CN108387482A - A kind of cementitious material slurry apparent density device for quick testing - Google Patents
A kind of cementitious material slurry apparent density device for quick testing Download PDFInfo
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- CN108387482A CN108387482A CN201810394938.4A CN201810394938A CN108387482A CN 108387482 A CN108387482 A CN 108387482A CN 201810394938 A CN201810394938 A CN 201810394938A CN 108387482 A CN108387482 A CN 108387482A
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- 239000002002 slurry Substances 0.000 title claims abstract description 76
- 239000000463 material Substances 0.000 title claims abstract description 60
- 238000012360 testing method Methods 0.000 title claims abstract description 36
- 239000007799 cork Substances 0.000 claims abstract description 17
- 238000000034 method Methods 0.000 claims abstract description 17
- 238000012546 transfer Methods 0.000 claims abstract description 8
- 239000003350 kerosene Substances 0.000 claims description 25
- 239000007788 liquid Substances 0.000 claims description 13
- 238000004364 calculation method Methods 0.000 claims description 5
- 238000010998 test method Methods 0.000 claims description 4
- 241001411320 Eriogonum inflatum Species 0.000 claims description 3
- 238000005303 weighing Methods 0.000 claims 1
- 238000005516 engineering process Methods 0.000 abstract description 3
- 238000001514 detection method Methods 0.000 abstract description 2
- 238000006073 displacement reaction Methods 0.000 abstract 3
- 239000011398 Portland cement Substances 0.000 description 6
- 239000000203 mixture Substances 0.000 description 6
- 239000004567 concrete Substances 0.000 description 5
- 239000000843 powder Substances 0.000 description 5
- 239000004568 cement Substances 0.000 description 4
- 238000013461 design Methods 0.000 description 3
- 238000010586 diagram Methods 0.000 description 3
- 239000002893 slag Substances 0.000 description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 3
- 239000011230 binding agent Substances 0.000 description 2
- 239000010881 fly ash Substances 0.000 description 2
- 239000007789 gas Substances 0.000 description 2
- 238000005259 measurement Methods 0.000 description 2
- 238000002156 mixing Methods 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 235000019738 Limestone Nutrition 0.000 description 1
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 1
- 229910000831 Steel Inorganic materials 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 239000003245 coal Substances 0.000 description 1
- 239000002131 composite material Substances 0.000 description 1
- 239000008358 core component Substances 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000005429 filling process Methods 0.000 description 1
- 238000000227 grinding Methods 0.000 description 1
- 229910052500 inorganic mineral Inorganic materials 0.000 description 1
- 239000006028 limestone Substances 0.000 description 1
- 239000011707 mineral Substances 0.000 description 1
- 239000004570 mortar (masonry) Substances 0.000 description 1
- 239000011148 porous material Substances 0.000 description 1
- 230000008092 positive effect Effects 0.000 description 1
- -1 pozzolanic admixture Substances 0.000 description 1
- 239000004576 sand Substances 0.000 description 1
- 229910021487 silica fume Inorganic materials 0.000 description 1
- 239000010959 steel Substances 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N9/00—Investigating density or specific gravity of materials; Analysing materials by determining density or specific gravity
- G01N9/02—Investigating density or specific gravity of materials; Analysing materials by determining density or specific gravity by measuring weight of a known volume
- G01N9/04—Investigating density or specific gravity of materials; Analysing materials by determining density or specific gravity by measuring weight of a known volume of fluids
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Abstract
本发明属于材料技术检测技术领域,公开了一种胶凝材料浆体表观密度快速测试装置,包括取样器、测量瓶和磨口瓶塞;所述取样器设置有移浆筒;所述移浆筒外侧套接有多个防摆橡胶圈,可以避免移浆筒在与测量瓶配套使用时发生摆动;所述移浆筒套接有活塞推杆;所述活塞推杆一端套接有移浆活塞;所述活塞推杆另一端一体设置有活塞手柄,所述测量瓶外侧刻设有刻度,所述磨口瓶塞的外侧直径与测量瓶的内侧直径相同,使得磨口瓶塞可以塞入测量瓶的开口内。本发明结构简单,成本低,可有效地被用于测试不同种类胶凝材料浆体的表观密度,测试过程简单、方便快捷。
The invention belongs to the technical field of material technology detection, and discloses a rapid testing device for the apparent density of gelatinous material slurry, which includes a sampler, a measuring bottle and a ground cork; the sampler is provided with a slurry transfer cylinder; There are multiple anti-swing rubber rings on the outside of the slurry cylinder, which can prevent the slurry displacement cylinder from swinging when it is used with the measuring bottle; the displacement cylinder is sleeved with a piston push rod; one end of the piston push rod is sleeved with a displacement pulp piston; the other end of the piston push rod is integrally provided with a piston handle, the outside of the measuring bottle is engraved with a scale, and the outer diameter of the ground cork is the same as the inner diameter of the measuring bottle, so that the ground cork can be plugged into the opening of the measuring bottle. The invention has simple structure and low cost, can be effectively used to test the apparent density of different kinds of cementitious material slurries, and the testing process is simple, convenient and quick.
Description
技术领域technical field
本发明属于材料技术检测技术领域,尤其涉及一种胶凝材料浆体表观密度快速测试装置。The invention belongs to the technical field of material technology detection, and in particular relates to a rapid testing device for apparent density of cementitious material slurry.
背景技术Background technique
目前,业内常用的现有技术是这样的:At present, the existing technologies commonly used in the industry are as follows:
胶凝材料作为多孔混凝土的核心组成部分,其浆体的表观密度是多孔混凝土配合比设计的关键指标。胶凝材料用量、浆体对多孔混凝土孔隙的填塞程度与多孔混凝土的孔隙率有着密切的关系,而浆体的表观密度直接影响着胶凝材料用量的大小、水胶比的确定以及拌合物的工作状态。对工作性能良好的胶凝材料浆体表观密度进行准确测试,保证胶凝材料用量以及浆体对砂石骨料的有效包裹和粘结,才能得到孔隙率和力学性能最佳的多孔混凝土结构。The cementitious material is the core component of porous concrete, and the apparent density of its slurry is a key index for the design of the mix ratio of porous concrete. The amount of cementitious material, the filling degree of the slurry to the pores of the porous concrete are closely related to the porosity of the porous concrete, and the apparent density of the slurry directly affects the amount of the cementitious material, the determination of the water-binder ratio and the mixing process. working state of the thing. Accurately test the apparent density of the cementitious material slurry with good working performance to ensure the amount of cementitious material and the effective wrapping and bonding of the slurry to the sand and gravel aggregate, in order to obtain a porous concrete structure with the best porosity and mechanical properties .
目前,现有技术中关于胶凝材料浆体表观密度的确定,一种方法是采用理论计算的方法,即通过测定组成胶凝材料浆体的各物料真密度,结合各物料的占比情况等已知条件直接计算混合物浆体密度。由于需要事先获取各类物料的真密度,除了实际操作耗时繁琐外,一方面增加了配合比设计的难度,一方面也降低了配合比设计的及时性和应变性。另一种方法是参考砂浆表观密度测试的方法,即测试固定体积容器中的浆体质量,再根据公式计算获得浆体表观密度。但一方面受浆体稠度影响,装料过程中裹挟的气体难于通过敲击排出,另一方面由于容器开口面积大,浆体试样需求量大,具体测试操作上存在一定难度,且这一方法测试的数值精确度欠佳。At present, in the prior art, one method for determining the apparent density of cementitious material slurry is to adopt a theoretical calculation method, that is, by measuring the true density of each material that makes up the cementitious material slurry, combined with the proportion of each material Calculate the slurry density of the mixture directly under known conditions. Due to the need to obtain the true density of various materials in advance, in addition to the time-consuming and cumbersome actual operation, on the one hand, it increases the difficulty of mix ratio design, and on the other hand, it also reduces the timeliness and adaptability of mix ratio design. Another method is to refer to the method of mortar apparent density test, that is, to test the mass of slurry in a fixed volume container, and then calculate the apparent density of slurry according to the formula. However, on the one hand, due to the influence of the slurry consistency, it is difficult to discharge the gas trapped in the filling process by knocking; on the other hand, due to the large opening area of the container, the demand for slurry samples is large, and there are certain difficulties in the specific test operation. The numerical precision of the method test is poor.
因此,研制一种能简单、有效、快速地测试胶凝材料浆体表观密度的装置,减少繁琐的测试过程,意义深远。Therefore, it is of far-reaching significance to develop a device that can simply, effectively and quickly test the apparent density of cementitious material slurry and reduce the tedious testing process.
综上所述,现有技术存在的问题是:In summary, the problems in the prior art are:
装料过程中裹挟的气体难于通过敲击排出,具体测试操作上存在一定难度,测试的数值精确度欠佳。The gas entrapped in the charging process is difficult to be discharged by knocking, and there are certain difficulties in the specific test operation, and the accuracy of the test value is not good.
解决上述技术问题的难度和意义:The difficulty and significance of solving the above technical problems:
难度在于受浆体稠度影响,另一方面由于容器开口面积大,浆体试样需求量大;意义在于可快速有效的对胶凝材料的表观密度进行检测,减少繁琐的测试过程。The difficulty lies in the influence of the consistency of the slurry. On the other hand, due to the large opening area of the container, the demand for slurry samples is large; the significance lies in the fact that the apparent density of the gelled material can be detected quickly and effectively, reducing the tedious testing process.
发明内容Contents of the invention
针对现有技术存在的问题,本发明提供了一种胶凝材料浆体表观密度快速测试装置。Aiming at the problems existing in the prior art, the invention provides a rapid testing device for the apparent density of cementitious material slurry.
本发明是这样实现的,一种胶凝材料浆体表观密度快速测试装置,包括取样器、测量瓶和磨口瓶塞;The present invention is achieved in this way, a quick testing device for the apparent density of cementitious material slurry, comprising a sampler, a measuring bottle and a ground cork;
所述取样器设置有移浆筒;The sampler is provided with a slurry transfer cylinder;
所述移浆筒外侧套接有多个防摆橡胶圈,可以避免移浆筒在与测量瓶配套使用时发生摆动;A plurality of anti-sway rubber rings are sleeved on the outside of the slurry transfer tube, which can prevent the slurry transfer tube from swinging when it is used in conjunction with the measuring bottle;
所述移浆筒套接有活塞推杆,活塞推杆长度略长于移浆筒长度;The pulp-moving cylinder is sleeved with a piston push rod, and the length of the piston push rod is slightly longer than the length of the pulp-moving cylinder;
所述活塞推杆一端套接有移浆活塞;One end of the piston push rod is sleeved with a slurry moving piston;
所述活塞推杆另一端一体设置有活塞手柄,活塞手柄直径略大于移浆筒外径。The other end of the piston push rod is integrally provided with a piston handle, and the diameter of the piston handle is slightly larger than the outer diameter of the slurry transfer cylinder.
进一步,所述测量瓶外侧刻设有刻度。Further, a scale is engraved on the outside of the measuring bottle.
进一步,所述磨口瓶塞的外侧直径与测量瓶的内侧直径相同,磨口瓶塞规格与测量瓶磨口相匹配,使得磨口瓶塞可以塞入测量瓶的开口内,并能密封良好。Further, the outer diameter of the ground cork is the same as the inner diameter of the measuring bottle, and the specification of the ground cork matches the grinding port of the measuring bottle, so that the ground cork can be inserted into the opening of the measuring bottle and can be sealed well .
本发明的另一目的在于提供一种所述胶凝材料浆体表观密度快速测试装置的胶凝材料浆体表观密度快速测试方法,所述胶凝材料浆体表观密度快速测试方法包括:将煤油注入干燥的测量瓶中,将磨口瓶塞塞入测量瓶中,在相同的环境温度下静置5分钟,记录液面高度h0,拔出磨口瓶塞,并称量煤油和测量瓶的质量;用取样器抽取需要检测表观密度的胶凝材料浆体,注入测量瓶的煤油中,塞好磨口瓶塞,轻轻摇晃测量瓶使受表面张力和压差影响裹附于浆体表面的气泡排出,在相同的环境温度下静置5分钟,记录液面高度h1,并称量胶凝材料浆体、煤油和测量瓶的总质量。Another object of the present invention is to provide a rapid testing method for the apparent density of the gelling material slurry of the rapid testing device for the apparent density of the gelling material slurry, the rapid testing method for the apparent density of the gelling material slurry includes : Pour kerosene into a dry measuring bottle, insert the ground cork into the measuring bottle, let stand at the same ambient temperature for 5 minutes, record the liquid level h 0 , pull out the ground cork, and weigh the kerosene and measure the quality of the bottle; use a sampler to extract the gelatinous material slurry that needs to be tested for apparent density, inject it into the kerosene in the measuring bottle, plug the ground stopper, and gently shake the measuring bottle to make it wrapped under the influence of surface tension and pressure difference. The air bubbles attached to the surface of the slurry are discharged, and stand at the same ambient temperature for 5 minutes, record the height h 1 of the liquid level, and weigh the total mass of the gelling material slurry, kerosene and the measuring bottle.
进一步,所述胶凝材料浆体表观密度的计算方法:Further, the calculation method of the apparent density of the cementitious material slurry:
其中:M0为煤油和测量瓶的总质量,M1为煤油、胶凝材料浆体试样和测量瓶的总质量,h0为未注入胶凝材料浆体时测量瓶中煤油液面高度,h1为注入胶凝材料浆体后测量瓶中煤油液面高度,D为测量瓶的瓶颈内壁直径。Among them: M 0 is the total mass of kerosene and measuring bottle, M 1 is the total mass of kerosene, cementitious material slurry sample and measuring bottle, h 0 is the height of kerosene liquid level in the measuring bottle when the cementitious material slurry is not injected , h 1 is the height of the kerosene liquid level in the measured bottle after injecting the cementitious material slurry, and D is the diameter of the inner wall of the neck of the measured bottle.
综上所述,本发明的优点及积极效果为:In summary, the advantages and positive effects of the present invention are:
设置有多个防摆橡胶圈,可以避免移浆筒在与测量瓶配套使用时发生摆动;本发明结构简单,成本低,可有效地被用于测试不同种类胶凝材料浆体的表观密度,测试过程简单、方便快捷。Multiple anti-swing rubber rings are provided to prevent the slurry transfer cylinder from swinging when it is used in conjunction with the measuring bottle; the invention has a simple structure and low cost, and can be effectively used to test the apparent density of different types of gelling material slurries , The test process is simple, convenient and quick.
将水泥或水泥+掺合料在不同水胶比下拌制成浆,分别按固定体积容器测试方法(方法1)和本发明测试方法(方法2)分3次测试同一浆体表观密度,数据见下表。其中,水泥密度为3.130×103kg/m3,矿粉密度为2.870×103kg/m3,硅灰密度为2.210×103kg/m3,水密度为0.998×103kg/m3,外加剂密度为1.092×103kg/m3。Mix cement or cement+admixture under different water-binder ratios to make slurry, test the same slurry apparent density for 3 times according to the fixed volume container test method (method 1) and the test method of the present invention (method 2) respectively, See the table below for the data. Among them, the density of cement is 3.130×10 3 kg/m 3 , the density of mineral powder is 2.870×10 3 kg/m 3 , the density of silica fume is 2.210×10 3 kg/m 3 , and the density of water is 0.998×10 3 kg/m 3 3. The density of the admixture is 1.092×10 3 kg/m 3 .
从上述实验数据可以看出,方法2相较于方法1,规避了测试操作过程中浆体裹挟引入额外空气不能彻底排出而导致的误差,3个测试值之间的波动小,测试结果更为稳定,更接近于理论计算值,更能反映胶凝材料制备成浆体后表观密度的真实情况。It can be seen from the above experimental data that method 2, compared with method 1, avoids the error caused by the introduction of additional air that cannot be completely discharged during the test operation. The fluctuation between the three test values is small, and the test results are more accurate. It is stable, closer to the theoretical calculation value, and can better reflect the real situation of the apparent density of the cementitious material after it is prepared into a slurry.
附图说明Description of drawings
图1是本发明实施例提供的胶凝材料浆体表观密度快速测试装置取样器结构示意图;Fig. 1 is the schematic diagram of the structure of the sampler of the cementitious material slurry apparent density rapid testing device provided by the embodiment of the present invention;
图2是本发明实施例提供的胶凝材料浆体表观密度快速测试装置磨口瓶塞结构示意图;Fig. 2 is a schematic diagram of the structure of the ground cork of the rapid testing device for the apparent density of the cementitious material slurry provided by the embodiment of the present invention;
图3是本发明实施例提供的胶凝材料浆体表观密度快速测试装置测量瓶结构示意图;Fig. 3 is a schematic diagram of the structure of the measuring bottle of the rapid testing device for the apparent density of the cementitious material slurry provided by the embodiment of the present invention;
图中:1、磨口瓶塞;2、测量瓶;3、刻度;4、防摆橡胶圈;5、活塞推杆;6、活塞手柄;7、移浆活塞;8、移浆筒;9、取样器。In the figure: 1. Ground bottle stopper; 2. Measuring bottle; 3. Scale; 4. Anti-swing rubber ring; 5. Piston push rod; 6. Piston handle; , Sampler.
具体实施方式Detailed ways
为能进一步了解本发明的发明内容、特点及功效,兹例举以下实施例,并配合附图详细说明如下。In order to further understand the content, features and effects of the present invention, the following examples are given, and detailed descriptions are given below with reference to the accompanying drawings.
如图1-3所示,本发明实施例提供的胶凝材料浆体表观密度快速测试装置设置有磨口瓶塞1、测量瓶2、刻度3、防摆橡胶圈4、活塞推杆5、活塞手柄6、移浆活塞7、移浆筒8和取样器9。As shown in Figures 1-3, the rapid testing device for the apparent density of cementitious material slurry provided by the embodiment of the present invention is provided with a ground bottle stopper 1, a measuring bottle 2, a scale 3, an anti-swing rubber ring 4, and a piston push rod 5 , a piston handle 6, a slurry-moving piston 7, a slurry-moving cylinder 8 and a sampler 9.
取样器9设置有移浆筒8,移浆筒8外侧套接有多个防摆橡胶圈4,移浆筒8套接有活塞推杆5,活塞推杆5一端套接有移浆活塞7,活塞推杆5另一端一体设置有活塞手柄6,测量瓶2外侧刻设有刻度3,磨口瓶塞1的外侧直径与测量瓶2的内侧直径相同。The sampler 9 is provided with a slurry-moving cylinder 8, and a plurality of anti-sway rubber rings 4 are sleeved on the outside of the slurry-moving cylinder 8. The slurry-moving cylinder 8 is socketed with a piston push rod 5, and one end of the piston push rod 5 is socketed with a slurry-moving piston 7. , the other end of the piston push rod 5 is integrally provided with a piston handle 6, the outside of the measuring bottle 2 is engraved with a scale 3, and the outside diameter of the ground cork 1 is the same as the inside diameter of the measuring bottle 2.
实施例:Example:
本实施例所采用的胶凝材料为硅酸盐水泥、普通硅酸盐水泥、矿渣硅酸盐水泥、火山灰质硅酸盐水泥、粉煤灰硅酸盐水泥、复合硅酸盐水泥以及上述水泥与粉煤灰、火山灰质混合材、石灰石粉、矿渣粉、钢渣粉或煤矸石粉等一种或几种辅助胶凝材料混合的混合物。The cementitious materials used in this example are Portland cement, ordinary Portland cement, slag Portland cement, pozzolanic Portland cement, fly ash Portland cement, composite Portland cement and the above cements It is a mixture mixed with one or more auxiliary cementitious materials such as fly ash, pozzolanic admixture, limestone powder, slag powder, steel slag powder or coal gangue powder.
胶凝材料浆体试样为上述胶凝材料与水或与水和外加剂充分混合搅拌制成的浆体。The gelling material slurry sample is a slurry made by thoroughly mixing and stirring the above-mentioned gelling material with water or with water and an additive.
将一定量的煤油注入干燥的测量瓶2中,将磨口瓶塞1塞入测量瓶2中,在相同的环境温度下静置5分钟,记录液面高度h0,拔出磨口瓶塞1,并称量煤油和测量瓶2的质量;用取样器9抽取一定量的需要检测表观密度的胶凝材料浆体,迅速注入测量瓶2的煤油中,保证胶凝材料浆体不粘附于测量瓶2内壁,且保证取样器9始终不与煤油液面相接触,塞好磨口瓶塞1,轻轻摇晃测量瓶2使受表面张力和压差影响裹附于浆体表面的气泡排出,在相同的环境温度下静置5分钟,记录液面高度h1(改为h1),并称量胶凝材料浆体、煤油和测量瓶2的总质量。Pour a certain amount of kerosene into the dry measuring bottle 2, insert the ground cork 1 into the measuring bottle 2, let it stand for 5 minutes at the same ambient temperature, record the liquid level h 0 , and pull out the ground cork 1, and weigh the quality of kerosene and measuring bottle 2; extract a certain amount of cementitious material slurry that needs to detect apparent density with sampler 9, and quickly inject it into the kerosene in measuring bottle 2 to ensure that the cementitious material slurry is not sticky Attached to the inner wall of the measuring bottle 2, and ensure that the sampler 9 is never in contact with the kerosene liquid surface, plug the ground cork 1, and gently shake the measuring bottle 2 to make the sampler 9 attached to the surface of the slurry affected by the surface tension and pressure difference The air bubbles are discharged, and stand at the same ambient temperature for 5 minutes, record the liquid level height h1 (change to h 1 ), and weigh the total mass of the gelling material slurry, kerosene and measuring bottle 2.
胶凝材料浆体表观密度的计算方法如下所示:The calculation method for the apparent density of cementitious material slurry is as follows:
其中:M0为煤油和测量瓶2的总质量,M1为煤油、胶凝材料浆体试样和测量瓶2的总质量,h0为未注入胶凝材料浆体时测量瓶2中煤油液面高度,h1为注入胶凝材料浆体后测量瓶2中煤油液面高度,D为测量瓶2的瓶颈内壁直径。Among them: M 0 is the total mass of kerosene and measuring bottle 2, M 1 is the total mass of kerosene, cementitious material slurry sample and measuring bottle 2, h 0 is the kerosene in measuring bottle 2 when the cementitious material slurry is not injected The height of the liquid level, h1 is the height of the kerosene liquid level in the measurement bottle 2 after injecting the cementitious material slurry, and D is the diameter of the inner wall of the neck of the measurement bottle 2.
以上所述仅是对本发明的较佳实施例而已,并非对本发明作任何形式上的限制,凡是依据本发明的技术实质对以上实施例所做的任何简单修改,等同变化与修饰,均属于本发明技术方案的范围内。The above descriptions are only preferred embodiments of the present invention, and are not intended to limit the present invention in any form. Any simple modifications made to the above embodiments according to the technical essence of the present invention, equivalent changes and modifications, all belong to this invention. within the scope of the technical solution of the invention.
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