CN108373864A - A kind of High Performance Corrosion Protective Coatings and preparation method thereof - Google Patents
A kind of High Performance Corrosion Protective Coatings and preparation method thereof Download PDFInfo
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Abstract
The invention belongs to paint fields, and in particular to a kind of High Performance Corrosion Protective Coatings and preparation method thereof, which is made of following raw material in parts by weight：25~32 parts of modified Nano activated carbon, 18~25 parts of white oil, 15~21 parts of modified zeolite powder, 1~2 part of rilanit special, 6~10 parts attapulgite modified, 5~8 parts of pumice sand, 2~4 parts of polyisobutene, 4~6 parts of modified alta-mud, 3~5 parts of polyvinyl alcohol, 3~4 parts of zinc chromate.High Performance Corrosion Protective Coatings antiseptic property of the present invention is excellent, term of validity limit for length, can be applied to the equipment anticorrosion under the conditions of aviation, ocean and other extreme environments.
Description
It is on October 21st, 2015 that the application, which is the applying date, entitled " a kind of application No. is 201510697546.1
The divisional application of the patent of High Performance Corrosion Protective Coatings and preparation method thereof ".
Technical field
The invention belongs to paint fields, and in particular to a kind of High Performance Corrosion Protective Coatings and preparation method thereof.
Background technology
In recent years, anticorrosive paint has become the important fresh combatants of paint field, is played in the development of the national economy more next
Bigger effect, development prospect are considerable.It is analyzed according to expert personage：Anticorrosive paint price is in obviously and rises to take advantage of a favourable situation now,
This is related in the application of ocean or aviation etc. with it.In recent years, each state all provided aviation and ocean in continuous increase
The dynamics of investment in source, since its environment is extreme, the surface corrosion of device therefor is very fast, this not only influences operational safety, returns
Repair and maintenance work bring very big burden, while bringing high maintenance cost, and reduce the length of service of equipment.
And existing anticorrosive paint is mostly formed by combining by base oil, antirust agent, antioxidant and macromolecule copolymer resin,
Easy and carbon deposit, dust etc. are mixed to form grease in use, to weaken the resistance to corrosion, in addition, extreme warm
Corrosion-inhibiting coating is also easy failure under the influence of the factors such as degree, illumination, moisture, to lose the corrosion protection to equipment.
In conclusion the preservative treatment of equipment surface becomes the previous problem urgently to be resolved hurrily of mesh under extreme condition.Tradition
Product gradually improves perfect, new product and constantly researches and develops appearance, to adapt to standard new in anticorrosion market and environmental regulation development
With require, it is still necessary to proactive, Continuous Innovation.
Invention content
In view of the above-mentioned problems, the present invention provides a kind of High Performance Corrosion Protective Coatings, antiseptic property is excellent, term of validity limit for length,
It can be applied to the equipment anticorrosion under the conditions of aviation, ocean and other extreme environments.
To solve the above problems, the invention is realized by the following technical scheme：
A kind of High Performance Corrosion Protective Coatings are made of the raw material of following parts by weight：25~32 parts of modified Nano activated carbon, white oil 18~
25 parts, it is 15~21 parts of modified zeolite powder, 1~2 part of rilanit special, 6~10 parts attapulgite modified, 5~8 parts of pumice sand, poly-
2~4 parts of isobutene, 4~6 parts of modified alta-mud, 3~5 parts of polyvinyl alcohol, 3~4 parts of zinc chromate.
According to above-mentioned High Performance Corrosion Protective Coatings, preferably it is made of the raw material of following parts by weight：Modified Nano activated carbon 28
Part, 21 parts of white oil, 18 parts of modified zeolite powder, 1.5 parts of rilanit special, 8 parts attapulgite modified, 6 parts of pumice sand, polyisobutene
3 parts, 5 parts of modified alta-mud, 4 parts of polyvinyl alcohol, 3.5 parts of zinc chromate.
According to above-mentioned High Performance Corrosion Protective Coatings, the attapulgite is made of following steps：
Attapulgite is submerged with deionized water, and suitable NaCl is added, after mixing, be ultrasonically treated 8 minutes, surpasses
Frequency of sound wave is 50KHz, then filters, dries, obtains attapulgite modified；Between the attapulgite, deionized water, NaCl
Weight ratio be 1：8：0.06.
This method generates violent energy by the cavitation of high-frequency ultrasonic, can not only sodium ion be sent into concave convex rod
The inner passage of soil（Sodium ion）, moreover it is possible to attapulgite's surface adhesion ingredient is removed, is avoided to bringing excessive impurity in coating into.
After this method will be attapulgite modified, make its surface that there is abundant anticorrosion functional group, and the specific surface area with bigger, make
Cross-linked structure is very fine and close in coating, further improves its antiseptic property.
According to above-mentioned High Performance Corrosion Protective Coatings, the modified Nano activated carbon is made of following steps：
（1）It after active carbon nanoparticles are sieved, is washed with water to remove its surface floating dust and impurity, until cleaning solution pH is 6~7；
（2）By gained active carbon nanoparticles and phosphoric acid solution with weight ratio 1：3 are uniformly mixed, and then, 18h are impregnated under room temperature, described
The mass percent concentration of phosphoric acid solution is 25%；
（3）Soak is separated by solid-liquid separation, the dry solid material of gained to get.
The present invention is modified active carbon nanoparticles using the phosphoric acid solution of certain concentration, and phosphoric acid is finally with the shape of metaphosphoric acid
Formula is trapped in active carbon nanoparticles, can not only reduce the pH value of active carbon nanoparticles, and activated carbon can also be made to generate abundanter hole
Structure contributes to the improvement of activated carbon structure and the generation of surface acidity functional group, and can be formed in a solvent with metal ion
Stablize absorption, to enhance fixed function of the activated carbon to inorganic pigment molecule.
According to above-mentioned High Performance Corrosion Protective Coatings, the modified zeolite powder is made of following steps：
（1）By a certain amount of zeolite powder to be modified with stirring at low speed（400 revs/min）3 minutes, then with high-speed stirred（800 revs/min）
10 minutes；
（2）Gamma-aminopropyl-triethoxy-silane and acetone are weighed respectively by the 0.5% of zeolite powder weight, 0.4%, and the two is mixed
It is added in zeolite powder after uniformly, with stirring at low speed（400 revs/min）3 minutes, then with high-speed stirred（800 revs/min）16 minutes；With
Particle dispersion, mobility are improved, bubble can be excluded when as coating raw material, keeps surface smooth, improves its insulation performance；
（3）Stearic acid is added by the 0.1% of zeolite powder weight, with high-speed stirred（800 revs/min）5 minutes, it is outstanding to further increase it
Floating, dispersion performance to get.Modification of the present invention is conducive to the affine of zeolite powder and macromolecule raw material, and zeolite powder is made to be more easy to
It suspends in dispersion.
There is modified zeolite powder obtained by this method unique lattice-like structure, internal void to have huge inner surface energy；
Pumice sand is a kind of porous extrusive igneous rocks, and pore volume accounts for 50% of rock or more, and zeolite powder and pumice sand rise in coating
To Water storage, the surface checking under extreme condition is prevented, plays interior maintenance action.
According to above-mentioned High Performance Corrosion Protective Coatings, the modified alta-mud is prepared from the following steps：
Bentonite raw ore is soaked in the NaOH aqueous solutions of mass concentration 20% after 6h, is filtered, then with acrylic acid, carboxylic first
Base cellulose, the mixing of N-N methylene-bisacrylamides, ball milling 2h in the ball mill after mixing are that means promote suction using ball-milling method
The insertion of water soluble acrylic acid and carboxymethyl cellulose between bentonite bed, is then added initiator ammonium persulfate, in 60 DEG C of water-baths
Middle heating 0.5h makes acrylic acid and carboxymethyl cellulose polymerize in bentonite structure interlayer, finally in 65 DEG C of vacuum drying chambers
It dry, pulverize to 150 mesh to get the modified alta-mud with nano composite structure.The bentonite raw ore, acrylic acid, carboxylic first
Weight ratio between base cellulose, N-N methylene-bisacrylamides, ammonium persulfate is 600：100：100：0.04：4, acrylic acid
Insertion with carboxymethyl cellulose simultaneously polymerize in situ, and the amount of heat released when using polymerization overcomes the library between bentonite bed
Logical sequence power makes bentonite generate splitting, and gained modified alta-mud water absorbent rate reaches 265g/g, when significantly extending the holding of moisture
Between.
Polyisobutene the model PB2400 or PB2300, are remarkably improved the weatherability of coating, meet extreme condition
Under performance.Zinc chromate can increase the antirust, anti-corrosion, heat-resisting function of material.Polyvinyl alcohol used is the poly- second of low polymerization degree
Enol, with excellent adhering, and its solution is easy film forming, and has unique strong adherence after forming a film, epithelium flexibility, puts down
Water resistance under slip, solvent resistance, protecting colloid, wearability and extreme condition.
The preparation method of the High Performance Corrosion Protective Coatings, includes the following steps：
（1）The white oil, rilanit special, polyisobutene and polyvinyl alcohol are added to the container, with 400 revs/min of stirring at low speed 5
Minute；
（2）The attapulgite modified, modified alta-mud, modified zeolite powder, pumice sand, modified Nano activated carbon are added, is mixed
It is fitted into ball milling 3h in ball mill after even；
（3）Finally, the zinc chromate is added, with 400 revs/min of stirring at low speed 30 minutes to get.
The positive beneficial effect of the present invention：
High Performance Corrosion Protective Coatings design science of the present invention assembles rationally, and antiseptic property is excellent, term of validity limit for length, thermal coefficient
It is low, it can be applied to the equipment anticorrosion under the conditions of aviation, ocean and other extreme environments.
Specific implementation mode
In order to make the purpose , technical scheme and advantage of the present invention be clearer, below in conjunction with specific embodiment, to this
Invention is further described.It should be appreciated that the specific embodiments described herein are merely illustrative of the present invention, it is not used to
Limit the present invention.
Embodiment 1
The present embodiment High Performance Corrosion Protective Coatings are made of the raw material of following parts by weight：28 parts of modified Nano activated carbon, white oil 21
Part, 8 parts attapulgite modified, 6 parts of pumice sand, 3 parts of polyisobutene, is modified 18 parts of modified zeolite powder, 1.5 parts of rilanit special
5 parts of bentonite, 4 parts of polyvinyl alcohol, 3.5 parts of zinc chromate, 1 part of pigment.
Wherein, attapulgite modified to be made of following steps：Attapulgite is submerged with deionized water, and is added suitable
NaCl, after mixing, carry out be ultrasonically treated 8 minutes, ultrasonic frequency 50KHz, then filter, dry to get；It is described recessed
Weight ratio between convex stick soil, deionized water, NaCl is 1：8：0.06.
The modified Nano activated carbon is made of following steps：
（1）It after active carbon nanoparticles are sieved, is washed with water to remove its surface floating dust and impurity, until cleaning solution pH is 6~7；
（2）By gained active carbon nanoparticles and phosphoric acid solution with weight ratio 1：3 are uniformly mixed, and then, 18h are impregnated under room temperature, described
The mass percent concentration of phosphoric acid solution is 25%；
（3）Soak is separated by solid-liquid separation, the dry solid material of gained to get.
The modified zeolite powder is made of following steps：
（1）By a certain amount of zeolite powder to be modified with 400 revs/min of stirring at low speed 3 minutes, then divided with 800 revs/min of high-speed stirreds 10
Clock；
（2）Gamma-aminopropyl-triethoxy-silane and acetone are weighed respectively by the 0.5% of zeolite powder weight, 0.4%, and the two is mixed
It is added in zeolite powder after uniformly, with 400 revs/min of stirring at low speed 3 minutes, then with 800 revs/min of high-speed stirreds 16 minutes；
（3）Stearic acid is added by the 0.1% of zeolite powder weight, with 800 revs/min of high-speed stirreds 5 minutes to get.
The modified alta-mud is prepared from the following steps：Bentonite raw ore is soaked in the NaOH of mass concentration 20%
It in aqueous solution after 6h, is filtered, then is mixed with acrylic acid, carboxymethyl cellulose, N-N methylene-bisacrylamides, after mixing
Then initiator ammonium persulfate is added in ball milling 2h in the ball mill, 0.5h is heated in 60 DEG C of water-baths, finally dry in 65 DEG C of vacuum
It is dry in dry case, then 150 mesh are crushed to get modified alta-mud；The bentonite raw ore, acrylic acid, carboxymethyl cellulose, N-
Weight ratio between N methylene-bisacrylamides, ammonium persulfate is 600：100：100：0.04：4.
The preparation method of the High Performance Corrosion Protective Coatings, includes the following steps：
（1）The white oil, rilanit special, polyisobutene and polyvinyl alcohol are added to the container, with 400 revs/min of stirring at low speed 5
Minute；
（2）The attapulgite modified, modified alta-mud, modified zeolite powder, pumice sand, modified Nano activated carbon are added, is mixed
It is fitted into ball milling 3h in ball mill after even；
（3）Finally, the zinc chromate is added, with 400 revs/min of stirring at low speed 30 minutes to get.
Anticorrosive paint obtained by the present embodiment carries out physicochemical property test, and surfacing is without miscellaneous piece；Anti-zoned hardness 5H (GB/T
6739-2006)；Adhesion 1 grade（GB/T 1720-1979）；800 DEG C of 120h of resistance to Thermal test：Paint film is complete, does not fall off（GB/T
1735-2009）；- 70 DEG C of 120h of low temperature resistant test：Paint film is complete, does not fall off；Alkali resistance is tested（120h）：It is not blistering, it does not rise
Wrinkle, does not fall off（GB/T 9265-2009）；Acid resistance is tested（120h）：It is not blistering, it is wrinkle resistant, it does not fall off（GB/T 9265-
2009）；Ageing-resistant test（1200h）：It is not blistering, it does not fall off, flawless（GB/T 13893-2008 ）；Thermal coefficient：0.06
W/m.k (800 DEG C × 3h), 0.11w/m.k (1000 DEG C × 3h) GB/T 10297-1998.
Embodiment 2
The present embodiment is substantially the same manner as Example 1, except that the weight proportion of material composition, preparation method and embodiment
1 is identical.Raw material and its parts by weight group become：32 parts of modified Nano activated carbon, 18 parts of white oil, 21 parts of modified zeolite powder, hydrogenation castor
1 part of sesame oil, 10 parts attapulgite modified, 5 parts of pumice sand, 4 parts of polyisobutene, 4 parts of modified alta-mud, 5 parts of polyvinyl alcohol, chromic acid
3 parts of zinc, 4 parts of pigment.
Anticorrosive paint obtained by the present embodiment carries out physicochemical property test, and surfacing is without miscellaneous piece；Anti-zoned hardness 4H (GB/T
6739-2006)；2 grades of adhesive force（GB/T 1720-1979）；800 DEG C of 120h of resistance to Thermal test：Paint film is complete, does not fall off（GB/T
1735-2009）；- 70 DEG C of 120h of low temperature resistant test：Paint film is complete, does not fall off；Alkali resistance is tested（120h）：It is not blistering, it does not rise
Wrinkle, does not fall off（GB/T 9265-2009）；Acid resistance is tested（120h）：It is not blistering, it is wrinkle resistant, it does not fall off（GB/T 9265-
2009）；Ageing-resistant test（1200h）：It is not blistering, it does not fall off, flawless（GB/T 13893-2008 ）；Thermal coefficient：0.15
W/m.k (800 DEG C × 3h), 0.23w/m.k (1000 DEG C × 3h) GB/T 10297-1998.
Embodiment 3
The present embodiment is substantially the same manner as Example 1, except that the weight proportion of material composition, preparation method and embodiment
1 is identical.Raw material and its parts by weight group become：25 parts of modified Nano activated carbon, 25 parts of white oil, 15 parts of modified zeolite powder, hydrogenation castor
2 parts of sesame oil, 6 parts attapulgite modified, 8 parts of pumice sand, 2 parts of polyisobutene, 6 parts of modified alta-mud, 3 parts of polyvinyl alcohol, chromic acid
4 parts of zinc.
Anticorrosive paint obtained by the present embodiment carries out physicochemical property test, and surfacing is without miscellaneous piece；Anti-zoned hardness 4H (GB/T
6739-2006)；Adhesion 1 grade（GB/T 1720-1979）；800 DEG C of 120h of resistance to Thermal test：Paint film is complete, does not fall off（GB/T
1735-2009）；- 70 DEG C of 120h of low temperature resistant test：Paint film is complete, does not fall off；Alkali resistance is tested（120h）：It is not blistering, it does not rise
Wrinkle, does not fall off（GB/T 9265-2009）；Acid resistance is tested（120h）：It is not blistering, it is wrinkle resistant, it does not fall off（GB/T 9265-
2009）；Ageing-resistant test（1200h）：It is not blistering, it does not fall off, flawless（GB/T 13893-2008 ）；Thermal coefficient：0.19
W/m.k (800 DEG C × 3h), 0.25 w/m.k (1000 DEG C × 3h) GB/T 10297-1998.
Embodiment 4
The present embodiment is substantially the same manner as Example 1, except that the weight proportion of material composition, preparation method and embodiment
1 is identical.Raw material and its parts by weight group become：25 parts of modified Nano activated carbon, 18 parts of white oil, 15 parts of modified zeolite powder, hydrogenation castor
1 part of sesame oil, 6 parts attapulgite modified, 5 parts of pumice sand, 2 parts of polyisobutene, 4 parts of modified alta-mud, 3 parts of polyvinyl alcohol, chromic acid
3 parts of zinc.
Anticorrosive paint obtained by the present embodiment carries out physicochemical property test, and surfacing is without miscellaneous piece；Anti-zoned hardness 4H (GB/T
6739-2006)；2 grades of adhesive force（GB/T 1720-1979）；800 DEG C of 120h of resistance to Thermal test：Paint film is complete, does not fall off（GB/T
1735-2009）；- 70 DEG C of 120h of low temperature resistant test：Paint film is complete, does not fall off；Alkali resistance is tested（120h）：It is not blistering, it does not rise
Wrinkle, does not fall off（GB/T 9265-2009）；Acid resistance is tested（120h）：It is not blistering, it is wrinkle resistant, it does not fall off（GB/T 9265-
2009）；Ageing-resistant test（1200h）：It is not blistering, it does not fall off, flawless（GB/T 13893-2008 ）；Thermal coefficient：
0.14w/m.k (800 DEG C × 3h), 0.18 w/m.k (1000 DEG C × 3h) GB/T 10297-1998.
Embodiment 5
The present embodiment is substantially the same manner as Example 1, except that the weight proportion of material composition, preparation method and embodiment
1 is identical.Raw material and its parts by weight group become：32 parts of modified Nano activated carbon, 25 parts of white oil, 21 parts of modified zeolite powder, hydrogenation castor
2 parts of sesame oil, 10 parts attapulgite modified, 8 parts of pumice sand, 4 parts of polyisobutene, 6 parts of modified alta-mud, 5 parts of polyvinyl alcohol, chromic acid
4 parts of zinc, 2 parts of pigment.
Anticorrosive paint obtained by the present embodiment carries out physicochemical property test, and surfacing is without miscellaneous piece；Anti-zoned hardness 5H (GB/T
6739-2006)；2 grades of adhesive force（GB/T 1720-1979）；800 DEG C of 120h of resistance to Thermal test：Paint film is complete, does not fall off（GB/T
1735-2009）；- 70 DEG C of 120h of low temperature resistant test：Paint film is complete, does not fall off；Alkali resistance is tested（120h）：It is not blistering, it does not rise
Wrinkle, does not fall off（GB/T 9265-2009）；Acid resistance is tested（120h）：It is not blistering, it is wrinkle resistant, it does not fall off（GB/T 9265-
2009）；Ageing-resistant test（1200h）：It is not blistering, it does not fall off, flawless（GB/T 13893-2008 ）；Thermal coefficient：
0.11w/m.k (800 DEG C × 3h), 0.14w/m.k (1000 DEG C × 3h) GB/T 10297-1998.
Claims (7)
1. a kind of High Performance Corrosion Protective Coatings, it is characterised in that：In parts by weight, it is made of following raw material：Modified Nano activated carbon
25~32 parts, 18~25 parts of white oil, 15~21 parts of modified zeolite powder, 1~2 part of rilanit special, attapulgite modified 6~10
Part, 5~8 parts of pumice sand, 2~4 parts of polyisobutene, 4~6 parts of modified alta-mud, 3~5 parts of polyvinyl alcohol, 3~4 parts of zinc chromate；
The modified zeolite powder is made of following steps：
（1）By a certain amount of zeolite powder to be modified with 400 revs/min of stirring at low speed 3 minutes, then divided with 800 revs/min of high-speed stirreds 10
Clock；
（2）Gamma-aminopropyl-triethoxy-silane and acetone are weighed respectively by the 0.5% of zeolite powder weight, 0.4%, and the two is mixed
It is added in zeolite powder after uniformly, with 400 revs/min of stirring at low speed 3 minutes, then with 800 revs/min of high-speed stirreds 16 minutes；
（3）Stearic acid is added by the 0.1% of zeolite powder weight, with 800 revs/min of high-speed stirreds 5 minutes to get.
2. High Performance Corrosion Protective Coatings according to claim 1, it is characterised in that：In parts by weight, it is made of following raw material：
It is 28 parts of modified Nano activated carbon, 21 parts of white oil, 18 parts of modified zeolite powder, 1.5 parts of rilanit special, 8 parts attapulgite modified, floating
6 parts of stone sand, 3 parts of polyisobutene, 5 parts of modified alta-mud, 4 parts of polyvinyl alcohol, 3.5 parts of zinc chromate.
3. High Performance Corrosion Protective Coatings according to claim 1 or 2, which is characterized in that described attapulgite modified by following
Step is made：
Attapulgite is submerged with deionized water, and suitable NaCl is added, after mixing, be ultrasonically treated 8 minutes, surpasses
Frequency of sound wave is 50KHz, then filter, dry to get；Weight ratio between the attapulgite, deionized water, NaCl is 1：
8：0.06.
4. High Performance Corrosion Protective Coatings according to claim 1 or 2, which is characterized in that the modified Nano activated carbon by with
Lower step is made：
（1）It after active carbon nanoparticles are sieved, is washed with water to remove its surface floating dust and impurity, until cleaning solution pH is 6~7；
（2）By gained active carbon nanoparticles and phosphoric acid solution with weight ratio 1：3 are uniformly mixed, and then, 18h are impregnated under room temperature, described
The mass percent concentration of phosphoric acid solution is 25%；
（3）Soak is separated by solid-liquid separation, the dry solid material of gained to get.
5. High Performance Corrosion Protective Coatings according to claim 1 or 2, which is characterized in that the modified alta-mud is by following step
Suddenly it is prepared：
Bentonite raw ore is soaked in the NaOH aqueous solutions of mass concentration 20% after 6h, is filtered, then with acrylic acid, carboxylic first
Then initiator persulfuric acid is added in base cellulose, the mixing of N-N methylene-bisacrylamides, ball milling 2h in the ball mill after mixing
Ammonium heats 0.5h in 60 DEG C of water-baths, finally dry in 65 DEG C of vacuum drying chambers, then is crushed to 150 mesh to get bentone
Soil；Weight between the bentonite raw ore, acrylic acid, carboxymethyl cellulose, N-N methylene-bisacrylamides, ammonium persulfate
Than being 600：100：100：0.04：4.
6. High Performance Corrosion Protective Coatings according to claim 1 or 2, it is characterised in that：The polyisobutene model
PB2400 or PB2300, the polyvinyl alcohol are polyvinyl alcohol with low degree of polymerization.
7. the preparation method of High Performance Corrosion Protective Coatings, includes the following steps described in a kind of claims 1 or 2：
（1）The white oil, rilanit special, polyisobutene and polyvinyl alcohol are added to the container, with 400 revs/min of stirring at low speed 5
Minute；
（2）The attapulgite modified, modified alta-mud, modified zeolite powder, pumice sand, modified Nano activated carbon are added, is mixed
It is fitted into ball milling 3h in ball mill after even；
（3）Finally, the zinc chromate is added, with 400 revs/min of stirring at low speed 30 minutes to get.
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| CN105153936A (en) | 2015-12-16 |
| CN105153936B (en) | 2018-04-17 |
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