CN108311705A - A kind of production equipment for producing titanium valve - Google Patents
A kind of production equipment for producing titanium valve Download PDFInfo
- Publication number
- CN108311705A CN108311705A CN201810125046.4A CN201810125046A CN108311705A CN 108311705 A CN108311705 A CN 108311705A CN 201810125046 A CN201810125046 A CN 201810125046A CN 108311705 A CN108311705 A CN 108311705A
- Authority
- CN
- China
- Prior art keywords
- retort
- fixedly installed
- alembic
- connecting tube
- charging aperture
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
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Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
- B22F9/00—Making metallic powder or suspensions thereof
- B22F9/02—Making metallic powder or suspensions thereof using physical processes
- B22F9/04—Making metallic powder or suspensions thereof using physical processes starting from solid material, e.g. by crushing, grinding or milling
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B34/00—Obtaining refractory metals
- C22B34/10—Obtaining titanium, zirconium or hafnium
- C22B34/12—Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08
- C22B34/1263—Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08 obtaining metallic titanium from titanium compounds, e.g. by reduction
- C22B34/1268—Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08 obtaining metallic titanium from titanium compounds, e.g. by reduction using alkali or alkaline-earth metals or amalgams
- C22B34/1272—Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08 obtaining metallic titanium from titanium compounds, e.g. by reduction using alkali or alkaline-earth metals or amalgams reduction of titanium halides, e.g. Kroll process
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- Life Sciences & Earth Sciences (AREA)
- Environmental & Geological Engineering (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Geology (AREA)
- Engineering & Computer Science (AREA)
- Chemical & Material Sciences (AREA)
- Manufacturing & Machinery (AREA)
- Materials Engineering (AREA)
- Mechanical Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Manufacture And Refinement Of Metals (AREA)
Abstract
The invention discloses a kind of production equipments for producing titanium valve, including the first retort, alembic, second retort, first charging aperture, first discharge nozzle, second charging aperture, second discharge nozzle, third connecting tube and grinder, first retort side is fixedly installed alembic, and alembic is connect by the first connecting tube with the first retort, the alembic side is fixedly installed the second retort, and second retort connect with alembic by the second connecting tube, the first retort top side is fixedly installed first charging aperture, pot bottom is fixed is equipped with the first discharge nozzle for first retort and distillation, the second retort top side is fixedly installed second charging aperture.The present invention can effectively improve reaction efficiency by motor and blender, by heating tube and protractor, can effectively control temperature in tank, by reverse osmosis, can effectively prevent gas backstreaming.
Description
Technical field
The present invention relates to a kind of production equipment, more particularly to a kind of production equipment for producing titanium valve.
Background technology
The manufacturing method of common titanium valve is that the reduction that is occurred in closed reactor using smart magnesium and titanium tetrachloride is anti-
Metal sponge titanium should be generated, is aoxidized in order to prevent, reaction process needs to be protected using argon gas, and titanium is needed to be ground
Mill, to obtain titanium valve, but titanium sponge production equipment in the related technology, the purity of the titanium sponge of output is poor, with section
The growth of skill level, cannot be satisfied the quality requirements to titanium sponge.For this purpose, it is proposed that a kind of production equipment for producing titanium valve.
Invention content
The main purpose of the present invention is to provide a kind of production equipments for producing titanium valve can have by motor and blender
The raising reaction efficiency of effect can effectively control temperature in tank by heating tube and protractor, can be effective by reverse osmosis
Gas backstreaming is prevented, the problems in background technology can be effectively solved.
To achieve the above object, the technical solution that the present invention takes is：
A kind of production equipment for producing titanium valve, including the first retort, alembic, the second retort, first charging aperture, first go out
Expects pipe, second charging aperture, the second discharge nozzle, third connecting tube and grinder, first retort side are fixedly installed steaming
Tank is evaporated, and alembic is connect by the first connecting tube with the first retort, the alembic side is fixedly installed the second reaction
Tank, and the second retort is connect by the second connecting tube with alembic, the first retort top side is fixedly installed
Pot bottom is fixed is equipped with the first discharge nozzle, the second retort top side for one feed inlet, first retort and distillation
It is fixedly installed second charging aperture, second reaction tank wall side is fixedly installed the second discharge nozzle, second reaction
Pot bottom is fixedly installed third connecting tube, and second retort side fixed set has grinder, and grinder passes through
Third connecting tube is connected with the second retort, is fixedly installed motor at the top of first retort and the second retort, institute
It states motor bottom and is fixedly installed blender, first retort, alembic and the second reaction top tank structure are fixedly installed
Heating tube, first retort, alembic and the second retort top are fixedly installed protractor, the distillation tank wall
Surface is fixedly installed controller, and the second reaction tank wall other side is fixedly installed gas entrance.
Further, the first charging aperture and second charging aperture bottom side are fixedly installed electromagnetic valve, described
First discharge nozzle, connecting tube, the second discharge nozzle, third connecting tube and the second connecting tube side are fixedly installed electromagnetic switch.
Further, the gas entrance side is fixedly installed counter-osmosis device.
Further, first retort, alembic and the second retort bottom side are fixedly installed support leg.
Further, the motor, protractor, electromagnetic switch, electromagnetic valve and grinder pass through conducting wire and controller
It is electrically connected.
Compared with prior art, the present invention has the advantages that：
1. by the first retort, alembic and the second retort, effectively solid reaction can be provided for the production of titanium valve and held
Device so that production is safer, by controller, opens the electromagnetic valve in first charging aperture, simultaneously closes off other all valves
Door switch.
By first charging aperture, can the first retort effectively be added in ilmenite, coke and chlorine, passes through controller
The electromagnetic valve in first charging aperture is closed, the heating tube on the first reaction top tank structure is opened simultaneously, it, will by observing protractor
Temperature in first retort is controlled to 900 degree, while opening motor again.
It drives blender to be operated by motor, effectively the raw material in the first retort can be stirred so that
Reaction is more abundant, opens the electromagnetic switch in the first connecting tube by controller so that the titanium tetrachloride in the first retort
Entered in alembic by connecting tube with ferric trichloride, after waiting a period of times.
By controller, the electromagnetic switch in the first connecting tube is closed, the heating tube in alembic is opened simultaneously, passes through
The thermometer number of degrees at the top of alembic are observed, are opened titanium tetrachloride and ferric trichloride fractionation according to different liquids boiling point difference.
The electromagnetic switch in the second connecting tube is opened by controller, can titanium tetrachloride be effectively imported into the second reaction
Tank after waiting for a period of time, is closed the electromagnetic switch in the second connecting tube by controller, is opened simultaneously in second charging aperture
Excessive magnesium is added in electromagnetic valve, and additions is waited to complete, after closing electromagnetic valve.
By gas entrance and counter-osmosis device, it can be effectively filled with argon gas, and gas backstreaming can be prevented again, passed through
Controller opens the heating tube in the second retort, observes protractor in the second retort so that the temperature in tank reaches 1000
Degree, then the motor opened in the second retort drive blender to be stirred so that reaction is more abundant.
After waiting for fully reaction, the temperature in the second retort is controlled by controller, inner wall liquid is steamed again
It evaporates so that it is in control titanium from third connection, titanium is imported by grinder by third connecting tube, effectively titanium can be ground,
By third discharge port, titanium valve can be effectively obtained, by the first discharge nozzle and the second discharge nozzle, the first reaction can effectively be discharged
Other substances in tank, alembic and the second retort, improve production efficiency.
Description of the drawings
Fig. 1 is that the present invention is used for a kind of overall structure diagram of production equipment that producing titanium valve.
Fig. 2 is that the present invention is used for a kind of gas entrance structural schematic diagram of production equipment that producing titanium valve.
In figure：1, the first retort；2, alembic；3, the second retort；4, motor；5, blender；6, first charging aperture；
7, heating tube；8, the first discharge nozzle；9, the first connecting tube；10, protractor；11, controller；12, gas entrance；13, second
Feed inlet；14, the second discharge nozzle；15, third connecting tube；16, electromagnetic switch；17, electromagnetic valve；18, counter-osmosis device；19, it props up
Support leg；20, the second connecting tube；21 grinders；22, third discharge nozzle.
Specific implementation mode
To make the technical means, the creative features, the aims and the efficiencies achieved by the present invention be easy to understand, with reference to
Specific implementation mode, the present invention is further explained.
As shown in Figs. 1-2, a kind of production equipment for producing titanium valve, including the first retort 1, alembic 2, the second retort
3, first charging aperture 6, the first discharge nozzle 8, second charging aperture 13, the second discharge nozzle 14, third connecting tube 15 and grinder 21, institute
It states 1 side of the first retort and is fixedly installed alembic 2, and alembic 2 is connect by the first connecting tube 9 with the first retort 1,
2 side of the alembic is fixedly installed the second retort 3, and the second retort 3 is connected by the second connecting tube 20 with alembic 2
It connects, 1 top side of the first retort is fixedly installed first charging aperture 6,2 bottom of first retort 1 and alembic
Fixed to be equipped with the first discharge nozzle 8,3 top side of the second retort is fixedly installed second charging aperture 13, and described second is anti-
3 outer wall side of tank is answered to be fixedly installed the second discharge nozzle 14,3 bottom of the second retort is fixedly installed third connecting tube
15, second retort, 3 side fixed set has grinder 21, and grinder 21 is anti-by third connecting tube 15 and second
Tank 3 is answered to be connected, 1 and second retort of the first retort, 3 top is fixedly installed motor 4, and 4 bottom of the motor is fixed
It is provided with blender 5, first retort 1, alembic 2 and 3 inner wall of the second retort are fixedly installed heating tube 7, institute
It states the first retort 1, alembic 2 and 3 top of the second retort and is fixedly installed protractor 10,2 outer wall table of the alembic
Face is fixedly installed controller 11, and second retort, the 3 outer wall other side is fixedly installed gas entrance 12.
Wherein, the first charging aperture 6 and 13 bottom side of second charging aperture are fixedly installed electromagnetic valve 17, described
First discharge nozzle 8, connecting tube 9, the second discharge nozzle 14, third connecting tube 15 and 20 side of the second connecting tube are fixedly installed electricity
Magnetic switch 16.
Wherein, 12 side of the gas entrance is fixedly installed counter-osmosis device 18.
Wherein, first retort 1, alembic 2 and 3 bottom side of the second retort are fixedly installed support leg
19。
Wherein, the motor 4, protractor 10, electromagnetic switch 16, electromagnetic valve 17 and grinder 21 pass through conducting wire and control
Device 11 processed is electrically connected.
It should be noted that the present invention is a kind of production equipment for producing titanium valve, when work, passes through the first retort 1, steams
Tank 2 and the second retort 3 are evaporated, effectively can provide solid reaction vessel for the production of titanium valve so that production is safer, leads to
Cross controller 11, open the electromagnetic valve 17 in first charging aperture 6, simultaneously close off other all valve switch, by first into
Material mouth 6, effectively can be added the first retort 1 by ilmenite, coke and chlorine, and first charging aperture 6 is closed by controller 11
On electromagnetic valve 17, open simultaneously the heating tube 7 on 1 inner wall of the first retort, by observe protractor 10, by first reaction
Temperature in tank 1 is controlled to 900 degree, while opening motor 4 again, drives blender 5 to be operated by motor 4, can be effective
Raw material in first retort 1 is stirred so that reaction is more abundant, is opened in the first connecting tube 9 by controller 11
Electromagnetic switch 16 so that titanium tetrachloride and ferric trichloride in the first retort 1 are entered by connecting tube 9 in alembic 2, etc.
After a period of time, by controller 11, the electromagnetic switch 16 in the first connecting tube 9 is closed, the heating in alembic 2 is opened simultaneously
Pipe 7, by observing 10 number of degrees of thermometer at the top of alembic 2, according to different liquids boiling point difference by titanium tetrachloride and tri-chlorination
Iron fractionation is opened, and the electromagnetic switch 16 in the second connecting tube 20 is opened by controller 11, can titanium tetrachloride effectively be imported the
Two retort 3 after waiting for a period of time, are closed the electromagnetic switch 16 in the second connecting tube 20 by controller 11, are opened simultaneously
Excessive magnesium is added in electromagnetic valve 17 in second charging aperture 13, and additions is waited to complete, and after closing electromagnetic valve, is entered by gas
Mouth 12 and counter-osmosis device 18, can effectively be filled with argon gas, and can prevent gas backstreaming again, and it is anti-to open second by controller 1
The heating tube 7 in tank 3 is answered, observes protractor 10 in the second retort so that the temperature in tank reaches 1000 degree, then opens second
Motor 4 in retort drives blender to be stirred so that reaction is more abundant, after waiting for fully reaction, passes through controller
Temperature in 11 the second retort 3 of control, again distills inner wall liquid so that obtains titanium from third connecting tube 15, leads to
It crosses third connecting tube 15 and titanium is imported into grinder 21, effectively titanium can be ground, by third discharge port 22, can effectively be obtained
It is anti-can to be effectively discharged by the first discharge nozzle 8 and the second discharge nozzle 14 for the first retort 1, alembic 2 and second to titanium valve
Other substances in tank 3 are answered, production efficiency is improved.
The above shows and describes the basic principles and main features of the present invention and the advantages of the present invention.The technology of the industry
Personnel are it should be appreciated that the present invention is not limited to the above embodiments, and the above embodiments and description only describe this
The principle of invention, without departing from the spirit and scope of the present invention, various changes and improvements may be made to the invention, these changes
Change and improvement all fall within the protetion scope of the claimed invention.The claimed scope of the invention by appended claims and its
Equivalent thereof.
Claims (5)
1. a kind of production equipment for producing titanium valve, including the first retort（1）, alembic（2）, the second retort（3）, first into
Material mouth（6）, the first discharge nozzle（8）, second charging aperture（13）, the second discharge nozzle（14）, third connecting tube（15）And grinder
（21）, first retort（1）Side is fixedly installed alembic（2）, and alembic（2）Pass through the first connecting tube（9）With
First retort（1）Connection, the alembic（2）Side is fixedly installed the second retort（3）, and the second retort（3）It is logical
Cross the second connecting tube（20）With alembic（2）Connection, first retort（1）Top side is fixedly installed first charging aperture
（6）, first retort（1）And alembic（2）Bottom is fixed to be equipped with the first discharge nozzle（8）, second retort（3）Top
Portion side is fixedly installed second charging aperture（13）, second retort（3）Outer wall side is fixedly installed the second discharge nozzle
（14）, second retort（3）Bottom is fixedly installed third connecting tube（15）, second retort（3）Side is fixed
Formula is provided with grinder（21）, and grinder（21）Pass through third connecting tube（15）With the second retort（3）It is connected, feature exists
In：First retort（1）With the second retort（3）Top is fixedly installed motor（4）, the motor（4）Bottom is solid
Surely it is provided with blender（5）, first retort（1）, alembic（2）With the second retort（3）Inner wall is fixedly installed
Heating tube（7）, first retort（1）, alembic（2）With the second retort（3）Top is fixedly installed protractor
（10）, the alembic（2）Outer wall surface is fixedly installed controller（11）, second retort（3）The outer wall other side is solid
Surely it is provided with gas entrance（12）.
2. a kind of production equipment for producing titanium valve according to claim 1, it is characterised in that：The first charging aperture（6）
And second charging aperture（13）Bottom side is fixedly installed electromagnetic valve（17）, first discharge nozzle（8）, connecting tube（9）、
Second discharge nozzle（14）, third connecting tube（15）With the second connecting tube（20）Side is fixedly installed electromagnetic switch（16）.
3. a kind of production equipment for producing titanium valve according to claim 1, it is characterised in that：The gas entrance（12）
Side is fixedly installed counter-osmosis device（18）.
4. a kind of production equipment for producing titanium valve according to claim 1, it is characterised in that：First retort（1）、
Alembic（2）With the second retort（3）Bottom side is fixedly installed support leg（19）.
5. a kind of production equipment for producing titanium valve according to claim 1, it is characterised in that：The motor（4）, protractor
（10）, electromagnetic switch（16）, electromagnetic valve（17）And grinder（21）Pass through conducting wire and controller（11）It is electrically connected.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810125046.4A CN108311705A (en) | 2018-02-07 | 2018-02-07 | A kind of production equipment for producing titanium valve |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810125046.4A CN108311705A (en) | 2018-02-07 | 2018-02-07 | A kind of production equipment for producing titanium valve |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN108311705A true CN108311705A (en) | 2018-07-24 |
Family
ID=62903077
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201810125046.4A Pending CN108311705A (en) | 2018-02-07 | 2018-02-07 | A kind of production equipment for producing titanium valve |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN108311705A (en) |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2003040418A1 (en) * | 2001-11-09 | 2003-05-15 | Sumitomo Titanium Corporation | Method for producing titanium material of low oxygen content |
| CN101386920A (en) * | 2007-09-13 | 2009-03-18 | 贵阳铝镁设计研究院 | Reduction-distillation method of titanium sponge and U type complex unit |
| CN102560152A (en) * | 2012-01-18 | 2012-07-11 | 深圳市新星轻合金材料股份有限公司 | Reaction device for producing titanium sponge |
| CN204522340U (en) * | 2015-03-19 | 2015-08-05 | 江西盛伟实业有限公司 | A kind of novel distillation still |
| CN205773427U (en) * | 2016-05-26 | 2016-12-07 | 宜宾天原集团股份有限公司 | The chlorination furnace of recyclable ferric chloride goes out furnace gas gas solid separation system |
-
2018
- 2018-02-07 CN CN201810125046.4A patent/CN108311705A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2003040418A1 (en) * | 2001-11-09 | 2003-05-15 | Sumitomo Titanium Corporation | Method for producing titanium material of low oxygen content |
| CN101386920A (en) * | 2007-09-13 | 2009-03-18 | 贵阳铝镁设计研究院 | Reduction-distillation method of titanium sponge and U type complex unit |
| CN102560152A (en) * | 2012-01-18 | 2012-07-11 | 深圳市新星轻合金材料股份有限公司 | Reaction device for producing titanium sponge |
| CN204522340U (en) * | 2015-03-19 | 2015-08-05 | 江西盛伟实业有限公司 | A kind of novel distillation still |
| CN205773427U (en) * | 2016-05-26 | 2016-12-07 | 宜宾天原集团股份有限公司 | The chlorination furnace of recyclable ferric chloride goes out furnace gas gas solid separation system |
Non-Patent Citations (1)
| Title |
|---|
| 野田敏男: "日本用高钛渣以镁还原法制取钛", 《国外轻金属》 * |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20180724 |
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| RJ01 | Rejection of invention patent application after publication |