CN108371640A - A kind of mock-strawberry oral nursing liquid and preparation method thereof - Google Patents
A kind of mock-strawberry oral nursing liquid and preparation method thereof Download PDFInfo
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- CN108371640A CN108371640A CN201711222256.7A CN201711222256A CN108371640A CN 108371640 A CN108371640 A CN 108371640A CN 201711222256 A CN201711222256 A CN 201711222256A CN 108371640 A CN108371640 A CN 108371640A
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- water
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- stirring
- strawberry
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q11/00—Preparations for care of the teeth, of the oral cavity or of dentures; Dentifrices, e.g. toothpastes; Mouth rinses
Abstract
The invention belongs to filed of daily-use chemical industry, and in particular to a kind of mock-strawberry oral nursing liquid and preparation method thereof.Including K12 0.3% 0.6%, mock-strawberry extracting solution 1% 5.2%, steviol glycoside 0.5% 0.8%, coolant agent WS 23 0.01% 0.08%, glycerine 1% 6%, edible ethanol 2% 6%, RH 60 1% 4%, sorbierite 1.1% 2.6%, 0.02% 0.06% essence of vitamin C 0.1% 0.25%, excess water.Mock-strawberry oral nursing liquid preparation method, includes the following steps：(1) pre-treatment of raw material；(2) water phase stirs；(3) preparation of oil phase；(4) stirring is mixed.Mock-strawberry oral nursing liquid produced by the invention has the effects that significant oral cleaning, antibacterial, plays good nursing efficacy, is different from the formula and preparation method of traditional mouth conditioning liquid, and new open one's minds is provided for the same industry.
Description
Technical field
The invention belongs to filed of daily-use chemical industry, are related to a kind of suitable common oral care health care, and in particular to a kind of mock-strawberry
Oral nursing liquid and preparation method thereof.
Background technology
People have generally formed the custom brushed teeth sooner or later, but primary two minutes processes of brushing teeth can not be protected for a long time
Oral environment；In addition it is not appropriate for cleaning oral cavity using toothpaste in some special occasions or crowd.Oral nursing liquid is exactly
Solves this series of problems.
Further, since mouth disease caused by various pathogenic bacteria is also common frdquently encountered disease in oral cavity, directly affect people's
Health.People also already prevent the generation of mouth disease by various oral care products.Currently, in detergents and cosmetic mouth
The major product of chamber nursing can be divided into toothpaste, gargle and flavorants, these products mainly play cleaning tooth, whitening tooth
Tooth, kills the effects that oral cavity harmful bacteria, pre- anti-caries, fresh breath at removal dental plaque, while to some mouths such as such as various focusing depths represented
The treatment of chamber disease also functions to certain positive effect.
Oral nursing liquid now is existed by alcohol, water, moisturizer, fragrance, solubilizer and including various antipathogenic compositions
The liquid of interior additive dissolving composition.With the raising of people's quality of life, also gradually go deep into people’s lives.Only not
Disconnected research and development new product can just meet the requirements higher and higher consumer.
Invention content
The present invention i.e. in view of the above technical problems, provides one kind with mock-strawberry oral nursing liquid as main component, effectively
Fill up prior art blank.
In order to solve the above technical problems, the present invention specifically provides following technical solution：
A kind of mock-strawberry oral nursing liquid, is grouped as by the group of following mass fraction：K12 (lauryl sodium sulfate) 0.3%-
0.6%, mock-strawberry extracting solution 1%-5.2%, steviol glycoside 0.5%-0.8%, coolant agent WS-230.01%-0.08%, glycerine
1%-6%, edible ethanol 2%-6%, RH-60 (rilanit special) 1%-4%, sorbierite 1.1%-2.6%, vitamin
C0.02%-0.06% essence 0.1%-0.25%.The concentration of extracting solution is 80%.
Mock-strawberry oral nursing liquid preparation method, includes the following steps：
(1) pre-treatment of raw material
Each raw material of precise, are positioned in corresponding special container, wherein the deionized water deposit water-bath weighed up
It is for use to be preheated to 50-60 degree, it, need to be prior to 50-60 degree water-bath heating and meltings rear ponderable quantity if the phenomenon that freezes occurs in RH-60；
The K12 weighed up is slowly added to while stirring in the deionized water for being preheated to 50-60 degree, spare after stirring and dissolving, is added
Clustering phenomena is avoided during entering；
Steviol glycoside, sodium benzoate, the sorbierite weighed up, vitamin C is respectively with spare after suitable water dissolution completely；
(2) water phase stirs
It is poured into premix bucket the 2/3 of water surplus and opens stirring operating mode, sequentially add steviol glycoside solution, benzoic acid
Sodium solution, K12 solution, sorbierite, vitamin c solution, remaining water clean each container, are added in premix bucket；
After sixty minutes, sampling observation mixed solution clarity extends mixing time until clear if clarity is inadequate for stirring
Clearly.After the completion of clarification, stirring is closed, it is spare；
When water temperature is relatively low, can not distinguish clarity of solution, appropriate prepare liquid is taken to be put into water-bath in the water-bath of 50-60 degree
After heating 1 minute, then observe clarity of solution；
(3) preparation of oil phase
Stirring and dissolving weighs up successively in 5/6 food grade ethanol solution WS-3, Mint Essence, mock-strawberry extracting solution, RH-
60, glycerine, before each material is added, a upper material need to be completely dissolved, and oil phase stirs after sixty minutes, and the molten of oil phase is observed in sampling
Situation is solved, if not being completely dissolved, extends mixing time until dissolving clarification, after the completion of clarification, closes stirring, it is spare.
(4) stirring is mixed
After water phase stirs, in the case where stirring open state, oil phase is poured slowly into premix bucket, then is eaten with remaining
Grade ethyl alcohol cleans oil phase container, and cleaning solution is added premix bucket, is stirred after sixty minutes after all mixing, sample detection pH value and outer
It sees, pH value 7.00-7.15, if pH value not up to requires, adds 10% sodium hydroxide solution fine tuning pH value；
It finally stirs 60 minutes, obtains finished product.
The reached advantageous effect of the present invention is：Mock-strawberry oral nursing liquid produced by the invention have significant oral cleaning,
The effects that antibacterial, plays good nursing efficacy, is different from the formula and preparation method of traditional mouth conditioning liquid, is provided newly for the same industry
Open one's minds.
Specific implementation mode
Below in conjunction with the embodiment of the present invention, technical scheme of the present invention is clearly and completely described, it is clear that institute
The embodiment of description is only a part of the embodiment of the present invention, instead of all the embodiments.Based on the embodiments of the present invention,
Every other embodiment obtained by those of ordinary skill in the art without making creative efforts, belongs to this hair
The range of bright protection.
Clear, complete description, certainly, described embodiment are carried out to the technical solution in patent of invention example below
The only a part of embodiment of the present invention, instead of all the embodiments.Based on embodiment in the present invention, ordinary skill
Personnel do not make the every other embodiment obtained under the premise of creative work, belong to the scope of the present invention.
A kind of mock-strawberry oral nursing liquid, is grouped as by the group of following mass fraction：K12 (lauryl sodium sulfate) 0.3%-
0.6%, mock-strawberry extracting solution 1%-5.2%, steviol glycoside 0.5%-0.8%, coolant agent WS-230.01%-0.08%, glycerine
1%-6%, edible ethanol 2%-6%, RH-60 (rilanit special) 1%-4%, sorbierite 1.1%-2.6%, vitamin
C0.02%-0.06% essence 0.1%-0.25%.Balance deionized water.
The concentration of the mock-strawberry extracting solution is 80%.
The preparation method of mock-strawberry oral nursing liquid, includes the following steps：
(1) whether control formula table look-up raw material is abundant, weighing.
(2) the good each raw material of mouthwash record of production table precise are pressed, is positioned in corresponding special container, will weigh up
Deionized water be put into water-bath to be preheated to 50-60 degree for use.If the phenomenon that freezes occurs in RH-60, a certain amount of RH- is first taken out
60 in beaker, is put into 50-60 degree water-bath heating and meltings, is then weighed up again by formula ratio.
(3) dissolving of K12
The K12 weighed up in advance is slowly added to be preheated in the 1000ml deionized waters of 50-60 degree while stirring, stirring is molten
It is spare after solution, not occur clustering phenomena during addition.
(4) steviol glycoside, sodium benzoate, sorbierite dissolving, vitamin C
The steviol glycoside, sodium benzoate, sorbierite weighed up in advance, vitamin C is completely standby with suitable water dissolution respectively
With.
(5) water phase stirs
It is poured into premix bucket the 2/3 of surplus water and opens stirring, it is molten then to pour into saccharin sodium solution, sodium benzoate successively
Liquid, K12 solution, sorbierite, vitamin c solution.Each container is cleaned with remaining water (leave and take 500 milliliters spare) after being finished down,
Enter to premix in bucket.Complete soln stirs 60 minutes after pouring into.Sampling observation clarity of solution prolongs if clarity is inadequate
Long stirring 20 minutes.After the completion of mixing time, stirring is closed, it is spare.
Note：When water temperature is relatively low, the clarity of solution can not seen, appropriate prepare liquid can be taken to be put into the water of 50-60 degree
Heating water bath 1 minute in bath further takes out the clarity of observation solution.
(6) preparation of oil phase
Stirring and dissolving weighs up successively in 5/6 food grade ethanol solution WS-3, Mint Essence, mock-strawberry extracting solution, RH-
60, glycerine.Before each material pours into, a upper material must be completely dissolved.Oil phase stirs 60 minutes.Sampling observation oil phase
Situation is dissolved, if undissolved complete, extends stirring until dissolving clarification.After the completion, stirring is closed, it is spare.
(7) stirring is mixed
After water phase stirs, in the case where stirring open state, oil phase is poured slowly into premix bucket.Again with remaining ethyl alcohol
Oil phase container is cleaned, cleaning, which finishes, pours into premix bucket.It is stirred 60 minutes after all mixing.Sample detection pH value and appearance.Such as
Fruit pH value does not reach standard requirement, and technologist is notified to handle.10% sodium hydroxide solution can be added to finely tune
PH value, when adjustment answer first lab scale adjustment qualified after put into production again, pH value standard is 7.00-7.15.
After stir 60 minutes.
It although an embodiment of the present invention has been shown and described, for the ordinary skill in the art, can be with
Understanding without departing from the principles and spirit of the present invention can carry out these embodiments a variety of variations, modification, replace
And modification, the scope of the present invention is defined by the appended.
Claims (2)
1. a kind of mock-strawberry oral nursing liquid, is grouped as by the group of following mass fraction：K120.3%-0.6%, mock-strawberry extracting solution
1%-5.2%, steviol glycoside 0.5%-0.8%, coolant agent WS-230.01%-0.08%, glycerine 1%-6%, edible ethanol
2%-6%, RH-601%-4%, sorbierite 1.1%-2.6%, vitamin C 0.02%-0.06% essence 0.1%-0.25%,
Excess water.
2. mock-strawberry oral nursing liquid preparation method according to claim 1, includes the following steps：
(1) pre-treatment of raw material
Each raw material of precise, are positioned in corresponding special container, wherein the deionized water deposit water-bath preheating weighed up
It is for use to 50-60 degree, it, need to be prior to 50-60 degree water-bath heating and meltings rear ponderable quantity if the phenomenon that freezes occurs in RH-60；
The K12 weighed up is slowly added to while stirring in the deionized water for being preheated to 50-60 degree, spare after stirring and dissolving, is added
Clustering phenomena is avoided in journey；
Steviol glycoside, sodium benzoate, the sorbierite weighed up, vitamin C is respectively with spare after suitable water dissolution completely；
(2) water phase stirs
It is poured into premix bucket the 2/3 of water surplus and opens stirring operating mode, it is molten to sequentially add steviol glycoside solution, sodium benzoate
Liquid, K12 solution, sorbierite, vitamin c solution, remaining water clean each container, are added in premix bucket；
After sixty minutes, sampling observation mixed solution clarity extends mixing time until clarification if clarity is inadequate for stirring.
After the completion of clarification, stirring is closed, it is spare；
When water temperature is relatively low, can not distinguish clarity of solution, appropriate prepare liquid is taken to be put into heating water bath in the water-bath of 50-60 degree
After 1 minute, then observe clarity of solution；
(3) preparation of oil phase
Stirring and dissolving weighs up successively in 5/6 food grade ethanol solution WS-3, Mint Essence, mock-strawberry extracting solution, RH-60,
Glycerine, before each material is added, a upper material need to be completely dissolved, and oil phase stirs after sixty minutes, the dissolving of sampling observation oil phase
Situation extends mixing time until dissolving clarification if not being completely dissolved, after the completion of clarification, closes stirring, spare.
(4) stirring is mixed
After water phase stirs, in the case where stir open state, oil phase is poured slowly into and is premixed in bucket, then with remaining food grade second
Alcohol cleans oil phase container, and cleaning solution is added premix bucket, is stirred after sixty minutes after all mixing, sample detection pH value and appearance, PH
Value is 7.00-7.15, if pH value not up to requires, adds 10% sodium hydroxide solution fine tuning pH value；
It finally stirs 60 minutes, obtains finished product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711222256.7A CN108371640A (en) | 2017-11-29 | 2017-11-29 | A kind of mock-strawberry oral nursing liquid and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711222256.7A CN108371640A (en) | 2017-11-29 | 2017-11-29 | A kind of mock-strawberry oral nursing liquid and preparation method thereof |
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| CN108371640A true CN108371640A (en) | 2018-08-07 |
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| CN201711222256.7A Pending CN108371640A (en) | 2017-11-29 | 2017-11-29 | A kind of mock-strawberry oral nursing liquid and preparation method thereof |
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Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101627965A (en) * | 2009-07-21 | 2010-01-20 | 清华大学 | Multifunctional pure natural mouthwash and preparation method thereof |
| EP2241198A1 (en) * | 2009-04-07 | 2010-10-20 | Fresenius Kabi Deutschland GmbH | Mucositis prevention supplement and treatment |
| CN102824511A (en) * | 2012-08-23 | 2012-12-19 | 何兆辉 | Miao medicine used for oralcavity and preparation technology |
| CN106491390A (en) * | 2016-12-13 | 2017-03-15 | 美晨集团股份有限公司 | A kind of persistently refrigerant antibacterial oral cavity cleaning and nursing liquid and preparation method thereof |
-
2017
- 2017-11-29 CN CN201711222256.7A patent/CN108371640A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP2241198A1 (en) * | 2009-04-07 | 2010-10-20 | Fresenius Kabi Deutschland GmbH | Mucositis prevention supplement and treatment |
| CN101627965A (en) * | 2009-07-21 | 2010-01-20 | 清华大学 | Multifunctional pure natural mouthwash and preparation method thereof |
| CN102824511A (en) * | 2012-08-23 | 2012-12-19 | 何兆辉 | Miao medicine used for oralcavity and preparation technology |
| CN106491390A (en) * | 2016-12-13 | 2017-03-15 | 美晨集团股份有限公司 | A kind of persistently refrigerant antibacterial oral cavity cleaning and nursing liquid and preparation method thereof |
Non-Patent Citations (1)
| Title |
|---|
| 赵秀贞: "《青草药彩色图谱》", 30 April 1997, 福建科学技术出版社 * |
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| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
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| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20180807 |
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| RJ01 | Rejection of invention patent application after publication |