CN108277500A - A kind of diamond electrorefining device - Google Patents
A kind of diamond electrorefining device Download PDFInfo
- Publication number
- CN108277500A CN108277500A CN201810334384.9A CN201810334384A CN108277500A CN 108277500 A CN108277500 A CN 108277500A CN 201810334384 A CN201810334384 A CN 201810334384A CN 108277500 A CN108277500 A CN 108277500A
- Authority
- CN
- China
- Prior art keywords
- diamond
- height
- fixed column
- electrolytic cell
- rotary box
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 229910003460 diamond Inorganic materials 0.000 title claims abstract description 27
- 239000010432 diamond Substances 0.000 title claims abstract description 27
- 238000003756 stirring Methods 0.000 claims abstract description 21
- 230000006835 compression Effects 0.000 claims abstract description 19
- 238000007906 compression Methods 0.000 claims abstract description 19
- 238000007789 sealing Methods 0.000 claims abstract description 19
- 239000007787 solid Substances 0.000 claims 1
- 239000011812 mixed powder Substances 0.000 abstract description 16
- 239000003792 electrolyte Substances 0.000 abstract description 7
- 230000000694 effects Effects 0.000 abstract description 3
- 238000005516 engineering process Methods 0.000 description 3
- 238000000034 method Methods 0.000 description 3
- 239000000843 powder Substances 0.000 description 3
- 230000002194 synthesizing effect Effects 0.000 description 3
- 230000005611 electricity Effects 0.000 description 2
- 238000005868 electrolysis reaction Methods 0.000 description 2
- 230000001360 synchronised effect Effects 0.000 description 2
- 241001074085 Scophthalmus aquosus Species 0.000 description 1
- 238000005260 corrosion Methods 0.000 description 1
- 230000007797 corrosion Effects 0.000 description 1
- 238000005520 cutting process Methods 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 238000000227 grinding Methods 0.000 description 1
- 238000009434 installation Methods 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 238000003825 pressing Methods 0.000 description 1
- 230000001681 protective effect Effects 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 239000004065 semiconductor Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25B—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
- C25B1/00—Electrolytic production of inorganic compounds or non-metals
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25B—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
- C25B15/00—Operating or servicing cells
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25B—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
- C25B15/00—Operating or servicing cells
- C25B15/08—Supplying or removing reactants or electrolytes; Regeneration of electrolytes
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Electrochemistry (AREA)
- Materials Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Electrolytic Production Of Non-Metals, Compounds, Apparatuses Therefor (AREA)
Abstract
The invention discloses a kind of diamond electrorefining devices, including electrolytic cell, the electrolytic cell bottom is equipped with stirring motor, the stirring motor output end is equipped with rotary shaft, the upper end of the rotary shaft is equipped with rotary box, the rotary box upper surface is provided with mounting groove, and putting bag is placed with inside the rotary box；The electrolytic cell side is equipped with loading plate, the loading plate bottom end is equipped with height-regulating motor, the loading plate upper end is equipped with height-regulating leading screw, lifter plate is installed on the height-regulating leading screw, the lifter plate bottom is equipped with fixed column, sealing clamp is installed on the outside of the fixed column, the sealing clamp bottom face is equipped with compression ring.Advantageous effect is：The fast assembling-disassembling that putting bag can be realized by compression ring and mounting groove cooperation, is easy to implement picking and placeing for mixed powder, helps to improve the performance of device；Rotary shaft is driven by stirring motor, so that rotary box is rotated, mixed powder is made to be come into full contact with electrolyte, help to improve electrolytic efficiency.
Description
Technical field
The present invention relates to diamond process units technical fields, and in particular to a kind of diamond electrorefining device.
Background technology
Diamond is machined to the primary raw material of jewelry, and hardness is high, wearability is good, is widely used in cutting, grinding, brill
It visits.Since diamond thermal conductivity is high, electrical insulating property is good, the heat sink of semiconductor device can be used as；There is excellent translucency
And corrosion resistance, it is also used widely in the electronics industry.In the production process for carrying out diamond, in order to improve diamond
Purity, need to crush diamond synthesizing stick, be electrolysed, to the medium metal that is mixed with of removal.
Applicants have discovered that at least there is following technical problem in the prior art：Current electrolysis unit is not easy to realize mixed
Picking and placeing for powder is closed, the performance of device is influenced；Device cannot achieve stirring simultaneously, and mixed powder is insufficient with electrolyte contacts,
Influence electrolytic efficiency.
Invention content
The purpose of the present invention is that solve the above-mentioned problems and provides a kind of diamond electrorefining device, to solve
Current electrolysis unit is not easy to realize picking and placeing for mixed powder in the prior art, influences the performance of device；Simultaneously device without
Method realizes stirring, and mixed powder is insufficient with electrolyte contacts, influences the technical problems such as electrolytic efficiency.Many skills provided by the invention
Preferred technical solution can realize the fast assembling-disassembling of putting bag by compression ring and mounting groove cooperation in art scheme, be easy to implement
Mixed powder picks and places, and helps to improve the performance of device；Rotary shaft is driven by stirring motor, rotary box is made to rotate, it is real
Now to the stirring of mixed powder, mixed powder can be made to be come into full contact with electrolyte, help to improve the technique effects such as electrolytic efficiency, in detail
See below elaboration.
To achieve the above object, the present invention provides following technical schemes：
A kind of diamond electrorefining device provided by the invention, including electrolytic cell, the electrolytic cell inner wall are equipped with cathode, institute
It states electrolytic cell bottom and stirring motor is installed, the output end of the stirring motor stretches into inside the electrolytic cell, the stirring electricity
The output end of machine is equipped with rotary shaft, and the upper end of the rotary shaft is equipped with rotary box, and the rotary box uses engraved structure,
The rotary box upper surface is provided with mounting groove, and putting bag is placed with inside the rotary box；
The electrolytic cell side is equipped with loading plate, and the loading plate bottom end is equipped with height-regulating motor, the loading plate upper end peace
Equipped with leading screw is turned up, the height-regulating leading screw is fixedly connected with the height-regulating motor；It is equipped with by nut on the height-regulating leading screw
Lifter plate, the lifter plate bottom are equipped with fixed column, and bottom is equipped with anode in the fixed column, and the anode is pierced by described
Fixed column；Sealing clamp is equipped with by bearing on the outside of the fixed column, the sealing clamp bottom face is equipped with compression ring, institute
It is corresponding with the mounting groove to state compression ring.
Using a kind of above-mentioned diamond electrorefining device, when use device, the mixed powder of diamond synthesizing stick is placed
It is sleeved on inside the rotary box inside the putting bag, and by the putting bag, described in height-regulating motor drive
Leading screw rotation is turned up, to make the lifter plate decline on the outside of the height-regulating leading screw, until the compression ring enters the peace
Inside tankage, and the upper surface of the sealing clamp and the rotary box is in close contact, and finally realizes the fixation of the putting bag,
So that the height-regulating motor is reversely rotated, just can realize the unlock of the stationary state of the putting bag, it is mixed to be easy to implement diamond
Picking and placeing for powder is closed, the performance of device is helped to improve；When being electrolysed, the stirring motor work passes through the rotation
Axis drives the rotary box rotation, described close since the sealing clamp is mounted on by bearing on the outside of the fixed column
Envelope pressing plate can be rotated with the rotary box, finally made the putting bag and the rotary box synchronous rotary, can be made diamond
Mixed powder comes into full contact with electrolyte, helps to improve electrolytic efficiency.
Preferably, the rotary shaft, the rotary box and the sealing clamp surface are coated with insulating film.
Preferably, the fixed column uses hollow structure, and the upper end of the fixed column passes through the lifter plate.
Preferably, the loading plate upper end is symmetrically installed with two guide posts, the guide post is located at the height-regulating silk
Thick stick both sides, and pass through the lifter plate.
Preferably, the external dimensions of the compression ring is equal with the inside dimension of the mounting groove, and matched using gap
It closes.
Preferably, the height dimension of the compression ring is less than the depth dimensions of the mounting groove.
Advantageous effect is：1, the quick of the putting bag can be realized by the compression ring and mounting groove cooperation
Dismounting, is easy to implement picking and placeing for mixed powder, helps to improve the performance of device；
2, the rotary shaft is driven by the stirring motor, the rotary box is made to rotate, realize the stirring to mixed powder, it can
So that mixed powder is come into full contact with electrolyte, helps to improve electrolytic efficiency.
Description of the drawings
In order to more clearly explain the embodiment of the invention or the technical proposal in the existing technology, to embodiment or will show below
There is attached drawing needed in technology description to be briefly described, it should be apparent that, the accompanying drawings in the following description is only this
Some embodiments of invention for those of ordinary skill in the art without creative efforts, can be with
Obtain other attached drawings according to these attached drawings.
Fig. 1 is the internal structure schematic diagram of the present invention；
Fig. 2 is the close-up schematic view of the present invention；
Fig. 3 is the right view of the present invention.
The reference numerals are as follows：
1, electrolytic cell；2, cathode；3, sealing clamp；301, compression ring；4, fixed column；5, lifter plate；6, leading screw is turned up；7, it carries
Plate；8, motor is turned up；9, rotary box；901, mounting groove；10, rotary shaft；11, stirring motor；12, anode；13, putting bag；14、
Guide post.
Specific implementation mode
To make the object, technical solutions and advantages of the present invention clearer, technical scheme of the present invention will be carried out below
Detailed description.Obviously, described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.Base
Embodiment in the present invention, those of ordinary skill in the art are obtained all without making creative work
Other embodiment belongs to the range that the present invention is protected.
Shown in Fig. 1-Fig. 3, the present invention provides a kind of diamond electrorefining device, including electrolytic cell 1, electrolytic cells
1 inner wall is equipped with cathode 2, and 1 bottom of electrolytic cell is equipped with stirring motor 11, and the output end of stirring motor 11 stretches into electrolytic cell 1
The output end in portion, stirring motor 11 is equipped with rotary shaft 10, and the upper end of rotary shaft 10 is equipped with rotary box 9, and rotary box 9 uses
Engraved structure, 9 upper surface of rotary box are provided with mounting groove 901, putting bag 13 are placed with inside rotary box 9；
1 side of electrolytic cell is equipped with loading plate 7, and 7 bottom end of loading plate, which is equipped with, is turned up motor 8, and 7 upper end of loading plate is equipped with height-regulating
Leading screw 6 is turned up leading screw 6 and is fixedly connected with motor 8 is turned up；It is turned up on leading screw 6 and lifter plate 5,5 bottom of lifter plate is equipped with by nut
Portion is equipped with fixed column 4, and bottom is equipped with anode 12 in fixed column 4, and anode 12 is pierced by fixed column 4；4 outside of fixed column passes through axis
It holds and sealing clamp 3 is installed, 3 bottom face of sealing clamp is equipped with compression ring 301, and compression ring 301 is corresponding with mounting groove 901.
As optional embodiment, rotary shaft 10, rotary box 9 and 3 surface of sealing clamp are coated with insulating film, in this way
Setting can play a protective role to rotary shaft 10, rotary box 9 and sealing clamp 3, help to improve the service life of device；
Fixed column 4 uses hollow structure, and the upper end of fixed column 4 passes through lifter plate 5, in this way setting to be easy to implement anode 12
Electrical connection；
7 upper end of loading plate is symmetrically installed with two guide posts 14, and guide post 14, which is located at, is turned up 6 both sides of leading screw, and passes through lifter plate
5, setting in this way can play lifter plate 5 guiding and position-limiting action, ensure that lifter plate 5 lifts steadily；
The external dimensions of compression ring 301 is equal with the inside dimension of mounting groove 901, and is gap-matched, and setting can in this way
It improves, the leakproofness between sealing clamp 3 and rotary box 9, prevents that diamond mixed powder is caused to reveal；
The height dimension of compression ring 301 is less than the depth dimensions of mounting groove 901, is convenient for putting bag 13 being pressed into mounting groove in this way
Inside 901, ensure the installation stability of putting bag 13.
Using the above structure, when use device, the mixed powder of diamond synthesizing stick is placed on inside putting bag 13, and will
Putting bag 13 is sleeved on inside rotary box 9, drives height-regulating leading screw 6 to rotate by the way that motor 8 is turned up, to make lifter plate 5 be turned up
6 outside of leading screw declines, until compression ring 301 enters inside mounting groove 901, and sealing clamp 3 and the upper surface of rotary box 9 are close
Contact, the final fixation for realizing putting bag 13, makes height-regulating motor 8 reversely rotate, just can realize the stationary state of putting bag 13
Unlock, be easy to implement picking and placeing for diamond mixed powder, help to improve the performance of device；When being electrolysed, stirring electricity
Machine 11 works, and drives rotary box 9 to rotate by rotary shaft 10, since sealing clamp 3 is mounted on 4 outside of fixed column by bearing,
Therefore sealing clamp 3 can be rotated with rotary box 9, finally make putting bag 13 and 9 synchronous rotary of rotary box, and diamond can be made mixed
It closes powder to come into full contact with electrolyte, helps to improve electrolytic efficiency.
The above description is merely a specific embodiment, but scope of protection of the present invention is not limited thereto, any
Those familiar with the art in the technical scope disclosed by the present invention, can easily think of the change or the replacement, and should all contain
Lid is within protection scope of the present invention.Therefore, protection scope of the present invention should be based on the protection scope of the described claims.
Claims (6)
1. a kind of diamond electrorefining device, including electrolytic cell（1）, it is characterised in that：The electrolytic cell（1）Inner wall is equipped with
Cathode（2）, the electrolytic cell（1）Bottom is equipped with stirring motor（11）, the stirring motor（11）Output end stretch into it is described
Electrolytic cell（1）Inside, the stirring motor（11）Output end rotary shaft is installed（10）, the rotary shaft（10）Upper end
Rotary box is installed（9）, the rotary box（9）Using engraved structure, the rotary box（9）Upper surface is provided with mounting groove
（901）, the rotary box（9）Inside is placed with putting bag（13）；
The electrolytic cell（1）Side is equipped with loading plate（7）, the loading plate（7）Bottom end is equipped with height-regulating motor（8）, described
Loading plate（7）Upper end is equipped with height-regulating leading screw（6）, the height-regulating leading screw（6）With the height-regulating motor（8）It is fixedly connected；It is described
Leading screw is turned up（6）It is upper that lifter plate is equipped with by nut（5）, the lifter plate（5）Bottom is equipped with fixed column（4）, described solid
Fixed column（4）Interior bottom is equipped with anode（12）, the anode（12）It is pierced by the fixed column（4）；The fixed column（4）Outside is logical
It crosses bearing and sealing clamp is installed（3）, the sealing clamp（3）Bottom face is equipped with compression ring（301）, the compression ring
（301）With the mounting groove（901）It is corresponding.
2. a kind of diamond electrorefining device according to claim 1, it is characterised in that：The rotary shaft（10）, institute
State rotary box（9）With the sealing clamp（3）Surface is coated with insulating film.
3. a kind of diamond electrorefining device according to claim 1, it is characterised in that：The fixed column（4）In
Hollow structure, and the fixed column（4）Upper end pass through the lifter plate（5）.
4. a kind of diamond electrorefining device according to claim 1, it is characterised in that：The loading plate（7）Upper end pair
Title is equipped with two guide posts（14）, the guide post（14）Positioned at the height-regulating leading screw（6）Both sides, and pass through the lifter plate
（5）.
5. a kind of diamond electrorefining device according to claim 1, it is characterised in that：The compression ring（301）It is outer
Portion's size and the mounting groove（901）Inside dimension it is equal, and be gap-matched.
6. a kind of diamond electrorefining device according to claim 2, it is characterised in that：The compression ring（301）Height
It spends size and is less than the mounting groove（901）Depth dimensions.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810334384.9A CN108277500A (en) | 2018-04-14 | 2018-04-14 | A kind of diamond electrorefining device |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810334384.9A CN108277500A (en) | 2018-04-14 | 2018-04-14 | A kind of diamond electrorefining device |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN108277500A true CN108277500A (en) | 2018-07-13 |
Family
ID=62811507
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201810334384.9A Pending CN108277500A (en) | 2018-04-14 | 2018-04-14 | A kind of diamond electrorefining device |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN108277500A (en) |
Citations (17)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO1992007664A1 (en) * | 1990-10-29 | 1992-05-14 | Diamond Technologies Company | Method of treating and depositing diamonds |
| CN1068153A (en) * | 1991-06-22 | 1993-01-20 | 中国有色金属工业总公司矿产地质研究院 | Artificial diamond purifying apparatus using electrical power to remove catalyst metal |
| CN2269403Y (en) * | 1996-05-08 | 1997-12-03 | 钟俊达 | Multifunctional artificial diamond synthetic block electrolytic device |
| CN101049929A (en) * | 2007-05-18 | 2007-10-10 | 河南中南工业有限责任公司 | Technical method for electrorefining diamond |
| CN102776526A (en) * | 2012-07-30 | 2012-11-14 | 中南钻石股份有限公司 | Recovery method of fine catalyst metal obtained after electrolysis and purification of synthetic diamond powder |
| JP2014095110A (en) * | 2012-11-08 | 2014-05-22 | Kobe Steel Ltd | Diamond electrode and manufacturing method thereof, and ozone generator using the diamond electrode |
| CN203923393U (en) * | 2014-05-14 | 2014-11-05 | 河南飞孟金刚石工业有限公司 | A kind of diamond synthetic rod electrolytic processing apparatus |
| CN204107577U (en) * | 2014-09-10 | 2015-01-21 | 河南省力量新材料有限公司 | Ultra-fine diamond is purified and is used graphite separator |
| CN204298476U (en) * | 2014-06-17 | 2015-04-29 | 中山大学 | A kind of modified electrode ultrasonic assistant in-pulp electrolysis device |
| CN104925804A (en) * | 2015-07-20 | 2015-09-23 | 三门峡天钻晶体材料有限公司 | Diamond synthesis rod physical dissociation purifying device and method |
| CN104941813A (en) * | 2015-06-04 | 2015-09-30 | 中南钻石有限公司 | Electric separation and purification process of artificial diamonds |
| CN104986761A (en) * | 2015-06-25 | 2015-10-21 | 河南黄河旋风股份有限公司 | Efficient electrolyte purified through artificial diamond |
| CN204752216U (en) * | 2015-07-20 | 2015-11-11 | 三门峡天钻晶体材料有限公司 | Physics of synthetic stick of diamond purification device that dissociates |
| CN106145105A (en) * | 2016-06-13 | 2016-11-23 | 安庆市凯立金刚石科技有限公司 | A kind of purification of diamond electrolyte |
| CN107254691A (en) * | 2017-06-13 | 2017-10-17 | 青岛聚鑫园工贸有限公司 | A kind of method by electric capacity comprehensive reutilization waste diamond tool valuable element |
| CN107308846A (en) * | 2017-06-16 | 2017-11-03 | 江苏大学 | A kind of automatic blending system |
| CN208038569U (en) * | 2018-04-14 | 2018-11-02 | 新郑市新材料专业孵化器服务中心 | A kind of diamond electrorefining device |
-
2018
- 2018-04-14 CN CN201810334384.9A patent/CN108277500A/en active Pending
Patent Citations (17)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO1992007664A1 (en) * | 1990-10-29 | 1992-05-14 | Diamond Technologies Company | Method of treating and depositing diamonds |
| CN1068153A (en) * | 1991-06-22 | 1993-01-20 | 中国有色金属工业总公司矿产地质研究院 | Artificial diamond purifying apparatus using electrical power to remove catalyst metal |
| CN2269403Y (en) * | 1996-05-08 | 1997-12-03 | 钟俊达 | Multifunctional artificial diamond synthetic block electrolytic device |
| CN101049929A (en) * | 2007-05-18 | 2007-10-10 | 河南中南工业有限责任公司 | Technical method for electrorefining diamond |
| CN102776526A (en) * | 2012-07-30 | 2012-11-14 | 中南钻石股份有限公司 | Recovery method of fine catalyst metal obtained after electrolysis and purification of synthetic diamond powder |
| JP2014095110A (en) * | 2012-11-08 | 2014-05-22 | Kobe Steel Ltd | Diamond electrode and manufacturing method thereof, and ozone generator using the diamond electrode |
| CN203923393U (en) * | 2014-05-14 | 2014-11-05 | 河南飞孟金刚石工业有限公司 | A kind of diamond synthetic rod electrolytic processing apparatus |
| CN204298476U (en) * | 2014-06-17 | 2015-04-29 | 中山大学 | A kind of modified electrode ultrasonic assistant in-pulp electrolysis device |
| CN204107577U (en) * | 2014-09-10 | 2015-01-21 | 河南省力量新材料有限公司 | Ultra-fine diamond is purified and is used graphite separator |
| CN104941813A (en) * | 2015-06-04 | 2015-09-30 | 中南钻石有限公司 | Electric separation and purification process of artificial diamonds |
| CN104986761A (en) * | 2015-06-25 | 2015-10-21 | 河南黄河旋风股份有限公司 | Efficient electrolyte purified through artificial diamond |
| CN104925804A (en) * | 2015-07-20 | 2015-09-23 | 三门峡天钻晶体材料有限公司 | Diamond synthesis rod physical dissociation purifying device and method |
| CN204752216U (en) * | 2015-07-20 | 2015-11-11 | 三门峡天钻晶体材料有限公司 | Physics of synthetic stick of diamond purification device that dissociates |
| CN106145105A (en) * | 2016-06-13 | 2016-11-23 | 安庆市凯立金刚石科技有限公司 | A kind of purification of diamond electrolyte |
| CN107254691A (en) * | 2017-06-13 | 2017-10-17 | 青岛聚鑫园工贸有限公司 | A kind of method by electric capacity comprehensive reutilization waste diamond tool valuable element |
| CN107308846A (en) * | 2017-06-16 | 2017-11-03 | 江苏大学 | A kind of automatic blending system |
| CN208038569U (en) * | 2018-04-14 | 2018-11-02 | 新郑市新材料专业孵化器服务中心 | A kind of diamond electrorefining device |
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| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
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| RJ01 | Rejection of invention patent application after publication | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20180713 |