CN108395784A - A kind of preparation method and product of suitable baking high-performance water-based damping coating material - Google Patents
A kind of preparation method and product of suitable baking high-performance water-based damping coating material Download PDFInfo
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- CN108395784A CN108395784A CN201810239829.5A CN201810239829A CN108395784A CN 108395784 A CN108395784 A CN 108395784A CN 201810239829 A CN201810239829 A CN 201810239829A CN 108395784 A CN108395784 A CN 108395784A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D133/00—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Coating compositions based on derivatives of such polymers
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/61—Additives non-macromolecular inorganic
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/61—Additives non-macromolecular inorganic
- C09D7/62—Additives non-macromolecular inorganic modified by treatment with other compounds
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/65—Additives macromolecular
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/70—Additives characterised by shape, e.g. fibres, flakes or microspheres
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K2201/00—Specific properties of additives
- C08K2201/002—Physical properties
- C08K2201/003—Additives being defined by their diameter
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K2201/00—Specific properties of additives
- C08K2201/014—Additives containing two or more different additives of the same subgroup in C08K
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/02—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group
- C08L2205/025—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group containing two or more polymers of the same hierarchy C08L, and differing only in parameters such as density, comonomer content, molecular weight, structure
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
- C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/14—Polymer mixtures characterised by other features containing polymeric additives characterised by shape
- C08L2205/16—Fibres; Fibrils
Abstract
The invention discloses a kind of preparation methods and product of suitable baking high-performance water-based damping coating material:1)Acrylic resin blending emulsion:30‑40;Deionized water:5‑10;Antifoaming agent:0.3‑0.8;Dispersant:0.3‑0.8;Modified calcium carbonate filler:80 mesh, 15 30;1000 mesh, 15 30;Sericite in powder:100 ~ 600 mesh, 10 20;Modified fibre:0.5‑1;Coalescents:1‑2;Thickener:0.4‑0.8;Wherein, the acrylic resin blending emulsion be blended according to a certain percentage in 10 degree, 20 degree, 40 degree of three kinds of emulsion acrylic resins by glass transition temperature respectively it is obtained;2)Acrylic resin blending emulsion, deionized water, antifoaming agent and dispersant are placed in stirring container, the stirring of 500rpm rotating speeds;3)Stirring container, the stirring of 1000rpm rotating speeds is added in modified calcium carbonate filler, sericite in powder, modified fibre, coalescents;4)Stirring container, the stirring of 1500rpm rotating speeds is added in thickener;5)It obtains and is suitble to baking high-performance water-based damping coating material, toast and do not crack at 80 degrees Celsius.
Description
Technical field
The present invention relates to aqueous damping coating, more particularly to a kind of preparation side of suitable baking high-performance water-based damping coating material
Method and product.
Background technology
Main damping paint has traditional polyurethane/polyethers constrained layer damping coating and aqueous damping in industry at present
Coating two major classes.The former can discharge mostly VOC and cannot extensive spraying application, make it unsuitable for the applications such as automotive field;
The current major defect of the latter is to be applied to usually crack when automotive field baking process.
Invention content
Against the above deficiency, the object of the present invention is to provide a kind of systems of suitable baking high-performance water-based damping coating material
Preparation Method and product, it is environment-protecting and non-poisonous, be suitble to spraying and knife-coat application, within the scope of -10 DEG C~50 DEG C wide temperature ranges recombination loss because
Son can be more than 0.05, and baking is not cracked.
The technical solution adopted by the present invention is:A kind of preparation method of suitable baking high-performance water-based damping coating material, it is special
Sign is, includes the following steps:
1) component of the following weight part ratio of preparation:
Acrylic resin blending emulsion:30-40;
Deionized water:5-10;
Antifoaming agent:0.3-0.8;
Dispersant:0.3-0.8;
Modified calcium carbonate filler:80 mesh, 15-30;1000 mesh, 15-30;
Sericite in powder:100~600 mesh, 10-20;
Modified fibre:0.5-1;
Coalescents:1-2;
Thickener:0.4-0.8;
Wherein, the acrylic resin blending emulsion is respectively by glass transition temperature in -10 degree, 20 degree, three kinds of 40 degree
Emulsion acrylic resin is blended according to a certain percentage to be made, and three kinds of emulsion acrylic resins are respectively 3-20 parts, 3-20 parts, 3-20
Part;
2) it by acrylic resin blending emulsion, deionized water, antifoaming agent and dispersant, is placed in stirring container, unlatching is stirred
Machine is mixed, speed governing to 500rpm rotating speeds is stirred 5 minutes;
3) stirring container is added in modified calcium carbonate filler, sericite in powder, modified fibre, coalescents, opens blender,
Speed governing to 1000rpm rotating speeds stir 10 minutes;
4) stirring container is added in thickener, opens blender, speed governing to 1500rpm rotating speeds is stirred 10 minutes;
5) it obtains and is suitble to baking high-performance water-based damping coating material.
It should be noted that the above-mentioned modified calcium carbonate filler referred to.So-called modified calcium carbonate is meant powdered whiting
Or precipitated calcium carbonate surface carries out activation process and is made, not only hydrophobization but also activation.Activated Calcium carbonate is imperceptible white
Color powder, odorless, tasteless, particle approximate spheres, grain size 0.1um have hereinafter, because particle surface has adsorbed one layer of fat soap
Colloidal activating performance is excellent white reinforcing filler.The above-mentioned coalescents referred to, also known as coalescing aid.It can promote high score
Sub- compound Plastic Flow and flexible deformation improve coalescence performance, the substance that can be formed a film within the scope of wide construction temperature.Often
For the strong solvent of ether alcohol class high polymer, such as propandiol butyl ether, propylene glycol methyl ether acetate.The above-mentioned modified fibre referred to
Also known as modified fibre refers to certain performances (such as hygroscopicity, the dyeing for making conventional chemical fiber species by means of method chemically or physically
Property, antistatic property, anti-flammability etc.) improved and a series of general name of Fresh fats that derives from, such as modified viscose fiber, modified poly-
Ester fiber, modified acrylic fibre, modified polyvinyl alcohol fabric etc.;It can be made into powdery when applying, and use respective performances
Modified fibre.
Further, in step 1), the antifoaming agent is mineral oil type antifoaming agent.Mineral oil antifoam agent it be it is a kind of can be
Disperse in water and becomes the lotion for having appropriate stability;Under acid and alkaline condition all effectively;Can be adapted for building coating,
Communal facility, knot engineering, ACE coatings, printing ink, adhesive, emulsion polymerization etc..Such as, section is federal, ten thousand one-tenth new etc. in using
The mineral oil type antifoaming agent of producer.
Further, in step 1), the dispersant be carboxyl acid copolymer salt dispersant of type (and or carboxylate dispersants,
Polycarboxylate salt dispersant), it can purchase goods on a selective basis on the market according to demand.
Further, in step 1), the thickener is polyurethanes association thickener.Polyurethane thickener, referred to as
HEUR is a kind of ethoxy based polyurethanes water-soluble polymer that hydrophobic group is modified, belongs to nonionic associative thickener.HEUR by
Hydrophobic group, hydrophilic chain and polyurethane agent three parts composition.Hydrophobic group plays association, is the determinant of thickening, typically oily
Base, octadecyl, dodecane phenyl, nonyl phenolic group etc..Hydrophilic chain can provide chemical stability and viscosity stability, and common is
Polyethers.HEUR strands are extended by polyurethane, and polyurethane used has IPDI, TDI, HMDI etc..Association type increases
Thick dose be structurally characterized in that hydrophobic group block.
A kind of suitable baking high-performance water-based damping coating material prepared by the method.
The present invention has the following advantages:It is surveyed according to national standard GB/T16406-1996 by damping paint made from above method
The complex loss factor for having more than 0.05 between -10~50 DEG C is tried, and toasts and does not crack at 80 degrees Celsius.
With reference to embodiment, the invention will be further described.
Specific implementation mode
Embodiment 1
It is suitble to the preparation method of baking high-performance water-based damping coating material, includes the following steps:
1) component of the following weight part ratio of preparation:
Acrylic resin blending emulsion:30-40;
Deionized water:5-10;
Antifoaming agent:0.3-0.8;
Dispersant:0.3-0.8;
Modified calcium carbonate filler:80 mesh, 15-30;1000 mesh, 15-30;
Sericite in powder:100~600 mesh, 10-20;
Modified fibre:0.5-1;
Coalescents:1-2;
Thickener:0.4-0.8;
Wherein, the acrylic resin blending emulsion is respectively by glass transition temperature in -10 degree, 20 degree, three kinds of 40 degree
Emulsion acrylic resin is blended according to a certain percentage to be made, and three kinds of emulsion acrylic resins are respectively 3-20 parts, 3-20 parts, 3-20
Part;
2) it by acrylic resin blending emulsion, deionized water, antifoaming agent and dispersant, is placed in stirring container, unlatching is stirred
Machine is mixed, speed governing to 500rpm rotating speeds is stirred 5 minutes;
3) stirring container is added in modified calcium carbonate filler, sericite in powder, modified fibre, coalescents, opens blender,
Speed governing to 1000rpm rotating speeds stir 10 minutes;
4) stirring container is added in thickener, opens blender, speed governing to 1500rpm rotating speeds is stirred 10 minutes;
5) it obtains and is suitble to baking high-performance water-based damping coating material.
The suitable baking high-performance water-based damping coating material prepared by the method.
Embodiment 2
It is suitble to the preparation method of baking high-performance water-based damping coating material, includes the following steps:
1) component of the following weight part ratio of preparation:
Acrylic resin blending emulsion:30;
Deionized water:5;
Antifoaming agent:0.3;
Dispersant:0.3;
Modified calcium carbonate filler:80 mesh, 15;1000 mesh, 15;
Sericite in powder:100~600 mesh, 10;
Modified fibre:0.5;
Coalescents:1;
Thickener:0.4;
Wherein, the acrylic resin blending emulsion is respectively by glass transition temperature in -10 degree, 20 degree, three kinds of 40 degree
Emulsion acrylic resin is blended according to a certain percentage to be made, three kinds of emulsion acrylic resins are respectively 20 parts, 20 parts, 20 parts (that is,
1:1:1);
2) it by acrylic resin blending emulsion, deionized water, antifoaming agent and dispersant, is placed in stirring container, unlatching is stirred
Machine is mixed, speed governing to 500rpm rotating speeds is stirred 5 minutes;
3) stirring container is added in modified calcium carbonate filler, sericite in powder, modified fibre, coalescents, opens blender,
Speed governing to 1000rpm rotating speeds stir 10 minutes;
4) stirring container is added in thickener, opens blender, speed governing to 1500rpm rotating speeds is stirred 10 minutes;
5) it obtains and is suitble to baking high-performance water-based damping coating material.
The suitable baking high-performance water-based damping coating material prepared by the method.
Embodiment 3
It is suitble to the preparation method of baking high-performance water-based damping coating material, includes the following steps:
1) component of the following weight part ratio of preparation:
Acrylic resin blending emulsion:40;
Deionized water:10;
Antifoaming agent:0.8;
Dispersant:0.8;
Modified calcium carbonate filler:80 mesh, 30;1000 mesh, 30;
Sericite in powder:100~600 mesh, 20;
Modified fibre:1;
Coalescents:2;
Thickener:0.8;
Wherein, the acrylic resin blending emulsion is respectively by glass transition temperature in -10 degree, 20 degree, three kinds of 40 degree
Emulsion acrylic resin is blended according to a certain percentage to be made, and three kinds of emulsion acrylic resins are respectively 3 parts, 20 parts, 3 parts;
2) it by acrylic resin blending emulsion, deionized water, antifoaming agent and dispersant, is placed in stirring container, unlatching is stirred
Machine is mixed, speed governing to 500rpm rotating speeds is stirred 5 minutes;
3) stirring container is added in modified calcium carbonate filler, sericite in powder, modified fibre, coalescents, opens blender,
Speed governing to 1000rpm rotating speeds stir 10 minutes;
4) stirring container is added in thickener, opens blender, speed governing to 1500rpm rotating speeds is stirred 10 minutes;
5) it obtains and is suitble to baking high-performance water-based damping coating material.
The suitable baking high-performance water-based damping coating material prepared by the method.
Embodiment 4
It is suitble to the preparation method of baking high-performance water-based damping coating material, includes the following steps:
1) component of the following weight part ratio of preparation:
Acrylic resin blending emulsion:35;
Deionized water:8;
Antifoaming agent:0.4;
Dispersant:0.4;
Modified calcium carbonate filler:80 mesh, 25;1000 mesh, 25;
Sericite in powder:100~600 mesh, 15;
Modified fibre:0.8;
Coalescents:1.5;
Thickener:0.5;
Wherein, the acrylic resin blending emulsion is respectively by glass transition temperature in -10 degree, 20 degree, three kinds of 40 degree
Emulsion acrylic resin is blended according to a certain percentage to be made, and three kinds of emulsion acrylic resins are respectively 20 parts, 3 parts, 20 parts;
2) it by acrylic resin blending emulsion, deionized water, antifoaming agent and dispersant, is placed in stirring container, unlatching is stirred
Machine is mixed, speed governing to 500rpm rotating speeds is stirred 5 minutes;
3) stirring container is added in modified calcium carbonate filler, sericite in powder, modified fibre, coalescents, opens blender,
Speed governing to 1000rpm rotating speeds stir 10 minutes;
4) stirring container is added in thickener, opens blender, speed governing to 1500rpm rotating speeds is stirred 10 minutes;
5) it obtains and is suitble to baking high-performance water-based damping coating material.
The suitable baking high-performance water-based damping coating material prepared by the method.
After tested, this is suitble to the suitable baking prepared by baking high-performance water-based damping coating material preparation method high-performance water-based
Damping paint has the complex loss factor more than 0.05 according to national standard GB/T16406-1996 tests between -10~50 DEG C,
And it toasts and does not crack at 80 degrees Celsius.
Present invention is not limited to the embodiments described above, using identical as the above embodiment of the present invention or approximate technology spy
Sign, and other obtained preparation methods and product for being suitble to toast high-performance water-based damping coating material, the protection model in the present invention
Within enclosing.
Claims (5)
1. a kind of preparation method of suitable baking high-performance water-based damping coating material, which is characterized in that include the following steps:
1)The component of the following weight part ratio of preparation:
Acrylic resin blending emulsion:30-40;
Deionized water:5-10;
Antifoaming agent:0.3-0.8;
Dispersant:0.3-0.8;
Modified calcium carbonate filler:80 mesh, 15-30;1000 mesh, 15-30;
Sericite in powder:100 ~ 600 mesh, 10-20;
Modified fibre:0.5-1;
Coalescents:1-2;
Thickener:0.4-0.8;
Wherein, the acrylic resin blending emulsion is respectively by glass transition temperature in -10 degree, 20 degree, 40 degree of three kinds of propylene
Acid resin lotion is blended according to a certain percentage to be made, and three kinds of emulsion acrylic resins are respectively 3-20 parts, 3-20 parts, 3-20 parts;
It is placed in acrylic resin blending emulsion, deionized water, antifoaming agent and dispersant in stirring container, opens blender, adjusts
Speed to 500rpm rotating speeds stir 5 minutes;
Stirring container is added in modified calcium carbonate filler, sericite in powder, modified fibre, coalescents, opens blender, speed governing is extremely
1000rpm rotating speeds stir 10 minutes;
Stirring container is added in thickener, opens blender, speed governing to 1500rpm rotating speeds is stirred 10 minutes;
It obtains and is suitble to baking high-performance water-based damping coating material.
2. the preparation method of suitable baking high-performance water-based damping coating material according to claim 1, which is characterized in that step
1)In, the antifoaming agent is mineral oil type antifoaming agent.
3. the preparation method of suitable baking high-performance water-based damping coating material according to claim 1, which is characterized in that step
1)In, the dispersant is carboxyl acid copolymer salt dispersant of type.
4. the preparation method of suitable baking high-performance water-based damping coating material according to claim 1, which is characterized in that step
1)In, the thickener is polyurethanes association thickener.
5. a kind of suitable baking high-performance water-based damping coating material prepared by one of Claims 1-4 the method.
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CN201810239829.5A CN108395784A (en) | 2018-03-22 | 2018-03-22 | A kind of preparation method and product of suitable baking high-performance water-based damping coating material |
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CN201810239829.5A CN108395784A (en) | 2018-03-22 | 2018-03-22 | A kind of preparation method and product of suitable baking high-performance water-based damping coating material |
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Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN109679426A (en) * | 2018-12-17 | 2019-04-26 | 万华化学集团股份有限公司 | A kind of aqueous damping coating and preparation method thereof |
CN112831228A (en) * | 2021-01-08 | 2021-05-25 | 东莞市迅杰通新材料有限公司 | Preparation method of water-based damping coating suitable for baking at 140 DEG C |
Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN106009956A (en) * | 2016-06-16 | 2016-10-12 | 西安航天三沃化学有限公司 | Waterborne damping coating for railway vehicles and preparation technology thereof |
CN106675283A (en) * | 2016-12-13 | 2017-05-17 | 苏州赛斯德工程设备有限公司 | Water-based anti-cracking coating and preparation method thereof |
-
2018
- 2018-03-22 CN CN201810239829.5A patent/CN108395784A/en active Pending
Patent Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN106009956A (en) * | 2016-06-16 | 2016-10-12 | 西安航天三沃化学有限公司 | Waterborne damping coating for railway vehicles and preparation technology thereof |
CN106675283A (en) * | 2016-12-13 | 2017-05-17 | 苏州赛斯德工程设备有限公司 | Water-based anti-cracking coating and preparation method thereof |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN109679426A (en) * | 2018-12-17 | 2019-04-26 | 万华化学集团股份有限公司 | A kind of aqueous damping coating and preparation method thereof |
CN112831228A (en) * | 2021-01-08 | 2021-05-25 | 东莞市迅杰通新材料有限公司 | Preparation method of water-based damping coating suitable for baking at 140 DEG C |
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Application publication date: 20180814 |