CN108404454A - A kind of water-oil separation device - Google Patents

A kind of water-oil separation device Download PDF

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Publication number
CN108404454A
CN108404454A CN201810299009.5A CN201810299009A CN108404454A CN 108404454 A CN108404454 A CN 108404454A CN 201810299009 A CN201810299009 A CN 201810299009A CN 108404454 A CN108404454 A CN 108404454A
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China
Prior art keywords
water
oil
oil separation
super
blender
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CN201810299009.5A
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Chinese (zh)
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CN108404454B (en
Inventor
赵悦超
杨成娟
田延岭
王福军
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Tianjin University
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Tianjin University
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D17/00Separation of liquids, not provided for elsewhere, e.g. by thermal diffusion
    • B01D17/02Separation of non-miscible liquids
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D17/00Separation of liquids, not provided for elsewhere, e.g. by thermal diffusion
    • B01D17/02Separation of non-miscible liquids
    • B01D17/0205Separation of non-miscible liquids by gas bubbles or moving solids
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D17/00Separation of liquids, not provided for elsewhere, e.g. by thermal diffusion
    • B01D17/02Separation of non-miscible liquids
    • B01D17/0208Separation of non-miscible liquids by sedimentation
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D17/00Separation of liquids, not provided for elsewhere, e.g. by thermal diffusion
    • B01D17/02Separation of non-miscible liquids
    • B01D17/0217Separation of non-miscible liquids by centrifugal force

Abstract

A kind of water-oil separation device includes:It is internally provided with the water-oil separation component of the super-hydrophobic super-oleophylic material block that can adsorb oil detached for realizing water-oil mixture, blender for being stirred to water-oil mixture and super-hydrophobic super-oleophylic material block is set in the water-oil separation component, it is arranged on water-oil separation component top and the connection blender is for driving blender to pass through the stirring driving machine structure that rotation carries out water-oil separation, and it is arranged in water-oil separation component bottom end for the oil extraction driving mechanism by driving the rotation of water-oil separation component that the oil of separator well is made to be discharged out of water-oil separation component.The secondary collection of fluid may be implemented in present invention combination centrifugal principle and gravity, is completed at the same time the cleaning of super-hydrophobic super-oleophylic material block, the repeatable utilization of realization device.The water-oil separation device manufacturing of the present invention is at low cost, disintegrate-quality is high, separative efficiency is high.

Description

A kind of water-oil separation device
Technical field
The present invention relates to a kind of water-oil separation devices.Make more particularly to a kind of filtering by super-hydrophobic super-oleophylic material With the water-oil separation device for realizing water-oil separation.
Background technology
In recent years, with the development of petroleum industry, water-oil separation is in industrial processes, marine transportation, liquid waste processing etc. It is widely used.Common water-oil separation method has Gravity separate, centrifugation, electrically separated, dissolved air flotation etc..But detach matter Amount is limited to.To solve this problem, the water-oil separation method based on super-hydrophobic super-oleophylic surfacing processing technology has become The research hotspot of domestic and foreign scholars.By technologies such as chemical etching, mechanical lapping, LBL self-assemblies to material surface It learns pattern modification and bond material surface chemical modification prepares and is provided simultaneously with super-hydrophobic and film or metal of super-oleophilic matter Net can effectively realize water-oil separation.For traditional water-oil separation method, the water-oil separation based on super-hydrophobic super-oleophylic material Technology can not only ensure that the water-oil separation of high quality also adapts to different water-oil factor examples.Therefore, in conjunction with super-hydrophobic super-oleophylic The water-oil separation method of surfacing technology of preparing is particularly important for the improvement for industrializing water-oil separation technology at this stage.
For realize high quality, low cost water-oil separation, need in conjunction with super-hydrophobic super-oleophylic surfacing processing technology with from Heart separation principle makes the repeatable utilization of realization device on the basis of ensureing that water-oil separation high quality and high efficiency is completed, passes through Water-oil separation is realized in the filtration of super-hydrophobic super-oleophylic material, and greasy dirt collection and super-hydrophobic super parent are realized by centrifugal principle The purification of light wood material;The preliminary mistake of waste liquid solid impurity can be realized by adjusting the structure size of super-hydrophobic super-oleophylic material in device Filter can be realized the purified treatment of oily wastewater by discharge pipe line engagement purifier again.
Invention content
The technical problem to be solved by the invention is to provide one kind set manufacturing cost it is cheap, it is repeatable utilize, separative efficiency High water-oil separation device.
The technical solution adopted in the present invention is:A kind of water-oil separation device includes:Oil can be adsorbed by being internally provided with Super-hydrophobic super-oleophylic material block for realizing water-oil mixture separation water-oil separation component, be arranged in the water-oil separation Blender in component for being stirred to water-oil mixture and super-hydrophobic super-oleophylic material block is arranged in the water-oil separation The stirring driving machine structure that component top and the connection blender are used to that blender to be driven to carry out water-oil separation by rotation, and It is arranged in water-oil separation component bottom end for by driving the rotation of water-oil separation component to make the oily from water oil of separator well From the oil extraction driving mechanism being discharged in component.
The water-oil separation component includes:Outer cylinder and the inner circle in outer cylinder for accommodating water-oil mixture Cylinder, the super-hydrophobic super-oleophylic material block are arranged in the inner cylinder, and the outer cylinder and inner cylinder are arranged concentrically and are total to With a bottom face and a upper end cover, the outer cylinder and inner cylindrical are at the interval for being useful for the oil that receiving is isolated, institute It states and is formed with the most oil-through holes for detaching oil into outer cylinder on the barrel of inner cylinder, the outer side center of the bottom face It is provided with the rotating shaft for being connected with the oil extraction driving mechanism, the inner cylindrical is corresponded on the bottom face at being useful for The water outlet of water isolated is discharged, the interval between the inner cylinder and outer cylinder is corresponded on the bottom face is formed with and be used for The oil outlet for the oil being separated is discharged, the axis for being useful for the agitating shaft through the blender is respectively formed on the upper end cover Hole corresponds to the inner cylindrical on the upper end cover at being useful for injecting the liquid injection port of water-oil mixture to inner cylinder.
The blender includes:The axis hole that one end is run through on the upper end cover in water-oil separation component connects the stirring The agitating shaft of the output shaft of driving mechanism, the agitating shaft other end are integrally attached to the center of the one side of connection floor, institute It states vertical on the another side of connection floor and is connected with 4 symmetrical stirring blades.
It is formed with multiple through-holes on each stirring blade.
The stirring driving machine structure includes:Driving motor is stirred, is connected with the output shaft of the stirring driving motor First shaft coupling, the agitating shaft of blender described in the output axis connection of the first shaft coupling.
The oil extraction driving mechanism includes oil extraction driving motor, is connected with the output shaft of the oil extraction driving motor Second shaft coupling, the rotating shaft of water-oil separation component described in the output axis connection of the second shaft coupling.
A kind of water-oil separation device of the present invention, the technological means handled by chemical attack and fluoride can be appointed The super-hydrophobic super-oleophylic material block for size of anticipating and then the water-oil separation for meeting arbitrary water-oil factor example water-oil mixture.It is former in conjunction with centrifugation Reason and gravity, may be implemented the secondary collection of fluid, are completed at the same time the cleaning of super-hydrophobic super-oleophylic material block, realization device Repeatable utilization.The participation of mixing component is to promote water-oil mixture to come into full contact with super-hydrophobic super-oleophylic material block same When, the infiltration of water-oil mixture in a device is also accelerated, the efficiency of water-oil separation process is improved.Super-hydrophobic super-oleophylic material Block is provided simultaneously with the repeatable characteristic utilized using low cost, common metal material.Thus, the water-oil separation device manufacturing It is at low cost, disintegrate-quality is high, separative efficiency is high.
Description of the drawings
Fig. 1 is a kind of overall structure diagram of water-oil separation device of the present invention;
Fig. 2 is the structural schematic diagram that water-oil separation component internal is not provided with super-hydrophobic super-oleophylic material block in the present invention;
Fig. 3 is the structural schematic diagram that water-oil separation component internal is provided with super-hydrophobic super-oleophylic material block in the present invention;
Fig. 4 is the structural schematic diagram of blender in the present invention.
1:Water-oil separation component 1.1:Inner cylinder
1.2:Outer cylinder 1.3:Rotating shaft
1.4:Bottom face 1.5:Water outlet
1.6:Oil outlet 1.7:Oil-through hole
1.8:Super-hydrophobic super-oleophylic material block 1.9:Axis hole
1.10 liquid injection port 1.11:Upper end cover
2:Stirring driving machine structure 2.1:Stir driving motor
2.2:First shaft coupling 3:Oil extraction driving mechanism
3.1:Oil extraction driving motor 3.2:Second shaft coupling
4:Blender 4.1:Agitating shaft
4.2:Connect floor 4.3:Stirring blade
4.4:Through-hole
Specific implementation mode
A kind of water-oil separation device of the present invention is described in detail with reference to embodiment and attached drawing.
As shown in Figure 1, a kind of water-oil separation device of the present invention, includes:The super thin of oil can be adsorbed by being internally provided with The water-oil separation component 1 for realizing water-oil mixture separation of the super lipophilic material block of water 1.8, is arranged in the water-oil separation group Blender 4 in part 1 for being stirred to water-oil mixture and super-hydrophobic super-oleophylic material block 1.8, setting is in water oil The stirring driving machine that 1 top of separation assembly and the connection blender 4 are used to that blender 4 to be driven to carry out water-oil separation by rotation Structure 2, and be arranged in 1 bottom end of water-oil separation component for by driving 1 rotation of water-oil separation component to make separator well The oil extraction driving mechanism 3 that oil is discharged out of water-oil separation component 1.
As shown in Figure 2 and Figure 3, the water-oil separation component 1 includes:Outer cylinder 1.2 and the use in outer cylinder 1.2 In the inner cylinder 1.1 for accommodating water-oil mixture, the super-hydrophobic super-oleophylic material block 1.8 is arranged in the inner cylinder 1.1, The outer cylinder 1.2 and inner cylinder 1.1 are arranged concentrically and share a bottom face 1.4 and a upper end cover 1.11, the outer circle Cylinder 1.2 and inner cylinder 1.1 are formed with the interval for accommodating the oil isolated, and are uniformly distributed on the barrel of the inner cylinder 1.1 Formation have the most oil-through holes 1.7 for detaching oil into outer cylinder 1.2, the outer side center setting of the bottom face 1.4 It is useful for the rotating shaft 1.3 being connected with the oil extraction driving mechanism 3, the formation of the inner cylinder 1.1 is corresponded on the bottom face 1.4 Be useful for the water outlet 1.5 of water that discharge is isolated, correspond on the bottom face 1.4 inner cylinder 1.1 and outer cylinder 1.2 it Between interval be formed with the oil outlet 1.6 for the oil being separated to be discharged, be respectively formed on the upper end cover 1.11 and be useful for Through the axis hole 1.9 of the agitating shaft 4.1 of the blender 4, corresponded on the upper end cover 1.11 inner cylinder 1.1 formed it is useful In the liquid injection port 1.10 for injecting water-oil mixture to inner cylinder 1.1.
The function of the water-oil separation component includes the drainage of water and fluid after water-oil separation and separation.Equipped with super-hydrophobic The inner sleeve of super lipophilic material block completes the separation of water-oil mixture with blender cooperation, is exported via bottom face lower part water outlet Water, after water-oil separation process, centrifugal force caused by the rotary motion that is provided via the rotating shaft of bottom face, in conjunction with uniform The inner cylinder of oil-through hole is distributed with so that fluid is detached with super-hydrophobic super-oleophylic material block, and fluid is adhered on outer cylinder inner wall, Then flowed out under the effect of gravity via the oil outlet being distributed on bottom face;Wherein, super-hydrophobic super-oleophylic material block is current What is generally used carries out the metal material that surface topography modification handles progress chemical modification via fluoride again by chemical attack. Pass through chemical means and be modified acquisition in metal material surface chemistry and pattern, shape size is adjustable, can play good water Oily separating effect ensures water-oil separation quality, is combined with separating component axis and the inner cylinder for being uniformly distributed circular hole, utilize centrifugation Principle and gravity can also be achieved the recycling of device, and of low cost, adaptability is good, and function admirable is cost-effective.
As shown in figure 4, the blender 4 includes:One end is run through on the upper end cover 1.11 in water-oil separation component 1 Axis hole 1.9 connects the agitating shaft 4.1 of the output shaft of the stirring driving machine structure 2, and 4.1 other end of the agitating shaft is integrally attached to Connect the center of the one side of floor 4.2, it is vertical on the another side of the connection floor 4.2 and be connected with 4 it is symmetrical The stirring blade 4.3 of distribution is each formed with multiple through-holes 4.4 on the stirring blade 4.3.
The blender 4 is mainly used for stirring the liquid-solid mixture of water-oil mixture and super-hydrophobic super-oleophylic material block, It is connect with stirring driving motor by first shaft coupling and realizes rotary motion, can realize that water oil is mixed during water-oil separation Conjunction liquid comes into full contact with super-hydrophobic super-oleophylic material block, while mixing being accelerated to improve flow rate, to ensure water oil High efficiency from process and high quality, it is compact in structure and convenient to use.And pass through 4 symmetrical thereon stirring with through-hole Blade is mixed, while reducing steering resistance, realizes being sufficiently stirred for mixture, with the super-hydrophobic super parent in water-oil separation component Oily material block completes water-oil separation process together;Super-hydrophobic super parent is determined according to the water-oil factor example of water-oil mixture and volume size The size of oily material block, and then determine the clear size of opening of stirring blade, ensure that its clear size of opening is much larger than super-hydrophobic super-oleophylic material Expect the size of block.On agitating shaft 4.1 be equipped with keyway, for and first shaft coupling realize key connection, first shaft coupling it is another End is connected with stirring driving motor output shaft, and three is fitted close provides flywheel moment for mixing component.It is high by connecting floor Be connected with agitating shaft to intensity high rigidity, agitating shaft by be keyed shaft coupling, shaft coupling stirring driving motor driving under, Agitating shaft rotation is driven, to which stirring action is completed in stirring blade revolution, water-oil mixture high quality and high efficiency is made to detach.
As shown in Figure 1, the stirring driving machine structure 2 includes:Driving motor 2.1 is stirred, electricity is driven with the stirring The connected first shaft coupling 2.2 of the output shaft of machine 2.1, the output shaft of the first shaft coupling 2.2 are connected by key connection mode The agitating shaft 4.1 of the blender 4.The oil extraction driving mechanism 3 includes oil extraction driving motor 3.1, is driven with the oil extraction The connected second shaft coupling 3.2 of the output shaft of dynamic motor 3.1, water oil described in the output axis connection of the second shaft coupling 3.2 Rotating shaft 1.3 from component 1.
A kind of water-oil separation device of the present invention implements form:
1, water-oil separation component 1 is connect by second shaft coupling 3.2 with oil extraction driving motor 3.1 first, and keeps suitable When mutual alignment, by the agitating shaft of the blender 4 in water-oil separation component 1 pass through first shaft coupling 2.2 with stirring drive Dynamic motor 2.1 connects, and keeps mutual alignment appropriate.
2, stirring driving motor 2.1 is opened, blender 4 turns round, and water-oil mixture, stirring blade are imported from liquid injection port 1.10 4.3 agitation super-hydrophobic super-oleophylic material blocks 1.8 and water-oil mixture, adsorb by the filtering of super-hydrophobic super-oleophylic material block and make With the water in water-oil mixture is flowed out via the water outlet of bottom face, and fluid is then adsorbed on super-hydrophobic super-oleophylic material block 1.8 On, separation completion stops stirring driving motor 2.1, opens oil extraction driving motor 3.1, realizes the entirety of water-oil separation component 1 Revolution at a high speed, under the action of the centrifugal force, the fluid being adhered on super-hydrophobic super-oleophylic material block 1.8 are thrown to outer sleeve wall, real The separation of existing fluid and super-hydrophobic super-oleophylic material block 1.8, stops oil extraction driving motor 3.1, fluid under the effect of gravity via Oil outlet flows out, and realizes the collection of fluid, in addition the super-hydrophobic super-oleophylic material block be metal material via chemical attack into Row surface topography is modified, fluoride processing carries out chemical modification acquisition.
The basic principles and main features and advantages of the present invention of the present invention are described above in association with attached drawing.Although Detailed description is carried out to the execution pattern of the present invention, the technical staff of the industry is not it will be appreciated that the present invention limits to In above-mentioned way of realization, the only the principle of the present invention described in the above embodiments and specification, those skilled in the art Member it can be seen that within the scope of the appended claims be used for implement the present invention many alternative designs and embodiments.It is not departing from For the present invention in a word with the situation under claimed range, these ways of realization all belong to the scope of protection of the present invention it It is interior.

Claims (6)

1. a kind of water-oil separation device, which is characterized in that include:The super-hydrophobic super-oleophylic material of oil can be adsorbed by being internally provided with The water-oil separation component (1) for realizing water-oil mixture separation for expecting block (1.8), is arranged in the water-oil separation component (1) The interior blender (4) for being stirred to water-oil mixture and super-hydrophobic super-oleophylic material block (1.8), setting is in water oil The stirring that separation assembly (1) top and the connection blender (4) are used to that blender (4) to be driven to carry out water-oil separation by rotation Driving mechanism (2), and setting drive water-oil separation component (1) to revolve in water-oil separation component (1) bottom end for passing through Turn the oil extraction driving mechanism (3) for making the oil of separator well be discharged out of water-oil separation component (1).
2. a kind of water-oil separation device according to claim 1, which is characterized in that water-oil separation component (1) packet It has included:Outer cylinder (1.2) and the inner cylinder (1.1) in outer cylinder (1.2) for accommodating water-oil mixture, described is super thin In the inner cylinder (1.1), the outer cylinder (1.2) and inner cylinder (1.1) are set super lipophilic material block (1.8) setting of water with one heart A bottom face (1.4) and a upper end cover (1.11) are set and share, the outer cylinder (1.2) and inner cylinder (1.1) are formed with For accommodating the oily interval isolated, it is formed with most on the barrel of the inner cylinder (1.1) and is used for outer cylinder (1.2) The oil-through hole (1.7) of interior separation oil, the outer side center of the bottom face (1.4) be provided with for the oil extraction driving mechanism (3) connected rotating shaft (1.3) correspond to the inner cylinder (1.1) on the bottom face (1.4) and is formed with and isolated for discharge Water water outlet (1.5), the interval between the inner cylinder (1.1) and outer cylinder (1.2) is corresponded on the bottom face (1.4) It is formed with the oil outlet (1.6) for the oil being separated to be discharged, is respectively formed on the upper end cover (1.11) and is useful for running through The axis hole (1.9) of the agitating shaft (4.1) of the blender (4) corresponds to the inner cylinder (1.1) shape on the upper end cover (1.11) At the liquid injection port (1.10) being useful for inner cylinder (1.1) injection water-oil mixture.
3. a kind of water-oil separation device according to claim 1, which is characterized in that the blender (4) includes:One Axis hole (1.9) of the end on the upper end cover (1.11) in water-oil separation component (1) connects the defeated of the stirring driving machine structure (2) The agitating shaft (4.1) of shaft, agitating shaft (4.1) other end are integrally attached to the center of the one side of connection floor (4.2), It is vertical and be connected with 4 symmetrical stirring blades (4.3) on the another side of the connection floor (4.2).
4. a kind of water-oil separation device according to claim 3, which is characterized in that each stirring blade (4.3) On be all formed with multiple through-holes (4.4).
5. a kind of water-oil separation device according to claim 1, which is characterized in that stirring driving machine structure (2) packet It has included:Driving motor (2.1) is stirred, the first shaft coupling (2.2) being connected with the output shaft of the stirring driving motor (2.1), The agitating shaft (4.1) of blender (4) described in the output axis connection of the first shaft coupling (2.2).
6. a kind of water-oil separation device according to claim 1, which is characterized in that oil extraction driving mechanism (3) packet Oil extraction driving motor (3.1) has been included, the second shaft coupling (3.2) being connected with the output shaft of the oil extraction driving motor (3.1), institute State the rotating shaft (1.3) of water-oil separation component (1) described in the output axis connection of second shaft coupling (3.2).
CN201810299009.5A 2018-04-04 2018-04-04 Water-oil separating device Active CN108404454B (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111729397A (en) * 2020-07-01 2020-10-02 李彩虹 Sewage processor with multi-stage treatment function

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2002066582A (en) * 2000-08-28 2002-03-05 Daiwa Kogyo Kk Biological treatment method for waste water containing oil content
CN1853770A (en) * 2005-04-27 2006-11-01 李兆辉 Modified adsorbent for oil component in water, its production and adsorber
CN101972559A (en) * 2010-10-21 2011-02-16 天津大学 Oil-water separating device and method
CN102872646A (en) * 2012-10-18 2013-01-16 昆山威胜达环保设备有限公司 Charge type coalescing-separating oil filter
CN208448703U (en) * 2018-04-04 2019-02-01 天津大学 A kind of water-oil separation device

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2002066582A (en) * 2000-08-28 2002-03-05 Daiwa Kogyo Kk Biological treatment method for waste water containing oil content
CN1853770A (en) * 2005-04-27 2006-11-01 李兆辉 Modified adsorbent for oil component in water, its production and adsorber
CN101972559A (en) * 2010-10-21 2011-02-16 天津大学 Oil-water separating device and method
CN102872646A (en) * 2012-10-18 2013-01-16 昆山威胜达环保设备有限公司 Charge type coalescing-separating oil filter
CN208448703U (en) * 2018-04-04 2019-02-01 天津大学 A kind of water-oil separation device

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111729397A (en) * 2020-07-01 2020-10-02 李彩虹 Sewage processor with multi-stage treatment function

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