CN108434013A - A kind of hair dye and preparation method thereof for making hair generate candy strip - Google Patents
A kind of hair dye and preparation method thereof for making hair generate candy strip Download PDFInfo
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- CN108434013A CN108434013A CN201810376360.XA CN201810376360A CN108434013A CN 108434013 A CN108434013 A CN 108434013A CN 201810376360 A CN201810376360 A CN 201810376360A CN 108434013 A CN108434013 A CN 108434013A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/29—Titanium; Compounds thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/41—Amines
- A61K8/415—Aminophenols
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/46—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing sulfur
- A61K8/463—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing sulfur containing sulfuric acid derivatives, e.g. sodium lauryl sulfate
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/10—Preparations for permanently dyeing the hair
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
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Abstract
The invention discloses a kind of hair dye for making hair generate candy strip, the mass percent of raw material and each raw material contained by the hair dye is：Propylene glycol 5~30%, cyclohexane 3~35%, isopropanol 6~28%, sodium perborate 1~2%, p-phenylenediamine sulfate 0.5~2%, resorcinol 0.1~0.8%, titanium oxide 1~50%, benzoic ether guar gum 0.5~10%, sodium glutamate 0.5~28%, sodium lauroyl sarcosine 0.01~2%.The present invention may be implemented in commonly hair dyeing program, obtain the effect of striated hair.It is time saving and energy saving, overcome manually-operated uncertainty.
Description
Technical field
The present invention relates to daily-use chemical industry technical fields, more particularly, to a kind of hair dyeing that hair can be dyed to candy strip
Agent and preparation method thereof.
Background technology
As people’s lives level is continuously improved, more and more people start to focus on the image of itself, hair dye industry
It is rapidly developed.Currently, hair dye is mostly oxidative hair dyes.Oxidative hair dyes include dyestuff intermediate, couplant,
Coordinate oxidant when dyeing, dyestuff intermediate and couplant penetrate into hair cortex, occur oxidation, coupling and condensation reaction formed compared with
Big dye molecule, is closed in hair fiber and is not easily removed, and achievees the purpose that have hair dyed for a long time.
But with individualized development, to the pursuit increasingly fashion of hair dyeing effect.The hair dyeing of striated is also fashion
A kind of mark.It is now to realize the hair dyeing of striated, needs colorist to carry out time sharing segment processing to hair, take time and effort.
Invention content
In view of the above-mentioned problems existing in the prior art, hair is made to generate candy strip the applicant provides a kind of
Hair dye and preparation method thereof.The present invention may be implemented in commonly hair dyeing program, obtain the effect of striated hair.Time saving province
Power overcomes manually-operated uncertainty.
Technical scheme is as follows：
A kind of hair dye for making hair generate candy strip, the mass percent of raw material and each raw material contained by the hair dye
For：
The grain size of each raw material of hair dye is 60~120 mesh.
A kind of preparation method of the hair dye, the preparation method include the following steps：
(1) by 0.5~2% p-phenylenediamine sulfate, 0.1~0.8% resorcinol, 1~50% titanium oxide, 0.5~
10% benzoic ether guar gum, 0.5~28% sodium glutamate, the mixing of 0.01~2% sodium lauroyl sarcosine, it is crushed to 80~
120 mesh；
(2) 1~2% sodium perborate is crushed to 60-80 mesh, be added in premix made from step (1), it is 7 to adjust pH
~10.5；
(3) by step (2) handle mixed material in be added 5~30% propylene glycol, 3~35% cyclohexanes, 6~
28% isopropanol is uniformly mixed；
(4) it is placed on the vial of logical nitrogen, 40 DEG C is heated to and is kept for 24 hours, being made described makes hair generate candy strip
Hair dye；Each raw material is calculated in mass percent.
In the step (3) in propylene glycol, cyclohexane, the total amount of isopropanol and hair dye other solid components solid-to-liquid ratio
It is 0.5~1.5.
The p-phenylenediamine sulfate compounds with 5- amino o-cresols, can obtain the hair dye of purple fringe.
The benzoic ether guar gum can also be substituted with sodium alginate.
The present invention is beneficial to be had technical effect that：
Typically hair dye is water-soluble, and due to the relationship of hydrogen bond, dyestuff is distributed relatively uniform on hair, can obtain
Uniform color.This hair dye uses oil-phase medium, and point of the polar substances in oil phase is adjusted with amino acid surfactant
Cloth.According to the proportioning of oil phase, the position that dyestuff intermediate enters hair can be adjusted, it is certain pretend with point dyestuff intermediate into
The concentration for entering hair is big, in other sites dyestuff intermediate enter hair concentration it is small, therefore the dye of striated can be obtained
Send out effect.
When hair dye hair dyeing of the present invention, to maintain each substance in specific particle size range, diffusion control could be eliminated
Influence, the striated hair dyeing effect needed.In hair dye, to keep water-less environment, a small amount of water that will promote dyestuff
Intermediate is uniformly distributed in hair, cannot get the effect of striped.
Specific implementation mode
With reference to embodiment, the present invention is specifically described.
Embodiment 1
A kind of preparation method of the hair dye, the preparation method include the following steps：
(1) by 2% p-phenylenediamine sulfate, 0.5% resorcinol, 1% titanium oxide, 0.5% benzoic ether guar gum,
18% sodium glutamate, the mixing of 1% sodium lauroyl sarcosine, are crushed to 80~120 mesh；
(2) 2% sodium perborate is crushed to 60-80 mesh, be added in premix made from step (1), it is 7.5 to adjust pH；
(3) 20% propylene glycol, 35% cyclohexane, 20% isopropanol is added in the mixed material handled by step (2),
It is uniformly mixed；
(4) it is placed on the vial of logical nitrogen, 40 DEG C is heated to and is kept for 24 hours, being made described makes hair generate candy strip
Hair dye.(each raw material is calculated in mass percent)
Embodiment 2
A kind of preparation method of the hair dye, the preparation method include the following steps：
(1) by 1.5% p-phenylenediamine sulfate, 0.1% resorcinol, 25% titanium oxide, 5% benzoic ether guar gum,
28% sodium glutamate, the mixing of 2% sodium lauroyl sarcosine, are crushed to 80~120 mesh；
(2) 1% sodium perborate is crushed to 60-80 mesh, be added in premix made from step (1), adjusting pH is
10.5；
(3) 30% propylene glycol, 3% cyclohexane, 28% isopropanol is added in the mixed material handled by step (2),
It is uniformly mixed；
(4) it is placed on the vial of logical nitrogen, 40 DEG C is heated to and is kept for 24 hours, being made described makes hair generate candy strip
Hair dye.(each raw material is calculated in mass percent)
Embodiment 3
A kind of preparation method of the hair dye, the preparation method include the following steps：
(1) by 0.5% p-phenylenediamine sulfate, 0.8% resorcinol, 50% titanium oxide, 10% benzoic ether guar gum,
0.5% sodium glutamate, the mixing of 0.2% sodium lauroyl sarcosine, are crushed to 80~120 mesh；
(2) 2% sodium perborate is crushed to 60-80 mesh, be added in premix made from step (1), it is 8.5 to adjust pH；
(3) 5% propylene glycol, 25% cyclohexane, 6% isopropanol is added in the mixed material handled by step (2), mixes
It closes uniform；
(4) it is placed on the vial of logical nitrogen, 40 DEG C is heated to and is kept for 24 hours, being made described makes hair generate candy strip
Hair dye.(each raw material is calculated in mass percent)
Embodiment 4
A kind of preparation method of the hair dye, the preparation method include the following steps：
(1) by 1.6% p-phenylenediamine sulfate, 0.4%5- amino o-cresol, 0.5% resorcinol, 1% titanium oxide,
0.5% benzoic ether guar gum, 18% sodium glutamate, the mixing of 1% sodium lauroyl sarcosine, are crushed to 80~120 mesh；
(2) 2% sodium perborate is crushed to 60-80 mesh, be added in premix made from step (1), it is 7.5 to adjust pH；
(3) 20% propylene glycol, 35% cyclohexane, 20% isopropanol is added in the mixed material handled by step (2),
It is uniformly mixed；
(4) it is placed on the vial of logical nitrogen, 40 DEG C is heated to and is kept for 24 hours, being made described makes hair generate candy strip
Hair dye.(each raw material is calculated in mass percent)
Embodiment 5
A kind of preparation method of the hair dye, the preparation method include the following steps：
(1) by 1.5% p-phenylenediamine sulfate, 0.1% resorcinol, 25% titanium oxide, 5% sodium alginate, 28% paddy
Propylhomoserin sodium, the mixing of 2% sodium lauroyl sarcosine, are crushed to 80~120 mesh；
(2) 1% sodium perborate is crushed to 60-80 mesh, be added in premix made from step (1), adjusting pH is
10.5；
(3) 30% propylene glycol, 3% cyclohexane, 28% isopropanol is added in the mixed material handled by step (2),
It is uniformly mixed；
(4) it is placed on the vial of logical nitrogen, 40 DEG C is heated to and is kept for 24 hours, being made described makes hair generate candy strip
Hair dye.(each raw material is calculated in mass percent)
Test case：
By 1~3 gained hair dye of the embodiment of the present invention, it is evenly coated on the hair of white that (holding head is issued on without watery
State), 30min is kept at room temperature, and hair is washed totally later, obtains the chequered with black and white hair of striated；By 4 gained of embodiment
Hair dye, for have hair dyed after, obtain the alternate striped of black purple；It carries out testing water-fastness, light shine for the hair applied after contaminating
Performance, test result is as shown in table 1：
Table 1
| Project | It is water-fastness/15 times | Fluorescent lamp photograph/100h | Ultraviolet lamp photograph/100h |
| Embodiment 1 | ΔE<4% | ΔE<3% | ΔE<5% |
| Embodiment 2 | ΔE<5% | ΔE<3% | ΔE<5% |
| Embodiment 3 | ΔE<5% | ΔE<4% | ΔE<4% |
| Embodiment 4 | ΔE<4% | ΔE<4% | ΔE<4% |
Note：Illumination test uses the international standard light source VERIVIDE COLOR ASSESMENT CABINET of Mei Si light sources Science and Technology Ltd. of Shenzhen.
Claims (6)
1. a kind of hair dye for making hair generate candy strip, which is characterized in that raw material and each raw material contained by the hair dye
Mass percent is：
2. hair dye according to claim 1, which is characterized in that the grain size of each raw material of hair dye is 60~120 mesh.
3. the preparation method of hair dye described in a kind of claim 1, which is characterized in that the preparation method includes the following steps：
(1) by 0.5~2% p-phenylenediamine sulfate, 0.1~0.8% resorcinol, 1~50% titanium oxide, 0.5~10% benzene
Formic acid esters guar gum, 0.5~28% sodium glutamate, the mixing of 0.01~2% sodium lauroyl sarcosine, are crushed to 80~120 mesh；
(2) 1~2% sodium perborate is crushed to 60-80 mesh, is added in premix made from step (1), adjust pH be 7~
10.5；
(3) 5~30% propylene glycol, 3~35% cyclohexanes, 6~28% different are added in the mixed material handled by step (2)
Propyl alcohol is uniformly mixed；
(4) it is placed on the vial of logical nitrogen, 40 DEG C is heated to and is kept for 24 hours, the dye for making hair generate candy strip is made
Send out agent；Each raw material is calculated in mass percent.
4. preparation method according to claim 3, which is characterized in that propylene glycol, cyclohexane, isopropyl in the step (3)
The solid-to-liquid ratio of other solid components is 0.5~1.5 in the total amount and hair dye of alcohol.
5. hair dye according to claim 1, which is characterized in that the p-phenylenediamine sulfate is multiple with 5- amino o-cresols
Match, the hair dye of purple fringe can be obtained.
6. hair dye according to claim 1, which is characterized in that the benzoic ether guar gum can also use sodium alginate
It substitutes.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810376360.XA CN108434013A (en) | 2018-04-25 | 2018-04-25 | A kind of hair dye and preparation method thereof for making hair generate candy strip |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810376360.XA CN108434013A (en) | 2018-04-25 | 2018-04-25 | A kind of hair dye and preparation method thereof for making hair generate candy strip |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN108434013A true CN108434013A (en) | 2018-08-24 |
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ID=63201559
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201810376360.XA Pending CN108434013A (en) | 2018-04-25 | 2018-04-25 | A kind of hair dye and preparation method thereof for making hair generate candy strip |
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| Country | Link |
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Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN85105089A (en) * | 1985-06-27 | 1986-12-24 | 徐自强 | Hair dye |
| JP2003070524A (en) * | 2001-09-06 | 2003-03-11 | Wataru Wakimoto | Method for dyeing hair in stripe and tool for the same |
| CN103957877A (en) * | 2011-11-24 | 2014-07-30 | 株式会社爱茉莉太平洋 | Foam-type hair dye composition for improving hair softness without dripping |
-
2018
- 2018-04-25 CN CN201810376360.XA patent/CN108434013A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN85105089A (en) * | 1985-06-27 | 1986-12-24 | 徐自强 | Hair dye |
| JP2003070524A (en) * | 2001-09-06 | 2003-03-11 | Wataru Wakimoto | Method for dyeing hair in stripe and tool for the same |
| CN103957877A (en) * | 2011-11-24 | 2014-07-30 | 株式会社爱茉莉太平洋 | Foam-type hair dye composition for improving hair softness without dripping |
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Application publication date: 20180824 |