CN108355602A - A kind of chemical industry pilot scale stage apparatus and its working method - Google Patents
A kind of chemical industry pilot scale stage apparatus and its working method Download PDFInfo
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- CN108355602A CN108355602A CN201810267519.4A CN201810267519A CN108355602A CN 108355602 A CN108355602 A CN 108355602A CN 201810267519 A CN201810267519 A CN 201810267519A CN 108355602 A CN108355602 A CN 108355602A
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- 238000000034 method Methods 0.000 title claims abstract description 26
- 239000000126 substance Substances 0.000 title claims abstract description 24
- 238000011020 pilot scale process Methods 0.000 title claims abstract description 20
- 238000006243 chemical reaction Methods 0.000 claims abstract description 125
- 239000013064 chemical raw material Substances 0.000 claims abstract description 43
- 230000009471 action Effects 0.000 claims abstract description 6
- 210000000080 chela (arthropods) Anatomy 0.000 claims description 52
- 239000000463 material Substances 0.000 claims description 20
- 239000011159 matrix material Substances 0.000 claims description 18
- 230000007246 mechanism Effects 0.000 claims description 16
- 239000002994 raw material Substances 0.000 claims description 5
- 230000008859 change Effects 0.000 claims description 2
- 238000010586 diagram Methods 0.000 description 8
- 241000222712 Kinetoplastida Species 0.000 description 5
- 230000008569 process Effects 0.000 description 5
- 238000005516 engineering process Methods 0.000 description 3
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- 230000009286 beneficial effect Effects 0.000 description 1
- 238000003889 chemical engineering Methods 0.000 description 1
- 238000001311 chemical methods and process Methods 0.000 description 1
- 238000012824 chemical production Methods 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/24—Stationary reactors without moving elements inside
- B01J19/2445—Stationary reactors without moving elements inside placed in parallel
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0053—Details of the reactor
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/24—Stationary reactors without moving elements inside
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J4/00—Feed or outlet devices; Feed or outlet control devices
- B01J4/001—Feed or outlet devices as such, e.g. feeding tubes
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J4/00—Feed or outlet devices; Feed or outlet control devices
- B01J4/008—Feed or outlet control devices
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Abstract
The invention discloses a kind of chemical industry pilot scale stage apparatus and its working methods comprising rack, reaction kettle, the first supporter, the first cross travel unit and charging component.Chemical raw material is added in dosage unit, pass through the movement of the first cross travel unit, to which charging component is moved to close to the position of reaction kettle, so that dosage unit is deep into aperture position, pass through the movement of the second cross travel unit, to which the chemical raw material in dosage unit is added in reaction kettle, the risk factor that operator is formed close to aperture position is eliminated, operator remotely can also realize the control action to the device by controller；Also, loading hopper has the function of function of measuring and is automatically added to, and realizes the function being automatically added in batches.
Description
Technical field
Technical field of the present invention belongs to chemical reaction device field, more particularly to a kind of chemical industry pilot scale stage apparatus
And its working method.
Background technology
Chemical process includes Chemical Engineering Technology or chemical production technology, in mainly converting raw material object to by chemical reaction
The method and process of mesosome or product specifically enumerate many factors such as the equipment for realizing this conversion.
Reaction kettle is the common device of chemical workshop.Reaction kettle can be understood as including the container of physical and chemical reaction,
By to this container structure optimization and parameter setting so that the temperature of process requirements, pressure, cooling meet the requirements.
Reaction kettle has been widely used for the fields such as pesticide, dyestuff, oil, chemical industry, rubber, medicine and food.
In chemical industry pilot plant, in the workshop for especially producing medicine intermediate, the specification of reaction kettle the most common are
100L, 300L, 500L and 1000L.It is a kind of chemical reaction kettle 1 of existing chemical workshop as shown in Figure 1, reaction kettle 1 is general
It is arranged on rack, can be for the vertical walking of operator station on rack, the charge door 2 of reaction kettle 1 is generally in top, charge door 2 one
As be it is closed by detachable lid 3, when need charging when just opening.Operator is on rack by charge door 2 to reaction
It is added in kettle and reacts required material.
However, there are many defects for this mode that chemical raw material is added into reaction kettle, such as in some cases, instead
It answers and has been in kettle in reaction, need to add material into reaction within a certain period of time, open charge door this when,
The gas in reaction kettle will certainly be caused to escape, especially operator causes damages to ambient enviroment, moreover, some gases are poison
Property is stronger.In addition, the action that chemical raw material is directly added in operator by charge door is also extremely dangerous, it is easy to which article is fallen
It falls in reaction kettle, such as operator is when being added material, there is hair in when situation that careless handle sleeve, glasses are fallen in reaction kettle
It is raw.In addition, in some cases, it is desirable to which material is added into reaction kettle in batches, this process generally requires to expend work people
Member's more time and muscle power.
Invention content
In order to solve the deficiency of above-mentioned prior art, the object of the present invention is to provide a kind of chemical industry pilot scale stage apparatus and its
Working method.
The invention thought of the present invention：A feeding device is arranged in position near reaction kettle, which, which has, adds
Material unit, and the dosage unit can move under the drive of the first cross travel unit so that dosage unit can be deep into
The aperture position of reaction kettle, to which chemical raw material be added into reaction kettle.
A kind of chemical industry pilot scale stage apparatus comprising rack, reaction kettle, the first supporter, the first cross travel unit and
Feed component：Reaction kettle is arranged on rack, and reaction kettle has opening, has detachable lid in opening, one of reaction kettle
Divide and be located on the upside of rack, a part for reaction kettle is arranged on the downside of rack；First supporter is arranged on rack；First laterally moves
Moving cell is arranged on the first supporter；The component that feeds is arranged on the first cross travel unit, and charging component includes second
Support body, the second cross travel unit and dosage unit, the second cross travel unit are arranged on the second supporter, and second laterally moves
Moving cell is connect with dosage unit, and the second cross travel unit can drive dosage unit to being open, and dosage unit is for loading
Chemical raw material；Wherein, dosage unit includes hollow cylinder, and the second cross travel unit can be moved in axial direction in hollow cylinder
Position dynamic, that the second cross travel unit is used to that the chemical raw material in hollow cylinder to be driven to be advanced into opening；Dosage unit is also wrapped
Loading hopper is included, loading hopper is arranged on hollow cylinder top, and loading hopper is connect by connecting tube with hollow cylinder, had in connecting tube
Flowmeter and electromagnetic valve.
Beneficial effects of the present invention are：Chemical raw material is added in dosage unit, the first cross travel unit is passed through
It is mobile, to which charging component is moved to close to the position of reaction kettle so that dosage unit is deep into aperture position, passes through second
It is close to eliminate operator to which the chemical raw material in dosage unit is added in reaction kettle for the movement of cross travel unit
The risk factor that aperture position is formed, operator remotely can also realize the control action to the device by controller；And
And loading hopper has the function of function of measuring and is automatically added to, and realizes the function being automatically added in batches.
One Preferable scheme is that, reaction kettle includes the first reaction kettle and the second reaction kettle, and the setting of the first supporter is the
Between one reaction kettle and the second reaction kettle, charging component includes the first charging component and the second charging component, the first charging component
For feeding into the first reaction kettle, the second charging component into the second reaction kettle for feeding, the first cross travel unit two
Side is connect with the first charging component and the second charging component respectively.
One Preferable scheme is that, the first supporter includes matrix and driving device, and driving device is connect with matrix, and drive
Dynamic device can be circled with kinetoplast, and the first cross travel unit is arranged on matrix.
One Preferable scheme is that, loading hopper include pincer attack mechanism, pincer attack mechanism be used for the lump material in loading hopper
It is struck, pincer attack mechanism includes upper pincer attack component and lower pincer attack component.
The working method of chemical industry pilot scale stage apparatus comprising step below：
S1：Chemical raw material is added into dosage unit, dismantles lid, it is opening-wide state to keep opening；
S2：First cross travel unit drives charging component to be moved to the direction of reaction kettle so that dosage unit is deep into opening
It is interior；Chemical raw material is added in loading hopper, electromagnetic valve is opened, it is former to the chemistry being added in hollow cylinder by flowmeter
Material is measured in real time, and chemical raw material, which is divided into, to be repeatedly added in hollow cylinder, the chemistry being added to each time in hollow cylinder
Raw material is pushed to the second cross travel unit in reaction kettle；
S3：Second cross travel unit moves in dosage unit so that the chemical raw material in dosage unit enters reaction kettle
It is interior；
S4：Second cross travel unit reverse movement resets, meanwhile, the first cross travel unit moves backward and drives charging single
Member resets.
One Preferable scheme is that, reaction kettle includes the first reaction kettle and the second reaction kettle, and the setting of the first supporter is the
Between one reaction kettle and the second reaction kettle, charging component includes the first charging component and the second charging component, the first charging component
For feeding into the first reaction kettle, the second charging component into the second reaction kettle for feeding, the first cross travel unit two
Side is connect with the first charging component and the second charging component respectively；The working method includes following step：To the first charging group
Chemical raw material is added in part and the second charging component, the first cross travel unit is moved first towards the direction of the first reaction kettle,
Second cross travel unit is added to the chemical raw material in the first charging component in the first reaction kettle, and then, first laterally moves
Moving cell is moved towards the direction of the second reaction kettle, and the chemical raw material in the second charging component is added in the second cross travel unit
Into the second reaction kettle.
One Preferable scheme is that, the first supporter includes matrix and driving device, and driving device is connect with matrix, and drive
Dynamic device can be circled with kinetoplast, and the first cross travel unit is arranged on matrix；The working method includes following
The step of：Driving device band kinetoplast rotates, and then drives the first cross travel unit and dosage unit moving in rotation to specified
Reaction kettle position.
One Preferable scheme is that, loading hopper include pincer attack mechanism, pincer attack mechanism be used for the lump material in loading hopper
It is struck, pincer attack mechanism includes upper pincer attack component and lower pincer attack component；The working method includes following step：Upper pincer attack group
When part is clamp position, lower pincer attack component is opening-wide state；Or when upper pincer attack component is opening-wide state, lower pincer attack component is
Clamp position；Alternatively, upper pincer attack component and lower pincer attack component are carried out at the same time pincer attack action.
Description of the drawings
Fig. 1 is a kind of existing structural schematic diagram of reaction kettle.
Fig. 2 is structural schematic diagram of the invention first embodiment in first state.
Fig. 3 is structural schematic diagram of the invention first embodiment in the second state.
Fig. 4 is the structural schematic diagram of the charging component of invention first embodiment.
Fig. 5 is the structural schematic diagram of the members of invention first embodiment.
Fig. 6 is the structural schematic diagram of the members of invention second embodiment.
Fig. 7 is the structural schematic diagram of the members of invention 3rd embodiment.
Fig. 8 is the structural schematic diagram of the members of invention fourth embodiment.
Wherein, reference numeral is：10, rack；20, reaction kettle；21, it is open；22, lid；23, the first reaction kettle；24,
Two reaction kettles；30, the first supporter；31, matrix；32, driving device；40, the first cross travel unit；50, feed component；
51, the second supporter；52, the second cross travel unit；53, dosage unit；54, hollow cylinder；55, loading hopper；56, it connects
Pipe；57, flowmeter；58, electromagnetic valve；75, inner wall；81, upper pincer attack component；82, lower pincer attack component；531, the first charging is single
Member；532, the second dosage unit.
Specific implementation mode
First embodiment：
As shown in Figures 2 to 5, the chemical industry pilot scale stage apparatus of the present embodiment includes rack 10, reaction kettle 20, the first supporter
30, the first cross travel unit 40 and charging component 50.
Reaction kettle 20 is arranged on rack 10, and reaction kettle 20 has opening 21, has detachable lid 22 in opening 21, instead
A part for kettle 20 is answered to be located at 10 upside of rack, another part setting of reaction kettle 20 is in 10 downside of rack.Opening 21 is mainly
Position for solid material to be added into reaction kettle 20, lid 22 can play opening 21 sealing process, and having can
Dismounting property.Rack 10 is operating platform, can be for the walking and operation of operator.
First supporter 30 is arranged on rack 10, and the quantity of the first supporter 30 can be multiple.First transverse shifting
Unit 40 is arranged on the first supporter 30.First cross travel unit 40 can be relative to the first supporter 30 in the horizontal direction
Upper movement, there are many type of drive, and the first cross travel unit is realized for example, by using the mode of motor-driven gear, rack
It is mobile；Either the mode of motor driving idler wheel realizes the movement of the first cross travel unit 40 or the side of electric motor driven screw
Formula, or push by the way of Driven by Hydraulic Cylinder the movement of the first cross travel unit 40, the first cross travel unit 40 with
The component 50 that feeds connects, to drive charging 50 movement in the horizontal direction of component.In actual job, in some cases,
Charging component 50 needs far from opening 21, and when chemical raw material is added into opening 21, then to need first charging component 50
Close to opening 21 or charging component 50 is deep into the opening 21 of reaction kettle 20, just facilitates subsequent step that chemistry is former in this way
Material is added in reaction kettle.
The component 50 that feeds is arranged on the first cross travel unit 40, and charging component 50 includes the second supporter 51, second
Cross travel unit 52 and dosage unit 53, the second cross travel unit 52 are arranged on the second supporter 51, and second laterally moves
Moving cell 52 is connect with dosage unit 53, and the second cross travel unit 53 can drive the chemical raw material in dosage unit 53 to opening
Mouthfuls 21, chemical raw material is mounted in dosage unit 53, to which chemical raw material is added in reaction kettle 20.Second transverse shifting list
There are many move modes of member 52, for example, by using the mode of electric motor driven screw, or by the way of motor-driven gear, or
Person is by the way of motor-driven gear and rack, specifically, the second cross travel unit 52 includes pushing plate, screw rod and electricity
Machine, electric motor driven screw move in the horizontal direction, and screw rod drives pushing plate to be moved in dosage unit 53, to which charging is single
Chemical raw material in member pushes in reaction kettle 20.
The dosage unit 53 of the present embodiment includes hollow cylinder 54, and the second cross travel unit 52 can in hollow cylinder 54
It in axial direction moves, the second cross travel unit 52 is used to that the chemical raw material in hollow cylinder 54 to be driven to be advanced into opening 21
Position.
Dosage unit 53 further includes loading hopper 55, the setting of loading hopper 55 on 54 top of hollow cylinder, loading hopper 55 with it is hollow
Cylinder 54 is connected by connecting tube 56, has flowmeter 57 and electromagnetic valve 58 in connecting tube 56.In some cases, it is desirable to point
Chemical raw material is added into reaction kettle 20 in batch, for example, in some reactions, needs that A materials are added at interval of half an hour
If 1KG is bound to cause working strength promotion, and be easy to make to operating personnel by the frequent multiple operation of staff
At harm, and the control for passing through control unit, it is only necessary to material be added at one time in loading hopper 55, loading hopper 55 can be according to
By the work of electromagnetic valve and flowmeter 57, material is added in hollow cylinder 54 in batches, and the object in hollow cylinder 54
Material can then be pushed to by the second cross travel unit 52 in reaction kettle 20.
The working method of the chemical industry pilot scale stage apparatus of the present embodiment includes following step：
S1：Chemical raw material is added into dosage unit 53, dismantles lid 22, it is opening-wide state to keep opening 21；Specifically, change
It learns raw material to be added in the loading hopper 55 of dosage unit 53, electromagnetic valve 58 is opened, by flowmeter 57 to being added to hollow
Chemical raw material in body 54 is measured in real time, and chemical raw material, which is divided into, to be repeatedly added in hollow cylinder 54, is added to each time
Chemical raw material in hollow cylinder 54 is pushed to the second cross travel unit 52 in reaction kettle 20；
S2：First cross travel unit 40 drives charging component 50 to be moved to the direction of reaction kettle 20 so that dosage unit 53 is deep
Enter into opening 21, i.e., converted to the state of Fig. 3 by Fig. 2, specific the says, and in fig. 2, charging component 50 is far from being open 21
, and in figure 3, charging component 50 has been deep into opening 21；
S3：Second cross travel unit 52 moves in dosage unit 53 so that the chemical raw material in dosage unit 53 enters
In reaction kettle 20；
S4：Second cross travel unit 52 reverse movement resets, meanwhile, the first cross travel unit 40 moves backward and drives and add
Material unit 53 resets, that is to say, that state as shown in Figure 3 is back to state shown in Fig. 2.
Second embodiment：
The chemical industry pilot scale stage apparatus of the present embodiment and above-mentioned first embodiment are essentially identical, only detailed with regard to its difference below
It introduces.
As shown in fig. 6, the reaction kettle of the present embodiment includes the first reaction kettle 23 and the second reaction kettle 24, the first supporter 30
It is arranged between the first reaction kettle 23 and the second reaction kettle 24, charging component 53 includes that the first charging component 531 and second feeds
Component 532, for feeding into the first reaction kettle 23, the second charging component 532 is used for the second reaction the first charging component 531
Charging in kettle 24,40 both sides of the first cross travel unit are connect with the first charging charging component 532 of component 531 and second respectively.
In actual production, generally requires multiple reaction kettles and carries out the same reaction in the same time, working efficiency can be improved in this way,
And rack 10 is usually to be equipped with multiple reaction kettles, just devises two reaction kettles here, feeding device setting is anti-at two
The position between kettle is answered, can thus to realize by the movement of the first cross travel unit two reaction kettles are added
Material process.The concrete structure of first cross travel unit is, for example,：Including a screw rod and motor, screw rod both sides are respectively with first
The charging component 532 of component 531 and second that feeds connects, and electric motor driven screw moves in the horizontal direction, to realize the first charging
Component 531 is moved to the direction of the first reaction kettle, or realizes that the second charging component 532 is moved to the direction of the second reaction kettle.
In addition, the first charging component 531 and second feeds, the concrete structure of component 532 also includes that supporter, mobile unit and charging are single
Member, structure and operation principle are identical as the charging component 53 in above-described embodiment.
The working method includes following step：Chemistry is added into the first charging charging component 532 of component 531 and second
Raw material, the first cross travel unit 40 are moved first towards the direction of the first reaction kettle 23, and the second cross travel unit is first
Chemical raw material in charging component 531 is added in the first reaction kettle 23, and then, the first cross travel unit 40 is anti-towards second
The direction of kettle 24 is answered to move, the chemical raw material in the second charging component 532 is added to second instead by the second cross travel unit 52
It answers in kettle 24.Here there are two the components that feeds for tool, and the second cross travel unit there are one being respectively provided in each charging component.
3rd embodiment：
The chemical industry pilot scale stage apparatus of the present embodiment and above-mentioned first embodiment are essentially identical, only detailed with regard to its difference below
It introduces.
As shown in fig. 7, first supporter 30 of the present embodiment includes matrix 31 and driving device 32, driving device 32 and base
Body 31 connects, and driving device 32 can be circled with kinetoplast 31, and the first cross travel unit 40 is arranged on matrix
31.There are three can having in some cases, rack, four or more reaction kettles, and the position among multiple reaction kettles
A feeding device is installed, by the rotation of driving device 32, and the charging component of the first cross travel unit 40 is moved
One end of a specified reaction kettle, the first cross travel unit 40 is provided with charging component 50, thereby realizes one
Charging component services the function of multiple reaction kettles simultaneously.
The working method includes following step：Driving device 32 is rotated with kinetoplast 31, and then drives first laterally to move
Moving cell 40 and 53 moving in rotation of dosage unit are to the position of specified reaction kettle.After having executed the order, first laterally moves
Moving cell 40 is again moved to charging component 50 position of the opening of specified reaction kettle, so the second cross travel unit again
Chemical raw material in dosage unit is added in reaction kettle.
Fourth embodiment：
The chemical industry pilot scale stage apparatus of the present embodiment and above-mentioned first embodiment are essentially identical, only detailed with regard to its difference below
It introduces.
As shown in figure 8, the loading hopper 55 of the present embodiment includes pincer attack mechanism, pincer attack mechanism is used for the bulk in loading hopper
Material is struck, and pincer attack mechanism includes upper pincer attack component 81 and lower pincer attack component 82.
The working method includes following step：When upper pincer attack component 81 is clamp position, lower pincer attack component 82 is unlimited
State；Or when upper pincer attack component 81 is opening-wide state, lower pincer attack component 82 is clamp position；Alternatively, upper pincer attack component 81
It is carried out at the same time pincer attack action with lower pincer attack component 82.Under some cases, block objects, this block objects are had in chemical raw material
When being added directly into reaction kettle, reaction process may be impacted, it, can be here just by converging the setting of component
These lump materials crush.When upper pincer attack component opens wide, lower pincer attack component is closed, and when the closing of upper pincer attack component, open lower folder
Component is hit, such mode can further promote the crushing efficiency to block objects, avoid unbroken solid material direct
It drops into hollow cylinder.
In other embodiments, further include control unit, control unit and the first cross travel unit, the second transverse shifting
Unit, electromagnetic valve, flowmeter, pincer attack mechanism, driving device connection.To be automatically controlled to the realization of these components, and control
Unit processed includes signal transmitting and receiving module, and user can remotely obtain the operation information of control unit by electronic equipment, grasp and add
Expect the charging situation of device, and realize the remote control to control unit, such as after user's remote input order, first laterally
Mobile unit is then moved to charging component close to the position of opening, after user inputs another order again, the second transverse shifting list
It is first then the chemical raw material in dosage unit is added in reaction kettle.
The foregoing is merely presently preferred embodiments of the present invention, is not intended to limit the invention, it is all the present invention spirit and
Within principle, any modification, equivalent replacement, improvement and so on should all be included in the protection scope of the present invention.
Claims (8)
1. a kind of chemical industry pilot scale stage apparatus, which is characterized in that including：
Rack；
Reaction kettle is arranged on the rack, and the reaction kettle has opening, has detachable lid in the opening, described
A part for reaction kettle is located on the upside of the rack, and a part for the reaction kettle is arranged on the downside of the rack；
First supporter is arranged on the rack；
First cross travel unit is arranged on first supporter；
Feed component, is arranged on first cross travel unit, and the charging component includes the second supporter, the second transverse direction
Mobile unit and dosage unit, second cross travel unit are arranged on second supporter, and described second laterally moves
Moving cell is connect with the dosage unit, and second cross travel unit can drive the dosage unit to the opening,
The dosage unit is for loading chemical raw material；
Wherein, the dosage unit includes hollow cylinder, and second cross travel unit can be along axis in the hollow cylinder
It is moved to direction, second cross travel unit is for driving the chemical raw material in the hollow cylinder to be advanced into the opening
Position；The dosage unit further includes loading hopper, loading hopper setting on the hollow cylinder top, the loading hopper with
The hollow cylinder is connected by connecting tube, has flowmeter and electromagnetic valve in the connecting tube.
2. chemical industry pilot scale stage apparatus according to claim 1, which is characterized in that
The loading hopper includes pincer attack mechanism, and the pincer attack mechanism is used to strike the lump material in the loading hopper,
The pincer attack mechanism includes upper pincer attack component and lower pincer attack component.
3. chemical industry pilot scale stage apparatus according to claim 2, which is characterized in that
The reaction kettle includes the first reaction kettle and the second reaction kettle, first supporter setting in first reaction kettle and
Between second reaction kettle, the charging component includes the first charging component and the second charging component, and the first charging component is used
It feeding in into first reaction kettle, the second charging component into second reaction kettle for feeding, and described first
Cross travel unit both sides are connect with the first charging component and the second charging component respectively.
4. chemical industry pilot scale stage apparatus according to claim 3, which is characterized in that
First supporter includes matrix and driving device, and the driving device is connect with described matrix, and the driving fills
Setting can drive described matrix to circle, and the first cross travel unit setting is on the matrix.
5. the working method of chemical industry pilot scale stage apparatus according to claim 1, which is characterized in that including following step
Suddenly：
S1：Chemical raw material is added into the dosage unit, dismantles the lid, it is opening-wide state to keep the opening；Change
It learns raw material to be added in the loading hopper, the electromagnetic valve is opened, by flowmeter to being added in the hollow cylinder
Chemical raw material is measured in real time, and chemical raw material, which is divided into, to be repeatedly added in the hollow cylinder, be added to each time it is described in
Chemical raw material in empty cylinder is pushed to second cross travel unit in the reaction kettle；
S2：First cross travel unit drives the charging component to be moved to the direction of the reaction kettle so that described to add
Material unit is deep into the opening；
S3：Second cross travel unit moves in the dosage unit so that the chemical raw material in the dosage unit
It enters in the reaction kettle；
S4：The second cross travel unit reverse movement resets, meanwhile, first cross travel unit moves backward and band
The dynamic charging component resets.
6. the working method of chemical industry pilot scale stage apparatus according to claim 5, which is characterized in that
The reaction kettle includes the first reaction kettle and the second reaction kettle, first supporter setting in first reaction kettle and
Between second reaction kettle, the charging component includes the first charging component and the second charging component, and the first charging component is used
It feeding in into first reaction kettle, the second charging component into second reaction kettle for feeding, and described first
Cross travel unit both sides are connect with the first charging component and the second charging component respectively；
The working method includes following step：Chemical raw material is added into the first charging component and the second charging component,
First cross travel unit is moved first towards the direction of first reaction kettle, and second cross travel unit is institute
The chemical raw material in the first charging component is stated to be added in first reaction kettle, then, first cross travel unit court
It is moved to the direction of second reaction kettle, the chemical raw material that second cross travel unit feeds described second in component
It is added in second reaction kettle.
7. the working method of chemical industry pilot scale stage apparatus according to claim 6, which is characterized in that
First supporter includes matrix and driving device, and the driving device is connect with described matrix, and the driving fills
Setting can drive described matrix to circle, and the first cross travel unit setting is on the matrix；
The working method includes following step：The driving device drives described matrix rotation, and then drives first cross
To mobile unit and dosage unit moving in rotation to the position of specified reaction kettle.
8. the working method of chemical industry pilot scale stage apparatus according to claim 7, which is characterized in that
The loading hopper includes pincer attack mechanism, and the pincer attack mechanism is used to strike the lump material in the loading hopper,
The pincer attack mechanism includes upper pincer attack component and lower pincer attack component；The working method includes following step：The upper pincer attack group
When part is clamp position, the lower pincer attack component is opening-wide state；It is described or when the upper pincer attack component is opening-wide state
Lower pincer attack component is clamp position；Alternatively, the upper pincer attack component and lower pincer attack component are carried out at the same time pincer attack action.
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| CN202655036U (en) * | 2012-06-13 | 2013-01-09 | 浙江康牧药业有限公司 | Reaction kettle with automatic feeding device |
| CN205731254U (en) * | 2016-06-27 | 2016-11-30 | 杭州圣传新材料科技有限公司 | A kind of reaction unit of auto feed |
| CN206392068U (en) * | 2017-01-16 | 2017-08-11 | 天津滨海洪发油墨有限公司 | A kind of Printing ink producing with automatic charging device energy-conservation reactor |
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Denomination of invention: A Chemical Pilot Platform Device and Its Working Method Effective date of registration: 20230922 Granted publication date: 20210105 Pledgee: Binzhou boxing sub branch of Qilu Bank Co.,Ltd. Pledgor: Shandong Jialong New Energy Co.,Ltd. Registration number: Y2023980058559 |
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