CN108246219A - A kind of temperature control reaction kettle - Google Patents
A kind of temperature control reaction kettle Download PDFInfo
- Publication number
- CN108246219A CN108246219A CN201810269735.2A CN201810269735A CN108246219A CN 108246219 A CN108246219 A CN 108246219A CN 201810269735 A CN201810269735 A CN 201810269735A CN 108246219 A CN108246219 A CN 108246219A
- Authority
- CN
- China
- Prior art keywords
- interlayer
- autoclave body
- temperature control
- control reaction
- tube
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
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Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0006—Controlling or regulating processes
- B01J19/0013—Controlling the temperature of the process
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00051—Controlling the temperature
- B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
- B01J2219/00087—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor
- B01J2219/0009—Coils
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Physical Or Chemical Processes And Apparatus (AREA)
Abstract
The invention discloses a kind of temperature control reaction kettle, including outer layer autoclave body, internal layer autoclave body, interlayer, cooling tube, heating tube.The present invention can accurately control reaction solution heating rate excessively, and reaction solution is promoted to be uniformly mixed, and promote reaction solution reaction process.
Description
Technical field
The present invention relates to a kind of temperature control reaction kettles.
Background technology
Traditional reaction kettle heat react when, usually because heating speed is too fast, and the rate of heat addition is non-at the uniform velocity causes anti-
Liquid bumping is answered, influences reaction process.Existing common means are first to heat postcooling, and heating is typically first filled using single pipe
Oil is heated, when needing cooling oil extraction cooled down into cooling water, defect is single pipe first water not easy cleaning after oil.
Invention content
The purpose of the present invention is to provide a kind of temperature control reaction kettles, it is intended to solve the above problems.
To achieve these goals, the technical scheme is that designing a kind of temperature control reaction kettle, including outer layer autoclave body, interior
Layer autoclave body, interlayer, cooling tube, heating tube；Interlayer is formed between the outer layer autoclave body and internal layer autoclave body；If it is equipped in the interlayer
Dry group cooling tube and several groups of heating tubes；The cooling tube and heating tube are intervally arranged.
Preferably, the cooling tube is equipped with two groups；The heating tube is equipped with one group；The heating tube is arranged in interlayer
Portion；Two groups of cooling tubes are separately positioned on the top and bottom of interlayer.
The heating tube and cooling tube of the present invention is intervally arranged in interlayer, and be carried out at the same time heating and cooling work, passes through
The flow of deep fat or cooling water adjusts the rate of heat addition in control heating tube and cooling tube.It is cold using two groups in the mode of optimization
But pipe and one group of heating tube, and heating tube is located at interlayer stage casing, cooling tube is located at interlayer both ends respectively can more preferably heat effect
Fruit, heating tube is located at stage casing and internal layer autoclave body contact surface is larger, convenient for heat transfer；And the liquid-tight degree of same volume thermal response is less than cold
Reaction solution；So the reacting liquid temperature that the cooling tube of interlayer epimere corresponds to internal layer autoclave body region is relatively low and sink；It reacts in stage casing
Liquid temperature is high, and reaction solution floats herein, so that reaction solution forms reflux in internal layer autoclave body, promotes the mixing of reaction solution
Uniformly.
The advantages of the present invention are：The present invention can accurately control reaction solution heating rate excessively, promote reaction
Liquid is uniformly mixed, and promotes reaction solution reaction process.
Description of the drawings
Fig. 1 is the schematic diagram of the present invention.
Wherein, outer layer autoclave body 1, internal layer autoclave body 2, interlayer 3, cooling tube 4, heating tube 5.
Specific embodiment
With reference to the accompanying drawings and examples, the specific embodiment of the present invention is further described.Following embodiment is only
For clearly illustrating technical scheme of the present invention, and it is not intended to limit the protection scope of the present invention and limits the scope of the invention.
Embodiment：
A kind of temperature control reaction kettle, including outer layer autoclave body 1, internal layer autoclave body 2, interlayer 3, cooling tube 4, heating tube 5；The outer layer autoclave body
Interlayer 3 is formed between 1 and internal layer autoclave body 2；Two groups of cooling tubes 4 and one group of heating tube 5 are equipped in the interlayer 3；The heating tube 5
It is arranged on the middle part of interlayer 3；Two groups of cooling tubes 4 are separately positioned on the top and bottom of interlayer 3.
The above is only the preferred embodiment of the present invention, it is noted that for the ordinary skill people of the art
For member, without departing from the technical principles of the invention, several improvements and modifications can also be made, these improvements and modifications
Also it should be regarded as protection scope of the present invention.
Claims (2)
1. a kind of temperature control reaction kettle, it is characterised in that：Including outer layer autoclave body, internal layer autoclave body, interlayer, cooling tube, heating tube；It is described
Interlayer is formed between outer layer autoclave body and internal layer autoclave body；Several groups of cooling tubes and several groups of heating tubes are equipped in the interlayer；It is described
Cooling tube and heating tube are intervally arranged.
2. a kind of temperature control reaction kettle according to claim 1, it is characterised in that：The cooling tube is equipped with two groups；It is described to add
Heat pipe is equipped with one group；The heating tube is arranged on the middle part of interlayer；Two groups of cooling tubes be separately positioned on interlayer upper end and
Lower end.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810269735.2A CN108246219A (en) | 2018-03-29 | 2018-03-29 | A kind of temperature control reaction kettle |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810269735.2A CN108246219A (en) | 2018-03-29 | 2018-03-29 | A kind of temperature control reaction kettle |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN108246219A true CN108246219A (en) | 2018-07-06 |
Family
ID=62747653
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201810269735.2A Pending CN108246219A (en) | 2018-03-29 | 2018-03-29 | A kind of temperature control reaction kettle |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN108246219A (en) |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0478885A1 (en) * | 1990-10-04 | 1992-04-08 | The B.F. Goodrich Company | Reactor vessel |
| CN203291835U (en) * | 2013-04-25 | 2013-11-20 | 浙江枧洋化工有限公司 | Coil type heating reaction kettle |
| CN203355722U (en) * | 2013-06-14 | 2013-12-25 | 湘潭市开元化学有限公司 | Stainless steel reaction kettle |
| CN205650199U (en) * | 2016-05-16 | 2016-10-19 | 盐城安顺化工有限公司 | Emulsion preparation facilities |
| CN106492738A (en) * | 2016-11-14 | 2017-03-15 | 东海县凯凯石英制品有限公司 | Large-scale consersion unit based on quartz |
-
2018
- 2018-03-29 CN CN201810269735.2A patent/CN108246219A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0478885A1 (en) * | 1990-10-04 | 1992-04-08 | The B.F. Goodrich Company | Reactor vessel |
| CN203291835U (en) * | 2013-04-25 | 2013-11-20 | 浙江枧洋化工有限公司 | Coil type heating reaction kettle |
| CN203355722U (en) * | 2013-06-14 | 2013-12-25 | 湘潭市开元化学有限公司 | Stainless steel reaction kettle |
| CN205650199U (en) * | 2016-05-16 | 2016-10-19 | 盐城安顺化工有限公司 | Emulsion preparation facilities |
| CN106492738A (en) * | 2016-11-14 | 2017-03-15 | 东海县凯凯石英制品有限公司 | Large-scale consersion unit based on quartz |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20180706 |
|
| RJ01 | Rejection of invention patent application after publication |