CN108251858B - A kind of technology of preparing equipment - Google Patents
A kind of technology of preparing equipment Download PDFInfo
- Publication number
- CN108251858B CN108251858B CN201810154386.XA CN201810154386A CN108251858B CN 108251858 B CN108251858 B CN 108251858B CN 201810154386 A CN201810154386 A CN 201810154386A CN 108251858 B CN108251858 B CN 108251858B
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- CN
- China
- Prior art keywords
- cavity
- connects
- siphunculus
- valve member
- end wall
- Prior art date
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Classifications
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- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25B—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
- C25B1/00—Electrolytic production of inorganic compounds or non-metals
- C25B1/01—Products
- C25B1/24—Halogens or compounds thereof
- C25B1/26—Chlorine; Compounds thereof
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- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25B—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
- C25B1/00—Electrolytic production of inorganic compounds or non-metals
- C25B1/01—Products
- C25B1/02—Hydrogen or oxygen
- C25B1/04—Hydrogen or oxygen by electrolysis of water
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25B—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
- C25B15/00—Operating or servicing cells
- C25B15/08—Supplying or removing reactants or electrolytes; Regeneration of electrolytes
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- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25B—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
- C25B9/00—Cells or assemblies of cells; Constructional parts of cells; Assemblies of constructional parts, e.g. electrode-diaphragm assemblies; Process-related cell features
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
- Y02E60/30—Hydrogen technology
- Y02E60/36—Hydrogen production from non-carbon containing sources, e.g. by water electrolysis
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Electrochemistry (AREA)
- Materials Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Filling Or Discharging Of Gas Storage Vessels (AREA)
- Thermal Insulation (AREA)
Abstract
The invention discloses a kind of technology of preparing equipment, including preparation facilities, first, which preserves device and second, preserves device, the preparation facilities includes shell A, cavity is provided in the shell A, it connects to be provided in the cavity lower end wall and be in charge of, it is described be in charge of left and right end face and connect be provided with valve member A, the valve member A end face outside, which connects, is provided with siphunculus A, described cavity lower end wall or so is opposite to be installed with inductor, the thermalization chamber in the shell A is installed with above the cavity, thermalization pipe is installed between end wall above and below the thermalization chamber, protrusion whorl mating connection in the upper surface the shell A is provided with locking block A and locking block B, present device structure is simple, it is easy to use, automatically the chlorine and hydrogen generated after liquor alumini chloridi electrolysis is preserved, effectively increase the efficiency of equipment.
Description
Technical field
The present invention relates to preparation technical fields, and in particular to a kind of technology of preparing equipment.
Background technique
In chemical experiment, need to use a large amount of Preparation equipment, for realizing the purpose of chemical experiment, wherein electricity
Solution liquor alumini chloridi is one of experiment important in laboratory, traditional Preparation equipment for generated in experiment the collection of gas compared with
For difficulty, collection efficiency is low, collects insufficient.
Summary of the invention
The purpose of the present invention is to provide a kind of technology of preparing equipment, can overcome the drawbacks described above of the prior art.
According to the present invention, a kind of technology of preparing equipment of present device, including preparation facilities, first preserve device and
Two preserve device, and the preparation facilities includes shell A, and cavity is provided in the shell A, connects and sets in the cavity lower end wall
Be equipped with and be in charge of, it is described be in charge of left and right end face and connect be provided with valve member A, the valve member A end face outside, which connects, is provided with siphunculus A, institute
It states cavity lower end wall or so and is installed with inductor relatively, be installed with the thermalization chamber in the shell A, institute above the cavity
It states and is installed with thermalization pipe between thermalization chamber or more end wall, protrusion whorl mating connection in the upper surface the shell A is provided with lock
Gu block A and the mating connection of locking block B, the locking block A upper surface screw are provided with cover plate B, the upper surface locking block B screw
Mating connection is provided with cover plate C, and the energization column A for visiting and extending outside out into the cavity and upwards is installed in the locking block A,
The outer surface energization column A and the position to connect the locking block A and cover plate B are installed with electrically isolated set A, on the energization column A
It is installed in the fixed live wire A in end face, the locking block B and visits into the cavity and extend upwards out external energization column B, it is described
The energization outer surface column B is installed with electrically isolated set with the position to connect the locking block B and cover plate C, and the upper surface energization column B is solid
It equipped with electric wire B, is connected in the wall of the cavity left end and is provided with siphunculus F, the left side the siphunculus F, which connects, is provided with valve member D, institute
It states the left side valve member D and connects and be provided with outer comb, be provided on the left of the outer comb positioned at external dryization case, the dryization case
It is inside provided with dryization chamber, dryization case described in the siphunculus D break-through simultaneously visits, the dryization chamber left and right sides end wall intracavitary into dryization
Between cover plate D is hingedly installed, connected in the wall of dryization chamber left end and be provided with extended siphunculus E to the left, the left end the siphunculus E
Face, which connects, is provided with valve member B, and the left side the valve member B, which connects, is provided with siphunculus D, and described second preserves device including being fixedly arranged on branch
The carrying case of support is provided with cavity groove in the carrying case, cavity groove, the cavity groove upper end wall is provided in the cavity groove right end wall
It is inside installed with pneumatic cylinder, the catch bar lower end surface of the pneumatic cylinder is installed with fixing piece, and the fixing piece front end face is fixed oriented
Left extended bend pipe, the bend pipe right side connects the siphunculus D for being provided with cavity groove described in break-through and connecting with the valve member B, institute
It states bend pipe lower left and is provided with support frame, support frame as described above right side, which is installed with, leads shifting rail, and described lead moves rail right side slip
Be provided with slipping block A, the right side the slipping block A is installed with shell B, is provided in the shell B and preserves chamber, described to preserve
It is connected in chamber lower end wall and is provided with siphunculus B, the lower end surface the siphunculus B, which connects, is provided with valve member C, and the lower end surface the valve member C connects
It is provided with siphunculus C, the socket of the outer surface the siphunculus C, which is provided with, preserves capsule, and the upper surface the shell B is provided with and the bend pipe phase
Pair and with the sealing valve A for preserving chamber and connecting, connect in the cavity right end wall and be provided with extended communicating pipe to the right, it is described
Right side connected and was provided with valve member E communicating pipe, and the right side the valve member E, which connects, is provided with siphunculus G, and described first preserves device packet
Include and be provided with storage chamber in the shell C, the shell C being set to below the siphunculus G, the upper surface the shell C be installed with
The sealing valve B that the storage chamber connects, the storage chamber lower section is installed with positioned at the interior cavity, the storage chamber lower end wall
The siphunculus for being provided with and visiting into the cavity is connected, the siphunculus lower end surface, which connects, is provided with valve member F, and the lower end surface the valve member F is logical
It connecing and is provided with siphunculus H, the cavity lower end wall, which connects to be provided with, connects pipe, and the pipe lower end surface that connects connects the related valve of setting,
The lower end surface the shell C is installed with support foot, and the case cylinder fixed with ground is provided with below the support foot, is set in the case cylinder
It is equipped with cavity portion, the lower end surface of the support foot offsets with the cavity portion lower end wall, and case cylinder bottom four is fixedly installed on angle
There is suspension column, the suspension column bottom surface is fixedly installed sucker, acoustic insulation shock-proof device is provided on the pneumatic cylinder.
Further technical solution, the inductor include the substrate being cooperatively connected with the cavity lower end wall screw, institute
It states and is provided with conduction chamber in substrate, sealing plate is installed between the conduction chamber left hand end wall, the conduction is intracavitary to be provided with electricity
Hinder induction tube, described resistance induction tube or so end face be installed with positioned at the intrabasement pipeline A and pipeline B, the pipeline A and
Pipeline B is connected with external control device, to realize temperature sensing control.
Further technical solution, dryization is intracavitary to have filled with dry agent, to improve dryization effect.
Further technical solution, the electric wire A are communicated with the cathode of total electricity, and the electric wire B is communicated with the anode of total electricity,
To realize the electrolysis of water.
Further technical solution, the cavity portion, storage chamber and cavity are provided with water, to improve the reliable of equipment
Property.
Further technical solution, the acoustic insulation shock-proof device include being fixed at the pneumatic cylinder left and right sides
Sound insulating pad and the shock-proof plate for being fixed at pneumatic cylinder front and rear sides face, the sound insulating pad are connected with the shock-proof plate.
The beneficial effects of the present invention are:
In the initial state due to present device, the pneumatic cylinder is in stop working state, the valve member A, valve member
B, valve member C, valve member D, valve member E, valve member F, pass valve and sealing valve B are in close state, and are not powered in the electric wire A and electric wire B,
To make above structure be located at initial position in the initial state, it can be adjusted in follow-up work, effectively improve equipment
Working regularity.
When equipment operation, the valve member A is opened, by liquor alumini chloridi by it is described be in charge of be passed through in the cavity, and will
The cavity is closed full of the rear valve member A, connects the electric wire A and electric wire B and power supply, in the cavity Inner electrolysis water,
So that the outer surface energization column A is generated hydrogen, the outer surface energization column B made to generate chlorine, the valve member D is opened, hydrogen by
The siphunculus F, valve member D and outer comb are intracavitary into dryization, by intracavitary dry agent dryization of dryization, the sliding
Block A drives the shell B to move to immediately below the bend pipe, and the sealing valve A and the bend pipe face, the pneumatic cylinder drive
The fixing piece is moved to move down, the sealing valve A is opened, make the bend pipe put in it is described preserve intracavitary, the sealing valve A is adopted
With the box-like structure of dynamic seal, it can still guarantee to seal after making the bend pipe enter the sealing valve A, the valve member B is opened, will
The hydrogen of dryization by the bend pipe be passed through it is described preserve on the upside of chamber, and the air for preserving chamber is pressed down against, the valve member C
Open, by surplus air be discharged into it is described preserve it is intracapsular, when it is described preserve it is intracavitary full of air when the valve member C, valve member B and sealing
Valve A is closed, and the slipping block A drives the shell B to run to loading place again, described in the chlorine entrance that the energization column B is generated
In communicating pipe, the valve member E is opened with sealing valve B, and chlorine is intracavitary into the storage, and the valve member F is opened with valve is closed, chlorine
Liquor alumini chloridi is squeezed into the cavity portion by the storage chamber and cavity, after being filled with chlorine in the storage chamber and cavity
The valve member F and pass valve are closed, then chlorine will be filled in the storage chamber and cavity, to realize efficient chlorine and hydrogen
Gas preparation.
When react carry out when, the sealing plate conducts the temperature of the cavity to the resistance induction tube, the resistance sense
Should pipe so that the electric current in the pipeline A and pipeline B is changed according to temperature change, give control device to issue signal, make the heat
Change the aqueous in cavity described in pipe work thermalization, be in the temperature of reaction and be suitble to state, so that the reaction for improving equipment is high
Effect property.
When only needing to preserve the chlorine of certain component, when chlorine just enters the cavity from the siphunculus H, the valve member
F can be closed, and keep the storage intracavitary full of chlorine, to improve the practicability of equipment.
Present device structure is simple, easy to use, preserves the chlorine and hydrogen generated after liquor alumini chloridi electrolysis automatically,
Effectively increase the efficiency of equipment.
The above, the specific embodiment only invented, but invent protection scope be not limited thereto, it is any without
The change or replacement that creative work is expected are crossed, should all be covered within the protection scope of invention.Therefore, the protection scope of invention
It should be determined by the scope of protection defined in the claims.
Detailed description of the invention
It, below will be to embodiment or existing in order to illustrate more clearly of inventive embodiments or technical solution in the prior art
Attached drawing needed in technical description is briefly described, it should be apparent that, the accompanying drawings in the following description is only to invent
Some embodiments for those of ordinary skill in the art without creative efforts, can also basis
These attached drawings obtain other attached drawings.
Fig. 1 is a kind of overall structure diagram of technology of preparing equipment of the invention；
Fig. 2 is the enlarged internal structural schematic diagram of inductor 143 in Fig. 1；
Fig. 3 is partial structural diagram of the invention；
Fig. 4 is Pneumatic cylinder structure schematic diagram in the present invention.
Specific embodiment
All features disclosed in this specification or disclosed all methods or in the process the step of, in addition to mutually exclusive
Feature and/or step other than, can combine in any way.
Any feature disclosed in this specification (including any accessory claim, abstract and attached drawing), except non-specifically chatting
It states, can be replaced by other alternative features that are equivalent or have similar purpose.That is, unless specifically stated, each feature is only
It is an example in a series of equivalent or similar characteristics.
As shown in Figs 1-4, a kind of technology of preparing equipment of the invention, including preparation facilities, first preserve device and second
Device is preserved, the preparation facilities includes shell A104, and cavity 103,103 lower end of cavity are provided in the shell A104
Connect to be provided in wall and be in charge of 100, it is described be in charge of 100 or so end faces and connect be provided with valve member A101, on the outside of the valve member A101
End face, which connects, is provided with siphunculus A102, and described 103 lower end wall of cavity or so is opposite to be installed with inductor 143, on the cavity 103
Side is installed with the thermalization chamber 127 in the shell A104, is installed with thermalization pipe between about 127 end wall of thermalization chamber
The mating connection of 128, the shell A104 upper surface protrusion whorl is provided with locking block A126 and locking block B130, the lock
Gu the mating connection of block A126 upper surface screw is provided with cover plate B125, locking block B130 upper surface screw, which is cooperatively connected, to be arranged
There is cover plate C131, the energization column A124 for visiting and extending outside out into the cavity 103 and upwards be installed in the locking block A126,
The outer surface energization column A124 is installed with electrically isolated set A123, institute with the position to connect the locking block A126 and cover plate B125
State be installed in the upper surface energization column A124 fixed live wire A122, the locking block B130 visit into the cavity 103 and upwards
Extend energization column B132 external out, the outer surface energization column B132 connects with the locking block B130 and cover plate C1315
Position is installed with electrically isolated set 133, the fixed live wire B134 in the upper surface energization column B132, in the 103 left end wall of cavity
It connects and is provided with siphunculus F121, the left side the siphunculus F121, which connects, is provided with valve member D120, and the left side the valve member D120 is logical
It connects and is provided with outer comb 119, be provided on the left of the outer comb 119 in external dryization case 109, the dryization case 109
It is provided with dryization chamber 108, dryization case 109 described in the siphunculus D116 break-through is simultaneously visited into the dryization chamber 108, the dryization chamber
Cover plate D118 is hingedly installed between 108 left and right sides end walls, connected in the 108 left end wall of dryization chamber be provided with it is extended to the left
The left side siphunculus E117, the siphunculus E117, which connects, is provided with valve member B110, the left side the valve member B110 connect be provided with it is logical
Pipe D116, described second to preserve device include the carrying case 150 for being fixedly arranged on support frame, is provided with cavity groove in the carrying case 150
166, cavity groove 151 is provided in the 166 right end wall of cavity groove, is installed with pneumatic cylinder 152 in 166 upper end wall of cavity groove, it is described
The catch bar lower end surface of pneumatic cylinder 152 is installed with fixing piece 153, and 153 front end face of fixing piece is installed with extended curved to the left
Pipe 154,154 right side of bend pipe connect the siphunculus for being provided with cavity groove 151 described in break-through and connecting with the valve member B110
D116,154 lower left of bend pipe are provided with support frame 158, and 158 right side of support frame as described above, which is installed with to lead, moves rail 159, described
That leads shifting 159 right side slip of rail is provided with slipping block A157, and the right side the slipping block A157 is installed with shell B115, institute
State to be provided in shell B115 and preserve chamber 114, it is described preserve to connect in 114 lower end wall of chamber be provided with siphunculus B111, the siphunculus
The lower end surface B111, which connects, is provided with valve member C113, and the lower end surface the valve member C113, which connects, is provided with siphunculus C112, the siphunculus
The socket of the outer surface C112 is provided with and preserves capsule 161, the upper surface the shell B115 be provided with it is opposite with the bend pipe 154 and with institute
It states and preserves the sealing valve A155 that chamber 114 connects, connected in the 103 right end wall of cavity and be provided with extended communicating pipe 146 to the right,
146 right side of communicating pipe, which connects, is provided with valve member E135, and the right side the valve member E135, which connects, is provided with siphunculus G136, institute
Stating first and preserving device includes being provided with storage chamber in the shell C137, the shell C137 being set to below the siphunculus G136
The upper surface 138, the shell C137 is installed with the sealing valve B170 connected with the storage chamber 138,138 lower section of storage chamber
It is installed with the cavity 165 being located in described 139, storage 138 lower end wall of chamber is connected to be provided with and be visited into the logical of the cavity 165
Pipe 146,146 lower end surface of siphunculus, which connects, is provided with valve member F141, and the lower end surface the valve member F141, which connects, is provided with siphunculus
H140,165 lower end wall of cavity, which connects to be provided with, connects pipe 163, and 163 lower end surface of pipe that connects connects the related valve of setting
The lower end surface 162, the shell C137 is installed with support foot 164, and the case cylinder fixed with ground is provided with below the support foot 164
171, cavity portion 172 is provided in the case cylinder 171, the lower end surface of the support foot 164 offsets with 172 lower end wall of cavity portion,
Suspension column 301 is fixedly installed on the angle of case cylinder 171 bottom four, 301 bottom surface of suspension column is fixedly installed sucker 302, institute
It states and is provided with acoustic insulation shock-proof device on pneumatic cylinder 152.
Valuably, wherein the inductor 143 includes the substrate being cooperatively connected with the 103 lower end wall screw of cavity
200, it is provided with conduction chamber 204 in the substrate 200, is installed between 204 left hand end wall of conduction chamber and seals plate 205, institute
It states in conduction chamber 204 and is provided with resistance induction tube 202,202 or so the end face of resistance induction tube is installed with positioned at the substrate
Pipeline A201 and pipeline B203, the pipeline A201 and pipeline B203 in 200 are connected with external control device, to realize temperature
Spend sensing control.
Valuably, wherein dry agent has been filled in the dryization chamber 108, to improve dryization effect.
Valuably, wherein the electric wire A122 is communicated with the cathode of total electricity, the positive phase of the electric wire B134 and total electricity
It is logical, to realize the electrolysis of water.
Valuably, wherein the cavity portion 172, storage chamber 138 and cavity 165 are provided with water, make chlorine in the storage chamber
Liquid is squeezed out after being preserved in 138, to improve the reliability of equipment.
Valuably, wherein the acoustic insulation shock-proof device include be fixed at 152 left and right sides of pneumatic cylinder every
Sound pad 1521 and the shock-proof plate 1522 for being fixed at the 152 front and rear sides face of pneumatic cylinder, the sound insulating pad 1521 and described
Shock-proof plate 1522 is connected, and the acoustic insulation shock-proof device can effectively reduce the noise and shake that the work of pneumatic cylinder 152 generates
It is dynamic.
In the initial state, the pneumatic cylinder 152 is in stop working state, the valve member A101, valve to present device
Part B110, valve member C113, valve member D120, valve member E135, valve member F141, pass valve 162 and sealing valve B170 are in close state, institute
It states and is not powered in electric wire A122 and electric wire B134.
When equipment operation, the valve member A101 is opened, and 100 are in charge of and are passed through the cavity liquor alumini chloridi by described
In 103, and the cavity 103 is closed full of the rear valve member A101, connects the electric wire A122 and electric wire B134 with power supply
It is logical, in the 103 Inner electrolysis water of cavity, so that the outer surface energization column A124 is generated hydrogen, make the energization column B132 appearance
Face generates chlorine, and the valve member D120 is opened, and hydrogen is entered described dry by the siphunculus F121, valve member D120 and outer comb 119
Change in chamber 108, by dry agent dryization in the dryization chamber 108, the slipping block A157 drives the shell B115 movement
To with immediately below the bend pipe 154, the sealing valve A155 and 154 face of bend pipe, the pneumatic cylinder 152 drives described solid
Determine part 153 to move down, the sealing valve A155 is opened, make the bend pipe 154 put in it is described preserve in chamber 114, the sealing
Valve A155 uses the box-like structure of dynamic seal, can still guarantee to seal after making the bend pipe 154 enter the sealing valve A155, institute
State valve member B110 opening, by the hydrogen of dryization by the bend pipe 154 be passed through it is described preserve 114 upside of chamber, and preserve chamber for described
114 air is pressed down against, and the valve member C113 is opened, by surplus air be discharged into it is described preserve in capsule 161, preserve chamber when described
The valve member C113, valve member B110 and sealing valve A155 are closed when being full of air in 114, and the slipping block A157 drives described again
Shell B115 runs to loading place, and the chlorine that the energization column B132 is generated entered in the communicating pipe 146, the valve member E135
It is opened with sealing valve B170, chlorine enters in the storage chamber 138, the valve member F141 and closes the opening of valve 162, and chlorine is by chlorination
Aluminum solutions are squeezed into the cavity portion 172 by the storage chamber 138 and cavity 165, are filled when in the storage chamber 138 and cavity 165
The valve member F141 is closed with valve 162 is closed after having expired chlorine, then will be filled with chlorine in the storage chamber 138 and cavity 165.
When react carry out when, the sealing plate 205 conducts the temperature of the cavity 103 to the resistance induction tube 202, institute
State resistance induction tube 202 makes the electric current in the pipeline A201 and pipeline B203 change according to temperature change, gives control device
Signal is issued, the aqueous in cavity 103 described in the work of thermalization pipe 128 thermalization is made, the temperature of reaction is in and is suitble to state.
When only needing to preserve the chlorine of certain component, when chlorine just enters the cavity 165 from the siphunculus H140, institute
Stating valve member F141 can close, and make in the storage chamber 138 full of chlorine.
The beneficial effects of the present invention are: in the initial state due to present device, the pneumatic cylinder is in and stops working
State, the valve member A, valve member B, valve member C, valve member D, valve member E, valve member F, pass valve and sealing valve B are in close state, the electricity
Be not powered in line A and electric wire B, so that above structure be made to be located at initial position in the initial state, can in follow-up work into
Row adjustment, effectively improves the working regularity of equipment.
When equipment operation, the valve member A is opened, by liquor alumini chloridi by it is described be in charge of be passed through in the cavity, and will
The cavity is closed full of the rear valve member A, connects the electric wire A and electric wire B and power supply, in the cavity Inner electrolysis water,
So that the outer surface energization column A is generated hydrogen, the outer surface energization column B made to generate chlorine, the valve member D is opened, hydrogen by
The siphunculus F, valve member D and outer comb are intracavitary into dryization, by intracavitary dry agent dryization of dryization, the sliding
Block A drives the shell B to move to immediately below the bend pipe, and the sealing valve A and the bend pipe face, the pneumatic cylinder drive
The fixing piece is moved to move down, the sealing valve A is opened, make the bend pipe put in it is described preserve intracavitary, the sealing valve A is adopted
With the box-like structure of dynamic seal, it can still guarantee to seal after making the bend pipe enter the sealing valve A, the valve member B is opened, will
The hydrogen of dryization by the bend pipe be passed through it is described preserve on the upside of chamber, and the air for preserving chamber is pressed down against, the valve member C
Open, by surplus air be discharged into it is described preserve it is intracapsular, when it is described preserve it is intracavitary full of air when the valve member C, valve member B and sealing
Valve A is closed, and the slipping block A drives the shell B to run to loading place again, described in the chlorine entrance that the energization column B is generated
In communicating pipe, the valve member E is opened with sealing valve B, and chlorine is intracavitary into the storage, and the valve member F is opened with valve is closed, chlorine
Liquor alumini chloridi is squeezed into the cavity portion by the storage chamber and cavity, after being filled with chlorine in the storage chamber and cavity
The valve member F and pass valve are closed, then chlorine will be filled in the storage chamber and cavity, to realize efficient chlorine and hydrogen
Gas preparation.
When react carry out when, the sealing plate conducts the temperature of the cavity to the resistance induction tube, the resistance sense
Should pipe so that the electric current in the pipeline A and pipeline B is changed according to temperature change, give control device to issue signal, make the heat
Change the aqueous in cavity described in pipe work thermalization, be in the temperature of reaction and be suitble to state, so that the reaction for improving equipment is high
Effect property.
When only needing to preserve the chlorine of certain component, when chlorine just enters the cavity from the siphunculus H, the valve member
F can be closed, and keep the storage intracavitary full of chlorine, to improve the practicability of equipment.
Present device structure is simple, easy to use, preserves the chlorine and hydrogen generated after liquor alumini chloridi electrolysis automatically,
Effectively increase the efficiency of equipment.
The above, the specific embodiment only invented, but invent protection scope be not limited thereto, it is any without
The change or replacement that creative work is expected are crossed, should all be covered within the protection scope of invention.Therefore, the protection scope of invention
It should be determined by the scope of protection defined in the claims.
Claims (6)
1. a kind of technology of preparing equipment, including preparation facilities, first preserves device and second and preserve device, the preparation facilities packet
Shell A is included, cavity is provided in the shell A, connects to be provided in the cavity lower end wall and be in charge of, it is described to be in charge of left and right end face
It connects and is provided with valve member A, the valve member A end face outside, which connects, is provided with siphunculus A, and described cavity lower end wall or so is opposite to be installed with
Inductor, the cavity top are installed with the thermalization chamber in the shell A, are installed between end wall above and below the thermalization chamber
Thermalization pipe, the mating connection of the upper surface shell A protrusion whorl are provided with locking block A and locking block B, the locking block A
Screw mating connection in upper surface is provided with cover plate B, and the mating connection of locking block B upper surface screw is provided with cover plate C, the lock
Gu being installed with the energization column A for visiting and extending outside out into the cavity and upwards, the outer surface energization column A and the lock in block A
Gu the position that block A and cover plate B connect is installed with electrically isolated set A, the fixed live wire A in the upper surface energization column A, the locking block
The energization column B for visiting and extending outside out into the cavity and upwards, the outer surface energization column B and the locking block B are installed in B
Electrically isolated set, the fixed live wire B in the upper surface energization column B, cavity left end wall are installed with the position to connect cover plate C
It inside connects and is provided with siphunculus F, the left side the siphunculus F, which connects, is provided with valve member D, and the left side the valve member D, which connects, to be provided with outside
Comb, the outer comb left side, which is provided with, is provided with dryization chamber, the siphunculus D in external dryization case, the dryization case
The case of dryization described in break-through is simultaneously visited intracavitary into dryization, is hingedly equipped with cover plate D between the dryization chamber left and right sides end wall, described
It is connected in the wall of dryization chamber left end and is provided with extended siphunculus E to the left, the left side the siphunculus E, which connects, is provided with valve member B, the valve
The left side part B, which connects, is provided with siphunculus D, and described second to preserve device include the carrying case for being fixedly arranged on support frame, the carrying case
It is inside provided with cavity groove, cavity groove is provided in the cavity groove right end wall, pneumatic cylinder, the air pressure are installed in the cavity groove upper end wall
The catch bar lower end surface of cylinder is installed with fixing piece, and the fixing piece front end face is installed with extended bend pipe to the left, and the bend pipe is right
End face connects the siphunculus D for being provided with cavity groove described in break-through and connecting with the valve member B, and the bend pipe lower left is provided with support
Frame, support frame as described above right side, which is installed with, leads shifting rail, and described lead moves rail right side slip and be provided with slipping block A, the cunning
Move the right side block A be installed with shell B, be provided in the shell B and preserve chamber, it is described preserve connected in chamber lower end wall be provided with it is logical
The lower end surface pipe B, the siphunculus B, which connects, is provided with valve member C, and the lower end surface the valve member C, which connects, is provided with siphunculus C, outside the siphunculus C
Surface socket, which is provided with, preserves capsule, and the upper surface the shell B is provided with opposite with the bend pipe and preserves what chamber connected with described
Valve A is sealed, is connected in the cavity right end wall and is provided with extended communicating pipe to the right, the communicating pipe right side, which connects, to be provided with
The right side valve member E, the valve member E, which connects, is provided with siphunculus G, and described first preserves device including being set to below the siphunculus G
Shell C, the shell C in be provided with storage chamber, the sealing valve that the upper surface the shell C is installed with and the storage chamber connects
B, the storage chamber lower section are installed with positioned at the interior cavity, and the storage chamber lower end wall is connected to be provided with and be visited into the cavity
Siphunculus, the siphunculus lower end surface, which connects, is provided with valve member F, and the lower end surface the valve member F, which connects, is provided with siphunculus H, the cavity
Lower end wall, which connects to be provided with, connects pipe, and the pipe lower end surface that connects connects the related valve of setting, and the lower end surface the shell C is installed with branch
It holds foot, the case cylinder fixed with ground is provided with below the support foot, be provided with cavity portion in the case cylinder, under the support foot
End face offsets with the cavity portion lower end wall, and suspension column is fixedly installed on the angle of case cylinder bottom four, and the suspension column bottom surface is fixed
It is provided with sucker, acoustic insulation shock-proof device is provided on the pneumatic cylinder.
2. a kind of technology of preparing equipment as described in claim 1, it is characterised in that: the inductor include under the cavity
The substrate that end wall screw is cooperatively connected is provided with conduction chamber in the substrate, is installed with envelope between the conduction chamber left hand end wall
Plywood, the conduction is intracavitary to be provided with resistance induction tube, and described resistance induction tube or so end face is installed in the substrate
Pipeline A and pipeline B, the pipeline A and pipeline B connected with external control device.
3. a kind of technology of preparing equipment as described in claim 1, it is characterised in that: dryization is intracavitary to have filled with dry agent.
4. a kind of technology of preparing equipment as described in claim 1, it is characterised in that: the electric wire A is communicated with the cathode of total electricity,
The electric wire B is communicated with the anode of total electricity.
5. a kind of technology of preparing equipment as described in claim 1, it is characterised in that: the cavity portion, storage chamber and cavity are built-in
There is water.
6. a kind of technology of preparing equipment as described in claim 1, it is characterised in that: the acoustic insulation shock-proof device includes that fixation is set
Set the pneumatic cylinder left and right sides sound insulating pad and be fixed at the shock-proof plate in pneumatic cylinder front and rear sides face, it is described
Sound insulating pad is connected with the shock-proof plate.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810154386.XA CN108251858B (en) | 2018-02-23 | 2018-02-23 | A kind of technology of preparing equipment |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810154386.XA CN108251858B (en) | 2018-02-23 | 2018-02-23 | A kind of technology of preparing equipment |
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| Publication Number | Publication Date |
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| CN108251858A CN108251858A (en) | 2018-07-06 |
| CN108251858B true CN108251858B (en) | 2019-01-25 |
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| CN201810154386.XA Expired - Fee Related CN108251858B (en) | 2018-02-23 | 2018-02-23 | A kind of technology of preparing equipment |
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Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2002012993A (en) * | 2000-06-30 | 2002-01-15 | Nippon Soda Co Ltd | Method for producing anhydrous aluminum chloride |
| CN103305862A (en) * | 2012-03-13 | 2013-09-18 | 温州大学 | Electrochemical production device and manufacturing method of high-alkalization-degree aluminum polychlorid and Al13 chloride |
| CN104641018A (en) * | 2012-06-29 | 2015-05-20 | 澳大利亚生物精制私人有限公司 | Process and apparatus for generating or recovering hydrochloric acid from metal salt solutions |
| CN106967993A (en) * | 2017-05-10 | 2017-07-21 | 东北大学 | A kind of electrolytic chlorination aluminum for aluminum oxide method |
| CN107177858A (en) * | 2017-05-10 | 2017-09-19 | 东北大学 | A kind of method that aluminium chloride electricity is converted into aluminum oxide |
-
2018
- 2018-02-23 CN CN201810154386.XA patent/CN108251858B/en not_active Expired - Fee Related
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2002012993A (en) * | 2000-06-30 | 2002-01-15 | Nippon Soda Co Ltd | Method for producing anhydrous aluminum chloride |
| CN103305862A (en) * | 2012-03-13 | 2013-09-18 | 温州大学 | Electrochemical production device and manufacturing method of high-alkalization-degree aluminum polychlorid and Al13 chloride |
| CN104641018A (en) * | 2012-06-29 | 2015-05-20 | 澳大利亚生物精制私人有限公司 | Process and apparatus for generating or recovering hydrochloric acid from metal salt solutions |
| CN106967993A (en) * | 2017-05-10 | 2017-07-21 | 东北大学 | A kind of electrolytic chlorination aluminum for aluminum oxide method |
| CN107177858A (en) * | 2017-05-10 | 2017-09-19 | 东北大学 | A kind of method that aluminium chloride electricity is converted into aluminum oxide |
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| Publication number | Publication date |
|---|---|
| CN108251858A (en) | 2018-07-06 |
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Effective date of registration: 20181212 Address after: 324109 Jinfeng Road, Hecun Town, Jiangshan City, Quzhou City, Zhejiang Province Applicant after: Jiangshan Biaolong Decoration Material Co., Ltd. Address before: 317500 No. 60 Jinhe Road, Wenling City, Taizhou City, Zhejiang Province Applicant before: Ye Guonian |
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