CN108314156A - A kind of thick waste liquid solid-liquid separating agent and preparation method thereof - Google Patents

A kind of thick waste liquid solid-liquid separating agent and preparation method thereof Download PDF

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Publication number
CN108314156A
CN108314156A CN201810255754.XA CN201810255754A CN108314156A CN 108314156 A CN108314156 A CN 108314156A CN 201810255754 A CN201810255754 A CN 201810255754A CN 108314156 A CN108314156 A CN 108314156A
Authority
CN
China
Prior art keywords
flocculant
preparation
waste liquid
separating agent
thick waste
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201810255754.XA
Other languages
Chinese (zh)
Inventor
石双
杨惠琳
张瑞
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Chemical Laboratory Center Of Ningxia Baota (co Ltd)
Original Assignee
Chemical Laboratory Center Of Ningxia Baota (co Ltd)
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Chemical Laboratory Center Of Ningxia Baota (co Ltd) filed Critical Chemical Laboratory Center Of Ningxia Baota (co Ltd)
Priority to CN201810255754.XA priority Critical patent/CN108314156A/en
Publication of CN108314156A publication Critical patent/CN108314156A/en
Pending legal-status Critical Current

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Classifications

    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00Treatment of water, waste water, or sewage
    • C02F1/52Treatment of water, waste water, or sewage by flocculation or precipitation of suspended impurities
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00Treatment of water, waste water, or sewage
    • C02F1/52Treatment of water, waste water, or sewage by flocculation or precipitation of suspended impurities
    • C02F1/5236Treatment of water, waste water, or sewage by flocculation or precipitation of suspended impurities using inorganic agents
    • C02F1/5245Treatment of water, waste water, or sewage by flocculation or precipitation of suspended impurities using inorganic agents using basic salts, e.g. of aluminium and iron
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00Treatment of water, waste water, or sewage
    • C02F1/52Treatment of water, waste water, or sewage by flocculation or precipitation of suspended impurities
    • C02F1/54Treatment of water, waste water, or sewage by flocculation or precipitation of suspended impurities using organic material
    • C02F1/56Macromolecular compounds

Abstract

The present invention relates to a kind of solid-liquid separating agent of thick waste liquid, the mass percent of the binder is:Thick waste liquid 75-85%, flocculant I 12-20%, flocculant II 2 6%, pH adjusting agent.The preparation method of the release agent, preparation process are as follows:The preparation of inorganic polymer flocculant, the preparation of organic polymer flocculant, the mixing of flocculant and waste liquid.The technical program is the separation advantage in conjunction with inorganic flocculating agent, organic flocculant and high polymer coagulant, can effectively solve the problems, such as thick waste liquid difficulty separation, have the characteristics that investment is small, at low cost, easy to use, separating effect is notable, can use at normal temperatures.

Description

A kind of thick waste liquid solid-liquid separating agent and preparation method thereof
Technical field
The present invention relates to a kind of solid-liquid separating agent, especially a kind of solid-liquid separating agent of thick waste liquid.
Background technology
Compared with other industry, pharmacy waste water, livestock-raising waste water and amylum wastewater are thick solid-liquid mixing Waste liquid, complicated component, peculiar smell are big, coloration is deep, are always China's pollution most serious, most intractable industrial wastewater.Especially There is a large amount of organic matter difficult to degrade in pharmacy waste water, livestock-raising waste water and amylum wastewater(Such as phenols, quinones), meeting The generations such as soil, air, underground water are seriously affected.Currently, the process problem of thick waste liquid solves to have become full society in time The emphasis and hot spot that can be paid close attention to are not only the needs of environmental protection, the essential condition of even more related July sustainable development.Cause This there is an urgent need to a kind of solid-liquid separating agent of thick waste liquid, puts into the processing of waste liquid instantly, existing this to change Awkward situation.
Invention content
Present invention aim to address defect in the prior art, a kind of environmental pollution that can effectively reduce waste water is provided and is asked Topic, and solid-liquid separating agent easy to use, at low cost.
A kind of thick waste liquid solid-liquid separating agent, the mass percent of component are:
Water 75-85%, flocculant I 12-20%, II 2-6% of flocculant, wherein flocculant I are inorganic flocculating agent, and flocculant II is Organic flocculant.
The flocculant I is the polymerization ferrous sulfate in inorganic flocculating agent.
The flocculant II is the polymerization of acrylamide in organic flocculant.
A kind of preparation method of thick waste liquid solid-liquid separating agent, preparation process are as follows:
1)The preparation of inorganic flocculating agent:Flocculant I is heated to 40-50 DEG C under a small amount of water stirring, waits for whole dissolvings Afterwards, spare after stirring 5-15min under keeping warm mode;
2)The preparation of organic flocculant:Flocculant II is heated to 25-40 DEG C under a small amount of water stirring, waits for whole dissolvings It is spare afterwards;
3)Flocculant mixes:By above-mentioned steps 1 in the state of stirring)The flocculant I prepared is slowly added in flocculant II, PH is adjusted after uniform solution to be formed, after being cooled to room temperature to neutrality as finished product.
Above-mentioned pH adjusting agent is technical grade solid.
The solid-liquid separating agent of the present invention is suitable for pharmacy waste water, livestock-raising waste water, starch wastewater etc. or its mixed waste liquor Processing.The present invention is compound using organic and inorganic flocculating agent, the advantages of having both inorganic and organic polymer coargulator, while gram Take single flocculant there are the shortcomings that.Is all had by good clean-up effect while being had for various industrial sewage and invests small, cost The features such as low, easy to use.
Specific implementation mode
Below by taking double centner as an example, this technology method is described in detail as follows.
Embodiment 1:
1)The preparation of inorganic flocculating agent:It weighs 15 kilograms of polymerization ferrous sulfate and is heated to 40-50 under a small amount of water stirring DEG C, it is spare after stirring 5-15min under keeping warm mode after all dissolving;
2)The preparation of organic flocculant:It weighs 5 kilograms of polymerization of acrylamide and is heated to 25-40 DEG C under a small amount of water stirring, It is spare after all dissolving;
3)Flocculant mixes:By above-mentioned steps 1 in the state of stirring)The polymerization ferrous sulfate prepared is slowly added to polymerization third In acrylamide, double centner is added water to after uniform solution to be formed, pH is adjusted after being cooled to room temperature to neutrality as finished product.
Embodiment 2:
1)The preparation of inorganic flocculating agent:It weighs 12 kilograms of polymerization ferrous sulfate and is heated to 40-50 under a small amount of water stirring DEG C, it is spare after stirring 5-15min under keeping warm mode after all dissolving;
2)The preparation of organic flocculant:It weighs 3 kilograms of polymerization of acrylamide and is heated to 25-40 DEG C under a small amount of water stirring, It is spare after all dissolving;
3)Flocculant mixes:By above-mentioned steps 1 in the state of stirring)The polymerization ferrous sulfate prepared is slowly added to polymerization third In acrylamide, double centner is added water to after uniform solution to be formed, pH is adjusted after being cooled to room temperature to neutrality as finished product.

Claims (4)

1. a kind of thick waste liquid solid-liquid separating agent, the mass percent of component are:
Water 75-85%, flocculant I 12-20%, II 2-6% of flocculant, wherein flocculant I are inorganic flocculating agent, and flocculant II is Organic flocculant.
2. thick waste liquid solid-liquid separating agent according to claim 1, it is characterised in that the flocculant I is inorganic wadding Polymerization ferrous sulfate in solidifying agent.
3. thick waste liquid solid-liquid separating agent according to claim 1, it is characterised in that the flocculant II is organic Polymerization of acrylamide in flocculant.
4. a kind of preparation method of thick waste liquid solid-liquid separating agent, preparation process are as follows:
1)The preparation of inorganic flocculating agent:Flocculant I is heated to 40-50 DEG C under a small amount of water stirring, waits for whole dissolvings Afterwards, spare after stirring 5-15min under keeping warm mode;
2)The preparation of organic flocculant:Flocculant II is heated to 25-40 DEG C under a small amount of water stirring, waits for whole dissolvings It is spare afterwards;
3)Flocculant mixes:By above-mentioned steps 1 in the state of stirring)The flocculant I prepared is slowly added in flocculant II, PH is adjusted after uniform solution to be formed, after being cooled to room temperature to neutrality as finished product.
CN201810255754.XA 2018-03-27 2018-03-27 A kind of thick waste liquid solid-liquid separating agent and preparation method thereof Pending CN108314156A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201810255754.XA CN108314156A (en) 2018-03-27 2018-03-27 A kind of thick waste liquid solid-liquid separating agent and preparation method thereof

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201810255754.XA CN108314156A (en) 2018-03-27 2018-03-27 A kind of thick waste liquid solid-liquid separating agent and preparation method thereof

Publications (1)

Publication Number Publication Date
CN108314156A true CN108314156A (en) 2018-07-24

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Family Applications (1)

Application Number Title Priority Date Filing Date
CN201810255754.XA Pending CN108314156A (en) 2018-03-27 2018-03-27 A kind of thick waste liquid solid-liquid separating agent and preparation method thereof

Country Status (1)

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CN (1) CN108314156A (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108911082A (en) * 2018-07-31 2018-11-30 宁夏宝塔石化煤化工研究院有限公司 A kind of processing method of potato starch processing waste water

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1041927A (en) * 1988-10-15 1990-05-09 华北制药厂 Method for the treatment of penicillin waste water
KR20100127340A (en) * 2009-05-26 2010-12-06 한밭대학교 산학협력단 The composition which contains dredged sediments for red algae removal and a method of preparing thereof
CN106316004A (en) * 2016-11-07 2017-01-11 平潭盖亚环保科技有限公司 High-concentration organic wastewater direct deep purification method

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1041927A (en) * 1988-10-15 1990-05-09 华北制药厂 Method for the treatment of penicillin waste water
KR20100127340A (en) * 2009-05-26 2010-12-06 한밭대학교 산학협력단 The composition which contains dredged sediments for red algae removal and a method of preparing thereof
CN106316004A (en) * 2016-11-07 2017-01-11 平潭盖亚环保科技有限公司 High-concentration organic wastewater direct deep purification method

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108911082A (en) * 2018-07-31 2018-11-30 宁夏宝塔石化煤化工研究院有限公司 A kind of processing method of potato starch processing waste water

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Application publication date: 20180724

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