CN108264065A - A kind of hopcalite agent waste water utilization device - Google Patents
A kind of hopcalite agent waste water utilization device Download PDFInfo
- Publication number
- CN108264065A CN108264065A CN201810220240.0A CN201810220240A CN108264065A CN 108264065 A CN108264065 A CN 108264065A CN 201810220240 A CN201810220240 A CN 201810220240A CN 108264065 A CN108264065 A CN 108264065A
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- Prior art keywords
- waste
- liquid
- water utilization
- cooling bay
- waste water
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
- B01D53/26—Drying gases or vapours
- B01D53/28—Selection of materials for use as drying agents
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01D—COMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
- C01D5/00—Sulfates or sulfites of sodium, potassium or alkali metals in general
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Organic Chemistry (AREA)
- Analytical Chemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Materials Engineering (AREA)
- Inorganic Chemistry (AREA)
- Heat Treatment Of Water, Waste Water Or Sewage (AREA)
Abstract
The invention discloses a kind of hopcalite agent waste water utilization devices, and the invention belongs to field of waste liquid treatment.The present invention includes collecting the waste collection storage tank of Huo Jiate waste liquids; the temperature bath for connecting with waste collection storage tank and being heated to flowing into its internal Huo Jiate waste liquid; the cooling bay for connecting with temperature bath and being crystallized to flowing into its internal Huo Jiate waste liquid; the blender of agent configuration is dried using cooling bay internal junction crystal as one of raw material; to the comminutor that the drier in blender is granulated, the drying device that the drier after granulation or cooling bay internal junction crystal are dried.The potential problem of the invention for solving waste liquor contamination environment well, it is precious to take with time-varying, and sodium sulphate product and drier is made, service society benefits the nation and the people and increases new income for enterprise.
Description
Technical field
The invention belongs to field of waste liquid treatment, and in particular to a kind of hopcalite agent waste water utilization device.
Background technology
It is well known that a large amount of waste liquid can be generated during hopcalite agent is prepared, because of the production of hopcalite agent
Process mainly chemically reacts early period, and the mixing for generating liquid dilute sulfuric acid and fluid sulphuric acid potassium and sodium sulphate is given up in the process
Liquid.Its processing mode is：
1. the waste liquid of sulfur acid and alkaline matter are neutralized, soda ash is such as added：
H2SO4(dilute)+Na2CO3=Na2SO4+H2O+CO2↑
Potassium sulfate has been that neutral salt is not involved in reacting.
It neutralizes and waste liquid is neutrality, main matter is potassium sulfate+sodium sulphate mixing liquid.
2. a large amount of tap water is added in waste liquid, dilution waste liquid (potassium sulfate+sodium sulphate), when salt in waste liquid (potassium sulfate,
Sodium sulphate mixed liquor) content it is seldom when, arrange outside waste liquid.
Note 1：Waste liquid at this time, first, salt content is very low, without recovery value；Second is that fluid sulphuric acid potassium, sodium sulphate are not easy
Separation, if separation, cost are too big.
Note 2：It is arranged outside waste liquid after dilution, surface meets environmental requirement, practical to have potential hazard to environment.Waste liquid enters certainly
After right environment, with the evaporation of moisture, salt concentration improves, and ultimately forms salt-soda soil.
Invention content
The technical problems to be solved by the invention are to provide a kind of hopcalite agent waste water utilization device, it is intended to Huo Jiala
Special agent waste liquid carries out secondary use, by extracting stage by stage, produces sodium sulphate product or drier.
In order to solve the above technical problems, the technical solution used in the present invention is：A kind of hopcalite agent waste water utilization dress
It puts, which is characterized in that the waste collection storage tank including collecting Huo Jiate waste liquids is connected with waste collection storage tank and to flowing into it
The temperature bath of portion's Huo Jiate waste liquids heating, the cooling for connecting with temperature bath and being crystallized to flowing into its internal Huo Jiate waste liquid
Pond, be dried using cooling bay internal junction crystal as one of raw material agent configuration blender, to the drier in blender into
The comminutor that row is granulated, the drying device that the drier after granulation or cooling bay internal junction crystal are dried.
Further technical solution is, further includes the separation of solid and liquid dress that separation of solid and liquid is carried out to cooling bay internal junction crystal
It puts.
Further technical solution is, valve two is equipped between the waste collection storage tank and temperature bath；The constant temperature
Valve three is equipped between pond and cooling bay.
Further technical solution is, is equipped between the waste collection storage tank and equipment for separating liquid from solid to waste collection
The pipe of storage tank drain, and pipe is equipped with valve one；By setting the pipe of valve four between the cooling bay and equipment for separating liquid from solid
Connection.
Further technical solution is, further includes packing machine, the packing machine dried finished product point to drying device
Packing.
Further technical solution is that the equipment for separating liquid from solid is centrifuge.
Further technical solution is that the temperature bath internal temperature is 45 ± 5 DEG C；The cooling bay internal temperature is
0 ± 5 DEG C, the drying and dehydrating temperature of the drying device is 100~102 DEG C.
Further technical solution is, further includes the filler pond that other fillers are added to blender.
Further technical solution is that the filler is iron chloride and swelled ground.
Further technical solution is, is equipped between the waste collection storage tank and equipment for separating liquid from solid and collects solid-liquid point
Waste collection slot from device internal liquid extracts drawing liquid pump and the control of waste liquid from waste collection slot to waste collection storage tank
The valve one of waste liquid flow velocity processed.
It is using advantageous effect caused by above-mentioned technical proposal：The present invention solves waste liquor contamination environment well
Potential problem, it is precious to take with time-varying, and sodium sulphate product and drier is made, service society is benefited the nation and the people and increased for enterprise
New income is added.
Description of the drawings
The present invention will be further described in detail below with reference to the accompanying drawings and specific embodiments.
Fig. 1 is the structure diagram of the present invention.
Specific embodiment
With reference to the attached drawing in the embodiment of the present invention, the technical solution in the embodiment of the present invention is carried out clear, complete
Ground describes, it is clear that described embodiment is only the part of the embodiment of the present invention, instead of all the embodiments.It is based on
Embodiment in the present invention, those of ordinary skill in the art are obtained every other without making creative work
Embodiment shall fall within the protection scope of the present invention.
Many details are elaborated in the following description to facilitate a thorough understanding of the present invention, still the present invention can be with
Implemented using other different from other manner described here, those skilled in the art can be without prejudice to intension of the present invention
In the case of do similar popularization, therefore the present invention is not limited by following public specific embodiment.
As shown in Figure 1, disclosure sets forth a kind of hopcalite agent waste water utilization devices, which is characterized in that including collecting
The waste collection storage tank of Huo Jiate waste liquids, the constant temperature for connecting with waste collection storage tank and being heated to flowing into its internal Huo Jiate waste liquid
Pond, the cooling bay for connecting with temperature bath and being crystallized to flowing into its internal Huo Jiate waste liquid, is made with cooling bay internal junction crystal
The blender of agent configuration is dried for one of raw material, to the comminutor that the drier in blender is granulated, after granulation
Drier or the drying device that is dried of cooling bay internal junction crystal.
Preferably, the equipment for separating liquid from solid that separation of solid and liquid is carried out to cooling bay internal junction crystal is further included.
Preferably, valve two is equipped between the waste collection storage tank and temperature bath；Between the temperature bath and cooling bay
Equipped with valve three.
Preferably, the pipe to waste collection storage tank drain is equipped between the waste collection storage tank and equipment for separating liquid from solid,
And pipe is equipped with valve one；By the way that the pipe of valve four is set to connect between the cooling bay and equipment for separating liquid from solid.
Preferably, packing machine, the packing machine dried finished product packing packaging to drying device are further included.
Preferably, the equipment for separating liquid from solid is centrifuge.
Preferably, the temperature bath internal temperature is 45 ± 5 DEG C；The cooling bay internal temperature is 0 ± 5 DEG C, described dry
The drying and dehydrating temperature of dry device is 100~102 DEG C.
Preferably, the filler pond that other fillers are added to blender is further included.
Preferably, the filler is iron chloride and swelled ground.
Preferably, it is equipped between the waste collection storage tank and equipment for separating liquid from solid and collects equipment for separating liquid from solid internal liquid
Waste collection slot, from waste collection slot to waste collection storage tank extract waste liquid drawing liquid pump and control waste liquid flow velocity valve
Men Yi.
In process of production, sodium sulphate finished product can be produced using the present apparatus, the drying comprising sodium sulphate can also be produced
Agent.Waste liquid is collected in waste collection tank inside, can open valve two, waste liquid is discharged into temperature bath, by heating removal portion
Divide steam, increase metabisulfite solution concentration, the removal of aqueous solvent can be precipitated sulfate crystal, by opening valve
Three flow into cooling bay, accelerate speed crystallization by cooling, crystallization can be made more, collect more crystalline solid, prepared as needed
If sodium sulphate finished product, inside the liquid merging equipment for separating liquid from solid inside cooling bay, crystalline solid is collected, waste liquid is discharged into waste liquid
It collects in storage tank, crystalline solid is placed in transmitting device (conveyer belt or belt conveyor) using lifting machine, is sent to drying plant, divides disk
Dress, be placed in drying device (baking oven) and be dried, recycle packing machine (pillow type packing machine, horizontal packing machine, upright packing machine it
One) it is packed.It is stored in storehouse.
To prepare drier, the crystalline solid matter utilization elevator inside cooling bay can be discharged into blender, added
The hygroscopic agents such as ferric trichloride, bentonite are prepared, and being packed into comminutor using elevator is granulated, naturally it is also possible to be set in advance
It puts a drier to make up a prescription pond, raw material needed for drier in drier is made up a prescription configuration, mixing in pond, is made carrying out comminutor
Grain；Then using transmitting device, semi-finished product feeding drying plant is dried.Finally packaging deposit storehouse.
Claims (10)
1. a kind of hopcalite agent waste water utilization device, which is characterized in that the waste collection storage tank including collecting Huo Jiate waste liquids,
The temperature bath for connecting with waste collection storage tank and being heated to flowing into its internal Huo Jiate waste liquid, connects with temperature bath and to flowing into it
Agent configuration is dried using cooling bay internal junction crystal as one of raw material for the cooling bay that internal Huo Jiate waste liquids are crystallized
Blender, to the comminutor that the drier in blender is granulated, to the drier after granulation or cooling bay internal junction crystal
The drying device being dried.
2. hopcalite agent waste water utilization device according to claim 1, which is characterized in that further include to cooling bay inside
Crystalline solid carries out the equipment for separating liquid from solid of separation of solid and liquid.
3. hopcalite agent waste water utilization device according to claim 1 or 2, which is characterized in that the waste collection storage
Valve two is equipped between tank and temperature bath；Valve three is equipped between the temperature bath and cooling bay.
4. hopcalite agent waste water utilization device according to claim 2, which is characterized in that the waste collection storage tank with
The pipe to waste collection storage tank drain is equipped between equipment for separating liquid from solid, and pipe is equipped with valve one；The cooling bay and solid-liquid
By the way that the pipe of valve four is set to connect between separator.
5. hopcalite agent waste water utilization device according to claim 1 or 2, which is characterized in that further include packing machine, institute
Stating packing machine, dried finished product packing is packed to drying device.
6. hopcalite agent waste water utilization device according to claim 2, which is characterized in that the equipment for separating liquid from solid is
Centrifuge.
7. hopcalite agent waste water utilization device according to claim 1 or 2, which is characterized in that inside the temperature bath
Temperature is 45 ± 5 DEG C；The cooling bay internal temperature is 0 ± 5 DEG C, and the drying and dehydrating temperature of the drying device is 100~102
℃。
8. hopcalite agent waste water utilization device according to claim 1 or 2, which is characterized in that further include to blender
Add the filler pond of other fillers.
9. hopcalite agent waste water utilization device according to claim 8, which is characterized in that the filler for iron chloride and
Swelled ground.
10. hopcalite agent waste water utilization device according to claim 2, which is characterized in that the waste collection storage tank
The waste collection slot for collecting equipment for separating liquid from solid internal liquid is equipped between equipment for separating liquid from solid, from waste collection slot to waste liquid
Storage tank is collected to extract the drawing liquid pump of waste liquid and control the valve one of waste liquid flow velocity.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810220240.0A CN108264065A (en) | 2018-03-16 | 2018-03-16 | A kind of hopcalite agent waste water utilization device |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810220240.0A CN108264065A (en) | 2018-03-16 | 2018-03-16 | A kind of hopcalite agent waste water utilization device |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN108264065A true CN108264065A (en) | 2018-07-10 |
Family
ID=62775070
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201810220240.0A Pending CN108264065A (en) | 2018-03-16 | 2018-03-16 | A kind of hopcalite agent waste water utilization device |
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| Country | Link |
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Citations (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN87103664A (en) * | 1987-05-15 | 1987-12-02 | 南京大学 | Synthetic glass factory cyanide wastewater treatment process method |
| JPH02237617A (en) * | 1989-03-08 | 1990-09-20 | Dai Ichi Kogyo Seiyaku Co Ltd | Production of granule of drying agent |
| CN1075664A (en) * | 1992-02-23 | 1993-09-01 | 谭勇军 | Moisture excluding and odor absorbing agent |
| CN1559665A (en) * | 2004-03-09 | 2005-01-05 | 杜建中 | Concave-convex rod clay composite drying agent |
| CN101954199A (en) * | 2009-07-17 | 2011-01-26 | 笹仓机械工程有限公司 | The solid state method of the solid state device of solution, waste liquid and solution, waste liquid |
| CN102030342A (en) * | 2010-10-26 | 2011-04-27 | 天脊煤化工集团股份有限公司 | Method and device for recovering anhydrous sodium sulfate from hydroxy benzotriazole production waste liquor |
| CN203545699U (en) * | 2013-10-21 | 2014-04-16 | 宁波大学 | Sodium sulfate-containing sewage treatment device |
| CN104140115A (en) * | 2014-08-25 | 2014-11-12 | 湖南江冶机电科技股份有限公司 | Method and device for recovering anhydrous sodium sulfate from filtrate after purification treatment of desulfurated lead plasters |
| CN104591464A (en) * | 2015-02-03 | 2015-05-06 | 石家庄工大化工设备有限公司 | Recycling method of high-salinity wastewater |
-
2018
- 2018-03-16 CN CN201810220240.0A patent/CN108264065A/en active Pending
Patent Citations (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN87103664A (en) * | 1987-05-15 | 1987-12-02 | 南京大学 | Synthetic glass factory cyanide wastewater treatment process method |
| JPH02237617A (en) * | 1989-03-08 | 1990-09-20 | Dai Ichi Kogyo Seiyaku Co Ltd | Production of granule of drying agent |
| CN1075664A (en) * | 1992-02-23 | 1993-09-01 | 谭勇军 | Moisture excluding and odor absorbing agent |
| CN1559665A (en) * | 2004-03-09 | 2005-01-05 | 杜建中 | Concave-convex rod clay composite drying agent |
| CN101954199A (en) * | 2009-07-17 | 2011-01-26 | 笹仓机械工程有限公司 | The solid state method of the solid state device of solution, waste liquid and solution, waste liquid |
| CN102030342A (en) * | 2010-10-26 | 2011-04-27 | 天脊煤化工集团股份有限公司 | Method and device for recovering anhydrous sodium sulfate from hydroxy benzotriazole production waste liquor |
| CN203545699U (en) * | 2013-10-21 | 2014-04-16 | 宁波大学 | Sodium sulfate-containing sewage treatment device |
| CN104140115A (en) * | 2014-08-25 | 2014-11-12 | 湖南江冶机电科技股份有限公司 | Method and device for recovering anhydrous sodium sulfate from filtrate after purification treatment of desulfurated lead plasters |
| CN104591464A (en) * | 2015-02-03 | 2015-05-06 | 石家庄工大化工设备有限公司 | Recycling method of high-salinity wastewater |
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| 卢芳仪, 卢爱军: "由含硫酸钠的废液直接制无水硫酸钠", 化工环保, vol. 17, no. 02, pages 105 - 110 * |
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