CN108362658A - Talcum powder content analysis and analysis method in a kind of polypropylene plastics - Google Patents
Talcum powder content analysis and analysis method in a kind of polypropylene plastics Download PDFInfo
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- CN108362658A CN108362658A CN201810187889.7A CN201810187889A CN108362658A CN 108362658 A CN108362658 A CN 108362658A CN 201810187889 A CN201810187889 A CN 201810187889A CN 108362658 A CN108362658 A CN 108362658A
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- talcum powder
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- FPAFDBFIGPHWGO-UHFFFAOYSA-N dioxosilane;oxomagnesium;hydrate Chemical compound O.[Mg]=O.[Mg]=O.[Mg]=O.O=[Si]=O.O=[Si]=O.O=[Si]=O.O=[Si]=O FPAFDBFIGPHWGO-UHFFFAOYSA-N 0.000 title claims abstract description 62
- 239000004743 Polypropylene Substances 0.000 title claims abstract description 59
- 229920001155 polypropylene Polymers 0.000 title claims abstract description 59
- -1 polypropylene Polymers 0.000 title claims abstract description 54
- 239000004033 plastic Substances 0.000 title claims abstract description 35
- 229920003023 plastic Polymers 0.000 title claims abstract description 35
- 238000004458 analytical method Methods 0.000 title claims abstract description 30
- 238000002329 infrared spectrum Methods 0.000 claims abstract description 10
- 239000000454 talc Substances 0.000 claims abstract description 9
- 229910052623 talc Inorganic materials 0.000 claims abstract description 9
- 235000012222 talc Nutrition 0.000 claims abstract description 9
- 239000000463 material Substances 0.000 claims description 9
- 229920002972 Acrylic fiber Polymers 0.000 claims 1
- 238000001514 detection method Methods 0.000 abstract description 2
- 238000000034 method Methods 0.000 description 7
- 238000004519 manufacturing process Methods 0.000 description 3
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 3
- 230000004048 modification Effects 0.000 description 3
- 238000012986 modification Methods 0.000 description 3
- 238000005516 engineering process Methods 0.000 description 2
- QQONPFPTGQHPMA-UHFFFAOYSA-N propylene Natural products CC=C QQONPFPTGQHPMA-UHFFFAOYSA-N 0.000 description 2
- 125000004805 propylene group Chemical group [H]C([H])([H])C([H])([*:1])C([H])([H])[*:2] 0.000 description 2
- 238000005070 sampling Methods 0.000 description 2
- 229920000178 Acrylic resin Polymers 0.000 description 1
- 239000004925 Acrylic resin Substances 0.000 description 1
- VGGSQFUCUMXWEO-UHFFFAOYSA-N Ethene Chemical compound C=C VGGSQFUCUMXWEO-UHFFFAOYSA-N 0.000 description 1
- 239000005977 Ethylene Substances 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000032683 aging Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000000739 chaotic effect Effects 0.000 description 1
- 239000004595 color masterbatch Substances 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 229920001577 copolymer Polymers 0.000 description 1
- 238000005260 corrosion Methods 0.000 description 1
- 230000007797 corrosion Effects 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 238000009659 non-destructive testing Methods 0.000 description 1
- 231100000252 nontoxic Toxicity 0.000 description 1
- 230000003000 nontoxic effect Effects 0.000 description 1
- 230000009965 odorless effect Effects 0.000 description 1
- 238000006116 polymerization reaction Methods 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 230000001954 sterilising effect Effects 0.000 description 1
- 238000004659 sterilization and disinfection Methods 0.000 description 1
- 229920005992 thermoplastic resin Polymers 0.000 description 1
Classifications
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N21/00—Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
- G01N21/17—Systems in which incident light is modified in accordance with the properties of the material investigated
- G01N21/25—Colour; Spectral properties, i.e. comparison of effect of material on the light at two or more different wavelengths or wavelength bands
- G01N21/31—Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry
- G01N21/35—Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry using infrared light
- G01N21/3563—Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry using infrared light for analysing solids; Preparation of samples therefor
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- Physics & Mathematics (AREA)
- Spectroscopy & Molecular Physics (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Analytical Chemistry (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- General Physics & Mathematics (AREA)
- Immunology (AREA)
- Pathology (AREA)
- Investigating Or Analysing Materials By Optical Means (AREA)
- Compositions Of Macromolecular Compounds (AREA)
Abstract
The invention discloses talcum powder content analysis and analysis method in a kind of polypropylene plastics of detection and analysis technical field, instrument parameter is arranged in (2):Wave number scanning range:4000cm‑1~650cm‑1, scan number:32, resolution ratio:4cm‑1;(3) polypropylene plastics that polypropylene, talcum powder and talcum powder content are 5%, 10%, 15%, 20%, 25%, 30% is scanned respectively carry out IR spectrum scanning;(4) determine that characteristic peak is 2950.69cm from polyacrylic infrared spectrogram‑1, 2919.21cm‑1, 2867.51cm‑1, 2850.39cm‑1, 1458.10cm‑1, 1376.43cm‑1;(5) determine that characteristic peak is 3675.56cm from the infrared spectrogram of talcum powder‑1, 1006.74cm‑1, 668.68cm‑1;(6) characteristic peak 1458.10cm is determined from the polypropylene plastics infrared spectrogram that talcum powder content is 5%, 10%, 15%, 20%, 25%, 30%‑1And 1006.74cm‑1Peak height, calculating compares;(7) matched curve, y=0.369x 1.048 are done according to content and ratio;(8) polypropylene specimen for scanning unknown talcum powder content, passes through characteristic peak 1458.10cm‑1And 1006.74cm‑1Peak height ratios bring curve into, acquire talcum powder content.
Description
Technical field
The present invention relates to detection and analysis technical field, talcum powder content analysis and analysis in specially a kind of polypropylene plastics
Method.
Background technology
Decaying total reflection (ATR) is a kind of sample mode of infrared spectrum, is difficult to detect in sample, non-destructive testing and sample
There is advantageous advantage in terms of the acquisition of product surface information.Plastics in process of production, due to additives such as addition color masterbatch, lead to
Translucidus is not often had, therefore conventional projective method sampling is difficult to directly prove effective.The convenience of ATR is mainly reflected in sample
Surface information directly acquires, and sampling efficiency is improved relative to traditional solvent method.
Polypropylene (PP) is a kind of thermoplastic resin made of propylene polymerization, and methyl is arranged in the same side of molecular backbone
Claim isotactic polypropylene, if the chaotic both sides for being arranged in molecular backbone of methyl claim random polypropylene, when methyl is arranged alternately in
The both sides of molecular backbone claim syndiotactic polypropylene.In the acrylic resin of general industry production, isotactic structural content is about 95%,
Remaining is random or syndiotactic polypropylene.Industrial products are using isotactic object as main component.Polypropylene also includes propylene and a small amount of ethylene
Including copolymer.Usually translucent colorless solid is odorless nontoxic.The highly crystallized due to compound with regular structure, therefore fusing point can be high
Up to 167 DEG C.Heat-resisting, corrosion-resistant, product can be its outstanding advantages with moise-heat sterilization.Density is small, is most light general-purpose plastics.Disadvantage
It is that low-temperature impact resistance is poor, it is more easy to aging, but can be overcome respectively by modification.
PP has stronger competitiveness for auto industry, but because its modulus and heat resistance are relatively low, impact strength is poor, because
This cannot be directly used as auto parts machinery, and what is used in car is MODIFIED PP product.Talcum powder is in the row such as medicine, food, makeups
The application of industry is relatively broad.It is then often used in the adjustment of plastics mechanical property in plastic industry, the talcum powder of different content adds
Add, the performance of base material can be influenced in various degree.
Practical content
The purpose of the present invention is to provide talcum powder content analysis and analysis methods in a kind of polypropylene plastics, in solution
State the problem of being proposed in background technology.
To achieve the above object, the present invention provides the following technical solutions:
(1) chosen material, connects external power supply, control switch detector device whether normal function;
(2) instrument parameter is set:Wave number scanning range:4000cm-1~650cm-1, scan number:32, resolution ratio:4cm-1;
(3) it is 5%, 10%, 15%, 20%, 25%, 30% to scan polypropylene, talcum powder and talcum powder content respectively
Polypropylene plastics carry out IR spectrum scanning;
(4) determine that characteristic peak is 2950.69cm from polyacrylic infrared spectrogram-1, 2919.21cm-1, 2867.51cm-1,
2850.39cm-1, 1458.10cm-1, 1376.43cm-1;
(5) determine that characteristic peak is 3675.56cm from the infrared spectrogram of talcum powder-1, 1006.74cm-1, 668.68cm-1;
(6) from the polypropylene plastics infrared spectrogram that talcum powder content is 5%, 10%, 15%, 20%, 25%, 30%
Determine characteristic peak 1458.10cm-1And 1006.74cm-1Peak height, calculating compares;
(7) matched curve, y=0.369x-1.048 are done according to content and ratio;
(8) polypropylene specimen for scanning unknown talcum powder content, passes through characteristic peak 1458.10cm-1And 1006.74cm-1's
Peak height ratios bring curve into, acquire talcum powder content
Compared with prior art, the beneficial effects of the invention are as follows:
1, in the polypropylene plastics talcum powder content analysis new method, it is easy to operate, it is easy to use, can be rapidly and efficiently
Retrieval PP in talcum powder content;
2 at the same the polypropylene plastics in talcum powder content analysis new method cost it is quick with respect to other analysis modes;
3 and suitable for QC departments carry out typical products in mass production tracking and analysis.
Description of the drawings
Fig. 1 is that content of the present invention and ratio make matched curve schematic diagram.
Specific implementation mode
Following will be combined with the drawings in the embodiments of the present invention, and technical solution in the embodiment of the present invention carries out clear, complete
Site preparation describes, it is clear that described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.It is based on
Embodiment in the present invention, it is obtained by those of ordinary skill in the art without making creative efforts every other
Embodiment shall fall within the protection scope of the present invention.
Referring to Fig. 1, the present invention provides a kind of technical solution:Talcum powder content analysis and analysis in a kind of polypropylene plastics
Method,
Embodiment 1:
(1) chosen material, connects external power supply, control switch detector device whether normal function;
(2) instrument parameter is set:Wave number scanning range:4000cm-1~650cm-1, scan number:32, resolution ratio:4cm-1;
(3) the polypropylene plastics progress infrared spectrum that polypropylene, talcum powder and talcum powder content are 5% is scanned respectively to sweep
It retouches;
(4) determine that characteristic peak is 2950.69cm from polyacrylic infrared spectrogram-1, 2919.21cm-1, 2867.51cm-1,
2850.39cm-1, 1458.10cm-1, 1376.43cm-1;
(5) determine that characteristic peak is 3675.56cm from the infrared spectrogram of talcum powder-1, 1006.74cm-1, 668.68cm-1;
(6) characteristic peak 1458.10cm is determined from the polypropylene plastics infrared spectrogram that talcum powder content is 5%-1With
1006.74cm-1Peak height, calculating compare ratio be 1.042;
(7) matched curve, y=0.369x-1.048 are done according to content and ratio;
(8) polypropylene specimen for scanning unknown talcum powder content, passes through characteristic peak 1458.10cm-1And 1006.74cm-1's
Peak height ratios bring curve into, acquire talcum powder content.
Content/% | 1458.10cm-1 | 1006.74cm-1 | Ratio |
5 | 3.191 | 3.325 | 1.042 |
Talcum powder content analysis and analysis method in a kind of polypropylene plastics,
Embodiment 2:
(1) chosen material, connects external power supply, control switch detector device whether normal function;
(2) instrument parameter is set:Wave number scanning range:4000cm-1~650cm-1, scan number:32, resolution ratio:4cm-1;
(3) polypropylene plastics that polypropylene, talcum powder and talcum powder content are 10% is scanned respectively carry out infrared spectrum
Scanning;
(4) determine that characteristic peak is 2919.21cm from polyacrylic infrared spectrogram-1;
(5) determine that characteristic peak is 3675.56cm from the infrared spectrogram of talcum powder-1, 1006.74cm-1, 668.68cm-1;
(6) characteristic peak 1458.10cm is determined from the polypropylene plastics infrared spectrogram that talcum powder content is 5%-1With
1006.74cm-1Peak height, calculating compares;
(7) matched curve, y=0.369x-1.048 are done according to content and ratio;
(8) polypropylene specimen for scanning unknown talcum powder content, passes through characteristic peak 1458.10cm-1And 1006.74cm-1's
Peak height ratios bring curve into, acquire talcum powder content.
Content/% | 1458.10cm-1 | 1006.74cm-1 | Ratio |
10 | 3.133 | 8.236 | 2.629 |
Talcum powder content analysis and analysis method in a kind of polypropylene plastics,
Embodiment 3:
(1) chosen material, connects external power supply, control switch detector device whether normal function;
(2) instrument parameter is set:Wave number scanning range:4000cm-1~650cm-1, scan number:32, resolution ratio:4cm-1;
(3) polypropylene plastics that polypropylene, talcum powder and talcum powder content are 15% is scanned respectively carry out infrared spectrum
Scanning;
(4) determine that characteristic peak is 2950.69cm from polyacrylic infrared spectrogram-1, 2919.21cm-1, 2867.51cm-1,
2850.39cm-1, 1458.10cm-1, 1376.43cm-1;
(5) determine that characteristic peak is 3675.56cm from the infrared spectrogram of talcum powder-1, 1006.74cm-1, 668.68cm-1;
(6) characteristic peak 1458.10cm is determined from the polypropylene plastics infrared spectrogram that talcum powder content is 5%-1With
1006.74cm-1Peak height, calculating compares;
(7) matched curve, y=0.369x-1.048 are done according to content and ratio;
(8) polypropylene specimen for scanning unknown talcum powder content, passes through characteristic peak 1458.10cm-1And 1006.74cm-1's
Peak height ratios bring curve into, acquire talcum powder content.
Content/% | 1458.10cm-1 | 1006.74cm-1 | Ratio |
15 | 3.027 | 12.972 | 4.285 |
Talcum powder content analysis and analysis method in a kind of polypropylene plastics,
Embodiment 4:
(1) chosen material, connects external power supply, control switch detector device whether normal function;
(2) instrument parameter is set:Wave number scanning range:4000cm-1~650cm-1, scan number:32, resolution ratio:4cm-1;
(3) polypropylene plastics that polypropylene, talcum powder and talcum powder content are 20% is scanned respectively carry out infrared spectrum
Scanning;
(4) determine that characteristic peak is 2950.69cm from polyacrylic infrared spectrogram-1, 2919.21cm-1, 2867.51cm-1,
2850.39cm-1, 1458.10cm-1, 1376.43cm-1;
(5) determine that characteristic peak is 3675.56cm from the infrared spectrogram of talcum powder-1, 1006.74cm-1, 668.68cm-1;
(6) characteristic peak 1458.10cm is determined from the polypropylene plastics infrared spectrogram that talcum powder content is 5%-1With
1006.74cm-1Peak height, calculating compares;
(7) matched curve, y=0.369x-1.048 are done according to content and ratio;
(8) polypropylene specimen for scanning unknown talcum powder content, passes through characteristic peak 1458.10cm-1And 1006.74cm-1's
Peak height ratios bring curve into, acquire talcum powder content.
Content/% | 1458.10cm-1 | 1006.74cm-1 | Ratio |
20 | 3.05 | 18.21 | 5.970 |
Talcum powder content analysis and analysis method in a kind of polypropylene plastics,
Embodiment 5:
(1) chosen material, connects external power supply, control switch detector device whether normal function;
(2) instrument parameter is set:Wave number scanning range:4000cm-1~650cm-1, scan number:32, resolution ratio:4cm-1;
(3) polypropylene plastics that polypropylene, talcum powder and talcum powder content are 25% is scanned respectively carry out infrared spectrum
Scanning;
(4) determine that characteristic peak is 2950.69cm from polyacrylic infrared spectrogram-1, 2919.21cm-1, 2867.51cm-1,
2850.39cm-1, 1458.10cm-1, 1376.43cm-1;
(5) determine that characteristic peak is 3675.56cm from the infrared spectrogram of talcum powder-1, 1006.74cm-1, 668.68cm-1;
(6) characteristic peak 1458.10cm is determined from the polypropylene plastics infrared spectrogram that talcum powder content is 5%-1With
1006.74cm-1Peak height, calculating compares;
(7) matched curve, y=0.369x-1.048 are done according to content and ratio;
(8) polypropylene specimen for scanning unknown talcum powder content, passes through characteristic peak 1458.10cm-1And 1006.74cm-1's
Peak height ratios bring curve into, acquire talcum powder content.
Content/% | 1458.10cm-1 | 1006.74cm-1 | Ratio |
25 | 2.795 | 23.333 | 8.348 |
Talcum powder content analysis and analysis method in a kind of polypropylene plastics,
Embodiment 6:
(1) chosen material, connects external power supply, control switch detector device whether normal function;
(2) instrument parameter is set:Wave number scanning range:4000cm-1~650cm-1, scan number:32, resolution ratio:4cm-1;
(3) polypropylene plastics that polypropylene, talcum powder and talcum powder content are 30% is scanned respectively carry out infrared spectrum
Scanning;
(4) determine that characteristic peak is 2950.69cm from polyacrylic infrared spectrogram-1, 2919.21cm-1, 2867.51cm-1,
2850.39cm-1, 1458.10cm-1, 1376.43cm-11;
(5) determine that characteristic peak is 3675.56cm from the infrared spectrogram of talcum powder-1, 1006.74cm-1, 668.68cm-1;
(6) characteristic peak 1458.10cm is determined from the polypropylene plastics infrared spectrogram that talcum powder content is 5%-1With
1006.74cm-1Peak height, calculating compares;
(7) matched curve, y=0.369x-1.048 are done according to content and ratio;
(8) polypropylene specimen for scanning unknown talcum powder content, passes through characteristic peak 1458.10cm-1And 1006.74cm-1's
Peak height ratios bring curve into, acquire talcum powder content.
Content/% | 1458.10cm-1 | 1006.74cm-1 | Ratio |
30 | 2.823 | 28.775 | 10.193 |
It although an embodiment of the present invention has been shown and described, for the ordinary skill in the art, can be with
Understanding without departing from the principles and spirit of the present invention can carry out these embodiments a variety of variations, modification, replace
And modification, the scope of the present invention is defined by the appended.
Claims (1)
1. talcum powder content analysis and analysis method in a kind of polypropylene plastics, including,
(1) chosen material, connects external power supply, control switch detector device whether normal function;
(2) instrument parameter is set:Wave number scanning range:4000cm-1~650cm-1, scan number:32, resolution ratio:4cm-1;
(3) scan polypropylene respectively, talcum powder and talcum powder content be 5%, 10%, 15%, 20%, 25%, 30% it is poly-
Acrylic plastic carries out IR spectrum scanning;
(4) determine that characteristic peak is 2950.69cm from polyacrylic infrared spectrogram-1, 2919.21cm-1, 2867.51cm-1,
2850.39cm-1, 1458.10cm-1, 1376.43cm-1;
(5) determine that characteristic peak is 3675.56cm from the infrared spectrogram of talcum powder-1, 1006.74cm-1, 668.68cm-1;
(6) it is determined from the polypropylene plastics infrared spectrogram that talcum powder content is 5%, 10%, 15%, 20%, 25%, 30%
Characteristic peak 1458.10cm-1And 1006.74cm-1Peak height, calculating compares;
(7) matched curve, y=0.369x-1.048 are done according to content and ratio;
(8) polypropylene specimen for scanning unknown talcum powder content, passes through characteristic peak 1458.10cm-1And 1006.74cm-1Peak height
Ratio brings curve into, acquires talcum powder content.
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Cited By (3)
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CN111398209A (en) * | 2020-05-04 | 2020-07-10 | 中钢集团郑州金属制品研究院有限公司 | Infrared spectrum method for measuring polyvinyl chloride content in hard polyvinyl chloride pipe |
CN112485215A (en) * | 2020-11-12 | 2021-03-12 | 北方华锦化学工业股份有限公司 | Method for quantitatively analyzing ethylene content in impact-resistant polypropylene by infrared spectroscopy |
CN114235735A (en) * | 2021-11-26 | 2022-03-25 | 北方华锦化学工业股份有限公司 | Method for quantitatively analyzing content of transparent agent in industrial transparent polypropylene by infrared spectroscopy |
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CN114235735A (en) * | 2021-11-26 | 2022-03-25 | 北方华锦化学工业股份有限公司 | Method for quantitatively analyzing content of transparent agent in industrial transparent polypropylene by infrared spectroscopy |
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