth noting that, the destructive process of insulation often becomes fragile under the action of heat, crack after vibrated, tide
After gas enters crack, very low voltage can also cause to discharge, and cause insulation breakdown.Secondly, exposed metallic conductor with
The increase of humidity, in general its oxidation corrosion can be accelerated, and especially in the case where it adheres to dust, oxidation overlooks meeting more
Soon, so that conductor connection place contact resistance is increased, cause hot-spot.Thus, the electrical equipment being in for a long time in wet environment, such as
It does not use moisture preventive measure, service life that can be greatly lowered, causes electric leakage, short circuit, so as to cause serious electric fault and accident.
Therefore, it is necessary to the adverse effect for preventing or reducing environmental condition to electric product reliability is taken, it is electrical to ensure
Properties in product work increase product reliability of operation in harsh environment.
Fire fighting, the repairing carried out regularly maintenance work, rather than had to run around all the time wears him out.Scram can be produced to company and be caused
Prodigious economic loss, thus it is very necessary to take corresponding measure with smaller input, therefore study a anti-tide-bound of nanometer
Combustion, which blocks agent prescription and preparation method, very important realistic meaning.
【Invention content】
The technical problem to be solved in the present invention is：It is not numerous to provide a kind of formula, prepares simply, can be moisture-proof, insulation is received
Rice moisture retardant blocks agent prescription and preparation method.
In order to achieve the above objectives, a kind of nanometer of moisture retardant of the present invention blocks agent prescription and preparation method, which is characterized in that
It calculates by following weight and is formulated by following components：Viscosity agent 50-60Kg, the 10000CPS viscosity agent of 107-5000CPS
380-390Kg, silicone oil 120-180Kg, active coarse whiting 45-55Kg, nano-calcium carbonate 90-110Kg, aluminium hydroxide 140-160Kg,
Antimony oxide 230-250Kg, Nano carbon white 10-20Kg, JT-316A curing agent 160-180Kg, 550 coupling agent 15-
16Kg, 560 coupling agent 4-5Kg, 801 toughener 2-4Kg, dibutyl tin laurate 5-6Kg, catalyst 1-2Kg.
In order to achieve the above objectives, a kind of nanometer of moisture retardant of the present invention blocks agent prescription and preparation method, institute
This nanometer moisture retardant stated blocks agent prescription, calculates by following weight and is formulated by following components：Silicone oil 130Kg, JT-
316A curing agent 170Kg, 550 coupling agent 15.5Kg, 560 coupling agent 4.2Kg, 801 toughener 3Kg, dibutyl tin laurate
5.3Kg, catalyst 1-2Kg.
A kind of nanometer of moisture retardant blocks agent prescription and preparation method, described in this nanometer moisture retardant envelope
Blocking agent formula and preparation method are as follows：
The first step checks whether equipment is clean,
Silicone oil 130Kg and JT-316A curing agent 170Kg is added into production equipment for second step, then booting stirring, stirring electricity
Machine speed-frequency is adjusted to 30-40Hz, while vacuumizing and reaching -0.09Mpa or more, timing 30 minutes,
Third walks, and after being mixed evenly, shuts down, releases vacuum, then 550 coupling agent 15.5Kg, 560 couplings are added into production equipment
Agent 4.2Kg, 801 toughener 3Kg, catalyst 1Kg, dibutyl tin laurate 5.3Kg, stirring motor speed-frequency are adjusted to
30-40Hz, while vacuumizing and reaching -0.09Mpa or more, timing 35 minutes,
4th step shuts down cooling and discharges, this preparation is labeled as B preparations.
In order to achieve the above objectives, a kind of nanometer of moisture retardant of the present invention blocks agent prescription and preparation method, institute
This nanometer moisture retardant stated blocks agent prescription, calculates by following weight and is formulated by following components：The 107-
The viscosity agent 55Kg of 5000CPS, 10,000 CPS viscosity agents 385Kg, 1000# silicone oil 176Kg, active coarse whiting 50Kg, nano-calcium carbonate
100Kg, aluminium hydroxide 150Kg, antimony oxide 240Kg, Nano carbon white 15Kg.
In order to achieve the above objectives, a kind of nanometer of moisture retardant of the present invention blocks agent prescription and preparation method, institute
This nanometer moisture retardant stated blocks agent prescription and preparation method is as follows：
The first step throws into whole liquid charging stocks in reaction kettle, and active coarse whiting 50Kg, nano-calcium carbonate 100Kg is added, and booting is stirred
It mixes, stirring motor speed-frequency is adjusted to 40Hz, stirs 15 minutes, shuts down, scrapes paddle,
Third walks, plus nano white carbon 15Kg, and booting stirring 15 minutes, stirring motor speed-frequency is adjusted to 40Hz, shuts down, scrapes
Paddle,
4th step adds remaining solid raw material, booting stirring, stirring motor speed-frequency to be adjusted to 40Hz, stir 15 minutes, heating
To 100 DEG C, shuts down, scrapes paddle,
5th step closes equipment tight, and booting stirring is started simultaneously at and vacuumized, and is vacuumized and is not less than -0.09Mpa, timing 120 minutes,
Speed-frequency 35-40Hz,
This preparation is labeled as A preparations by the 5th step, sampling and testing, consistency 13.5-14cm.
In order to achieve the above objectives, a kind of nanometer of moisture retardant of the present invention blocks agent prescription and preparation method, institute
A kind of nanometer of moisture retardant stated blocks agent prescription and preparation method, which is characterized in that the A preparations and B preparations is abundant
It is used after mixing, using 40-60 minutes latter, Self-leveling diameter 17.5cm-18.5cm is carried out if be not achieved using catalyst
Adjustment finally shuts down until its mixture Self-leveling diameter 17.5cm-18.5cm, scrapes paddle, discharging, barrelling sale.
【Specific implementation mode】
A kind of nanometer of moisture retardant of the present invention blocks agent prescription and preparation method, which is characterized in that by following weight
Amount is calculated and is formulated by following components：Viscosity agent 50-60Kg, 10000CPS the viscosity agent 380-390Kg of 107-5000CPS,
Silicone oil 120-180Kg, active coarse whiting 45-55Kg, nano-calcium carbonate 90-110Kg, aluminium hydroxide 140-160Kg, antimony oxide
230-250Kg, Nano carbon white 10-20Kg, JT-316A curing agent 160-180Kg, 550 coupling agent 15-16Kg, 560 coupling agents
4-5Kg, 801 toughener 2-4Kg, dibutyl tin laurate 5-6Kg, catalyst 1-2Kg.
Further, the preferred implementation of agent prescription and preparation method is blocked in a kind of nanometer of moisture retardant of the present invention
In example, described in this nanometer moisture retardant block agent prescription, calculate by following weight and be formulated by following components：Silicone oil
130Kg, JT-316A curing agent 170Kg, 550 coupling agent 15.5Kg, 560 coupling agent 4.2Kg, 801 toughener 3Kg, tin dilaurate
Dibutyl tin 5.3Kg, catalyst 1-2Kg.
Further, the preferred implementation of agent prescription and preparation method is blocked in a kind of nanometer of moisture retardant of the present invention
Example in, described in this nanometer moisture retardant block agent prescription and preparation method it is as follows：
The first step checks whether equipment is clean,
Silicone oil 130Kg and JT-316A curing agent 170Kg is added into production equipment for second step, then booting stirring, stirring electricity
Machine speed-frequency is adjusted to 30-40Hz, while vacuumizing and reaching -0.09Mpa or more, timing 30 minutes,
Third walks, and after being mixed evenly, shuts down, releases vacuum, then 550 coupling agent 15.5Kg, 560 couplings are added into production equipment
Agent 4.2Kg, 801 toughener 3Kg, catalyst 1Kg, dibutyl tin laurate 5.3Kg, stirring motor speed-frequency are adjusted to
30-40Hz, while vacuumizing and reaching -0.09Mpa or more, timing 35 minutes,
4th step shuts down cooling and discharges, this preparation is labeled as B preparations.
Further, the preferred implementation of agent prescription and preparation method is blocked in a kind of nanometer of moisture retardant of the present invention
In example, described in this nanometer moisture retardant block agent prescription, calculate by following weight and be formulated by following components：It is described
The viscosity agent 55Kg of 107-5000CPS, 10,000 CPS viscosity agents 385Kg, 1000# silicone oil 176Kg, active coarse whiting 50Kg, nano-sized carbon
Sour calcium 100Kg, aluminium hydroxide 150Kg, antimony oxide 240Kg, Nano carbon white 15Kg.
Further, the preferred implementation of agent prescription and preparation method is blocked in a kind of nanometer of moisture retardant of the present invention
Example in, described in this nanometer moisture retardant block agent prescription and preparation method it is as follows：
The first step throws into whole liquid charging stocks in reaction kettle, and active coarse whiting 50Kg, nano-calcium carbonate 100Kg is added, and booting is stirred
It mixes, stirring motor speed-frequency is adjusted to 40Hz, stirs 15 minutes, shuts down, scrapes paddle,
Third walks, plus nano white carbon 15Kg, and booting stirring 15 minutes, stirring motor speed-frequency is adjusted to 40Hz, shuts down, scrapes
Paddle,
4th step adds remaining solid raw material, booting stirring, stirring motor speed-frequency to be adjusted to 40Hz, stir 15 minutes, heating
To 100 DEG C, shuts down, scrapes paddle,
5th step closes equipment tight, and booting stirring is started simultaneously at and vacuumized, and is vacuumized and is not less than -0.09Mpa, timing 120 minutes,
Speed-frequency 35-40Hz,
This preparation is labeled as A preparations by the 5th step, sampling and testing, consistency 13.5-14cm.
Further, the preferred implementation of agent prescription and preparation method is blocked in a kind of nanometer of moisture retardant of the present invention
In example, described in a kind of nanometer of moisture retardant block agent prescription and preparation method, which is characterized in that by the A preparations and B
Preparation uses after being sufficiently mixed, using 40-60 minutes latter, Self-leveling diameter 17.5cm-18.5cm, if be not achieved, using urging
Agent is adjusted, and until its mixture Self-leveling diameter 17.5cm-18.5cm, is finally shut down, is scraped paddle, discharging, barrelling sale.
The technical problem to be solved in the present invention is：It is not numerous to provide a kind of formula, prepares simply, can be moisture-proof, insulation is received
Rice moisture retardant blocks agent prescription and preparation method.
Claims (6)
1. a kind of nanometer of moisture retardant of the present invention blocks agent prescription and preparation method, which is characterized in that by following weight calculate by
Following components is formulated：Viscosity agent 50-60Kg, 10000CPS the viscosity agent 380-390Kg, silicone oil 120- of 107-5000CPS
180Kg, active coarse whiting 45-55Kg, nano-calcium carbonate 90-110Kg, aluminium hydroxide 140-160Kg, antimony oxide 230-
250Kg, Nano carbon white 10-20Kg, JT-316A curing agent 160-180Kg, 550 coupling agent 15-16Kg, 560 coupling agent 4-
5Kg, 801 toughener 2-4Kg, dibutyl tin laurate 5-6Kg, catalyst 1-2Kg.
2. a kind of nanometer of moisture retardant according to claim 1 blocks agent prescription and preparation method, which is characterized in that described
This nanometer moisture retardant block agent prescription, calculate by following weight and be formulated by following components：Silicone oil 130Kg, JT-
316A curing agent 170Kg, 550 coupling agent 15.5Kg, 560 coupling agent 4.2Kg, 801 toughener 3Kg, dibutyl tin laurate
5.3Kg, catalyst 1-2Kg.
3. a kind of nanometer of moisture retardant according to claim 2 blocks agent prescription and preparation method, which is characterized in that described
This nanometer moisture retardant block agent prescription and preparation method it is as follows：
The first step checks whether equipment is clean,
Silicone oil 130Kg and JT-316A curing agent 170Kg is added into production equipment for second step, then booting stirring, stirring electricity
Machine speed-frequency is adjusted to 30-40Hz, while vacuumizing and reaching -0.09Mpa or more, timing 30 minutes,
Third walks, and after being mixed evenly, shuts down, releases vacuum, then 550 coupling agent 15.5Kg, 560 couplings are added into production equipment
Agent 4.2Kg, 801 toughener 3Kg, catalyst 1Kg, dibutyl tin laurate 5.3Kg, stirring motor speed-frequency are adjusted to
30-40Hz, while vacuumizing and reaching -0.09Mpa or more, timing 35 minutes,
4th step shuts down cooling and discharges, this preparation is labeled as B preparations.
4. a kind of nanometer of moisture retardant according to claim 1 blocks agent prescription and preparation method, which is characterized in that described
This nanometer moisture retardant block agent prescription, calculate by following weight and be formulated by following components：107-5000CPS's is viscous
Spend agent 55Kg, 10,000 CPS viscosity agents 385Kg, 1000# silicone oil 176Kg, active coarse whiting 50Kg, nano-calcium carbonate 100Kg, hydroxide
Aluminium 150Kg, antimony oxide 240Kg, Nano carbon white 15Kg.
5. a kind of nanometer of moisture retardant according to claim 4 blocks agent prescription and preparation method, which is characterized in that described
This nanometer moisture retardant block agent prescription and preparation method it is as follows：
The first step throws into whole liquid charging stocks in reaction kettle, and active coarse whiting 50Kg, nano-calcium carbonate 100Kg is added, and booting is stirred
It mixes, stirring motor speed-frequency is adjusted to 40Hz, stirs 15 minutes, shuts down, scrapes paddle,
Third walks, plus nano white carbon 15Kg, and booting stirring 15 minutes, stirring motor speed-frequency is adjusted to 40Hz, shuts down, scrapes
Paddle,
4th step adds remaining solid raw material, booting stirring, stirring motor speed-frequency to be adjusted to 40Hz, stir 15 minutes, heating
To 100 DEG C, shuts down, scrapes paddle,
5th step closes equipment tight, and booting stirring is started simultaneously at and vacuumized, and is vacuumized and is not less than -0.09Mpa, timing 120 minutes,
Speed-frequency 35-40Hz,
This preparation is labeled as A preparations by the 5th step, sampling and testing, consistency 13.5-14cm.
6. a kind of nanometer of moisture retardant according to claim 3 or 5 blocks agent prescription and preparation method, which is characterized in that
It is used after the A preparations and B preparations are sufficiently mixed, using 40-60 minutes latter, Self-leveling diameter 17.5cm-18.5cm, such as
Fruit is not achieved, and is adjusted using catalyst, until its mixture Self-leveling diameter 17.5cm-18.5cm, finally shuts down, scrapes
Paddle, discharging, barrelling are sold.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810433917.9A CN108504282A (en) | 2018-05-08 | 2018-05-08 | A kind of nanometer of moisture retardant blocks agent prescription and preparation method |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN201810433917.9A CN108504282A (en) | 2018-05-08 | 2018-05-08 | A kind of nanometer of moisture retardant blocks agent prescription and preparation method |
Publications (1)
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| CN108504282A true CN108504282A (en) | 2018-09-07 |
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Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104610905A (en) * | 2014-12-30 | 2015-05-13 | 福建瑞森化工有限公司 | High-voltage-insulation sealing adhesive |
| CN106497500A (en) * | 2016-11-02 | 2017-03-15 | 嘉善天胶装饰材料有限公司 | A kind of structure glue and preparation method thereof |
| CN106634798A (en) * | 2016-11-02 | 2017-05-10 | 嘉善天胶装饰材料有限公司 | Fireproof glue and manufacturing method thereof |
-
2018
- 2018-05-08 CN CN201810433917.9A patent/CN108504282A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104610905A (en) * | 2014-12-30 | 2015-05-13 | 福建瑞森化工有限公司 | High-voltage-insulation sealing adhesive |
| CN106497500A (en) * | 2016-11-02 | 2017-03-15 | 嘉善天胶装饰材料有限公司 | A kind of structure glue and preparation method thereof |
| CN106634798A (en) * | 2016-11-02 | 2017-05-10 | 嘉善天胶装饰材料有限公司 | Fireproof glue and manufacturing method thereof |
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