CN108425261A - Steam explosion pulping equipment - Google Patents

Steam explosion pulping equipment Download PDF

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Publication number
CN108425261A
CN108425261A CN201710081715.8A CN201710081715A CN108425261A CN 108425261 A CN108425261 A CN 108425261A CN 201710081715 A CN201710081715 A CN 201710081715A CN 108425261 A CN108425261 A CN 108425261A
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CN
China
Prior art keywords
chimney
dust
cavity charge
warehouse
charge containers
Prior art date
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Pending
Application number
CN201710081715.8A
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Chinese (zh)
Inventor
梁志鹏
淡贵添
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Guangxi Glory Technology Co Ltd
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Guangxi Glory Technology Co Ltd
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Application filed by Guangxi Glory Technology Co Ltd filed Critical Guangxi Glory Technology Co Ltd
Priority to CN201710081715.8A priority Critical patent/CN108425261A/en
Publication of CN108425261A publication Critical patent/CN108425261A/en
Pending legal-status Critical Current

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Classifications

    • DTEXTILES; PAPER
    • D21PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21BFIBROUS RAW MATERIALS OR THEIR MECHANICAL TREATMENT
    • D21B1/00Fibrous raw materials or their mechanical treatment
    • D21B1/04Fibrous raw materials or their mechanical treatment by dividing raw materials into small particles, e.g. fibres
    • D21B1/12Fibrous raw materials or their mechanical treatment by dividing raw materials into small particles, e.g. fibres by wet methods, by the use of steam
    • D21B1/30Defibrating by other means
    • D21B1/36Explosive disintegration by sudden pressure reduction

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  • Engineering & Computer Science (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Wood Science & Technology (AREA)
  • Mechanical Engineering (AREA)
  • Processing Of Solid Wastes (AREA)

Abstract

The present invention relates to machinery equipment field, specially a kind of steam explosion pulping equipment, including vacuum pump, negative pressure drain tank and cavity charge containers, one end of the negative pressure drain tank is connect with vacuum pump, the discharge port of the negative pressure drain tank and the feed inlet of cavity charge containers connect, the top of the cavity charge containers is additionally provided with chimney device, the discharging port of the cavity charge containers is connected with slurries collecting tank, the top of the chimney device is connected with dust discharge tube, the dust discharge tube is connected with dust collecting box, the lower part of chimney device is also associated with sewage conduct, the sewage conduct is connected with dirty water collecting tank, with simple in structure, crushing efficiency is high;The features such as quality of production is stablized, environmentally-friendly sanitary.

Description

Steam explosion pulping equipment
Technical field
The present invention relates to machinery equipment field, specifically a kind of steam explosion pulping equipment.
Background technology
Lignin is to pass through ehter bond by benzene oxide unit(-O-)With carbon key(C-C)What is be formed by connecting has natural aromatic High-molecular compound.In plant fiber, content of lignin is only second to cellulose and hemicellulose, is the third-largest natural organic Object accounts for about 5-30%.The mankind are with a history of thousands of years to the research of cellulose, but are from 1930 to the research of lignin Year starts, and develops slower.Wooden to be known as good dispersibility, anti-flammability, solvent-resisting, thermal stability, molecule has more Kind active function groups(Aromatic radical, phenolic hydroxyl group, alcoholic extract hydroxyl group, carbonyl, methoxyl group, carboxyl and conjugated double bond etc.), in modern industry There is higher utility value;Current good lignin has been widely used, and developed lignin product is up to more than 200 in the world Kind.
In China, bagasse is a kind of important agricultural product waste resource, and bagasse is that a kind of agricultural product of sugaring are discarded Object often produces the bagasse that one ton of sucrose just will produce about one ton.Particularly developed countries of more and more country The trans-utilization of the renewable resources such as agricultural product castoff is included in the grand strategy of Sustainable Socioeconomic Development, and agricultural product are discarded Biomass efficiently uses, and has become one of the emphasis of mankind nowadays sustainable development.Contain a large amount of fiber in bagasse The natural high molecular substances such as element, lignin, hemicellulose.These bagasses in addition to being used for papermaking on a small quantity, burnt by the overwhelming majority at present Fall or discard, not only wastes resources, but also seriously pollutes the environment.Therefore, if can be isolated from bagasse good Lignin is applied to industrial production, it will generates huge economic benefit and ecological benefits.The separating lignin in bagasse needs It to be first processed into the fiber of sugarcane flocculence more fine crushing to bagasse and the slurry of liquid-type, traditional method is made Mechanical crushing method and chemical treatment are usually used, however, mechanical crushing method is difficult to cell being effectively crushed, causes extraction efficiency It is low;And chemical disruption methods easily cause the change of extract structure and activity reduces or inactivation, and secondary dirt can be generated to environment Dye, it is often more important that inside plant tissues fail thoroughly to be crushed.Therefore, how by bagasse explosion at the sugarcane of flocculence Slurry material, with obtain can from bagasse slurry extraction efficiency higher, the equipment and technology of the lignin of better quality, be one urgently Technical barrier to be solved.
Invention content
The purpose of the present invention is to provide it is a kind of by bagasse explosion at the bagasse slurry of flocculence structure is simple, matter Stable steam explosion pulping equipment is measured, the production cost of the separating lignin from bagasse is reduced, to solve above-mentioned background skill The problem of being proposed in art.
To achieve the above object, the present invention provides the following technical solutions:
This steam explosion pulping equipment, it is characterised in that:Including vacuum pump, negative pressure drain tank and cavity charge containers, the negative pressure emptying One end of tank is connect with vacuum pump, and the discharge port of the negative pressure drain tank and the feed inlet of cavity charge containers connect, the cavity charge containers Top is additionally provided with chimney device, and the discharging port of the cavity charge containers is connected with slurries collecting tank, and the top of the chimney device connects It is connected to dust discharge tube, the dust discharge tube is connected with dust collecting box, and the lower part of chimney device is also associated with sewage conduct, The sewage conduct is connected with dirty water collecting tank.
Cavity charge containers described above include tank body, feed inlet and slurries delivery outlet, and the feed inlet is set to the top of tank body, into Material mouth inlet is equipped with blow-off valve, and the slurries delivery outlet is equipped with slurries conveyance conduit.
Chimney device described above includes water injector, chimney warehouse, Funnel Cover, dust emission mouth and discharge of wastewater mouth, Water injector is provided in the chimney warehouse, chimney warehouse side is additionally provided with dust emission mouth, pacifies at the top of chimney warehouse It is equipped with discharge of wastewater mouth equipped with Funnel Cover winged outside dust, the bottom of chimney warehouse is prevented.
It is the downward hemispherical shape structure of recess at the top of above-described Funnel Cover.
Compared with prior art, the beneficial effects of the invention are as follows:
1. simple in structure, crushing efficiency is high.The present invention uses steam explosion technology, that is, the explosion for applying steam ejection principle to realize Process carries out a kind of pretreated equipment to bagasse, this equipment will infilter the steam molecule instantaneous relase of bagasse organization internal Finish, internal steam work is made to be converted into mechanical energy and act on bagasse histocyte interlayer, to less energy by sugarcane Slag thoroughly decomposes.Due to not only avoiding chemically treated secondary pollution problem, but also solve that current biological treatment efficiency is low to be lacked Fall into, so the present invention carries out steam blasting using negative pressure drain tank and cavity charge containers to bagasse, substantially increase broken speed and Recovery rate reduces the production cost of lignin, has easy to operate, and low energy consumption, and the broken production efficiency of this equipment is than tradition Mechanical crushing method efficiency improve three times or more.
2. stable quality, environmentally-friendly sanitary.The steam explosion pulping equipment of the present invention is equipped with chimney device on cavity charge containers, The top of the chimney device is connected with dust discharge tube, effectively can fully lead to the dust generated in crushing process in time The delivery pipe for crossing dust emission mouth and connection that chimney warehouse is equipped with is discharged into dust collecting box;In addition, in chimney warehouse inner cavity It is additionally provided with water injector, it is timely that the dust generated in production is drenched to the discharge of wastewater mouth being equipped with by the bottom of chimney warehouse The waste water of generation is discharged into dirty water collecting tank from sewage conduct;In addition, being equipped with the downward hemisphere of recess at the top of chimney warehouse The Funnel Cover of shape and structure well prevents dust and flies upward outward.This equipment is not only suitble to bagasse explosion into flocculence Bagasse slurry can be also suitably used for biological medicine, food with obtaining from bagasse slurry extraction efficiency higher crushing technology Product, the breaking method of the various solid-liquids such as fine chemistry industry, this equipment not will produce secondary pollution compared with traditional chemical processing, right The protection of environment plays a good role.
Description of the drawings
Fig. 1 is the front view structure simplified schematic diagram of the present invention.
Fig. 2 is the front view structure simplified schematic diagram of cavity charge containers 5.
Part name and serial number in figure:
Vacuum pump 1, feedstock transportation pipeline 2, negative pressure drain tank 3, blow-off pipe 4, cavity charge containers 5, blow-off valve 6, chimney device 7, dust Delivery pipe 8, slurries conveyance conduit 9, slurries collecting tank 10, sewage conduct 11, dirty water collecting tank 12, dust collecting box 13, tank body 14, feed inlet 15, water injector 16, chimney storehouse 17, Funnel Cover 18, dust emission mouth 19, discharge of wastewater mouth 20, slurries delivery outlet 21。
Specific implementation mode
Following will be combined with the drawings in the embodiments of the present invention, and technical solution in the embodiment of the present invention carries out clear, complete Site preparation describes, it is clear that described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.It is based on Embodiment in the present invention, it is obtained by those of ordinary skill in the art without making creative efforts every other Embodiment shall fall within the protection scope of the present invention.
Shown in Fig. 1 and Fig. 2, the present invention provides a kind of technical solution:
This steam explosion pulping equipment, including vacuum pump 1, feedstock transportation pipeline 2, negative pressure drain tank 3, blow-off pipe 4, cavity charge containers 5, Blow-off valve 6, chimney device 7, dust discharge tube 8, slurries conveyance conduit 9, slurries collecting tank 10, sewage conduct 11, sewage collecting Case 12, dust collecting box 13, tank body 14, feed inlet 15, water injector 16, chimney storehouse 17, Funnel Cover 18, dust emission mouth 19, One end of discharge of wastewater mouth 20 and slurries delivery outlet 21, the negative pressure drain tank 3 is connected by feedstock transportation pipeline 2 and vacuum pump 1 It connects, the discharge port of the negative pressure drain tank 3 is connect by blow-off pipe 4 with the feed inlet of cavity charge containers 5, the top of the cavity charge containers 5 It is additionally provided with chimney device 7, the discharge port end of the cavity charge containers 5 is connected with slurries collecting tank 10, and the top of the chimney device 7 connects It is connected to dust discharge tube 8, the dust discharge tube 8 is connected with dust collecting box 13, and the lower part of chimney device 7 is also associated with sewage Pipeline 11, the sewage conduct 11 are connected with dirty water collecting tank 12(Shown in Fig. 1);
The cavity charge containers 5 include tank body 14, feed inlet 15 and slurries delivery outlet 21, and the feed inlet 15 is set to the upper of tank body 14 Portion, 15 inlet of feed inlet are equipped with blow-off valve 6, and the slurries delivery outlet 21 is equipped with slurries conveyance conduit 9;The chimney device 7 Including water injector 16, chimney warehouse 17, Funnel Cover 18, dust emission mouth 19 and discharge of wastewater mouth 20, the chimney warehouse 17 It is inside provided with water injector 16,17 side of chimney warehouse is additionally provided with dust emission mouth 19, and the bottom of chimney warehouse 17 is equipped with waste water Floss hole 20, the top of chimney warehouse 17 are also equipped with the Funnel Cover 18 of the downward hemispherical shape structure of recess so that production The dust that process generates falls into the bottom of chimney warehouse 17 and is discharged into dirty water collecting tank in time from discharge of wastewater mouth 20 in time 12, secondary pollution will not be generated to environment(Shown in Fig. 2).
The operation principle of the present invention is that:
This equipment is to use steam blasting i.e. steam explosion(Steam Explosion), it is the explosion realized using steam ejection principle Process carries out pretreated technology to bagasse.This equipment be will infilter bagasse organization internal steam molecule instantaneous relase it is complete Finish, so that internal steam work is converted into mechanical energy and act on bagasse histocyte interlayer, the fiber in plant cell is lignin It bonds, under high temperature, high steam effect, cellulose crystallity improves, and the degree of polymerization declines, hemicellulose fraction degradation, wood Quality softens, and lateral strength of connection declines, or even softening is plastic, when the material sudden pressure reduction full of steam, in hole Gas play expansion, generate " explosion " effect, can be partially stripped lignin, and be fiber fines by raw material tearing.Present device Steam blasting can play the role of following several respects:First, the effect of class acidic hydrolysis and thermal degradation:During steam blasting, High-pressure hot steam enters in fibrous raw material, and penetrates into the gap inside bagasse fibre, due to the synergy of water vapour and heat Class acid degradation and the thermal degradation of bagasse fibre raw material, lower-molecular substance dissolution are generated, fibrous polymer degree declines;Second is that class Mechanical breaking acts on:When high steam discharges, penetrated into the hot steam molecule inside bagasse fibre in a manner of air-flow from More closed hole high speed abrupt release comes out, and the high speed moment flowing of fibrous inside and surrounding hot steam makes fiber Mechanical breaking to a certain extent.This fracture is not showed only as the fracture of the key in cellulose macromolecule, and reduction end group increases, fine The destruction of the internal hydrogen bond of dimension element, is also embodied by the destruction of the destruction and partially crystallizable area of amorphous region;Third, hydrogen bond destruction: During steam blasting, water vapour is penetrated into each hole of bagasse fibre and is formed with the part of hydroxyl on cellulose molecular chain Hydrogen bond.High temperature, high pressure and aqueous condition can aggravate the destruction to cellulose inside hydrogen bond again simultaneously, and dissociate new hydroxyl, Increase the adsorption capacity of bagasse.Moment pressure release explosion makes each interpore water vapour moment in bagasse be rejected to air In, interrupt the hydrogen bond in Bagasse-cellulose.Cellulose is by rapid cooling to room temperature while intramolecular hydrogen bond is broken so that Cellulose supramolecular structure is " frozen ", only least a portion of hydrogen bond recombination.Solvent molecule is set to be easily accessible piece interlayer in this way, and The solvent of infiltration further carries out solvation with Bagasse-cellulose macromolecular chain, and causes the destruction of hydrogen bond in remaining molecules, The movement for accelerating glucose ring group finally results in the complete destruction of other crystalline regions, until being completely dissolved;Fourth, structural rearrangement is made With:Under high temperature, high pressure, Bagasse-cellulose intramolecular hydrogen bond is increased by a degree of destruction, the mobility of cellulose chain Add, is conducive to cellulose and changes to ordered structure, meanwhile, the fracture of cellulose molecular chain makes cellulose chain be easier to rearrange. To dissociate the feedstock into the bagasse slurry of flocculence with less energy, since this equipment had both avoided chemically treated two Secondary pollution problem, and solve the problems, such as that current biological treatment efficiency is low, it is the biomass conversion most promising pretreatment in field Technology.
It although an embodiment of the present invention has been shown and described, for the ordinary skill in the art, can be with Understanding without departing from the principles and spirit of the present invention can carry out these embodiments a variety of variations, modification, replace And modification, the scope of the present invention is defined by the appended.

Claims (4)

1. a kind of steam explosion pulping equipment, it is characterised in that:Including vacuum pump(1), negative pressure drain tank(3)And cavity charge containers(5), The negative pressure drain tank(3)One end and vacuum pump(1)Connection, the negative pressure drain tank(3)Discharge port and cavity charge containers(5)'s Feed inlet connects, the cavity charge containers(5)Top be additionally provided with chimney device(7), the cavity charge containers(5)Discharging port be connected with Slurries collecting tank(10), the chimney device(7)Top be connected with dust discharge tube(8), the dust discharge tube(8)Connection There is dust collecting box(13), chimney device(7)Lower part be also associated with sewage conduct(11), the sewage conduct(11)It is connected with Dirty water collecting tank(12).
2. steam explosion pulping equipment according to claim 1, it is characterised in that:The cavity charge containers(5)Including tank body (14), feed inlet(15)With slurries delivery outlet(21), the feed inlet(15)Set on tank body(14)Top, feed inlet(15)Enter Blow-off valve is equipped at mouthful(6), the slurries delivery outlet(21)Equipped with slurries conveyance conduit(9).
3. steam explosion pulping equipment according to claim 1, it is characterised in that:The chimney device(7)Including water spray Device(16), chimney warehouse(17), Funnel Cover(18), dust emission mouth(19)And discharge of wastewater mouth(20), the chimney warehouse (17)Inside it is provided with water injector(16), the chimney warehouse(17)Side is additionally provided with dust emission mouth(19), chimney warehouse (17)Top, which is equipped with, prevents Funnel Cover winged outside dust(18), chimney warehouse(17)Bottom be equipped with discharge of wastewater mouth(20).
4. steam explosion pulping equipment according to claim 3, it is characterised in that:The Funnel Cover(18)Top is recessed The downward hemispherical shape structure of mouth.
CN201710081715.8A 2017-02-15 2017-02-15 Steam explosion pulping equipment Pending CN108425261A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201710081715.8A CN108425261A (en) 2017-02-15 2017-02-15 Steam explosion pulping equipment

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Application Number Priority Date Filing Date Title
CN201710081715.8A CN108425261A (en) 2017-02-15 2017-02-15 Steam explosion pulping equipment

Publications (1)

Publication Number Publication Date
CN108425261A true CN108425261A (en) 2018-08-21

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109554791A (en) * 2018-11-28 2019-04-02 际华三五四二纺织有限公司 A method of cellulose fibre flax high-count yarn is produced with cotton spinning equipment

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102050951A (en) * 2010-11-10 2011-05-11 山东龙力生物科技股份有限公司 Cleaner production method of functional lignin
CN102230284A (en) * 2011-05-06 2011-11-02 西南交通大学 Ultrasonic-assistant steam explosion pretreatment process for extracting straw cellulose of crops
CN202440714U (en) * 2012-02-22 2012-09-19 重庆恒远晋通科技有限公司 Negative pressure steam explosive device
CN204000427U (en) * 2014-05-30 2014-12-10 泰安米铎碳能源科技有限公司 A kind of jetting storehouse with dust and vapor collection device
CN106152164A (en) * 2015-03-18 2016-11-23 徐应乐 Chimney dust collecting device
CN206486740U (en) * 2017-02-15 2017-09-12 广西洋荣科技有限公司 Steam explosion pulping equipment

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102050951A (en) * 2010-11-10 2011-05-11 山东龙力生物科技股份有限公司 Cleaner production method of functional lignin
CN102230284A (en) * 2011-05-06 2011-11-02 西南交通大学 Ultrasonic-assistant steam explosion pretreatment process for extracting straw cellulose of crops
CN202440714U (en) * 2012-02-22 2012-09-19 重庆恒远晋通科技有限公司 Negative pressure steam explosive device
CN204000427U (en) * 2014-05-30 2014-12-10 泰安米铎碳能源科技有限公司 A kind of jetting storehouse with dust and vapor collection device
CN106152164A (en) * 2015-03-18 2016-11-23 徐应乐 Chimney dust collecting device
CN206486740U (en) * 2017-02-15 2017-09-12 广西洋荣科技有限公司 Steam explosion pulping equipment

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109554791A (en) * 2018-11-28 2019-04-02 际华三五四二纺织有限公司 A method of cellulose fibre flax high-count yarn is produced with cotton spinning equipment
CN109554791B (en) * 2018-11-28 2021-06-18 际华三五四二纺织有限公司 Method for producing cellulose fiber flax high count yarn by cotton spinning equipment

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