CN108329981A - A kind of wearproof lubricant and preparation method - Google Patents

A kind of wearproof lubricant and preparation method Download PDF

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Publication number
CN108329981A
CN108329981A CN201810153639.1A CN201810153639A CN108329981A CN 108329981 A CN108329981 A CN 108329981A CN 201810153639 A CN201810153639 A CN 201810153639A CN 108329981 A CN108329981 A CN 108329981A
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Prior art keywords
base oil
lubricating oil
ball
succimide
oil
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CN201810153639.1A
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蒋秋菊
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Dalian Holy Education Consulting Co Ltd
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Dalian Holy Education Consulting Co Ltd
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Priority to CN201810153639.1A priority Critical patent/CN108329981A/en
Publication of CN108329981A publication Critical patent/CN108329981A/en
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    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10MLUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M169/00Lubricating compositions characterised by containing as components a mixture of at least two types of ingredient selected from base-materials, thickeners or additives, covered by the preceding groups, each of these compounds being essential
    • C10M169/04Mixtures of base-materials and additives
    • C10M169/048Mixtures of base-materials and additives the additives being a mixture of compounds of unknown or incompletely defined constitution, non-macromolecular and macromolecular compounds
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10MLUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M125/00Lubricating compositions characterised by the additive being an inorganic material
    • C10M125/26Compounds containing silicon or boron, e.g. silica, sand
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10MLUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2201/00Inorganic compounds or elements as ingredients in lubricant compositions
    • C10M2201/04Elements
    • C10M2201/041Carbon; Graphite; Carbon black
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10MLUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2201/00Inorganic compounds or elements as ingredients in lubricant compositions
    • C10M2201/06Metal compounds
    • C10M2201/062Oxides; Hydroxides; Carbonates or bicarbonates
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10MLUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2201/00Inorganic compounds or elements as ingredients in lubricant compositions
    • C10M2201/087Boron oxides, acids or salts
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10MLUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2205/00Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions
    • C10M2205/02Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions containing acyclic monomers
    • C10M2205/0206Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions containing acyclic monomers used as base material
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10MLUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2215/00Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant compositions
    • C10M2215/086Imides
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10MLUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2217/00Organic macromolecular compounds containing nitrogen as ingredients in lubricant compositions
    • C10M2217/06Macromolecular compounds obtained by functionalisation op polymers with a nitrogen containing compound
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10NINDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2030/00Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
    • C10N2030/04Detergent property or dispersant property
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10NINDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2030/00Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
    • C10N2030/06Oiliness; Film-strength; Anti-wear; Resistance to extreme pressure

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Lubricants (AREA)

Abstract

The present invention relates to a kind of wearproof lubricant and preparation methods, belong to lubricating oil field.Wearproof lubricant, the lubricating oil is by base oil and antiwear additive in mass ratio 100:1 ~ 10 composition, wherein the base oil is grouped as by following groups by mass percentage:PAO:2 ~ 5%, viscosity index improver:0 ~ 12%, pour-point depressant:0 ~ 3%, surplus Group III base oil;Mass parts are pressed in the lubrication oil antiwear agent, are grouped as by following groups:Lube base oil:30 ~ 70,hBN nanometer sheets:5~10;Nano-graphene:5~10;Aluminium hydroxide:3~5;Boron oxide:0.5~5;Polyisobutene succinimide 1 ~ 2;Aliphatic amine polyoxyethylene ether 1 ~ 2, succimide:1~5.Lubricating oil provided by the invention, service life is long, while the secondary wear extent that rubs reduces, and improves the secondary service life of friction, it is possible to prevente effectively from the deposition of greasy filth and carbon distribution, avoids the generation blocked.

Description

A kind of wearproof lubricant and preparation method
Technical field
The present invention relates to a kind of wearproof lubricant and preparation methods, belong to lubricating oil field.
Background technology
Lubricating oil is used in various types automobile, on mechanical equipment to reduce the liquid of friction, protection machinery and workpiece Or semisolid lubricants, the effects that mainly playing lubrication, cooling, antirust, cleaning, sealing and buffer.Lubricating oil is generally by base oil It is formed with additive two parts.Base oil is the main component of lubricating oil, decides that the fundamental property of lubricating oil, additive then may be used The deficiency of base oil aspect of performance is made up and improved, certain new performances is assigned, is the important component of lubricating oil.
Abrasion refers to that the complex behavior that secondary two relative motion surfaces of friction are constantly lost or are deformed at work is existing As, the abrasion of low friction pair can effectively be dropped using lubrication technology, but it is still inevitable.In especially tangible automobile engine, Cylinder during the motion, will produce a kind of high temperature extreme pressure environment, and under the environment, friction mill can occur for the secondary metal surface that rubs Damage forms gully or rough defect in metal surface.Meanwhile automobile engine is in the process of running, will produce product Carbon;Imperfect combustion fuel oil also will produce greasy filth simultaneously, greasy filth be mingled in lubricating oil or be attached to cylinder wall and other On parts, the bad phenomenons such as lubricating oil viscosity increases or cylinder blocks are caused, the normal operation of engine is influenced.
Invention content
In order to solve the above technical problems, a kind of wearproof lubricant lubricating oil of present invention offer is by base oil and antiwear additive group At the antiwear additive can solve cylindrical metal surfaces wear problem, and can avoid carbon distribution and greasy filth etc. and be attached to metal surface.
A kind of wearproof lubricant, the lubricating oil is by base oil and antiwear additive in mass ratio 100:1 ~ 10 composition, wherein
The base oil is grouped as by following groups by mass percentage:PAO:2 ~ 5%, viscosity index improver:0 ~ 12%, pour point depression Agent:0 ~ 3%, surplus Group III base oil;
Mass parts are pressed in the lubrication oil antiwear agent, are grouped as by following groups:Lube base oil:30 ~ 70,h- BN nanometer sheets:5~ 10;Nano-graphene:5~10;Aluminium hydroxide:3~5;Boron oxide:0.5~5;Polyisobutene succinimide 1 ~ 2;Fatty amine polyoxy Vinethene 1 ~ 2, succimide:1 ~ 5,
Wherein, describedh- BN nanometer sheets are made as follows:It, will under nitrogen atmosphereh- BN powders press quality with succimide Than being 1:100~1:200 mixing, carry out ball milling, 500 ~ 1000 r/min of rotational speed of ball-mill, Ball-milling Time is extremely in planetary ball mill Less for 24 hours;Powder after ball milling is placed in water, at least 72h is impregnated, it is dry, both.
Group III base oil of the present invention is that hydroisomerizing dewaxes III class base oils, such as HVI classes, MVI classes, specifically such as HVI-75SN, HVI-100SN, HVI-150SN, HVI-200SN etc..
Oil lubrication oil base oil described in antiwear additive of the present invention is Group III base oil.Its selection principle is:Institute It is identical as the lube base oil that lubricating oil is to be added with base oil.Granular antiwear additive is scattered in a small amount of base oil in advance In, it is ensured that convenience when addition and dispersibility.
Further, describedh- BN nanometer sheets are made as follows:It, will under nitrogen atmosphereh- BN powders are sub- with succinyl Amine is 1 in mass ratio:150~1:180 mixing, carry out ball milling, 600 ~ 800 r/min of rotational speed of ball-mill, ball milling in planetary ball mill 24 ~ 36h of time;Powder after ball milling is placed in water, 72 ~ 144h is impregnated, it is dry, both.
Further preferably, the lubricating oil presses mass parts with antiwear additive, is grouped as by following groups:
Lube base oil:30 ~ 70,h- BN nanometer sheets:5~10;Nano-graphene:5~10;Aluminium hydroxide:3~5;Boron oxide:1~ 3;Polyisobutene succinimide 1.5 ~ 2;Aliphatic amine polyoxyethylene ether 1 ~ 2, succimide:2~5.
Further preferably, the lubricating oil presses mass parts with antiwear additive, is grouped as by following groups:
Lube base oil:30 ~ 70,h- BN nanometer sheets:5~8;Nano-graphene:7~10;Aluminium hydroxide:4~5;Boron oxide:2~ 3;Polyisobutene succinimide 1.5 ~ 2;Aliphatic amine polyoxyethylene ether 1 ~ 2, succimide:2~5.
Further preferably, the mass parts of the lube base oil are 50 ~ 60.
The present invention further provides the preparation methods of above-mentioned lubricating oil antiwear additive, including following processing steps:
S1 will under nitrogen atmosphereh- BN powders are 1 in mass ratio with succimide:100~1:200 mixing, in planetary ball mill Ball milling is carried out in machine, 500 ~ 1000 r/min of rotational speed of ball-mill, Ball-milling Time is at least for 24 hours;Powder after ball milling is placed in water, is soaked At least 72h is steeped, it is dry, it obtainsh- BN nanometer sheets;
S2 is mixed antiwear additive raw material by material rate in sealing device, is excluded in sealing device using nitrogen after mixing Then air carries out it ultrasonic disperse, 1 ~ 6h of jitter time obtains suspension,
S3, by PAO, viscosity index improver, pour-point depressant, suspension obtained by S2 is placed in Group III base oil in proportion, and 70 ~ 90 At least 1h is stirred at DEG C, both.
In all technical solutions of the present invention, the preferably described base oil is grouped as by following groups by mass percentage:PAO:2~ 5%, viscosity index improver:1 ~ 10%, pour-point depressant:0.5 ~ 3%, surplus Group III base oil.
It is further preferred that the base oil, is grouped as by following groups by mass percentage:PAO:2 ~ 5%, viscosity index (VI) Modifier:3 ~ 8%, pour-point depressant:0.5 ~ 2%, surplus Group III base oil.
In all technical solutions of the present invention, it is preferably to describedhThe average grain diameter of-BN powders is 5 ~ 20 microns, further excellent It is selected as 10 ~ 20 microns, most preferably 10 microns.
In all technical solutions of the present invention, it is preferably to which the nano-graphene has parameters described below characteristic:The number of plies:1 ~ 20, Size is 2 ~ 10 microns, 35 ~ 58m of specific surface area2/g。
Further, it is preferable to which the nano-graphene has parameters described below characteristic:The number of plies:1 ~ 15, size is 5 ~ 8 microns, 42 ~ 45m of specific surface area2/g。
Beneficial effects of the present invention are:Lubricating oil of the present invention is made of base oil and antiwear additive, in the antiwear additive Includingh- BN nanometer sheets and nano-graphene.First willh- BN powders carry out lift-off processing, obtainh- BN nanometer sheets, the nanometer sheet The surface protection film that deposition assembling forms multiple-layer stacked, the abrasion for preventing friction secondary can be carried out in surface of friction pair.Meanwhile it is wear-resistant Aluminium hydroxide and boron oxide in agent can form the aluminium borate of wearability in surface of friction pair, withh- BN nanometer sheets and nanometer stone Black alkene is formed together composite functional material layer, further increases the wear resistence of surface of friction pair and ensures while less its is worn Gap appropriate is kept between cylinder and piston.Meanwhile polyisobutene succinimide is especially used, aliphatic amine polyoxyethylene Ether, succimide are compounded, and can effectively be prevented carbon distribution and greasy filth from being deposited in surface of friction pair, be further ensured resistance to Grind the formation of layer.In addition, succimide can ensurehWhen-BN nanometer sheets mix dispersion with base oil and other groups, do not send out Raw assembling aggregation.Lubricating oil provided by the invention, service life is long, while the secondary wear extent that rubs reduces, and it is secondary to improve friction Service life avoid the generation blocked it is possible to prevente effectively from the deposition of greasy filth and carbon distribution.
Specific implementation mode
The protection domain of invention is not limited to following embodiment disclosure of that, and invention is carried out simple deformation and combined Within all belonging to the scope of protection of the present invention.
It is used in following embodimentsh- BN nanometer sheets are made as follows:It is 10 micro- by average grain diameter under nitrogen atmosphere Riceh- BN powders are 1 in mass ratio with succimide:180 mixing, carry out ball milling, rotational speed of ball-mill in planetary ball mill 800 r/min, Ball-milling Time 36h;Powder after ball milling is placed in water, 96h is impregnated, it is dry, both.
Nano-graphene used in following embodiments has parameters described below characteristic:The number of plies:1 ~ 15, size is 5 ~ 8 microns, compares table 42 ~ 45m of area2/g。
III base oils in base oil described in following embodiments are Group III base oil HVI-100SN;In the antiwear additive Base oil used is Group III base oil HVI-100SN;The pour-point depressant is vinyl acetate-fumarate copolymer;It is described viscous Degree index improver is viscosity index improver OCP.
Embodiment 1
A kind of lubricating oil, the lubricating oil is by base oil and antiwear additive in mass ratio 100:5 compositions, wherein the base oil is pressed Mass percent is grouped as by following groups:PAO:4%, viscosity index improver:3%, pour-point depressant:1.5%, surplus Group III basis Oil;
The antiwear additive presses mass parts, is grouped as by following groups:Lube base oil:60,h- BN nanometer sheets:5;Nano-graphite Alkene:7;Aluminium hydroxide:3;Boron oxide:2;Polyisobutene succinimide 2;Aliphatic amine polyoxyethylene ether 1.5, succimide: 3,
Above-mentioned lubricating oil is made as follows:Antiwear additive raw material is mixed in sealing device by material rate, it is sharp after mixing The air in sealing device is excluded with nitrogen, ultrasonic disperse is then carried out to it, jitter time 4h obtains suspension;By PAO, Viscosity index improver, pour-point depressant, suspension are placed in Group III base oil in proportion, and 2h is stirred at 90 DEG C, both.
Embodiment 2
A kind of lubricating oil, the lubricating oil is by base oil and antiwear additive in mass ratio 100:5 compositions, wherein the base oil is pressed Mass percent is grouped as by following groups:PAO:4%, viscosity index improver:3%, pour-point depressant:1.5%, surplus Group III basis Oil;
The antiwear additive presses mass parts, is grouped as by following groups:Lube base oil:50,h- BN nanometer sheets:5;Nano-graphite Alkene:5;Aluminium hydroxide:4;Boron oxide:2;Polyisobutene succinimide 1.5;Aliphatic amine polyoxyethylene ether 2, succimide: 3,
Above-mentioned lubricating oil is made as follows:Antiwear additive raw material is mixed in sealing device by material rate, it is sharp after mixing The air in sealing device is excluded with nitrogen, ultrasonic disperse is then carried out to it, jitter time 4h obtains suspension;By PAO, Viscosity index improver, pour-point depressant, suspension are placed in Group III base oil in proportion, and 2h is stirred at 90 DEG C, both.
Embodiment 3
A kind of lubricating oil, the lubricating oil is by base oil and antiwear additive in mass ratio 100:5 compositions, wherein the base oil is pressed Mass percent is grouped as by following groups:PAO:4%, viscosity index improver:3%, pour-point depressant:1.5%, surplus Group III basis Oil;
The antiwear additive presses mass parts, lube base oil:60,h- BN nanometer sheets: 8;Nano-graphene:5;Aluminium hydroxide: 5;Boron oxide:2;Polyisobutene succinimide 2;Aliphatic amine polyoxyethylene ether 2, succimide:2,
Above-mentioned lubricating oil is made as follows:Antiwear additive raw material is mixed in sealing device by material rate, it is sharp after mixing The air in sealing device is excluded with nitrogen, ultrasonic disperse is then carried out to it, jitter time 4h obtains suspension;By PAO, Viscosity index improver, pour-point depressant, suspension are placed in Group III base oil in proportion, and 2h is stirred at 90 DEG C, both.
Embodiment 4
A kind of lubricating oil, the lubricating oil is by base oil and antiwear additive in mass ratio 100:5 compositions, wherein the base oil is pressed Mass percent is grouped as by following groups:PAO:4%, viscosity index improver:3%, pour-point depressant:1.5%, surplus Group III base oil;
The antiwear additive presses mass parts, is grouped as by following groups:Lube base oil:70,h- BN nanometer sheets: 9;Nano-graphite Alkene:6;Aluminium hydroxide: 5;Boron oxide:1;Polyisobutene succinimide 2;Aliphatic amine polyoxyethylene ether 2, succimide:5,
Above-mentioned lubricating oil is made as follows:Antiwear additive raw material is mixed in sealing device by material rate, it is sharp after mixing The air in sealing device is excluded with nitrogen, ultrasonic disperse is then carried out to it, jitter time 4h obtains suspension;By PAO, Viscosity index improver, pour-point depressant, suspension are placed in Group III base oil in proportion, and 2h is stirred at 90 DEG C, both.
Application examples 1 ~ 4
1 ~ 4 gained lubricating oil of embodiment is subjected to wear test, test force 500N, test speed in friction wear testing machine For 2500r/min, test period 48h, after running 48 hours, the results are shown in table below for sample relevant parameter.

Claims (6)

1. a kind of wearproof lubricant, the lubricating oil is by base oil and antiwear additive in mass ratio 100:1 ~ 10 composition, wherein
The base oil is grouped as by following groups by mass percentage:PAO:2 ~ 5%, viscosity index improver:0 ~ 12%, pour point depression Agent:0 ~ 3%, surplus Group III base oil;
Mass parts are pressed in the lubrication oil antiwear agent, are grouped as by following groups:Lube base oil:30 ~ 70,h- BN nanometer sheets:5~ 10;Nano-graphene:5~10;Aluminium hydroxide:3~5;Boron oxide:0.5~5;Polyisobutene succinimide 1 ~ 2;Fatty amine polyoxy Vinethene 1 ~ 2, succimide:1 ~ 5,
Wherein, describedh- BN nanometer sheets are made as follows:It, will under nitrogen atmosphereh- BN powders press quality with succimide Than being 1:100~1:200 mixing, carry out ball milling, 500 ~ 1000 r/min of rotational speed of ball-mill, Ball-milling Time is extremely in planetary ball mill Less for 24 hours;Powder after ball milling is placed in water, at least 72h is impregnated, it is dry, both.
2. lubricating oil according to claim 1, characterized in that describedh- BN nanometer sheets are made as follows:Nitrogen atmosphere It, will under enclosingh- BN powders are 1 in mass ratio with succimide:150~1:180 mixing, carry out ball milling in planetary ball mill, Rotational speed of ball-mill 600 ~ 800 r/min, 24 ~ 36h of Ball-milling Time;Powder after ball milling is placed in water, 72 ~ 144h is impregnated, it is dry, Both.
3. lubricating oil according to claim 1, characterized in that the lubricating oil presses mass parts with antiwear additive, by following groups It is grouped as:
Lube base oil:30 ~ 70,h- BN nanometer sheets:5~10;Nano-graphene:5~10;Aluminium hydroxide:3~5;Boron oxide:1~ 3;Polyisobutene succinimide 1.5 ~ 2;Aliphatic amine polyoxyethylene ether 1 ~ 2, succimide:2~5.
4. lubricating oil according to claim 1, characterized in that the lubricating oil presses mass parts with antiwear additive, by following groups It is grouped as:
Lube base oil:30 ~ 70,h- BN nanometer sheets:5~8;Nano-graphene:7~10;Aluminium hydroxide:4~5;Boron oxide:2~ 3;Polyisobutene succinimide 1.5 ~ 2;Aliphatic amine polyoxyethylene ether 1 ~ 2, succimide:2~5.
5. lubricating oil according to claim 1, characterized in that the mass parts of the lube base oil are 50 ~ 60.
6. the preparation method of lubricating oil described in claim 1, it is characterised in that:Including following processing steps:
S1 will under nitrogen atmosphereh- BN powders are 1 in mass ratio with succimide:100~1:200 mixing, in planetary ball mill Ball milling is carried out in machine, 500 ~ 1000 r/min of rotational speed of ball-mill, Ball-milling Time is at least for 24 hours;Powder after ball milling is placed in water, is soaked At least 72h is steeped, it is dry, it obtainsh- BN nanometer sheets;
S2 is mixed antiwear additive raw material by material rate in sealing device, is excluded in sealing device using nitrogen after mixing Then air carries out it ultrasonic disperse, 1 ~ 6h of jitter time obtains suspension,
S3, by PAO, viscosity index improver, pour-point depressant, suspension obtained by S2 is placed in Group III base oil in proportion, and 70 ~ 90 At least 1h is stirred at DEG C, both.
CN201810153639.1A 2018-02-22 2018-02-22 A kind of wearproof lubricant and preparation method Withdrawn CN108329981A (en)

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Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101070505A (en) * 2006-05-10 2007-11-14 韩永存 Anti-wear restoring agent and its preparing method and use
CN107090326A (en) * 2017-04-21 2017-08-25 四川碳世界科技有限公司 A kind of lubricating oil containing modified hexagonal boron nitride and graphene complex and preparation method thereof

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101070505A (en) * 2006-05-10 2007-11-14 韩永存 Anti-wear restoring agent and its preparing method and use
CN107090326A (en) * 2017-04-21 2017-08-25 四川碳世界科技有限公司 A kind of lubricating oil containing modified hexagonal boron nitride and graphene complex and preparation method thereof

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
胡春华等: "《装备摩擦表面润滑技术及应用》", 30 November 2012 *

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