CN108204933A - A kind of anti-rut agent and the evaluation method of building stones adhesiveness - Google Patents

A kind of anti-rut agent and the evaluation method of building stones adhesiveness Download PDF

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Publication number
CN108204933A
CN108204933A CN201711311946.XA CN201711311946A CN108204933A CN 108204933 A CN108204933 A CN 108204933A CN 201711311946 A CN201711311946 A CN 201711311946A CN 108204933 A CN108204933 A CN 108204933A
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China
Prior art keywords
rut agent
building stones
adhesiveness
denoted
rut
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CN201711311946.XA
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Inventor
樊长昕
马德崇
王威
杜素军
丰功吉
李雪莲
舒兴旺
周亚军
郭赢赢
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Shanxi Province Transport Science Research Institute
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Shanxi Province Transport Science Research Institute
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Priority to CN201711311946.XA priority Critical patent/CN108204933A/en
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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N5/00Analysing materials by weighing, e.g. weighing small particles separated from a gas or liquid
    • G01N5/04Analysing materials by weighing, e.g. weighing small particles separated from a gas or liquid by removing a component, e.g. by evaporation, and weighing the remainder

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  • Physics & Mathematics (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Compositions Of Macromolecular Compounds (AREA)
  • Testing Resistance To Weather, Investigating Materials By Mechanical Methods (AREA)
  • Road Paving Structures (AREA)

Abstract

The invention belongs to Highway Test technical field, it particularly relates to a kind of anti-rut agent and the evaluation method of building stones adhesiveness.It includes the following steps:The clean dried stone sample of appropriate 2.36~9.5mm sizes is taken, is denoted as m1, it is put into more than heating and thermal insulation 5h in 180 ± 2 DEG C of baking ovens;According to engineering actual interpolation amount, dry anti-rut agent sample is weighed in proportion, is denoted as m2;Mixture is discharged into clean enamel tray, sealer, is put into 80 DEG C of freezing more than 1h, striping after taking-up is immediately placed in 120 DEG C of baking ovens with shaking table function, and be heated 30min, and 100rmp shakings scrape anti-rut agent and weigh, are denoted as m3;Quality sticking ratio is calculated, value is bigger, represents that anti-rut agent and building stones adhesiveness are better.Compared with prior art, this method is easy to operate, favorable repeatability, intuitively can rapidly evaluate the adhesiveness quality of anti-rut agent and building stones, be of great significance to construction production.

Description

A kind of anti-rut agent and the evaluation method of building stones adhesiveness
Technical field
The invention belongs to Highway Test technical field, it particularly relates to be adhered to a kind of anti-rut agent and building stones The evaluation method of property.
Background technology
In recent years, because anti-rut agent class product has excellent pavement performance and easy addition manner, in highway construction Fairly large application is achieved in the market with maintenance.Anti-rut agent part wire drawing during mixing and stirring into plastic optical fibre, is collecting It puts up a bridge in material skeleton and is crosslinked and forms fiber and steel bar reinforced effect, therefore anti-rut agent and building stones adhesiveness are particularly significant.
At present, anti-rut agent mainly passes through anti-rut agent with building stones adhesiveness there is no Direct Test method and index Physical property itself and the performance of asphalt reflect indirectly.The physical index of anti-rut agent, mainly including appearance, close Degree, softening point, melt index etc.;The performance of asphalt, mainly from high-temperature stability, low-temperature cracking-resistance, water resistant damageability Etc. judgement.These Test model synthetic techniques are complicated for operation, and the used time is longer, it is difficult to evaluate anti-rut agent and building stones to quicklook The quality of adhesiveness.
This law weight reduction to be used measures the anti-rut agent quality for participating in building stones adhesiveness, but weight reduction must be measured when filling sample And the quality after cleaning sample.If sample cleaning is unclean, clear up it is inaccurate if the container mass after sample, easily to meter Calculation causes error.
Invention content
In order to solve the above technical problems, the present invention provides a kind of anti-rut agent and the evaluation method of building stones adhesiveness, it should Method is easy to operate, quick and precisely, favorable repeatability.
A kind of anti-rut agent of the present invention and the evaluation method of building stones adhesiveness, the evaluation method specific steps are such as Under:1) by screening used for asphalt mixture of gathering materials, washing, drying, if obtaining the clean dried stone sample of 2.36~9.5mm sizes It is dry;2) appropriate stone sample is weighed, is denoted as m1, it is put into more than heating and thermal insulation 5h in 180 ± 2 DEG C of baking ovens;3) according to engineering reality Additive amount, it is several to weigh dry anti-rut agent sample in proportion, is denoted as m2;4) mixing device is preheated into 30min at 180 ± 2 DEG C Afterwards, stone sample and anti-rut agent are added in simultaneously, stirs 90s;5) mixture is discharged into clean enamel tray, sealer, be put into- 80 DEG C of freezing more than 1h, striping after taking-up are immediately placed in 120 DEG C of baking ovens with shaking table function, and be heated 30min, 100rmp shakings, It scrapes anti-rut agent to weigh, is denoted as m3;6) using calculating quality sticking ratio Δ=(m2-m3)/m2× 100% for anti-rut agent with The evaluation index of building stones adhesiveness.
Compared with prior art, the evaluation method of anti-rut agent of the present invention and building stones adhesiveness in different building stones and After anti-rut agent stirring, how much is amount adhere in stone surface by comparing anti-rut agent, calculating quality sticking ratio Δ=(m2- m3)/m2× 100%, value is bigger, represents that anti-rut agent and building stones adhesiveness are better.This method is easy to operate, favorable repeatability, The adhesiveness quality of anti-rut agent and building stones intuitively can be rapidly evaluated, the research and development, construction, production of anti-rut agent are respectively provided with Great importance.
Specific embodiment
The evaluation method of anti-rut agent of the present invention and building stones adhesiveness is made with reference to specific embodiment further Illustrate, but protection scope of the present invention is not limited to this.
Embodiment 1
The project profile of the present embodiment is:Facing stone limestone AC-20 anti-rut agent pitches in certain asphalt pavement of highway Mixture material designs, and addition content is the 0.4% of quality of asphalt mixtures.Existing tri- kinds of brand anti-rut agents of A, B, C.
It is evaluated using anti-rut agent and the method for building stones adhesiveness.
1) by the screening of AC-20 limestone aggregates, washing, drying, the clean dried building stones sample of 2.36~9.5mm sizes is obtained Product are several;
2) appropriate stone sample is weighed, is denoted as m1, it is put into more than heating and thermal insulation 5h in 180 ± 2 DEG C of baking ovens;
3) according to engineering actual interpolation amount, it is several to weigh dry three kinds of brand anti-rut agent A, B, C samples in proportion, is denoted as m2
4) stone sample and anti-rut agent after 180 ± 2 DEG C preheat 30min are added in by mixing device simultaneously, stirred 90s;
5) mixture is discharged into clean enamel tray, sealer, is put into -80 DEG C of freezing more than 1h, striping after taking-up is put immediately Enter 120 DEG C of baking ovens with shaking table function, be heated 30min, and 100rmp shakings scrape anti-rut agent and weigh, are denoted as m3
6) using calculating quality sticking ratio Δ=(m2-m3)/m2× 100% is anti-rut agent and the evaluation of building stones adhesiveness Index, quality sticking ratio.Result of the test is shown in Table 1.
1 different brands anti-rut agent of table and limestone adhesiveness test result
From 1 result of the test of table it is found that tri- kinds of brand anti-rut agents of A, B, C carry out adhesiveness examination with middle face layer with limestone It tests, A=36.60%B=6.93%, C=25.27%.A is maximum, shows the adhesiveness of the building stones and brand A anti-rut agents most It is good, it is proposed that Design and procurement selects brand A.
Embodiment 2
The project profile of the present embodiment is:Certain asphalt pavement of highway upper layer basalt AC-13 anti-rut agent pitch Mixture material designs, and addition content is the 0.4% of quality of asphalt mixtures.Existing tri- kinds of brand anti-rut agents of A, B, C.
It is evaluated using anti-rut agent and the method for building stones adhesiveness.
1) by the screening of AC-13 basalt aggregates, washing, drying, the clean dried building stones sample of 2.36~9.5mm sizes is obtained Product are several;
2) appropriate stone sample is weighed, is denoted as m1, it is put into more than heating and thermal insulation 5h in 180 ± 2 DEG C of baking ovens;
3) according to engineering actual interpolation amount, it is several to weigh dry three kinds of brand anti-rut agent A, B, C samples in proportion, is denoted as m2
4) stone sample and anti-rut agent after 180 ± 2 DEG C preheat 30min are added in by mixing device simultaneously, stirred 90s;
5) mixture is discharged into clean enamel tray, sealer, is put into -80 DEG C of freezing more than 1h, striping after taking-up is put immediately Enter 120 DEG C of baking ovens with shaking table function, be heated 30min, and 100rmp shakings scrape anti-rut agent and weigh, are denoted as m3
6) using calculating quality sticking ratio Δ=(m2-m3)/m2× 100% is anti-rut agent and the evaluation of building stones adhesiveness Index, quality sticking ratio.Result of the test is shown in Table 2.
2 different brands anti-rut agent of table and basalt adhesiveness test result
From 1 result of the test of table it is found that tri- kinds of brand anti-rut agents of A, B, C and upper layer carry out adhesiveness examination with basalt It tests, A=27.11%B=7.01%, C=48.32%.C is maximum, shows the adhesiveness of the building stones and brand C anti-rut agents most It is good, it is proposed that Design and procurement selects brand C.
Embodiment 3
The project profile of the present embodiment is:Certain level-one asphalt highway upper layer uses anti-rut agent asphalt material Material design, addition content are the 0.4% of quality of asphalt mixtures.Existing limestone, basalt, the other building stones of three type of diabase.
It is evaluated using anti-rut agent and the method for building stones adhesiveness.
1) by limestone, limestone, the other screening of gathering materials of three type of diabase, washing, drying, 2.36~9.5mm is obtained The clean dried stone sample of size is several;
2) appropriate stone sample is weighed respectively, is denoted as m1, it is put into more than heating and thermal insulation 5h in 180 ± 2 DEG C of baking ovens;
3) according to engineering actual interpolation amount, it is several to weigh dry anti-rut agent sample in proportion, is denoted as m2
4) stone sample and anti-rut agent after 180 ± 2 DEG C preheat 30min are added in by mixing device simultaneously, stirred 90s;
5) mixture is discharged into clean enamel tray, sealer, is put into -80 DEG C of freezing more than 1h, striping after taking-up is put immediately Enter 120 DEG C of baking ovens with shaking table function, be heated 30min, and 100rmp shakings scrape anti-rut agent and weigh, are denoted as m3
6) using calculating quality sticking ratio Δ=(m2-m3)/m2× 100% is anti-rut agent and the evaluation of building stones adhesiveness Index, quality sticking ratio.Result of the test is shown in Table 3.
3 anti-rut agent of table and different building stones adhesiveness test results
From 3 result of the test of table it is found that limestone, basalt, the other building stones of three type of diabase and anti-rut agent respectively into Row adhesiveness test, basalt=49.20% of limestone=24.64%, diabase=32.37%.Basalt is maximum, shows this The adhesiveness of basalt and anti-rut agent is best, it is proposed that Design and procurement selects basalt.
Embodiment 4
Weight reduction measures anti-rut agent (LM-K) quality in enamel tray:By quality m2180 ± 2 DEG C of anti-rut agent add in In clean enamel tray, room temperature is placed, sealer is put into -80 DEG C of freezing more than 1h, and striping after taking-up is immediately placed in band shaking table function 120 DEG C of baking ovens, be heated 30min, 100rmp shaking, scrape anti-rut agent and weigh, be denoted as m3
Control group
Weight reduction measures anti-rut agent (LM-K) quality in enamel tray:By quality m2180 ± 2 DEG C of anti-rut agent add in In clean enamel tray, room temperature is placed, sealer is put into -20 DEG C of freezing more than 1h, and striping after taking-up is immediately placed in band shaking table function 60 DEG C of baking ovens, be heated 30min, 100rmp shaking, scrape anti-rut agent and weigh, be denoted as m3
4 embodiment 4 of table and the m3 results of control group
From 4 result of the test of table it is found that when weighing anti-rut agent, for anti-rut agent is prevented to be bonded on enamel tray, by pole It after cryogenic freezing, then heats and shakes immediately, removed conducive to Rut resistance so that measurement is more accurate, for requiring stringent work Skill, result are particularly important.

Claims (1)

1. a kind of anti-rut agent and the evaluation method of building stones adhesiveness, which is characterized in that the evaluation method is as follows:
1) by screening used for asphalt mixture of gathering materials, washing, drying, the clean dried stone sample of 2.36~9.5mm sizes is obtained;
2) stone sample is weighed, is denoted as m1, it is put into more than heating and thermal insulation 5h in 180 ± 2 DEG C of baking ovens;
3) according to engineering actual interpolation amount, dry anti-rut agent sample is weighed in proportion, is denoted as m2
4) stone sample and anti-rut agent after 180 ± 2 DEG C preheat 30min are added in by mixing device simultaneously, stirs 90s;
5) mixture is discharged into clean enamel tray, sealer, is put into -80 DEG C of freezing more than 1h, striping after taking-up is immediately placed in band 120 DEG C of baking ovens of shaking table function, be heated 30min, and 100rmp shakings scrape anti-rut agent and weigh, are denoted as m3
6) using calculating quality sticking ratio Δ=(m2-m3)/m2× 100% is anti-rut agent and the evaluation index of building stones adhesiveness.
CN201711311946.XA 2017-12-11 2017-12-11 A kind of anti-rut agent and the evaluation method of building stones adhesiveness Pending CN108204933A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111307645A (en) * 2019-12-30 2020-06-19 湖北富邦新材料有限公司 Method for rapidly measuring dust on surface of granular fertilizer

Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103059587A (en) * 2012-12-14 2013-04-24 北京中交路通科技发展有限公司 Anti-rutting modifying agent used for asphalt pavement and asphalt mixture containing anti-rutting modifying agent
CN103900957A (en) * 2014-04-28 2014-07-02 内蒙古工业大学 Method for testing interfacial bond behavior of road asphalt mixture
CN105571975A (en) * 2016-01-22 2016-05-11 武汉理工大学 Method for quantitatively analyzing adhesion of asphalt and aggregate
CN106568669A (en) * 2016-11-10 2017-04-19 同济大学 Method of testing adhesion of rock asphalt
CN106814181A (en) * 2016-12-16 2017-06-09 河海大学 One kind specific surface of aggregate from asphalt is peeled off and reclaims bitumen samples method
CN106895676A (en) * 2015-12-19 2017-06-27 西安瑞联新材料股份有限公司 A kind of thermostatic drying chamber with oscillation functions
CN108195693A (en) * 2017-12-11 2018-06-22 山西省交通科学研究院 A kind of evaluation method of low temperature performance of asphalt

Patent Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103059587A (en) * 2012-12-14 2013-04-24 北京中交路通科技发展有限公司 Anti-rutting modifying agent used for asphalt pavement and asphalt mixture containing anti-rutting modifying agent
CN103900957A (en) * 2014-04-28 2014-07-02 内蒙古工业大学 Method for testing interfacial bond behavior of road asphalt mixture
CN106895676A (en) * 2015-12-19 2017-06-27 西安瑞联新材料股份有限公司 A kind of thermostatic drying chamber with oscillation functions
CN105571975A (en) * 2016-01-22 2016-05-11 武汉理工大学 Method for quantitatively analyzing adhesion of asphalt and aggregate
CN106568669A (en) * 2016-11-10 2017-04-19 同济大学 Method of testing adhesion of rock asphalt
CN106814181A (en) * 2016-12-16 2017-06-09 河海大学 One kind specific surface of aggregate from asphalt is peeled off and reclaims bitumen samples method
CN108195693A (en) * 2017-12-11 2018-06-22 山西省交通科学研究院 A kind of evaluation method of low temperature performance of asphalt

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111307645A (en) * 2019-12-30 2020-06-19 湖北富邦新材料有限公司 Method for rapidly measuring dust on surface of granular fertilizer

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