CN108342098A - A kind of aqueous pigment preparations - Google Patents

A kind of aqueous pigment preparations Download PDF

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Publication number
CN108342098A
CN108342098A CN201810036560.0A CN201810036560A CN108342098A CN 108342098 A CN108342098 A CN 108342098A CN 201810036560 A CN201810036560 A CN 201810036560A CN 108342098 A CN108342098 A CN 108342098A
Authority
CN
China
Prior art keywords
parts
anion
pigment
water
aqueous pigment
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201810036560.0A
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Chinese (zh)
Inventor
陈铁山
周翔
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Shanghai Lian Cai Chemical Trade Co Ltd
Original Assignee
Shanghai Lian Cai Chemical Trade Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Shanghai Lian Cai Chemical Trade Co Ltd filed Critical Shanghai Lian Cai Chemical Trade Co Ltd
Priority to CN201810036560.0A priority Critical patent/CN108342098A/en
Publication of CN108342098A publication Critical patent/CN108342098A/en
Pending legal-status Critical Current

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Classifications

    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09BORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
    • C09B67/00Influencing the physical, e.g. the dyeing or printing properties of dyestuffs without chemical reactions, e.g. by treating with solvents grinding or grinding assistants, coating of pigments or dyes; Process features in the making of dyestuff preparations; Dyestuff preparations of a special physical nature, e.g. tablets, films
    • C09B67/0071Process features in the making of dyestuff preparations; Dehydrating agents; Dispersing agents; Dustfree compositions
    • C09B67/008Preparations of disperse dyes or solvent dyes
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09BORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
    • C09B67/00Influencing the physical, e.g. the dyeing or printing properties of dyestuffs without chemical reactions, e.g. by treating with solvents grinding or grinding assistants, coating of pigments or dyes; Process features in the making of dyestuff preparations; Dyestuff preparations of a special physical nature, e.g. tablets, films
    • C09B67/0071Process features in the making of dyestuff preparations; Dehydrating agents; Dispersing agents; Dustfree compositions
    • C09B67/0084Dispersions of dyes
    • C09B67/0085Non common dispersing agents
    • C09B67/0086Non common dispersing agents anionic dispersing agents
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09BORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
    • C09B67/00Influencing the physical, e.g. the dyeing or printing properties of dyestuffs without chemical reactions, e.g. by treating with solvents grinding or grinding assistants, coating of pigments or dyes; Process features in the making of dyestuff preparations; Dyestuff preparations of a special physical nature, e.g. tablets, films
    • C09B67/0071Process features in the making of dyestuff preparations; Dehydrating agents; Dispersing agents; Dustfree compositions
    • C09B67/0092Dyes in solid form
    • C09B67/0095Process features in the making of granulates

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Dispersion Chemistry (AREA)
  • Inks, Pencil-Leads, Or Crayons (AREA)
  • Paints Or Removers (AREA)
  • Pigments, Carbon Blacks, Or Wood Stains (AREA)

Abstract

A kind of aqueous pigment preparations, the present invention relates to pigment technology fields;It is made of following parts by weight ingredient:800 1200 parts of water, 1,200 1300 parts of anion emulsifier, phthalocyanine blue b filter cake are given money as a gift 1,000 1500 parts of (pigment solid content 40% ± 2%), 100 200 parts of dispersant, 10 20 parts of antifoaming agent.Its Dust Capacity is few, realizes clean manufacturing, to human body safety, reduces grinding technics, more energy efficient environmental protection, the distribution of excellent initial size so that pigment coloring intensity higher reduces pigment cost, and practicability is stronger.

Description

A kind of aqueous pigment preparations
Technical field
The present invention relates to pigment technology fields, and in particular to a kind of aqueous pigment preparations.
Background technology
The dispersion process that the application of organic pigment has to pass through pigment makes granules of pigments reaches can direct requirement Grain size.More traditional water-based system application mode is that pigment toner is ground by grinder.It is prepared into original mill base, It is then added to the system for needing to colour.
Pigment preparations be it is a kind of using resin or dispersion as the granules of pigments of carrier cladding in the form of, it can be direct It is added to the coloring system for needing to colour, color depth as required adjusts additive amount, or mill base is first made, then adds.Pre- point Dispersed pigment apply clean manufacturing, it is healthy and safe, energy saving on have great significance.Pigment preparations are graininess or piece Shape has good powder fluidity, and dust is small, is greatly improved to environment and health of human body.It is made simultaneously using filter cake pre- Disperse pigment, reduces the grinding technics of mill base production, reduce energy consumption.
The prior art is primarily present some problems, such as:The initial size of pigment must be retained by being to grind just, Using the dispersant inclusion pigment particle of water-based system, in pigment water-washing process, dispersant can lose with flow, it would be highly desirable to change Into.
Invention content
In view of the defects and deficiencies of the prior art, the present invention intends to provide a kind of simple for process, reasonable design Aqueous pigment preparations, Dust Capacity is few, realizes clean manufacturing, to human body safety, reduces grinding technics, more energy efficient environmental protection, Excellent initial size distribution so that pigment coloring intensity higher reduces pigment cost, and practicability is stronger.
To achieve the above object, the technical solution adopted by the present invention is:It is made of following parts by weight ingredient:Water 800- 1200 parts, 1200-1300 parts of anion emulsifier, phthalocyanine blue b filter cake give money as a gift (pigment solid content 40% ± 2%) 1000-1500 Part, 100-200 parts of dispersant, 10-20 parts of antifoaming agent.
Further, the aqueous pigment preparations are made of following parts by weight ingredient:900-1000 parts of water, anion 1200-1250 parts of emulsifier, phthalocyanine blue b filter cake are given money as a gift 1300-1500 parts of (pigment solid content 40% ± 2%), dispersant 150- 200 parts, 15-20 parts of antifoaming agent.
Further, the aqueous pigment preparations are made of following parts by weight ingredient:It is 1000 parts of water, anionic emulsifying 1221 parts of agent, phthalocyanine blue filter cake are given money as a gift 1200 parts of (pigment solid content 40% ± 2%) B, 180 parts of dispersant, 18 parts of antifoaming agent.
Further, the anion emulsifier is by 073 anion emulsifiers of EPA and BV conc anion emulsifiers The mass ratio of composition, 073 anion emulsifiers of EPA and BV conc anion emulsifiers is 1:7, wherein the BV conc The activity of anion emulsifier is 50%.
The processing flow of the present invention is as follows:1000-1500 parts of phthalocyanine blue b filter cake is given money as a gift (pigment solid content 40% ± 2%) and in 1200-1250 parts of the suitable water of anion emulsifier input, mashing stirs evenly, and is then added 100-200 parts Dispersant continues plus water is adjusted to pigment content 20% or so until stirring evenly, and the total flow of water is 800-1200 parts, 10-20 parts of antifoaming agent is added, is dried by Pressuresprayingdrier, then detection packaging, you can.
Further, the tower height 17100mm of the Pressuresprayingdrier, tower diameter 3200mm, power 22KW, evaporation It is 300kg/h to measure, and between operating pressure 1-3MP, hot blast temperature is 105-120 DEG C, and mode of heating is that electricity adds fire coal(Oil)Hot wind Stove, rate of recovery 96-98%.
With the above structure, the present invention has the beneficial effect that:
1, clean manufacturing;
2, dust is reduced, the person is safer;
3, grinding technics is reduced, it is more energy efficient;
4, excellent initial size distribution, makes 85% pigment content reach former pigment coloring intensity higher;
5, pigment cost is reduced.
Specific implementation mode
Present embodiment(Embodiment one)The technical solution adopted is that:It is made of following parts by weight ingredient:Water 800 Part, 1200 parts of anion emulsifier, phthalocyanine blue b filter cake gives money as a gift 1000 parts of (pigment solid content 40% ± 2%), 100 parts of dispersant, 10 parts of antifoaming agent.
Further, the anion emulsifier is by 1050 parts of 073 anion emulsifiers of EPA and 150 parts of BV Conc anion emulsifiers form, wherein the activity of the BV conc anion emulsifiers is 50%.
The processing flow of present embodiment is as follows:1000 parts of phthalocyanine blue b filter cake is given money as a gift (pigment solid content 40% ± 2%) and in 1200 parts of the suitable water of anion emulsifier input, mashing stirs evenly, and 100 parts of dispersant is then added, Until stirring evenly, continues plus water is adjusted to pigment content 20% or so, the total flow of water is 800 parts(Without pigment filter cake Included water), 10 parts of antifoaming agent is added, is dried by Pressuresprayingdrier, then detection packaging, you can.
Further, the model YPG-300 of the Pressuresprayingdrier, tower height 17100mm, tower diameter 3200mm, Power is 22KW, and between evaporation capacity 300kg/h, operating pressure 1-3MP, hot blast temperature is 105-120 DEG C, and mode of heating is electricity Add fire coal(Oil)Hot-blast stove, rate of recovery 96-98%.
After above-mentioned technique, present embodiment has the beneficial effect that:Present embodiment provides a kind of technique letter Single, the aqueous pigment preparations of reasonable design, Dust Capacity is few, realizes clean manufacturing, to human body safety, reduces grinding work Skill, more energy efficient environmental protection, the distribution of excellent initial size so that pigment coloring intensity higher reduces pigment cost, and practicability is more By force.
Embodiment two:
Aqueous pigment preparations described in the present embodiment are made of following parts by weight ingredient:1000 parts of water, anion emulsifier 1235 parts, phthalocyanine blue b filter cake gives money as a gift 1400 parts of (pigment solid content 40% ± 2%), 150 parts of dispersant, 15 parts of antifoaming agent.
Further, the anion emulsifier is by 1085 parts of EPA073 anion emulsifiers and 155 parts BVconc anion emulsifiers form, wherein the activity of the BVconc anion emulsifiers is 50%.
In the processing flow of the present embodiment in addition between the content of each component and embodiment one there are other than different, remaining behaviour It is identical as embodiment one to make step.
Embodiment three:
Aqueous pigment preparations described in the present embodiment are made of following parts by weight ingredient:1000 parts of water, anion emulsifier 1216 parts, phthalocyanine blue b filter cake gives money as a gift 1200 parts of (pigment solid content 40% ± 2%), 180 parts of dispersant, 18 parts of antifoaming agent.
Further, the anion emulsifier is by 1064 parts of EPA073 anion emulsifiers and 152 parts BVconc anion emulsifiers form, wherein the activity of the BVconc anion emulsifiers is 50%.
In the processing flow of the present embodiment in addition between the content of each component and embodiment one there are other than different, remaining behaviour It is identical as embodiment one to make step.
The above is merely illustrative of the technical solution of the present invention and unrestricted, and those of ordinary skill in the art are to this hair The other modifications or equivalent replacement that bright technical solution is made, as long as it does not depart from the spirit and scope of the technical scheme of the present invention, It is intended to be within the scope of the claims of the invention.

Claims (6)

1. a kind of aqueous pigment preparations, it is characterised in that:It is made of following parts by weight ingredient:800-1200 parts of water, it is cloudy from Sub- emulsifier 1200-1300 parts, phthalocyanine blue b filter cake gives money as a gift 1000-1500 parts of (pigment solid content 40% ± 2%), dispersant 100- 200 parts, 10-20 parts of antifoaming agent.
2. a kind of aqueous pigment preparations according to claim 1, it is characterised in that:The aqueous pigment preparations by Following parts by weight ingredient composition:900-1000 parts of water, 1200-1250 parts of anion emulsifier, phthalocyanine blue b filter cake are given money as a gift (pigment Solid content 40% ± 2%) 1300-1500 parts, 150-200 parts of dispersant, 15-20 parts of antifoaming agent.
3. a kind of aqueous pigment preparations according to claim 1, it is characterised in that:The aqueous pigment preparations by Following parts by weight ingredient composition:1000 parts of water, 1221 parts of anion emulsifier, phthalocyanine blue b filter cake are given money as a gift (pigment solid content 40% ± 2%) 1200 parts, 180 parts of dispersant, 18 parts of antifoaming agent.
4. a kind of aqueous pigment preparations according to claim 1, it is characterised in that:The anion emulsifier by 073 anion emulsifiers of EPA and BVconc anion emulsifiers composition, EPA073 anion emulsifiers and BVconc anion The mass ratio of emulsifier is 1:7, wherein the activity of the BVconc anion emulsifiers is 50%.
5. a kind of aqueous pigment preparations, it is characterised in that:Its processing flow is as follows:1000-1500 parts of phthalocyanine blue b is filtered Cake and 1200-1300 parts of anion emulsifier are put into suitable water, and mashing stirs evenly, and are then added 100-200 parts Dispersant continues until stirring evenly plus water is adjusted to pigment content 20% or so, the total flow of water is 800-1200 parts (Water is carried without pigment filter cake), 10-20 parts of antifoaming agent is added, is dried by Pressuresprayingdrier, is then detected Packaging, you can.
6. a kind of aqueous pigment preparations according to claim 5, it is characterised in that:The Pressuresprayingdrier Between tower height 17100mm, tower diameter 3200mm, power 22KW, evaporation capacity 300kg/h, operating pressure 1-3MP, hot blast temperature It it is 105-120 DEG C, mode of heating is electricity plus coal-fired hot-blast stove, rate of recovery 96-98%.
CN201810036560.0A 2018-01-15 2018-01-15 A kind of aqueous pigment preparations Pending CN108342098A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201810036560.0A CN108342098A (en) 2018-01-15 2018-01-15 A kind of aqueous pigment preparations

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201810036560.0A CN108342098A (en) 2018-01-15 2018-01-15 A kind of aqueous pigment preparations

Publications (1)

Publication Number Publication Date
CN108342098A true CN108342098A (en) 2018-07-31

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Family Applications (1)

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CN201810036560.0A Pending CN108342098A (en) 2018-01-15 2018-01-15 A kind of aqueous pigment preparations

Country Status (1)

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CN (1) CN108342098A (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112048189A (en) * 2020-08-26 2020-12-08 宣城亚邦化工有限公司 System and method for preparing phthalocyanine blue P.B.15 by direct slurry acid swelling method

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112048189A (en) * 2020-08-26 2020-12-08 宣城亚邦化工有限公司 System and method for preparing phthalocyanine blue P.B.15 by direct slurry acid swelling method

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Application publication date: 20180731