CN108444989A - A kind of honey authenticity and quality appraisal detection method - Google Patents

A kind of honey authenticity and quality appraisal detection method Download PDF

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Publication number
CN108444989A
CN108444989A CN201810092731.1A CN201810092731A CN108444989A CN 108444989 A CN108444989 A CN 108444989A CN 201810092731 A CN201810092731 A CN 201810092731A CN 108444989 A CN108444989 A CN 108444989A
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China
Prior art keywords
honey
test tube
added
luster
observation
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CN201810092731.1A
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Chinese (zh)
Inventor
汪昌宏
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Anhui Hongshun Source Biotechnology Co Ltd
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Anhui Hongshun Source Biotechnology Co Ltd
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Priority to CN201810092731.1A priority Critical patent/CN108444989A/en
Publication of CN108444989A publication Critical patent/CN108444989A/en
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    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N21/00—Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
    • G01N21/75—Systems in which material is subjected to a chemical reaction, the progress or the result of the reaction being investigated
    • G01N21/77—Systems in which material is subjected to a chemical reaction, the progress or the result of the reaction being investigated by observing the effect on a chemical indicator
    • G01N21/78—Systems in which material is subjected to a chemical reaction, the progress or the result of the reaction being investigated by observing the effect on a chemical indicator producing a change of colour
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N21/00—Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
    • G01N21/75—Systems in which material is subjected to a chemical reaction, the progress or the result of the reaction being investigated
    • G01N21/77—Systems in which material is subjected to a chemical reaction, the progress or the result of the reaction being investigated by observing the effect on a chemical indicator
    • G01N21/82—Systems in which material is subjected to a chemical reaction, the progress or the result of the reaction being investigated by observing the effect on a chemical indicator producing a precipitate or turbidity
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N21/00—Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
    • G01N21/75—Systems in which material is subjected to a chemical reaction, the progress or the result of the reaction being investigated
    • G01N21/77—Systems in which material is subjected to a chemical reaction, the progress or the result of the reaction being investigated by observing the effect on a chemical indicator
    • G01N21/78—Systems in which material is subjected to a chemical reaction, the progress or the result of the reaction being investigated by observing the effect on a chemical indicator producing a change of colour
    • G01N2021/786—Systems in which material is subjected to a chemical reaction, the progress or the result of the reaction being investigated by observing the effect on a chemical indicator producing a change of colour with auxiliary heating for reaction

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  • Physics & Mathematics (AREA)
  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Plasma & Fusion (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Investigating Or Analysing Materials By The Use Of Chemical Reactions (AREA)

Abstract

The invention discloses a kind of honey authenticity and quality appraisal detection method, specific detecting step is as follows：It takes the honey of 3 5g samples to be put into test tube, 30 40 DEG C of heating is carried out to test tube, observes honey crystallization state in test tube；0.2 0.4 milliliters of iodine solutions are instilled into test tube, and test tube is carried out to rock observation；3 5g pure water are added into test tube again, after shaking test tube makes honey component dissolve, it is 1 that proportion, which is added,:The alcohol of 5 95% concentration, rocks observation again；Separately take a step 1）The honey of 3 5g samples instill 0.3 0.5 milliliters of AgNO after the water dilution of 4 times of equivalent is added3Solution carries out rocking observation；The quality of honey distinguishes：Distinguish that sample honey generates suspended matter color and luster, the redder color and luster the better, otherwise the lighter color and luster the poorer.Technical scheme of the present invention, by the way that iodine solution, alcohol, AgNO are added in sample honey3Solution observes honey state, distinguishing whether mix sucrose, starch, maltose, salt in honey, detects the true and false and quality method is simple, easy to operation.

Description

A kind of honey authenticity and quality appraisal detection method
Technical field
The present invention relates to the technical field of honey identification more particularly to a kind of honey authenticities and quality appraisal detection method.
Background technology
China is honey big export country in the world, containing sucrose, starch, maltose, salt in honey inferior, causes market true False honey difficulty distinguishes, price is made to be difficult to be improved, to increase beekeeper's bee-keeping cost.Existing honey doping content detection side Method can distinguish honey authenticity by inspection laboratory or human body sense organ, and lab test procedures are complicated, time-consuming, efficiency is low, Of high cost, TLC machine of the especially stealthy syrup in general laboratory is difficult to test out.And by human body sense organ then need through Abundant people is tested to distinguish, to increase discrimination difficulty, for this purpose, it is proposed that a kind of honey authenticity and quality identification detection side Method.
Invention content
To solve the defect of prior art, the invention discloses a kind of honey authenticity and quality appraisal detection methods.
The invention discloses a kind of honey authenticity and quality appraisal detection method, specific detecting step is as follows：
1）It takes the honey of 3-5g samples to be put into test tube, 30-40 DEG C of heating is carried out to test tube, observes honey crystallization shape in test tube State, if mixing sucrose in honey, crystallized honey surface plate is binded up one's hair firmly, is often formed lump after heated and is sunk to bottom；
2）0.2-0.4 milliliters of iodine solutions are instilled into test tube, and test tube is carried out to rock observation, if there is blue, red, green three's face Color can detect in honey sample and mix starch；
3）3-5g pure water is added into test tube again, after shaking test tube makes honey component dissolve, it is 1 that proportion, which is added,:5 95% concentration Alcohol, rock observation again, if there is milky white color substance, illustrate to mix maltose in sample honey；
4）Separately take a step 1）The honey of 3-5g samples instill 0.3-0.5 milliliters after the water dilution of 4 times of equivalent is added AgNO3Solution carries out rocking observation, illustrates to mix salt in sample honey if finding white precipitate；
5）The quality of honey distinguishes：Distinguish sample honey generate suspended matter color and luster, the redder color and luster the better, on the contrary color and luster it is more light more Difference.
Advantageous effect is：By the way that iodine solution, alcohol, AgNO are added in sample honey3Solution observes honey state, distinguishing Sucrose, starch, maltose, salt whether are mixed in other honey, detect the true and false and quality method is simple, it is easy to operation.
Specific implementation mode
Embodiment 1
The invention discloses a kind of honey authenticity and quality appraisal detection method, specific detecting step is as follows：
1）It takes the honey of 3g samples to be put into test tube, 30 DEG C of heating is carried out to test tube, honey crystallization state in test tube is observed, if bee Sucrose is mixed in honey, crystallized honey surface plate is binded up one's hair firmly, is often formed lump after heated and is sunk to bottom；
2）0.2 milliliter of iodine solution is instilled into test tube, and test tube is carried out to rock observation, it, can if there is blue, red, green three's color Starch is mixed to detect in honey sample；
3）3g pure water is added into test tube again, after shaking test tube makes honey component dissolve, it is 1 that proportion, which is added,:5 95% concentration Alcohol rocks observation again, if there is milky white color substance, illustrates to mix maltose in sample honey；
4）Separately take a step 1）The honey of 3g samples instill 0.3 milliliter of AgNO after the water dilution of 4 times of equivalent is added3It is molten Liquid carries out rocking observation, illustrates to mix salt in sample honey if finding white precipitate；
5）The quality of honey distinguishes：Distinguish sample honey generate suspended matter color and luster, the redder color and luster the better, on the contrary color and luster it is more light more Difference.
Embodiment 2
The invention discloses a kind of honey authenticity and quality appraisal detection method, specific detecting step is as follows：
1）It takes the honey of 4g samples to be put into test tube, 35 DEG C of heating is carried out to test tube, honey crystallization state in test tube is observed, if bee Sucrose is mixed in honey, crystallized honey surface plate is binded up one's hair firmly, is often formed lump after heated and is sunk to bottom；
2）0.3 milliliter of iodine solution is instilled into test tube, and test tube is carried out to rock observation, it, can if there is blue, red, green three's color Starch is mixed to detect in honey sample；
3）4g pure water is added into test tube again, after shaking test tube makes honey component dissolve, it is 1 that proportion, which is added,:5 95% concentration Alcohol rocks observation again, if there is milky white color substance, illustrates to mix maltose in sample honey；
4）Separately take a step 1）The honey of 4g samples instill 0.4 milliliter of AgNO after the water dilution of 4 times of equivalent is added3It is molten Liquid carries out rocking observation, illustrates to mix salt in sample honey if finding white precipitate；
5）The quality of honey distinguishes：Distinguish sample honey generate suspended matter color and luster, the redder color and luster the better, on the contrary color and luster it is more light more Difference.
Embodiment 3
The invention discloses a kind of honey authenticity and quality appraisal detection method, specific detecting step is as follows：
1）It takes the honey of 5g samples to be put into test tube, 40 DEG C of heating is carried out to test tube, honey crystallization state in test tube is observed, if bee Sucrose is mixed in honey, crystallized honey surface plate is binded up one's hair firmly, is often formed lump after heated and is sunk to bottom；
2）0.4 milliliter of iodine solution is instilled into test tube, and test tube is carried out to rock observation, it, can if there is blue, red, green three's color Starch is mixed to detect in honey sample；
3）5g pure water is added into test tube again, after shaking test tube makes honey component dissolve, it is 1 that proportion, which is added,:5 95% concentration Alcohol rocks observation again, if there is milky white color substance, illustrates to mix maltose in sample honey；
4）Separately take a step 1）The honey of 5g samples instill 0.5 milliliter of AgNO after the water dilution of 4 times of equivalent is added3It is molten Liquid carries out rocking observation, illustrates to mix salt in sample honey if finding white precipitate；
5）The quality of honey distinguishes：Distinguish sample honey generate suspended matter color and luster, the redder color and luster the better, on the contrary color and luster it is more light more Difference.
Finally it should be noted that：Above example is only to illustrate the present invention and not limits technology described in the invention Scheme；Therefore, although this specification with reference to above-mentioned each embodiment to present invention has been detailed description, this Field it is to be appreciated by one skilled in the art that still can modify to the present invention or equivalent replacement；And all do not depart from this The technical solution of the spirit and scope of invention and its improvement should all be covered in scope of the presently claimed invention.

Claims (1)

1. a kind of honey authenticity and quality appraisal detection method, which is characterized in that its specific detecting step is as follows：
It takes the honey of 3-5g samples to be put into test tube, 30-40 DEG C of heating is carried out to test tube, observes honey crystallization state in test tube；
0.2-0.4 milliliters of iodine solutions are instilled into test tube, and test tube is carried out to rock observation；
3-5g pure water is added into test tube again, after shaking test tube makes honey component dissolve, it is 1 that proportion, which is added,:5 95% concentration Alcohol rocks observation again；
Separately take a step 1）The honey of 3-5g samples instill 0.3-0.5 milliliters of AgNO after the water dilution of 4 times of equivalent is added3 Solution carries out rocking observation；
The quality of honey distinguishes：Distinguish that sample honey generates suspended matter color and luster, the redder color and luster the better, otherwise the lighter color and luster the poorer.
CN201810092731.1A 2018-01-31 2018-01-31 A kind of honey authenticity and quality appraisal detection method Pending CN108444989A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201810092731.1A CN108444989A (en) 2018-01-31 2018-01-31 A kind of honey authenticity and quality appraisal detection method

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CN201810092731.1A CN108444989A (en) 2018-01-31 2018-01-31 A kind of honey authenticity and quality appraisal detection method

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CN108444989A true CN108444989A (en) 2018-08-24

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Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN86100651A (en) * 1986-01-20 1986-10-01 李高增 The fast simple method of testing of honey authenticity
CN101871875A (en) * 2010-06-02 2010-10-27 何庆生 Honey authenticity and quality appraisal detection method
KR20120124654A (en) * 2011-05-04 2012-11-14 대한민국(농촌진흥청장) Analysis of the purity of honey, using pollen mixed in honey

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN86100651A (en) * 1986-01-20 1986-10-01 李高增 The fast simple method of testing of honey authenticity
CN101871875A (en) * 2010-06-02 2010-10-27 何庆生 Honey authenticity and quality appraisal detection method
KR20120124654A (en) * 2011-05-04 2012-11-14 대한민국(농촌진흥청장) Analysis of the purity of honey, using pollen mixed in honey

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